CN110409174A - A kind of phenols environmental protection finishing agent and preparation method thereof - Google Patents
A kind of phenols environmental protection finishing agent and preparation method thereof Download PDFInfo
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- CN110409174A CN110409174A CN201910725769.2A CN201910725769A CN110409174A CN 110409174 A CN110409174 A CN 110409174A CN 201910725769 A CN201910725769 A CN 201910725769A CN 110409174 A CN110409174 A CN 110409174A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/238—Tannins, e.g. gallotannic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention provides a kind of phenols environmental protection finishing agents and preparation method thereof, and finishing agent is prepared by the raw material of following parts by weight: 50-80 parts of phenols liposome particle, 5-10 parts of citric acid, 3-6 parts of tannic acid, 4-8 parts of dialkyl dimethyl glycine betaine, 3-7 parts of hydroxypropyl methyl cellulose, 4-9 parts of dioctyl sodium sulfosuccinate, 15-30 parts of water；Wherein the phenolic compound in the phenols liposome particle includes the one or more combination of ellagic acid, tea polyphenols, arbutin and resveratrol.The finishing agent makes fabric have good antimicrobial form after handling fabric, and fabric carries out bacteriostasis rate after soaping 10 times and remains to reach 90% or more, to illustrate that finishing agent is with good stability.The finishing agent is green and pollution-free simultaneously, meets the quality requirements environmentally protective to modern product.Therefore the finishing agent is with important application prospects in field of textiles.
Description
Technical field
The invention belongs to field of textiles, and in particular to a kind of phenols environmental protection finishing agent and preparation method thereof.
Background technique
With the continuous improvement of people's living standards, demand of the people to textile is not only embodied in wearing, resisting cold etc.
Aspect, it is higher and higher to the Functional Requirement of textile, and functional textile generally require finishing functions are carried out to it and
.The finishing functions of textile assign the performances such as its excellent use, safety, appearance, and multifunction finishing agent is then with chemistry, life
The development of the multidisciplinary technology such as object medicine, polymer composite, photochemistry, thermodynamics, electricity, ecology gets up
A kind of functional finishing agent.Since the finishing functions of textile are for the certain specific performances of textile, thus purpose
By force, effect is good, and value-added content of product is also high.Textile is clear using purpose and range after functional treatment, also deep to be disappeared
The person of expense welcomes.The application range of functional textile is relatively broad, is such as used as biomedical tissue and organ；For preventing to cure
Antibacterial diseases prevention, the physical therapy body shaping of health and beauty；Fire-retardant, the antistatic of special trade, high/low temperature protection；Domestic environment changes
Kind, dust suction noise control, women and children's physiological hygiene, mite killing is antifouling, refuses oily water repellent, all kinds of radiation protections etc..Also, from the point of view of development,
The arrangement content and application range of functional textile are also constantly expanding, and are just gradually penetrating into the production and arrangement of common product
In the process.
However the production of functional textile cannot impact ecological environment, nuisance spilling, pernicious gas and dirt
The discharge of water can directly contribute soil and underground water pollution, and the deterioration of natural ecological environment and biotic population is caused to lack of proper care or disappear
It goes out.These are all not permitted in world environments protective tissue and national governments.It is close that all kinds of chemical assistants will not only be studied with it
Phase ecology influence power will also study its long-acting ecology influence power, it is ensured that its permanent safety.Therefore, in functional textile
During arrangement, biodegradable auxiliary agent should be used, as far as possible to ensure Environmental security.
Summary of the invention
Above of the existing technology in order to solve the problems, such as, the purpose of the present invention is to provide a kind of phenols environmental protection finishing agents
And preparation method thereof.
To achieve the goals above, the present invention the following technical schemes are provided:
A kind of phenols environmental protection finishing agent, is prepared by the raw material of following parts by weight: 50-80 parts of phenols liposome particle, lemon
5-10 parts sour, 3-6 parts of tannic acid, 4-8 parts of dialkyl dimethyl glycine betaine, 3-7 parts of hydroxypropyl methyl cellulose, succinic acid two are pungent
4-9 parts of ester sodium sulfonate, 15-30 parts of water；
Wherein the phenolic compound in the phenols liposome particle includes ellagic acid, tea polyphenols, arbutin and resveratrol
One or more combination；
The preparation method of the phenols liposome particle the following steps are included:
(1) it weighs phenolic compound by corresponding parts by weight to be scattered in deionized water, so that the mass fraction of phenolic compound is
30-50wt%；Eucalyptus oil, clove oil are stirred with polyglycerol polyricinoleate and are mixed and made into oily phase；
(2) phenols aqueous solution in step (1) is added in oil-phase solution under stirring conditions, continues to be stirred and will be warm
Degree is slowly increased to 75 DEG C, stirs and reflection system is down to room temperature after 40-60min, mixture A is made；
(3) cocoanut fatty acid diethanolamide is added into mixture A, continues to be stirred 1-2h at a temperature of 55 DEG C,
Obtain phenols liposome particle.
Preferably, a kind of phenols environmental protection finishing agent of the present invention, is prepared: phenols by the raw material of following parts by weight
60-70 parts of liposome particle, 5-8 parts of citric acid, 4-6 parts of tannic acid, 5-7 parts of dialkyl dimethyl glycine betaine, hydroxypropyl methyl
4-6 parts of cellulose, 5-8 parts of dioctyl sodium sulfosuccinate, 18-16 parts of water.
Preferably, a kind of phenols environmental protection finishing agent of the present invention, is prepared: phenols by the raw material of following parts by weight
65 parts of liposome particle, 8 parts of citric acid, 4.5 parts of tannic acid, 6 parts of dialkyl dimethyl glycine betaine, hydroxypropyl methyl cellulose 5
Part, 7 parts of dioctyl sodium sulfosuccinate, 22 parts of water.
Further, in the preparation process of the phenols liposome particle, the parts by weight of following raw material are as follows: eucalyptus oil 10-
20 parts, 12-18 parts of clove oil, 6-12 parts of cocoanut fatty acid diethanolamide, 8-15 parts of polyglycerol polyricinoleate.
The preparation method of phenols environmental protection finishing agent of the present invention, which comprises the following steps:
(1) phenols liposome particle is dissolved in aqueous solution, is to slowly warm up to 40-60 DEG C in the condition of stirring, then successively added
Enter dialkyl dimethyl glycine betaine, hydroxypropyl methyl cellulose and dioctyl sodium sulfosuccinate, keeps this thermotonus 2-4h；
(2) reaction system of step (1) is down to room temperature, citric acid and tannic acid is added under stirring conditions, in room temperature after
Continuous stirring 20-40min, obtains phenols environmental protection finishing agent.
The utility model has the advantages that the finishing agent is the present invention provides a kind of phenols environmental protection finishing agent and preparation method thereof with phenols rouge
Antibacterial raw material based on plastid particle, then compounded with other function auxiliary agent, to improve the comprehensive performance of finishing agent.This hair
The phenolic substances of bright selection is obtained from extracted form natural plant, and natural environmental-protective is pollution-free, meets environmentally protective to modern product
Quality requirements.
The fabric that different finishing agents are handled is carried out 10 times being tested for the property after soaping and is obtained, bacteriostasis rate remains to reach
90% or more, to illustrate that finishing agent is with good stability.It is learnt by comparative example, phenols liposome particle is to finishing agent
Anti-microbial property play the role of conclusive, and citric acid and tannic acid are to the stability and anti-microbial property for maintaining finishing agent
Raising also function to important role.
Specific embodiment
The invention will now be further described with reference to specific embodiments, but examples are merely exemplary, not to this hair
Bright range constitutes any restrictions.It will be understood by those skilled in the art that without departing from the spirit and scope of the invention
Can with the details and forms of the technical scheme of the invention are modified or replaced, but these modification and replacement each fall within it is of the invention
In protection scope.
Embodiment 1
A kind of phenols environmental protection finishing agent, is prepared by the raw material of following parts by weight: 65 parts of phenols liposome particle, citric acid 8
Part, 4.5 parts of tannic acid, 6 parts of dialkyl dimethyl glycine betaine, 5 parts of hydroxypropyl methyl cellulose, dioctyl sodium sulfosuccinate 7
Part, 22 parts of water；
The preparation method of the phenols liposome particle the following steps are included:
(1) it weighs phenolic compound by corresponding parts by weight to be scattered in deionized water, so that the mass fraction of phenolic compound is
40wt%；15 parts of eucalyptus oil, 15 parts of clove oil are stirred with 11 parts of polyglycerol polyricinoleate and are mixed and made into oily phase；
(2) phenols aqueous solution in step (1) is added in oil-phase solution under stirring conditions, continues to be stirred and will be warm
Degree is slowly increased to 75 DEG C, stirs and reflection system is down to room temperature after 50min, mixture A is made；
(3) 9 parts of cocoanut fatty acid diethanolamide are added into mixture A, continues to be stirred at a temperature of 55 DEG C
1.5h obtains phenols liposome particle；
Wherein the phenolic compound in the phenols liposome particle is the ellagic acid and tea polyphenols that mass ratio is 1:1.
The preparation method of phenols environmental protection finishing agent of the present invention, comprising the following steps:
(1) phenols liposome particle is dissolved in aqueous solution, is to slowly warm up to 50 DEG C in the condition of stirring, then sequentially adds two
Alkyl dimethyl betaine, hydroxypropyl methyl cellulose and dioctyl sodium sulfosuccinate keep this thermotonus 3h；
(2) reaction system of step (1) is down to room temperature, citric acid and tannic acid is added under stirring conditions, in room temperature after
Continuous stirring 30min, obtains phenols environmental protection finishing agent.
Embodiment 2
A kind of phenols environmental protection finishing agent, is prepared by the raw material of following parts by weight: 50 parts of phenols liposome particle, citric acid 5
Part, 3 parts of tannic acid, 4 parts of dialkyl dimethyl glycine betaine, 3 parts of hydroxypropyl methyl cellulose, 4 parts of dioctyl sodium sulfosuccinate,
15 parts of water；
The preparation method of the phenols liposome particle the following steps are included:
(1) it weighs phenolic compound by corresponding parts by weight to be scattered in deionized water, so that the mass fraction of phenolic compound is
30wt%；10 parts of eucalyptus oil, 12 parts of clove oil are stirred with 8 parts of polyglycerol polyricinoleate and are mixed and made into oily phase；
(2) phenols aqueous solution in step (1) is added in oil-phase solution under stirring conditions, continues to be stirred and will be warm
Degree is slowly increased to 75 DEG C, stirs and reflection system is down to room temperature after 40min, mixture A is made；
(3) 6 parts of cocoanut fatty acid diethanolamide are added into mixture A, continues to be stirred 1h at a temperature of 55 DEG C,
Obtain phenols liposome particle.
Wherein the phenolic compound in the phenols liposome particle is arbutin.
The preparation method of phenols environmental protection finishing agent of the present invention, comprising the following steps:
(1) phenols liposome particle is dissolved in aqueous solution, is to slowly warm up to 40 DEG C in the condition of stirring, then sequentially adds two
Alkyl dimethyl betaine, hydroxypropyl methyl cellulose and dioctyl sodium sulfosuccinate keep this thermotonus 2h；
(2) reaction system of step (1) is down to room temperature, citric acid and tannic acid is added under stirring conditions, in room temperature after
Continuous stirring 20min, obtains phenols environmental protection finishing agent.
Embodiment 3
A kind of phenols environmental protection finishing agent, is prepared by the raw material of following parts by weight: 60 parts of phenols liposome particle, citric acid 6
Part, 4 parts of tannic acid, 5 parts of dialkyl dimethyl glycine betaine, 4 parts of hydroxypropyl methyl cellulose, 5 parts of dioctyl sodium sulfosuccinate,
20 parts of water；
The preparation method of the phenols liposome particle the following steps are included:
(1) it weighs phenolic compound by corresponding parts by weight to be scattered in deionized water, so that the mass fraction of phenolic compound is
35wt%；12 parts of eucalyptus oil, 14 parts of clove oil are stirred with 10 parts of polyglycerol polyricinoleate and are mixed and made into oily phase；
(2) phenols aqueous solution in step (1) is added in oil-phase solution under stirring conditions, continues to be stirred and will be warm
Degree is slowly increased to 75 DEG C, stirs and reflection system is down to room temperature after 45min, mixture A is made；
(3) 8 parts of cocoanut fatty acid diethanolamide are added into mixture A, continues to be stirred at a temperature of 55 DEG C
1.2h obtains phenols liposome particle.
Wherein the phenolic compound in the phenols liposome particle is resveratrol.
The preparation method of phenols environmental protection finishing agent of the present invention, comprising the following steps:
(1) phenols liposome particle is dissolved in aqueous solution, is to slowly warm up to 45 DEG C in the condition of stirring, then sequentially adds two
Alkyl dimethyl betaine, hydroxypropyl methyl cellulose and dioctyl sodium sulfosuccinate keep this thermotonus 2.5h；
(2) reaction system of step (1) is down to room temperature, citric acid and tannic acid is added under stirring conditions, in room temperature after
Continuous stirring 25min, obtains phenols environmental protection finishing agent.
Embodiment 4
A kind of phenols environmental protection finishing agent, is prepared by the raw material of following parts by weight: 80 parts of phenols liposome particle, citric acid 10
Part, 6 parts of tannic acid, 8 parts of dialkyl dimethyl glycine betaine, 7 parts of hydroxypropyl methyl cellulose, 9 parts of dioctyl sodium sulfosuccinate,
30 parts of water；
The preparation method of the phenols liposome particle the following steps are included:
(1) it weighs phenolic compound by corresponding parts by weight to be scattered in deionized water, so that the mass fraction of phenolic compound is
50wt%；20 parts of eucalyptus oil, 18 parts of clove oil are stirred with 15 parts of polyglycerol polyricinoleate and are mixed and made into oily phase；
(2) phenols aqueous solution in step (1) is added in oil-phase solution under stirring conditions, continues to be stirred and will be warm
Degree is slowly increased to 75 DEG C, stirs and reflection system is down to room temperature after 60min, mixture A is made；
(3) 12 parts of cocoanut fatty acid diethanolamide are added into mixture A, continues to be stirred at a temperature of 55 DEG C
2h obtains phenols liposome particle；
Wherein the phenolic compound in the phenols liposome particle is the tea polyphenols and resveratrol that mass ratio is 1:1.
The preparation method of phenols environmental protection finishing agent of the present invention, comprising the following steps:
(1) phenols liposome particle is dissolved in aqueous solution, is to slowly warm up to 60 DEG C in the condition of stirring, then sequentially adds two
Alkyl dimethyl betaine, hydroxypropyl methyl cellulose and dioctyl sodium sulfosuccinate keep this thermotonus 4h；
(2) reaction system of step (1) is down to room temperature, citric acid and tannic acid is added under stirring conditions, in room temperature after
Continuous stirring 40min, obtains phenols environmental protection finishing agent.
Comparative example 1
Comparative example 1 the difference from embodiment 1 is that, phenols liposome particle is not added in comparative example 1.
Comparative example 2
Comparative example 2 the difference from embodiment 1 is that, be not added with citric acid and tannic acid in comparative example 2.
Functional modifier made from embodiment 1-4 and comparative example 1 is subjected to impregnation, bath raio to real silk fabric respectively
For 1:30, dipping temperature is 40 DEG C, dip time 1h, takes out real silk fabric after having handled and washes and dry.
The fabric that different finishing agents are handled is carried out 10 times being tested for the property after soaping, test result is as shown in table 1, from
Obtained in table 1, finishing agent produced by the present invention is soaped after handling fabric through 10 times, bacteriostasis rate remain to reach 90% with
On, to illustrate that finishing agent is with good stability.It is learnt by comparative example, antibacterial of the phenols liposome particle to finishing agent
Performance plays the role of conclusive, and citric acid and tannic acid are in the raising to the stability and anti-microbial property that maintain finishing agent
Also function to important role.
Table 1
。
Claims (5)
1. a kind of phenols environmental protection finishing agent, which is characterized in that be prepared by the raw material of following parts by weight: phenols liposome particle
50-80 parts, 5-10 parts of citric acid, 3-6 parts of tannic acid, 4-8 parts of dialkyl dimethyl glycine betaine, hydroxypropyl methyl cellulose 3-7
Part, 4-9 parts of dioctyl sodium sulfosuccinate, 15-30 parts of water；
Wherein the phenolic compound in the phenols liposome particle includes ellagic acid, tea polyphenols, arbutin and resveratrol
One or more combination；
The preparation method of the phenols liposome particle the following steps are included:
(1) it weighs phenolic compound by corresponding parts by weight to be scattered in deionized water, so that the mass fraction of phenolic compound is
30-50wt%；Eucalyptus oil, clove oil are stirred with polyglycerol polyricinoleate and are mixed and made into oily phase；
(2) phenols aqueous solution in step (1) is added in oil-phase solution under stirring conditions, continues to be stirred and will be warm
Degree is slowly increased to 75 DEG C, stirs and reflection system is down to room temperature after 40-60min, mixture A is made；
(3) cocoanut fatty acid diethanolamide is added into mixture A, continues to be stirred 1-2h at a temperature of 55 DEG C,
Obtain phenols liposome particle.
2. a kind of phenols environmental protection finishing agent according to claim 1, which is characterized in that prepared by the raw material of following parts by weight
It forms: 60-70 parts of phenols liposome particle, 5-8 parts of citric acid, 4-6 parts of tannic acid, 5-7 parts of dialkyl dimethyl glycine betaine, hydroxyl
4-6 parts of propyl methocel, 5-8 parts of dioctyl sodium sulfosuccinate, 18-16 parts of water.
3. a kind of phenols environmental protection finishing agent according to claim 1, which is characterized in that prepared by the raw material of following parts by weight
It forms: 65 parts of phenols liposome particle, 8 parts of citric acid, 4.5 parts of tannic acid, 6 parts of dialkyl dimethyl glycine betaine, hydroxypropyl first
5 parts of base cellulose, 7 parts of dioctyl sodium sulfosuccinate, 22 parts of water.
4. a kind of phenols environmental protection finishing agent according to claim 1, which is characterized in that the system of the phenols liposome particle
During standby, the parts by weight of following raw material are as follows: 10-20 parts of eucalyptus oil, 12-18 parts of clove oil, coco-nut oil fatty acid diethanol
6-12 parts of amide, 8-15 parts of polyglycerol polyricinoleate.
5. the preparation method of the described in any item phenols environmental protection finishing agents of claim 1-4, which is characterized in that including following step
It is rapid:
(1) phenols liposome particle is dissolved in aqueous solution, is to slowly warm up to 40-60 DEG C in the condition of stirring, then successively added
Enter dialkyl dimethyl glycine betaine, hydroxypropyl methyl cellulose and dioctyl sodium sulfosuccinate, keeps this thermotonus 2-4h；
(2) reaction system of step (1) is down to room temperature, citric acid and tannic acid is added under stirring conditions, in room temperature after
Continuous stirring 20-40min, obtains phenols environmental protection finishing agent.
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| CN104532559A (en) * | 2014-11-13 | 2015-04-22 | 苏州威尔德工贸有限公司 | A silk/cotton fabric afterfinish method based on tea polyphenol |
| CN105544192A (en) * | 2016-01-21 | 2016-05-04 | 苏州经贸职业技术学院 | Natural antibacterial finishing agent and preparation method thereof |
| CN105816337A (en) * | 2016-04-19 | 2016-08-03 | 东南大学 | Composite polyphenol active materials-loaded solid lipid particle and preparation method thereof |
| CN106436323A (en) * | 2016-10-11 | 2017-02-22 | 漳州市鼎鑫电子科技有限公司 | Natural antibacterial and deodorizing finishing agent for non-woven fabrics and preparation method of finishing agent |
-
2019
- 2019-08-07 CN CN201910725769.2A patent/CN110409174A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102614091A (en) * | 2011-01-27 | 2012-08-01 | 夏强 | Resveratrol nanostructured lipid carrier and preparation method thereof |
| CN103757894A (en) * | 2013-12-31 | 2014-04-30 | 天津工业大学 | Method for preparing natural antibacterial and anti-ultraviolet functional finishing agent with Tieguanyin tea stalks |
| CN104532559A (en) * | 2014-11-13 | 2015-04-22 | 苏州威尔德工贸有限公司 | A silk/cotton fabric afterfinish method based on tea polyphenol |
| CN105544192A (en) * | 2016-01-21 | 2016-05-04 | 苏州经贸职业技术学院 | Natural antibacterial finishing agent and preparation method thereof |
| CN105816337A (en) * | 2016-04-19 | 2016-08-03 | 东南大学 | Composite polyphenol active materials-loaded solid lipid particle and preparation method thereof |
| CN106436323A (en) * | 2016-10-11 | 2017-02-22 | 漳州市鼎鑫电子科技有限公司 | Natural antibacterial and deodorizing finishing agent for non-woven fabrics and preparation method of finishing agent |
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Application publication date: 20191105 |