CN1104505A

CN1104505A - Preparation of soluble tortoise and/or soft-shelled turtle powders

Info

Publication number: CN1104505A
Application number: CN93121577A
Authority: CN
Inventors: 朱圣田; 朱江
Original assignee: Individual
Current assignee: Individual
Priority date: 1993-12-28
Filing date: 1993-12-28
Publication date: 1995-07-05

Abstract

The soluble tortoise and/or soft-shelled turtle powders can be dissolved in water easily and make higher absorbing and digesting rate in human body. It features simple process and no cyclic derivates which are harmful to human body.

Description

Preparation of soluble tortoise and/or soft-shelled turtle powders

The invention belongs to the preparation method of Medicines and Health Product, especially prepare the preparation method of solubility QUANGUI and/or Trionyx sinensis (Wiegmann) powder, be applicable to the nourishing healthy of human body, the occasion of nourishing and fit keeping function.

Carapax et Plastrum Testudinis, Carapax Trionycis are the elite parts in the testudinate, have YIN nourishing, heat clearing away, removing heat from blood, invigorating the liver and kidney, YANG hyperactivity suppressing, keep fit effects such as strong bone and hard masses softening and resolving." Bencao Jingshu ": " Testudinis, Trionyx sinensis Wiegmann diformazan, herbal classic is led similar generally.The thing of the two salty Zhiyin, Carapax Trionycis are walked the liver kidney tonifying with relieving restlessness, and the logical heart of Carapax Et Plastrum Testudinis is gone into kidney with YIN nourishing." Carapax et Plastrum Testudinis, Carapax Trionycis be salty, sweet, flat, is the tonic of a salty cold, it and most of tonic is warm in nature, heat is dry nourish just the opposite.The modern medicine scientific research proves: contain protein, fat, animal colloid, ostelin in Carapax et Plastrum Testudinis, the Carapax Trionycis, organic calcium and some trace element.Existing process technology to Carapax et Plastrum Testudinis/Carapax Trionycis has methods such as employing QUANGUI/Trionyx sinensis (Wiegmann) cold drying, normal temperature drying and hyperthermia drying, treat to adopt the method for physics, machinery to clay into power after Testudinis/Trionyx sinensis Wiegmann drying, make product, such powder, it is the solid, shaped powder, water insoluble, human body can not directly absorb, and its bioavailability is low.And the employing high-temperature oven drying method also exists bake out temperature and is difficult to control, and the easy coking of protein easily forms cyclic derivatives, and some of them have intensive mutagenesis, and are harmful.

The objective of the invention is to overcome the weak point of bringing with physics, mechanical means processing Testudinis or Trionyx sinensis Wiegmann in the prior art, adopt advanced technology, make water soluble, the QUANGUI that easily is absorbed by the body and/or Trionyx sinensis (Wiegmann) powder product, its technology is easy, human body effective rate of utilization height.

The present invention is achieved through the following technical solutions: get Carapax et Plastrum Testudinis and/or Carapax Trionycis, and moistening with acid, placed 12-36 hour, drain, put in the reactor, add suitable quantity of water, be heated to steam gauge pressure 0.2-2.0Kg/CM in the reactor ²Kept 1-5 hour, after decompression is cooled off slightly, filtered while hot is condensed into thick shape, and filtrate adds protease hydrolysis, heat then and make the protease deactivation get enzymolysis solution, filtering residue adds suitable quantity of water, makes into paste, adds acid again, be mixed with and contain acid concentration 5%-40%(volume ratio) suspension, heat to 80 ± 40 ℃, kept 12-48 hour, it is 4-6 that lime water is transferred pH value, get supernatant, obtain the acid hydrolysis solution of Carapax et Plastrum Testudinis and/or Carapax Trionycis, or filtering residue is directly worn into the Carapax et Plastrum Testudinis more than 100 orders and/or the suspension slurry of Carapax Trionycis, merge enzymolysis solution and acid hydrolysis solution, the suspension slurry of enzymolysis solution and Carapax et Plastrum Testudinis and/or Carapax Trionycis, concentrate,, promptly make the soluble powder product of Carapax et Plastrum Testudinis and/or Carapax Trionycis through vacuum drying or spray drying, powder moisture is no more than 4%, above-mentioned powder-product can be mixed the meat of Testudinis and/or Trionyx sinensis Wiegmann, the internal organs dry powder is made better solubility QUANGUI of health-care effect and/or Trionyx sinensis (Wiegmann) powder product, the meat of Testudinis and/or Trionyx sinensis Wiegmann, the proportioning of internal organs dry powder and solubility Carapax et Plastrum Testudinis and/or turtle ' s carapace powder is 3-7: the 7-3(weight ratio).

The present invention is described further by following examples

Embodiment 1:

Get Carapax et Plastrum Testudinis and/or Carapax Trionycis 50 grams, it is moistening to add acetic acid, places 24 hours, and taking-up drains, and puts in the reactor, adds 1.5 kilograms in water, is heated to the interior steam pressure of reactor to gauge pressure 0.4Kg/CM ²Kept 2 hours, after decompression is cooled off slightly, filtered while hot, filtrate is chilled to 50 ℃, add 0.3 gram protease hydrolysis,, promptly get enzymolysis solution again through the deactivation of heating, stand-by, filtering residue adds water to 250 milliliters, stirs down slowly to add hydrochloric acid, is mixed with acid concentration 15%(volume ratio) suspension, be warmed to 80 ℃, keep 24 hours lime water and transfer pH value, get supernatant, merge with enzymolysis solution at 4-6, stir evenly, also can be spray-dried through vacuum drying, promptly obtain the soluble powder product of Carapax et Plastrum Testudinis and/or Carapax Trionycis, powder moisture is no more than 4%.

Embodiment 2

Get Carapax et Plastrum Testudinis and/or Carapax Trionycis 100 grams, it is moistening to add 20% lactic acid, places 30 hours, drains, and puts in the reactor, adds 1 kilogram in water, feeds high-pressure saturated steam to gauge pressure 1.4Kg/CM ², kept decompression 1.5 hours, cooled and filtered slightly, filtrate is chilled to 50 ℃, adds 0.5 gram protease hydrolysis, and heating makes enzyme-deactivating, stand-by, filtering residue is worn into the above suspension slurry of 100 orders and enzymolysis solution merges, and stirs evenly, through vacuum drying or spray drying, promptly make the soluble powder product of Carapax et Plastrum Testudinis and/or Carapax Trionycis, the water content of this product is no more than 4%.

Embodiment 3

The dry powder that Testudinis and/or Carnis Trionycis, internal organs are made, with the soluble powder of embodiment 1, Carapax et Plastrum Testudinis that embodiment 2 makes and/or Carapax Trionycis by Carnis Testudinis, visceral meal: solubility Tortoise Shell=3: the 7(weight ratio), Carnis Trionycis, visceral meal: solubility turtle ' s carapace powder=7: the 3(weight ratio), Testudinis and Carnis Trionycis, visceral meal: solubility Tortoise Shell and turtle ' s carapace powder=5: the ratio mixing 5(weight ratio), make the QUANGUI and/or the Trionyx sinensis (Wiegmann) soluble powder product that have more the medicinal health-care effect, its water content is no more than 4%.

QUANGUI and/or Trionyx sinensis (Wiegmann) powder product with the inventive method preparation, soluble in water, easily absorbed absorption of human body utilization rate height, but suitability for industrialized production by human consumption, technology is easy, spray-dried or vacuum drying is difficult for forming harmful cyclic derivatives, obeys safety for a long time, reliably, have bigger implementary value and economic results in society.

Claims

1, the preparation method of a kind of solubility QUANGUI and/or Trionyx sinensis (Wiegmann) powder is characterized in that Carapax et Plastrum Testudinis and/or Carapax Trionycis are used acid soakage 12-36 hour, drains in the rearmounted reactor, adds suitable quantity of water, and being heated to the interior steam pressure of reactor is gauge pressure 0.2-2.0Kg/CM ²Kept 1-5 hour, decompression, cool off the back filtered while hot slightly, filtrate adds protease hydrolysis, and inactivator gets enzymolysis solution then, filtering residue adds suitable quantity of water, make into pasty state, add acid again, be mixed with the suspension that contains acid concentration 5%-40% (volume ratio), heat to 80 ± 40 ℃ and kept 12-48 hour, it is 4-6 that lime water is transferred PH, gets supernatant, gets acid hydrolysis solution, or filtering residue directly worn into the Carapax et Plastrum Testudinis more than 100 orders and/or the suspension slurry of Carapax Trionycis, merge enzymolysis solution and acid hydrolysis solution, the suspension slurry of enzymolysis solution and Carapax et Plastrum Testudinis and/or Carapax Trionycis, mixing, concentrate, after vacuum drying or the spray drying, promptly make the soluble powder product of Carapax et Plastrum Testudinis and/or Carapax Trionycis, its water content is no more than 4%, with the Testudinis of making and/or the meat of Trionyx sinensis Wiegmann, the internal organs dry powder joins in solubility Carapax et Plastrum Testudinis and/or the turtle ' s carapace powder, mixing is formulated, and its proportioning is: the meat of Testudinis and/or Trionyx sinensis Wiegmann, internal organs dry powder: solubility Carapax et Plastrum Testudinis and/or turtle ' s carapace powder are 3-7: 7-3 (weight ratio).