CN110420144A - A kind of roxburgh rose flower mildy wash and preparation method thereof - Google Patents

A kind of roxburgh rose flower mildy wash and preparation method thereof Download PDF

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Publication number
CN110420144A
CN110420144A CN201910809658.XA CN201910809658A CN110420144A CN 110420144 A CN110420144 A CN 110420144A CN 201910809658 A CN201910809658 A CN 201910809658A CN 110420144 A CN110420144 A CN 110420144A
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roxburgh rose
mildy wash
rose flower
flower
preparation
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谭书明
陈小敏
宋长军
陈萍
黄颖
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Guizhou University
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Guizhou University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of roxburgh rose flower mildy wash and preparation method thereof; by weight percentage; it include Rosa roxburghii Tratt flower extract 25-35%, polyacrylic acid 13-23%, glycerol 14-20%, glycerin monostearate 1.4-1.8%, isopropyl palmitate 0.01-0.06%, cocounut oil acyl glycine potassium 2-7%, lauroyl propylhomoserin sodium 2-7%, CAB-35 1-3%, sodium benzoate 0.1-0.2% and essence 0.02-0.05%, remaining is water.While mildy wash of the invention is good with face cleaning effect, also has mildness strong, stimulate small feature;In addition, method of the invention can maximize the useful value for retaining Rosa roxburghii Tratt, the loss of nutrient is reduced.

Description

A kind of roxburgh rose flower mildy wash and preparation method thereof
Technical field
The present invention relates to a kind of mildy wash and preparation method thereof, especially a kind of roxburgh rose flower mildy wash and preparation method thereof.
Background technique
Rosa roxburghii Tratt is the fruit also known as thatch pears, oblonga of rosaceous plant rosa roxburghii, is a kind of natural plant of dual-purpose of drug and food Object.Rich in nutrients such as vitamin C abundant, organic acid, microelement, polyphenol, flavones, superoxide dismutases in Rosa roxburghii Tratt Matter has beauty face-whitening-nourishing, anti-aging, crease-resistant and other effects.
Facial cleanser belongs to skin-cleaning cosmetics, the purpose is to remove the dirt on skin, makes skin refreshing, helps to maintain skin Skin normal physiological condition.When facial cleanser cleans skin, the object (i.e. matrix) of cleaning is human skin, is adhered to dirt above Dirt is substantially sebum and fragments of stratum corneum and its oxygenolysis object (dirt), or glutinous cosmetics together are residual therewith Stay object.These residual metabolites be it is unstable, can with the oxygen in air, or deposition molecule reaction.When being exposed to sunlight Or with the presence of bacterium on skin, it may occur that various physical chemistry and biochemical reaction form the object of some possible injury skins Matter.Thus, even healthy skin, skin cleaning is also process necessary to skin nursing.In addition, for sensitivity or crisp Weak skin more needs especially to clean and nurse due to its characteristic.For problematic skin type, it is necessary to consider to wash emphatically The mildness of face milk and safety.
However, existing mildy wash at present on the market often contains more chemical component, dry skin, allergy are easily caused Equal side effects.
Summary of the invention
The object of the present invention is to provide a kind of roxburgh rose flower mildy wash and preparation method thereof.Mildy wash of the invention has While face cleaning effect is good, also has mildness strong, stimulate small feature;In addition, method of the invention can maximize reservation The useful value of Rosa roxburghii Tratt, reduces the loss of nutrient.
Technical solution of the present invention: a kind of roxburgh rose flower mildy wash includes by weight percentage Rosa roxburghii Tratt flower extract 25-35%, polyacrylic acid 13-23%, glycerol 14-20%, glycerin monostearate 1.4-1.8%, isopropyl palmitate 0.01- 0.06%, cocounut oil acyl glycine potassium 2-7%, lauroyl propylhomoserin sodium 2-7%, CAB-35 1-3%, sodium benzoate 0.1-0.2% and perfume (or spice) Smart 0.02-0.05%, remaining is water.
Roxburgh rose flower mildy wash above-mentioned includes by weight percentage Rosa roxburghii Tratt flower extract 28-32%, polyacrylic acid 16-20%, glycerol 16-18%, glycerin monostearate 1.5-1.7%, isopropyl palmitate 0.03-0.05%, cocounut oil acyl glycine Potassium 3-5%, lauroyl propylhomoserin sodium 3-5%, CAB-35 1.5-2.5%, sodium benzoate 0.13-0.17% and essence 0.03-0.04%, Remaining is water.
Roxburgh rose flower mildy wash above-mentioned includes by weight percentage Rosa roxburghii Tratt flower extract 30, polyacrylic acid 18, sweet Oil 17%, glycerin monostearate 1.6%, isopropyl palmitate 0.04%, cocounut oil acyl glycine potassium 4%, lauroyl propylhomoserin sodium 4%, CAB-35 2%, sodium benzoate 0.15% and essence 0.03%, remaining is water.
A kind of method of aforementioned roxburgh rose flower mildy wash, includes the following steps:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of picking being cleaned and is dried, and is put into the extraction of salt water distillation, is obtained roxburgh rose flower Extract;
2) after polyacrylic acid is dissolved in water homogeneous 3-5 minutes in vacuum emulsification pot, coconut palm then the preparation of mildy wash: is added Oleoyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 55- 60 DEG C, continue to stir 5-20min, then after keeping the temperature 15-25min cooling water temperature to 45 DEG C or less;It is eventually adding roxburgh rose flower extraction Object, isopropyl palmitate, sodium benzoate and essence are discharged after stirring, are stood.
The preparation method of roxburgh rose flower mildy wash above-mentioned, the concentration of salt water described in step 1) are 4%, brine temp 45-55 ℃。
The preparation method of roxburgh rose flower mildy wash above-mentioned, the solid-to-liquid ratio of roxburgh rose flower and salt water described in step 1) are 1:20.
The preparation method of roxburgh rose flower mildy wash above-mentioned, the time of distillation described in step 1) are 6-8h.
Beneficial effects of the present invention
The present invention is by using Rosa roxburghii Tratt flower extract as primary raw material, and the other compositions of reasonable preparation mildy wash, guarantee it is clean Under the premise of the effect of face, the content of natural materials is increased, reduces the specific gravity of chemical component, strengthens the mild of mildy wash Property, reduce mildy wash to the stimulation of skin.In addition, the present invention is prepared by above-mentioned technique, it can be as far as possible The useful component retained in Rosa roxburghii Tratt, reduce loss, to improve mildy wash for the effect of face cleaning and skin care.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but is not intended as the foundation limited the present invention.
The embodiment of the present invention
Embodiment 1: a method of roxburgh rose flower mildy wash being prepared, steps are as follows:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of 10g picking is cleaned and is dried, the salt water (temperature of 200ml 4% is put into 50 DEG C) in distillation extract 7h, obtain Rosa roxburghii Tratt flower extract;
2) preparation of mildy wash: after polyacrylic acid is dissolved in water in vacuum emulsification pot homogeneous 4 minutes, cocounut oil is then added Acyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 57 DEG C, Continue to stir 15min, then after keeping the temperature 20min cooling water temperature to 45 DEG C or less;It is different to be eventually adding Rosa roxburghii Tratt flower extract, palmitinic acid Propyl ester, sodium benzoate and essence are discharged after stirring, are stood;
Step 2 by weight percentage, Rosa roxburghii Tratt flower extract 30, polyacrylic acid 18, glycerol 17%, glycerin monostearate 1.6%, isopropyl palmitate 0.04%, cocounut oil acyl glycine potassium 4%, lauroyl propylhomoserin sodium 4%, CAB-35 2%, sodium benzoate 0.15% and essence 0.03%, remaining is water.
Embodiment 2: a method of roxburgh rose flower mildy wash being prepared, steps are as follows:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of 10g picking is cleaned and is dried, the salt water (temperature of 200ml 4% is put into 45 DEG C) in distillation extract 6h, obtain Rosa roxburghii Tratt flower extract;
2) preparation of mildy wash: after polyacrylic acid is dissolved in water in vacuum emulsification pot homogeneous 3 minutes, cocounut oil is then added Acyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 55 DEG C, Continue to stir 5min, then after keeping the temperature 15min cooling water temperature to 45 DEG C or less;It is different to be eventually adding Rosa roxburghii Tratt flower extract, palmitinic acid Propyl ester, sodium benzoate and essence are discharged after stirring, are stood;
Step 2 includes that Rosa roxburghii Tratt flower extract 28%, polyacrylic acid 16%, glycerol 16%, monostearate are sweet by weight percentage Grease 1.5%, isopropyl palmitate 0.03%, cocounut oil acyl glycine potassium 3%, lauroyl propylhomoserin sodium 3%, CAB-35 1.5%, benzene first Sour sodium 0.13% and essence 0.03%, remaining is water.
Embodiment 3: a method of roxburgh rose flower mildy wash being prepared, steps are as follows:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of 10g picking is cleaned and is dried, the salt water (temperature of 200ml 4% is put into 55 DEG C) in distillation extract 8h, obtain Rosa roxburghii Tratt flower extract;
2) preparation of mildy wash: after polyacrylic acid is dissolved in water in vacuum emulsification pot homogeneous 5 minutes, cocounut oil is then added Acyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 60 DEG C, Continue to stir 20min, then after keeping the temperature 25min cooling water temperature to 45 DEG C or less;It is different to be eventually adding Rosa roxburghii Tratt flower extract, palmitinic acid Propyl ester, sodium benzoate and essence are discharged after stirring, are stood;
Step 2 includes that Rosa roxburghii Tratt flower extract 32%, polyacrylic acid 20%, glycerol 18%, monostearate are sweet by weight percentage Grease 1.7%, isopropyl palmitate 0.05%, cocounut oil acyl glycine potassium 5%, lauroyl propylhomoserin sodium 5%, CAB-35 2.5%, benzene first Sour sodium 0.17% and essence 0.04%, remaining is water.
Embodiment 4: a method of roxburgh rose flower mildy wash being prepared, steps are as follows:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of 10g picking is cleaned and is dried, the salt water (temperature of 200ml 4% is put into 48 DEG C) in distillation extract 6.5h, obtain Rosa roxburghii Tratt flower extract;
2) preparation of mildy wash: after polyacrylic acid is dissolved in water in vacuum emulsification pot homogeneous 3.5 minutes, coconut palm is then added Oleoyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 56 DEG C, continue to stir 10min, then after keeping the temperature 18min cooling water temperature to 45 DEG C or less;It is eventually adding Rosa roxburghii Tratt flower extract, palm Isopropyl propionate, sodium benzoate and essence are discharged after stirring, are stood;
Step 2 includes that Rosa roxburghii Tratt flower extract 25%, polyacrylic acid 13%, glycerol 14%, monostearate are sweet by weight percentage Grease 1.4%, isopropyl palmitate 0.01%, cocounut oil acyl glycine potassium 2%, lauroyl propylhomoserin sodium 2%, CAB-35 1%, benzoic acid Sodium 0.1% and essence 0.02%, remaining is water.
Embodiment 5: a method of roxburgh rose flower mildy wash being prepared, steps are as follows:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of 10g picking is cleaned and is dried, the salt water (temperature of 200ml 4% is put into 53 DEG C) in distillation extract 7.5h, obtain Rosa roxburghii Tratt flower extract;
2) preparation of mildy wash: after polyacrylic acid is dissolved in water in vacuum emulsification pot homogeneous 4.5 minutes, coconut palm is then added Oleoyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 58 DEG C, continue to stir 18min, then after keeping the temperature 22min cooling water temperature to 45 DEG C or less;It is eventually adding Rosa roxburghii Tratt flower extract, palm Isopropyl propionate, sodium benzoate and essence are discharged after stirring, are stood;
Step 2 includes that Rosa roxburghii Tratt flower extract 35%, polyacrylic acid 23%, glycerol 20%, monostearate are sweet by weight percentage Grease 1.8%, isopropyl palmitate 0.06%, cocounut oil acyl glycine potassium 7%, lauroyl propylhomoserin sodium 7%, CAB-35 3%, benzoic acid Sodium 0.2% and essence 0.05%, remaining is water.
The preferable specific embodiment of the above, only the invention, but the protection scope of the invention is not It is confined to this, anyone skilled in the art is in the technical scope that the invention discloses, according to the present invention The technical solution of creation and its inventive concept are subject to equivalent substitution or change, should all cover the invention protection scope it It is interior.

Claims (7)

1. a kind of roxburgh rose flower mildy wash, it is characterised in that: include Rosa roxburghii Tratt flower extract 25-35%, poly- by weight percentage Acrylic acid 13-23%, glycerol 14-20%, glycerin monostearate 1.4-1.8%, isopropyl palmitate 0.01-0.06%, cocounut oil acyl Glycine potassium 2-7%, lauroyl propylhomoserin sodium 2-7%, CAB-35 1-3%, sodium benzoate 0.1-0.2% and essence 0.02-0.05%, Remaining is water.
2. roxburgh rose flower mildy wash according to claim 1, it is characterised in that: include roxburgh rose flower by weight percentage Extract 28-32%, polyacrylic acid 16-20%, glycerol 16-18%, glycerin monostearate 1.5-1.7%, isopropyl palmitate 0.03-0.05%, cocounut oil acyl glycine potassium 3-5%, lauroyl propylhomoserin sodium 3-5%, CAB-35 1.5-2.5%, sodium benzoate 0.13-0.17% and essence 0.03-0.04%, remaining is water.
3. roxburgh rose flower mildy wash according to claim 2, it is characterised in that: include roxburgh rose flower by weight percentage Extract 30, polyacrylic acid 18, glycerol 17%, glycerin monostearate 1.6%, isopropyl palmitate 0.04%, cocounut oil acyl glycine Potassium 4%, lauroyl propylhomoserin sodium 4%, CAB-35 2%, sodium benzoate 0.15% and essence 0.03%, remaining is water.
4. a kind of method for preparing any one of claim 1-3 roxburgh rose flower mildy wash, which is characterized in that including walking as follows It is rapid:
1) preparation of Rosa roxburghii Tratt flower extract: the Rosa roxburghii Tratt fresh flower of picking being cleaned and is dried, and is put into the extraction of salt water distillation, is obtained roxburgh rose flower Extract;
2) after polyacrylic acid is dissolved in water homogeneous 3-5 minutes in vacuum emulsification pot, coconut palm then the preparation of mildy wash: is added Oleoyl glycine potassium, lauroyl propylhomoserin sodium, CAB-35, glycerol and glycerin monostearate stir evenly, and then heat to 55- 60 DEG C, continue to stir 5-20min, then after keeping the temperature 15-25min cooling water temperature to 45 DEG C or less;It is eventually adding roxburgh rose flower extraction Object, isopropyl palmitate, sodium benzoate and essence are discharged after stirring, are stood.
5. the preparation method of roxburgh rose flower mildy wash according to claim 4, it is characterised in that: salt water described in step 1) it is dense Degree be 4%, 45-55 DEG C of brine temp.
6. the preparation method of roxburgh rose flower mildy wash according to claim 4, it is characterised in that: roxburgh rose flower described in step 1) with The solid-to-liquid ratio of salt water is 1:20.
7. the preparation method of roxburgh rose flower mildy wash according to claim 4, it is characterised in that: distillation described in step 1) when Between be 6-8h.
CN201910809658.XA 2019-08-29 2019-08-29 A kind of roxburgh rose flower mildy wash and preparation method thereof Pending CN110420144A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111297765A (en) * 2020-04-14 2020-06-19 遵义医科大学珠海校区 Roxburgh rose extract and antibacterial application thereof
CN114129485A (en) * 2021-12-21 2022-03-04 南京华开生物科技有限公司 Moisturizing amino acid facial cleanser and preparation process thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104490663A (en) * 2014-12-04 2015-04-08 云南人羞花化妆品有限公司 Pseudo-ginseng facial cleanser and preparation method thereof
CN106727201A (en) * 2015-11-20 2017-05-31 周丽 A kind of lavender mildy wash
CN107669589A (en) * 2017-10-27 2018-02-09 厦门特吉生物科技有限公司 A kind of Rosa roxburghii shampoo

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104490663A (en) * 2014-12-04 2015-04-08 云南人羞花化妆品有限公司 Pseudo-ginseng facial cleanser and preparation method thereof
CN106727201A (en) * 2015-11-20 2017-05-31 周丽 A kind of lavender mildy wash
CN107669589A (en) * 2017-10-27 2018-02-09 厦门特吉生物科技有限公司 A kind of Rosa roxburghii shampoo

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柯杨 等: "正交实验法优选金刺梨花精油提取工艺条件", 《食品研究与开发》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111297765A (en) * 2020-04-14 2020-06-19 遵义医科大学珠海校区 Roxburgh rose extract and antibacterial application thereof
CN114129485A (en) * 2021-12-21 2022-03-04 南京华开生物科技有限公司 Moisturizing amino acid facial cleanser and preparation process thereof
CN114129485B (en) * 2021-12-21 2023-10-10 南京华开生物科技有限公司 Moisturizing amino acid facial cleanser and preparation process thereof

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Application publication date: 20191108