CN110403022A - One kind being suitable for 0 ~ 12 month ready-to-feed infant milk and preparation method thereof - Google Patents
One kind being suitable for 0 ~ 12 month ready-to-feed infant milk and preparation method thereof Download PDFInfo
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- CN110403022A CN110403022A CN201810400000.9A CN201810400000A CN110403022A CN 110403022 A CN110403022 A CN 110403022A CN 201810400000 A CN201810400000 A CN 201810400000A CN 110403022 A CN110403022 A CN 110403022A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C21/00—Whey; Whey preparations
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C21/00—Whey; Whey preparations
- A23C21/04—Whey; Whey preparations containing non-milk components as source of fats or proteins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C21/00—Whey; Whey preparations
- A23C21/06—Mixtures of whey with milk products or milk components
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C21/00—Whey; Whey preparations
- A23C21/08—Whey; Whey preparations containing other organic additives, e.g. vegetable or animal products
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The present invention provides a kind of ready-to-feed infant milk and preparation method thereof for being suitable for 0 ~ 12 month, the ready-to-feed infant milk each component content is under the premise of meeting infant formula national standard, also contain polypeptide and carragheen, the content of the polypeptide is that every 100ml liquid milk contains 180.0mg or more；The content of the carragheen is that every 100ml liquid milk contains 0.005~0.03g.
Description
Technical field
The present invention relates to a kind of ready-to-feed infant milks and preparation method thereof, in particular to are suitable for 0~12 month consumption by infants
Ready-to-feed infant milk and preparation method thereof, belong to baby milk technical field.
Background technique
Infant stage is of great significance, and the growth and development of the baby in this period is very fast, and the demand to nutrition is very
Height not only needs feeding nutrition equilibrium, comprehensive food, with greater need for digestible food, because of digestion and the generation of cradle
Thank to systematic growth also and be not it is very perfect, especially to those since work requirements or physical condition etc. cause breast-feeding to lack
Baby for digestible food be undoubtedly most suitable selection.But the milk powder substitute type in current China market is seldom,
Be suitble to consumption by infants nutrient supplement food type be also it is limited, infant stage is mainly based on baby milk and rice flour, product
Mainly solid-state form；Due to the limitation such as life and eating habit, material conditions it is difficult to ensure that daily normal nutrition intake.Cause
This, jumps out the limitation of existing product form, and the infant formula for developing high-quality has critically important society and economic meaning
Justice.
For baby, best food is breast milk, because containing nutriment and increasing necessary to infant physical growth in breast milk
The ingredient of strong infant immunity also has more and more people to recognize breast-feeding although breast-feeding is all being advocated in the whole world
Importance, but the breastfeeding rate of China is being gradually reduced at present for various reasons, the especially mother of urban population
Newborn feeding rate decrease speed is faster.So being taken in for relatively high, the comparatively faster crowd of rhythm of life to this part, nutrition
Comprehensively, quality is higher, reconstitutes and is easily undoubtedly only selection for milk product.
In addition to breast milk, cow's milk is due to its is from a wealth of sources and breast milk composition is closer to as the main milk powder substitute of baby.
But cow's milk protein and breast milk proteins have differences in composition, and the casein in cow's milk is easy to be formed in baby's stomach larger
Grumeleuse, lead to baby's indigestion；Beta lactoglobulin easily causes the allergic reaction etc. of baby.Therefore, it is necessary to carry out to cow's milk
Improvement appropriate makes it closer to the nutritional ingredient of breast milk, is not only suitable for baby's digestion to produce but also meets infant nutrition need
The milk replacer wanted.It is popular in external many national ready-to-feed infant milks, and the infant formula in China is also mainly with solid
Based on baby milk, compared with baby milk, ready-to-feed infant milk has lot of advantages, such as does not need to reconstitute, constant concentration, nursing side
Just, safety and sanitation etc..Infant formula develops to liquid direction has become trend of the times, at present to-feed infant cream market at home
Also in blank, development prospect is wide, it is contemplated that arrives the year two thousand twenty, formula liquid milk will have hundred million yuan of 3-5 of the market share.
For ready-to-feed infant milk, too many differences are had no on formula, the technological difficulties for producing the product are product
Sterilization treatment and stability in terms of.CN101313702A discloses a kind of 6 to 12 months baby's liquid milks and straight with injecting type
The preparation method of sterilization is connect, sterilization treatment is carried out to product using UHT steam jet type direct sterilization technology.
CN102630760A discloses a kind of infant formula concentrated milk and preparation method thereof, and UHT mode is used to sterilize product
Processing.CN102511557A discloses a kind of ready-to-feed infant milk and its production method suitable for coming into being by 6 months, using film mistake
Filter and low-heat Bactericidal composite mode handle thermo-responsive Water-solubility Material.
It can be seen that each Dairy Enterprise is respectively adopted different sterilization technologies and goes to handle such product from the above prior art,
The problem of protein denaturation precipitation and stability can mainly occur in high-temperature sterilization due to such product, as using improving
Low-temperature treatment rule can face the uncontrollable problem of microorganism, thus, such product almost all employs a large amount of stable emulsifying
Agent goes to make up the defect of product thermostabilization fermentation, this is very unfavorable for cleaning products label.
In summary, that there is a need in the field to provide a kind of thermal stability is good, spatter property is good, is easy digestion and was not easy to cause
Quick ready-to-feed infant milk and preparation method thereof.
Summary of the invention
It is needed in view of reality, one of the objects of the present invention is to provide a kind of liquid suitable for 0~12 month baby
It is good to obtain a kind of stability to it in the case of addition stabilizer few as far as possible by high temperature sterilization for baby milk
Liquid baby milk.
Another object of the present invention is to provide the preparation methods of above-mentioned ready-to-feed infant milk.
To achieve the above object, the present invention provides a kind of ready-to-feed infant milk suitable for 0~12 month, with its every 100KJ
The corresponding ready-to-feed infant milk meter of heat, it includes: the protein of 0.45~0.70g, the fat of 1.05~1.40g, 2.2~3.3g
Carbohydrate, 0.07~0.33g linoleic acid, >=12mg linseed oil, 14~43 μ g vitamin As, 0.25~0.60 μ g dimension life
Plain D, 0.12~0.20mg vitamin E, 1.0~6.5 μ g vitamin K1s, 14~72 μ g vitamin B1s, 19~119 μ g vitamins
B2,8.5~45.0 μ g vitamin B6s, 0.025~0.360 μ g vitamin B12,70~360 μ g niacin, 2.5~12.0 μ g folic acid,
96~478 μ g pantothenic acid, 2.5~17.0mg vitamin C, 0.4~2.4 μ g biotin, 5~14mg sodium, 14~43mg potassium, 8.5~
29.0 μ g copper, 1.2~3.6mg magnesium, 0.10~0.36mg iron, 0.12~0.36mg zinc, 1.2~24 μ g manganese, 12~35mg calcium, 6
~24mg phosphorus, 2.5~14.0 μ g iodine, 12~38mg chlorine, 0.48~1.90 μ g selenium ,≤3mg taurine, 1.7~12.0mg choline；
Ready-to-feed infant milk described in every 100mL contains the heat of 250~295KJ, and the ready-to-feed infant milk contains polypeptide simultaneously
And carragheen, the content of the polypeptide are that every 100ml liquid milk contains 180.0mg or more, preferably contain 200.0~450.0mg；It is described
The content of carragheen is that every 100ml liquid milk contains 0.005~0.03g.
Ready-to-feed infant milk each component content of the present invention is meeting infant formula national standard (GB10765-2010)
Under the premise of, innovative to be added to polypeptide and carragheen simultaneously in ready-to-feed infant milk, the two collective effect significantly improves
The thermal stability of baby's liquid milk passes through stability of the high temperature sterilization without influencing finished product, is in particular in whole production
Product precipitation capacity and fat floating amount significantly reduce, and in addition finished product also has good color.It is compared with existing ready-to-feed infant milk,
Stable emulsifying system of the present invention greatly simplifies, and cleans Product labelling more.Furthermore compared with existing ready-to-feed infant milk, this hair
Bright baby milk can be improved baby's abilities of digestive and absorption, reduce anaphylaxis due to containing polypeptide.Formulated infant milk nutrition of the invention
Equilibrium, quality is stablized, easy to carry, without reconstituting or diluting, drinks conveniently.
The present invention is outer without especially indicating, and content or ratio of the present invention each mean weight or weight ratio.
In the present invention, the content of peptides in the ready-to-feed infant milk is measured using trichloroacetic acid method.As described above, every
Polypeptide of the 100ml liquid milk containing 180.0mg or more, preferably 200.0~450.0mg, such as 226.0mg/100ml, 285.0mg/
100ml。
As described above, the dosage of carragheen is ready-to-feed infant milk carragheen containing 0.005~0.03g described in every 100ml.Such as
0.010g/100ml, 0.015g/100ml, 0.020g/100ml, 0.025g/100ml, 0.030g/100ml etc..
Newborn peptide of the invention can be formed in the polypeptide in above-mentioned content range in preparation method, such as in preparation method
Raw material using protease to raw milk etc. containing protein is hydrolyzed, and the raw material containing polypeptide prepared can also directly be added
It adds in liquid milk, such as can directly add hydrolysis desalted whey powder.In certain embodiments of the present invention, it is preferable that institute
Stating ready-to-feed infant milk is made in the ready-to-feed infant milk by adding part or all of protein by the emulsified material after protease hydrolyzed
Content of peptides is that every 100ml contains 180.0~450.0mg.It is highly preferred that the emulsified material by after protease hydrolyzed includes raw milk
One of hydrolyzate, hydrolysis desalted whey powder, hydrolysis concentrated whey protein powder are a variety of.In some embodiments, described
The content of peptides of raw milk hydrolyzate is 3.0~9.0mg/mL.In some embodiments, the hydrolysis desalted whey powder is more
Peptide content is 12.0~36.0mg/g.In some embodiments, the content of peptides of the hydrolysis concentrated whey protein powder is
80.0~392.0mg/g, usually 80.0~240.0mg/g.
In certain embodiments of the present invention, it is preferable that the raw material of ready-to-feed infant milk described in every 1000Kg, which forms, includes
Following component: 128.5~320Kg of raw milk hydrolyzate, hydrolysis 20~90Kg of desalted whey powder, hydrolysis concentrated whey protein powder 0
~18Kg, 8.9~15.5Kg of anhydrous butter oil, 10.0~15.4Kg of vegetable oil, 0~25.4Kg of lactose, multi-vitamins 0.32~
0.6Kg, 0.64~0.96Kg of composite mineral matter, 0.075~0.115Kg of choline, 0.065~0.095Kg of taurine, carragheen
0.05~0.3Kg, 0.05~0.25Kg of citric acid, remaining benefit are filled with water to 1000Kg.
Preferably, the raw milk hydrolyzate in above-mentioned ready-to-feed infant milk is formed by milk.It is highly preferred that the raw milk water
Solving content of peptides in liquid is 3.0~9.0mg/mL.
Preferably, the hydrolysis desalted whey powder in above-mentioned ready-to-feed infant milk is formed by desalted whey powder.It is highly preferred that should
Content of peptides is 12.0~36.0mg/g in desalted whey powder.
Preferably, the hydrolysis concentrated whey protein powder in above-mentioned ready-to-feed infant milk is formed by concentrated whey protein powder.More
Preferably, content of peptides is 80.0~240.0mg/g in the hydrolysis concentrated whey protein powder.
The raw material composition of ready-to-feed infant milk of the present invention is based on but is not limited to formula provided by the invention, can be in this hair
Increase the nutrient for being conducive to infants growth and development on the basis of bright offer formula.Such as MFGM (butterfat ball film), DHA, newborn iron
Albumen etc..
The raw material composition of ready-to-feed infant milk of the present invention is based on but is not limited to formula provided by the invention, can be in this hair
Other raw-food materials (other protein raw materials or unsaturated fatty acid, phosphatide etc.) and emulsification are added on the basis of bright offer formula
Agent (glycerin monostearate, citric acid fatty glyceride, dosage is referring to national standard), stabilizer (locust bean gum, guar gum
Deng, dosage referring to national standard) etc. food additives.
On the other hand, the present invention provides the preparation method of above-mentioned ready-to-feed infant milk comprising following steps:
(1) it gets all the ready or prepares and the material and other raw materials of polypeptide are provided, and be mixed, supply total weight with water；
(2) homogeneous is carried out to the mixed material that step (1) obtains；Preferably, level-one homogenization pressure be 15~20MPa,
Double-stage homogenization pressure carries out homogeneous under the conditions of being 3~5MPa；
(3) material after step (2) homogeneous is sterilized, it is preferable that sterilization processing is carried out using UHT, it is highly preferred that
2~5s is handled at 130~140 DEG C to be sterilized；
(4) cooling the ready-to-feed infant milk is carried out to the material after sterilization.
In some embodiments, step (1) directly prepares the material of the offer polypeptide, which includes following step
It is rapid:
(1.1) emulsified material for being partially or wholly used for providing protein in the ready-to-feed infant milk is carried out heat treatment makes wherein
Albuminous degeneration, then which is cooled to the temperature for being suitable for protease hydrolytic, and add water before cooling or after cooling,
Formed system to be hydrolyzed (preferably, first add water in the emulsified material of protein in the ready-to-feed infant milk is provided, then again into
Row heat treatment)；
(1.2) protease is added in the solution after cooling obtained to step (1.1) to be hydrolyzed, heat inactivation egg after hydrolysis
White enzyme obtains the material of the offer polypeptide.
In the above-mentioned method for preparing the material that polypeptide is provided, it is preferable that described to be used to provide the described to-feed infant
The emulsified material of protein includes one in raw milk, desalted whey powder, whey protein concentrate or other emulsified materials containing protein in milk
Kind is a variety of.
In the above-mentioned method for preparing the material that polypeptide is provided, it is preferable that the albumen in the system to be hydrolyzed
Matter concentration is 3.0%~20.0%.
In the above-mentioned method for preparing the material that polypeptide is provided, it is preferable that it is added before protease, it is described wait hydrolyze
System in the mass ratio of water be 80%~90% or so to be advisable.
In the above-mentioned method for preparing the material that polypeptide is provided, it is preferable that in step (2), the protease is
Meet the compound protein that GB2760 mixes one or more of protease of protease requirements in food according to different proportion
Enzyme.It is highly preferred that the protease is compound protease, which includes the neutral proteinase that weight ratio is 3~8:1
F (Validase FP Concentrate) and neutral proteinase G (Protease GBW).The additive amount of the protease is to account for
The 0.4%~0.9% of protein substrate quality.
In the above-mentioned method for preparing the material that polypeptide is provided, it is preferable that the addition protease, which is hydrolyzed, is
It is hydrolyzed under the conditions of the optimum temperature of protease, pH, hydrolysis time is that the content for the polypeptide for generating hydrolysis reaches most
Content of peptides in finished product ready-to-feed infant milk, selective hydrolysis time are 0.5~5.0h.
The sterilization mode or combinations thereof that prior art routine can be used in step (3) of the present invention, as long as reaching bactericidal effect
, since inventive formulation has thermal stability, it is contemplated that UHT sterilization can be used in the simplification of technique.
As described above, in make to form products material containing both quantitative polypeptide in ready-to-feed infant milk of the present invention
Part or all of Protein material is hydrolyzed or is by directly adding protein hydrolysate (hydrolyzing lactoalbumin, caseinhydrolysate
Deng) raw material is used as to produce product.
Preferably, the preparation method of above-mentioned ready-to-feed infant milk includes the following steps:
(1.1) will be partially or wholly used for providing the emulsified material of protein in the ready-to-feed infant milk be hybridly prepared into water it is molten
Liquid, and carry out heat treatment make protein denaturation therein, then which is cooled to the temperature for being suitable for protease hydrolytic；
(1.2) protease is added in the solution after cooling obtained to step (1.1) in its optimal temperature and pH condition
Under be hydrolyzed to product polypeptide content and meet the requirements, heat, which inactivates the protease, after hydrolysis must provide the material of polypeptide；
(1.3) material for the offer polypeptide for obtaining step (1.2) and remaining raw material mix, and supply gross weight with water
Amount；
(2) homogeneous is carried out to the mixed material that step (1.3) obtain；It is that 15~20MPa, second level are equal in level-one homogenization pressure
Matter pressure carries out homogeneous under the conditions of being 3~5MPa；
(3) material after step (2) homogeneous is sterilized, carries out UHT under the conditions of 2~5s is handled at 130~140 DEG C
Sterilization；
(4) cooling the ready-to-feed infant milk is carried out to the material after sterilization.
The present invention routinely technology can carry out sterile filling to gained ready-to-feed infant milk.The raw material that the present invention uses is food
Grade, it is commercially available.The water that the present invention uses is that water is routinely used in this field, and deionized water is more suitable for.
In summary, the present invention provides the ready-to-feed infant milks and its system of a kind of consumption by infants for being suitable for 0~12 month
Preparation Method has the following beneficial effects:
(1) present invention can be discharged polypeptide using biological enzymolysis technology protein hydrolysate and using this as in finished product stabilising system
One kind, with carragheen collective effect while reaching preferable stablizing effect, simplify product stability system composition, cleaning produce
Product label；
(2) the problem of invention also overcomes albuminous degeneration precipitates during the preparation process due to formulated infant milk, improves
The thermal stability of product makes it that the mode of high-temperature sterilization can be used, simplifies production technology；
(3) present invention, which is alleviated, leads to baby's indigestion due to more containing high molecular weight protein due to formulated infant milk
The phenomenon that；
(4) caused by the present invention is possible to alleviate baby because of edible macromolecular milk protein (mainly beta lactoglobulin)
Allergic phenomena.
Detailed description of the invention
Fig. 1 is the flow diagram that the embodiment of the present invention 1 prepares ready-to-feed infant milk.
Specific embodiment
In order to which technical characteristic of the invention, purpose and beneficial effect are more clearly understood, now in conjunction with specific implementation
Example and technical solution of the present invention is carried out described further below, it should be understood that these examples be merely to illustrate the present invention rather than
It limits the scope of the invention.In embodiment, each Starting reagents material is commercially available, test method without specific conditions
For conventional method known to fields and normal condition, or according to condition proposed by apparatus manufacturer.
Polypeptide in following embodiment is measured by trichloroacetic acid method comprising following steps:
(1) standard curve making: taking glutathione standard solution (0.8mg/mL), successively draw above-mentioned solution 0,1,2,3,
4,5mL is placed in 6 test tubes, respectively plus 3mL biuret reagent, is settled to 10mL with distilled water, and 60 DEG C of water-baths develop the color 5min, water
It is ceaselessly vibrated during bath, then cools to room temperature (25~35 DEG C), OD value is measured under 310nm and (blank pair is done with the 1st pipe
According to).Using peptide concentration as abscissa X (mg/mL), OD value is ordinate Y, makes standard curve.
(2) 2.5mL sample solution is taken, trichloroacetic acid (TCA) aqueous solution of 2.5mL 10% (w/v) is added, it is mixed in whirlpool
It closes and is uniformly mixed on instrument, stand 20min, be then centrifuged 10min at 3500r/min.
(3) the above-mentioned solution of 1.0mL is taken to set in a test tube, addition biuret reagent 3.0mL (sample liquid: biuret reagent=3:
2, v/v), in being uniformly mixed on whirlpool mixed instrument, 60 DEG C of water-baths colour developings 5min, 2000r/min are centrifuged 10min.
(4) supernatant is taken to measure OD value under 310nm, reference standard curve obtains the peptide concentration C in sample solution
(mg/m L), and then can determine content of peptides in sample.
Embodiment 1
The present invention provides a kind of formulated infant milk and preparation method thereof, the dry matter content of the formulated infant milk is
12.5wt.%, the component that every 1000Kg formulated infant milk is included are as follows: raw milk hydrolyzate 255.75Kg, hydrolysis desalination cream
Clear powder 61.50Kg, anhydrous butter oil 14.5Kg, vegetable oil 10.0Kg, lactose 9.5Kg, multi-vitamins 0.32Kg, composite mineral matter
0.64Kg, choline 0.075Kg, taurine 0.065Kg, carragheen 0.15Kg, citric acid 0.05Kg, remaining benefit are filled with water to
1000Kg。
As shown in Fig. 1 flow chart, the preparation method of the formulated infant milk includes the following steps:
(1) it after the fresh raw milk of 255.75Kg being carried out an acceptance inspection, filter and purified, is then heat-treated at 80 DEG C
10min makes albuminous degeneration, which is cooled to 55 DEG C；
(2) (by neutral proteinase F, (Validase FP Concentrate, is purchased from addition protease in Xiang Shangshu solution
In Royal DSM trade (Shanghai) Co., Ltd.) and neutral proteinase G (Protease GBW is purchased from Royal DSM
Trade (Shanghai) Co., Ltd.) compound protease that is mixed according to the ratio of 5:1) it is digested, compound protease adds
Dosage is the 0.4% of substrate protein content, 1.0h is hydrolyzed while stirring under the conditions of 55 DEG C, by above-mentioned solution under the conditions of 80 DEG C
10min inactivated proteases are heated, raw milk hydrolyzate is obtained；Content of peptides in the raw milk hydrolyzate is measured by trichloroacetic acid method
For 4.5mg/mL.
(3) solution after above-mentioned hydrolysis (is hydrolyzed into polypeptide in desalted whey powder with 61.50Kg hydrolysis desalted whey powder respectively
Content is 34.8mg/g), 0.15Kg carragheen, 14.5Kg anhydrous butter oil and the mixing of 10.0Kg vegetable oil, it is then that solution is cooling
After to 60 DEG C be added 0.32Kg multi-vitamins, 0.64Kg composite mineral matter, 0.075Kg choline, 0.065Kg taurine,
0.05Kg citric acid is mixed, and supplies 1000Kg with water；
(4) by above-mentioned mixed feed liquid in the case where level-one homogenization pressure is 15-20MPa, double-stage homogenization pressure is 3-5MPa
Homogenization；
(5) feed liquid after above-mentioned homogeneous is handled to 2-5s at 130-140 DEG C and carries out UHT sterilization；
(6) it by sterile filling after the feed liquid cooling after above-mentioned UHT sterilization processing, is got product after examination.
Trichloroacetic acid method is used to detect in above-mentioned finished product content of peptides as 3.29g/kg.
Comparative example 1
It is replaced outside hydrolysis desalted whey powder except raw milk is without enzymolysis processing, and with desalted whey powder, other and reality
The product formula for applying example 1 is consistent with preparation method, prepares a formulated infant milk, in this, as comparative example 1.
1 preparation method of comparative example is as follows, and raw material and technique meet relevant national standard.
The dry matter content of the formulated infant milk is 12.5wt.%, and the component that every 1000Kg formulated infant milk is included is such as
Under: raw milk 255.75Kg, desalted whey powder 61.50Kg, anhydrous butter oil 14.5Kg, vegetable oil 10.0Kg, lactose 9.5Kg, answer
Close vitamin 0.32Kg, composite mineral matter 0.64Kg, choline 0.075Kg, taurine 0.065Kg, carragheen 0.15Kg, citric acid
0.05Kg, remaining benefit are filled with water to 1000Kg.
(1) first desalted whey powder is dissolved at 80 DEG C or so with the water for accounting for ingredient total amount 30%, then respectively will in order
Examination, filtering and purified 255.75Kg raw milk, 0.15Kg carragheen and 14.5Kg anhydrous butter oil and 10.0Kg plant
It is oily to be mixed with above-mentioned dissolved material；
(2) by remaining unclassified stores 9.5Kg lactose, 0.32Kg multi-vitamins, 0.64Kg grandidierite after being cooled to 60 DEG C
Substance, 0.075Kg choline, 0.065Kg taurine, 0.05Kg citric acid are added in above-mentioned (1) material and supply 1000Kg progress
Dissolution；
(3) by above-mentioned mixed feed liquid in the case where level-one homogenization pressure is 15-20MPa, double-stage homogenization pressure is 3-5MPa
Homogenization；
(4) feed liquid after above-mentioned homogeneous is handled to 2-5s at 130-140 DEG C and carries out UHT sterilization；
(5) it by sterile filling after the feed liquid cooling after above-mentioned UHT sterilization processing, is got product after examination.
Trichloroacetic acid method is used to detect in above-mentioned finished product content of peptides as 1.69g/kg.
Comparative example 2
In addition to not adding stabilizer carragheen, other are consistent with the product formula of embodiment 1 and preparation method, prepare
A formulated infant milk, in this, as comparative example 2.
2 preparation method of comparative example is as follows, and raw material and technique meet relevant national standard.
The dry matter content of the formulated infant milk is 12.5wt.%, and the component that every 1000Kg formulated infant milk is included is such as
Under: raw milk hydrolyzate 255.75Kg, hydrolysis desalted whey powder 61.50Kg, anhydrous butter oil 14.5Kg, vegetable oil 10.0Kg, cream
Sugared 9.5Kg, multi-vitamins 0.32Kg, composite mineral matter 0.64Kg, choline 0.075Kg, taurine 0.065Kg, citric acid
0.05Kg, remaining benefit are filled with water to 1000Kg.
Wherein, the preparation method of the formulated infant milk includes the following steps:
(1) examination, filtering and purified raw milk are carried out heat treatment 10min at 80 DEG C makes albuminous degeneration, then
The solution is cooled to 55 DEG C；
(2) (by neutral proteinase F, (Validase FP Concentrate, is purchased from addition protease in Xiang Shangshu solution
In Royal DSM trade (Shanghai) Co., Ltd.) and neutral proteinase G (Protease GBW is purchased from Royal DSM
Trade (Shanghai) Co., Ltd.) compound protease that is mixed according to the ratio of 5:1) it is digested, compound protease adds
Dosage is the 0.4% of substrate protein content, 1.0h is hydrolyzed while stirring under the conditions of 55 DEG C, by above-mentioned solution under the conditions of 80 DEG C
10min inactivated proteases are heated, raw milk hydrolyzate is obtained；Content of peptides in the raw milk hydrolyzate is measured by trichloroacetic acid method
For 4.5mg/mL.
(3) solution after above-mentioned hydrolysis (is hydrolyzed into polypeptide in desalted whey powder with 61.50Kg hydrolysis desalted whey powder respectively
Content is 34.8mg/g), 14.5Kg anhydrous butter oil and the mixing of 10.0Kg vegetable oil, it is multiple that 0.32Kg is added after being subsequently cooled to 60 DEG C
It closes vitamin, 0.64Kg composite mineral matter, 0.075Kg choline, 0.065Kg taurine, 0.05Kg citric acid to be mixed, uses water
Supply 1000Kg；
(4) by above-mentioned mixed feed liquid in the case where level-one homogenization pressure is 15-20MPa, double-stage homogenization pressure is 3-5MPa
Homogenization；
(5) feed liquid after above-mentioned homogeneous is handled to 2-5s at 130-140 DEG C and carries out UHT sterilization；
(6) it by sterile filling after the feed liquid cooling after above-mentioned UHT sterilization processing, is got product after examination.
Trichloroacetic acid method is used to detect in above-mentioned finished product content of peptides as 3.29g/kg.
Effect example 1
For the formulated infant milk made from the embodiment of the present invention 1, press " national food safety standard infant formula "
GB10765-2010 is reference, compares evaluation with the nutritive index of comparative example 1,2, comparing result is as shown in table 1.It will implement
Example 1, comparative example 1, in comparative example 2 products obtained therefrom according in " national food safety standard infant formula " GB10765-2010
Method detect each index, acquired results are as shown in table 1 below, GB10765-2010 is also listed in table 1 to the regulation of indices:
The evaluation of 1 nutritive index of table
Embodiment 1 and formulated infant milk items nutritive index made from comparative example 1 and comparative example 2 are several as can be seen from Table 1
There is no difference, meets and required as defined in " national food safety standard infant formula " GB10765-2010, be suitble to 0-
12 month infants are directly edible.
Effect example 2
The estimation of stability of infant formula milk of the present invention:
It is put as test sample in room temperature (10-25 DEG C or so) using the product of the embodiment of the present invention 1 and comparative example 1, comparative example 2
Observation is set, color, precipitation capacity, fat were carried out to above-mentioned 3 groups of formulated infant milks respectively at room temperature 7 days, 30 days and 60 days
Float-amount is tested.
Precipitation capacity is measured using centrifugal process: by sample as in centrifuge tube, 3000 turns centrifugal treating 15 minutes, sufficiently take out
Sediment weight is weighed after supernatant.
Fat floating amount uses tape measure: product sterile filling stands and places in the colorimetric cylinder of 100mL.It is standing
The fat deposit thickness for the ruler measurement milk superficial white for being 0.5mm with precision across glass bottle wall under state, sight when reading
Head-up.
Product color evaluation method are as follows: 5 food organoleptic evaluation assistant directors is asked to carry out the color of above-mentioned 3 groups of formulated infant milks
Evaluation, the average value that final color evaluation result takes 5 people to give a mark, comparing result are as shown in table 3.Color evaluation is using 5 points of scorings
Method of inspection, scale type and conversion fraction value are as shown in table 2 below:
Table 2
| Hobby | It is very good | It is good | Generally | It is bad | It is very bad |
| Score | 5 | 4 | 3 | 2 | 1 |
3 estimation of stability of table
Formulated infant milk of the invention places 7 days substantially without any at normal temperature it can be seen from stability test data
Variation, the precipitation capacity that embodiment generates after placing 30 days is minimum, but comparative example 1, the precipitation capacity of 2 products are compared compared with embodiment and existed
Notable difference, precipitation capacity is larger, and the present invention is significantly mentioned by carrying out appropriate hydrolysis to protein and adding certain carragheen
The overall stability of to-feed infant formula milk is risen.When only carrying out appropriate hydrolysis to protein respectively or only adding carragheen,
The stability of system is all unable to reach the effect being used cooperatively.
Formulated infant milk and preparation method thereof of the invention is proved by stability experiment data, can be obtained and is suitable for fortune
Defeated, sale shelf life and shelf-life.
It can be seen from above-mentioned experimental data formulated infant milk nutrition of the invention comprehensively and excellent in stability, it is more important
Be albumen refinement can be obtained using preparation method of the invention and the high based infant formula products of thermal stability, product are beneficial
Digestion, is more advantageous to the overall absorption of infant nutrition.
Embodiment 2
The present invention provides a kind of formulated infant milk and preparation method thereof, the dry matter content of the formulated infant milk is
12.5wt.%, the component that every 1000Kg formulated infant milk is included are as follows: raw milk hydrolyzate 255.75Kg, hydrolysis desalination cream
Clear powder 61.50Kg, anhydrous butter oil 14.5Kg, vegetable oil 10.0Kg, lactose 9.5Kg, multi-vitamins 0.32Kg, composite mineral matter
0.64Kg, choline 0.075Kg, taurine 0.065Kg, carragheen 0.20Kg, citric acid 0.05Kg, remaining benefit are filled with water to
1000Kg。
As shown in Fig. 1 flow chart, the preparation method of the formulated infant milk includes the following steps:
(1) it after the fresh raw milk of 255.75Kg being carried out an acceptance inspection, filter and purified, is then heat-treated at 80 DEG C
10min makes albuminous degeneration, which is cooled to 55 DEG C；
(2) protease A mano2SD (being purchased from Amano Enzyme Inc.) is added in Xiang Shangshu solution to be digested,
The additive amount of protease is the 0.3% of substrate protein content, hydrolyzes 1.0h while stirring under the conditions of 55 DEG C, above-mentioned solution is existed
10min inactivated proteases are heated under the conditions of 80 DEG C, obtain raw milk hydrolyzate；The raw milk hydrolyzate is measured by trichloroacetic acid method
Middle content of peptides is 4.0mg/mL.
(3) solution after above-mentioned hydrolysis (is hydrolyzed into polypeptide in desalted whey powder with 61.50Kg hydrolysis desalted whey powder respectively
Content is 34.8mg/g), 0.15Kg carragheen, 14.5Kg anhydrous butter oil and the mixing of 10.0Kg vegetable oil, it is then that solution is cooling
After to 60 DEG C be added 0.32Kg multi-vitamins, 0.64Kg composite mineral matter, 0.075Kg choline, 0.065Kg taurine,
0.05Kg citric acid is mixed, and supplies 1000Kg with water；
(4) by above-mentioned mixed feed liquid in the case where level-one homogenization pressure is 15-20MPa, double-stage homogenization pressure is 3-5MPa
Homogenization；
(5) feed liquid after above-mentioned homogeneous is handled to 2-5s at 130-140 DEG C and carries out UHT sterilization；
(6) it by sterile filling after the feed liquid cooling after above-mentioned UHT sterilization processing, is got product after examination.
Trichloroacetic acid method is used to detect in above-mentioned finished product content of peptides as 3.16g/kg.
Requirement is all satisfied using the finished product nutritive index and stability of this method preparation.
Embodiment 3
The present invention provides a kind of formulated infant milk and preparation method thereof, the dry matter content of the formulated infant milk is
12.5wt.%, the component that every 1000Kg formulated infant milk is included are as follows: raw milk hydrolyzate 255.75Kg, hydrolysis desalination cream
Clear powder 61.50Kg, anhydrous butter oil 14.5Kg, vegetable oil 10.0Kg, lactose 9.5Kg, multi-vitamins 0.32Kg, composite mineral matter
0.64Kg, choline 0.075Kg, taurine 0.065Kg, carragheen 0.10Kg, citric acid 0.05Kg, remaining benefit are filled with water to
1000Kg。
As shown in Fig. 1 flow chart, the preparation method of the formulated infant milk includes the following steps:
(1) it after the fresh raw milk of 255.75Kg being carried out an acceptance inspection, filter and purified, is then heat-treated at 80 DEG C
10min makes albuminous degeneration, which is cooled to 50 DEG C；
(2) protease A mano C100 (being purchased from Amano Enzyme Inc.) is added in Xiang Shangshu solution and carries out enzyme
Solution, the additive amount of protease are the 0.4% of substrate protein content, hydrolyze 1.0h while stirring under the conditions of 50 DEG C, will be above-mentioned molten
Liquid heats 10min inactivated proteases under the conditions of 80 DEG C, obtains raw milk hydrolyzate；The raw milk water is measured by trichloroacetic acid method
Solving content of peptides in liquid is 3.0mg/mL.
(3) solution after above-mentioned hydrolysis (is hydrolyzed into polypeptide in desalted whey powder with 61.50Kg hydrolysis desalted whey powder respectively
Content is 34.8mg/g), 0.15Kg carragheen, 14.5Kg anhydrous butter oil and the mixing of 10.0Kg vegetable oil, it is then that solution is cooling
After to 60 DEG C be added 0.32Kg multi-vitamins, 0.64Kg composite mineral matter, 0.075Kg choline, 0.065Kg taurine,
0.05Kg citric acid is mixed, and supplies 1000Kg with water；
(4) by above-mentioned mixed feed liquid in the case where level-one homogenization pressure is 15-20MPa, double-stage homogenization pressure is 3-5MPa
Homogenization；
(5) feed liquid after above-mentioned homogeneous is handled to 2-5s at 130-140 DEG C and carries out UHT sterilization；
(6) it by sterile filling after the feed liquid cooling after above-mentioned UHT sterilization processing, is got product after examination.
Trichloroacetic acid method is used to detect in above-mentioned finished product content of peptides as 2.90g/kg.
Requirement is all satisfied using the finished product nutritive index and stability of this method preparation.
Embodiment 4
The present invention provides a kind of formulated infant milk and preparation method thereof, the dry matter content of the formulated infant milk is
12.5wt.%, the component that every 1000Kg formulated infant milk is included are as follows: raw milk hydrolyzate 255.75Kg, hydrolysis desalination cream
Clear powder 61.50Kg, anhydrous butter oil 14.5Kg, vegetable oil 10.0Kg, lactose 9.5Kg, multi-vitamins 0.32Kg, composite mineral matter
0.64Kg, choline 0.075Kg, taurine 0.065Kg, carragheen 0.25Kg, citric acid 0.05Kg, remaining benefit are filled with water to
1000Kg。
As shown in Fig. 1 flow chart, the preparation method of the formulated infant milk includes the following steps:
(1) it after the fresh raw milk of 255.75Kg being carried out an acceptance inspection, filter and purified, is then heat-treated at 80 DEG C
10min makes albuminous degeneration, which is cooled to 50 DEG C；
(2) neutral proteinase Neutrase (believing enzyme preparation Co., Ltd purchased from Novi) is added in Xiang Shangshu solution to carry out
Enzymatic hydrolysis, the additive amount of protease are the 0.8% of substrate protein content, hydrolyze 1.0h while stirring under the conditions of 50 DEG C, will be above-mentioned
Solution heats 10min inactivated proteases under the conditions of 80 DEG C, obtains raw milk hydrolyzate；The raw milk is measured by trichloroacetic acid method
Content of peptides is 8.0mg/mL in hydrolyzate.
(3) solution after above-mentioned hydrolysis (is hydrolyzed into polypeptide in desalted whey powder with 61.50Kg hydrolysis desalted whey powder respectively
Content is 34.8mg/g), 0.15Kg carragheen, 14.5Kg anhydrous butter oil and the mixing of 10.0Kg vegetable oil, it is then that solution is cooling
After to 60 DEG C be added 0.32Kg multi-vitamins, 0.64Kg composite mineral matter, 0.075Kg choline, 0.065Kg taurine,
0.05Kg citric acid is mixed, and supplies 1000Kg with water；
(4) by above-mentioned mixed feed liquid in the case where level-one homogenization pressure is 15-20MPa, double-stage homogenization pressure is 3-5MPa
Homogenization；
(5) feed liquid after above-mentioned homogeneous is handled to 2-5s at 130-140 DEG C and carries out UHT sterilization；
(6) it by sterile filling after the feed liquid cooling after above-mentioned UHT sterilization processing, is got product after examination.
Trichloroacetic acid method is used to detect in above-mentioned finished product content of peptides as 4.19g/kg.
Requirement is all satisfied using the finished product nutritive index and stability of this method preparation.
Finally, it is stated that: above embodiments are merely to illustrate implementation process and feature of the invention, rather than limit this hair
Bright technical solution, although the present invention has been described in detail with reference to the above embodiments, those skilled in the art answer
Work as understanding: it is still possible to modify or equivalently replace the present invention, without departing from the spirit and scope of the present invention any
Modification or part replacement, should all cover in protection scope of the present invention.
Claims (10)
1. a kind of ready-to-feed infant milk suitable for 0~12 month, in terms of the corresponding ready-to-feed infant milk of its every 100KJ heat, packet
Contain: the protein of 0.45~0.70g, the fat of 1.05~1.40g, the carbohydrate of 2.2~3.3g, 0.07~0.33g are sub-
Oleic acid, >=12mg linseed oil, 14~43 μ g vitamin As, 0.25~0.60 μ g vitamin D, 0.12~0.20mg vitamin E, 1.0
~6.5 μ g vitamin K1s, 14~72 μ g vitamin B1s, 19~119 μ g vitamin B2s, 8.5~45.0 μ g vitamin B6s, 0.025
~0.360 μ g vitamin B12,70~360 μ g niacin, 2.5~12.0 μ g folic acid, 96~478 μ g pantothenic acid, 2.5~17.0mg dimension
Raw element C, 0.4~2.4 μ g biotin, 5~14mg sodium, 14~43mg potassium, 8.5~29.0 μ g copper, 1.2~3.6mg magnesium, 0.10~
0.36mg iron, 0.12~0.36mg zinc, 1.2~24 μ g manganese, 12~35mg calcium, 6~24mg phosphorus, 2.5~14.0 μ g iodine, 12~
38mg chlorine, 0.48~1.90 μ g selenium ,≤3mg taurine, 1.7~12.0mg choline；
Ready-to-feed infant milk described in every 100mL contains the heat of 250~295KJ, and the ready-to-feed infant milk contains polypeptide and card simultaneously
Glue is drawn, the content of the polypeptide is that every 100ml liquid contains 180.0mg or more, preferably contains 200.0~450.0mg；The carragheen
Content be every 100ml liquid milk contain 0.005~0.03g, preferably contain 0.01-0.025g.
2. ready-to-feed infant milk according to claim 1, wherein the ready-to-feed infant milk is by adding part or all of albumen
Matter makes the every 100ml of content of peptides in the ready-to-feed infant milk containing 180.0mg or more by the emulsified material after protease hydrolyzed.
3. liquid baby milk according to claim 2, wherein the emulsified material by after protease hydrolyzed includes raw milk water
Solve one of liquid, hydrolysis desalted whey powder, hydrolysis concentrated whey protein powder or a variety of；
Preferably, the content of peptides of the raw milk hydrolyzate is 3.0~9.0mg/mL；
Preferably, the content of peptides of the hydrolysis desalted whey powder is 12.0~36.0mg/g；
Preferably, the content of peptides of the hydrolysis concentrated whey protein powder is 80.0~392.0mg/g.
4. ready-to-feed infant milk described in any one of claim 1 to 3, wherein ready-to-feed infant milk described in every 1000Kg
Raw material composition includes following component: 128.5~320Kg of raw milk hydrolyzate, hydrolysis 20~90Kg of desalted whey powder, hydrolysis concentration
0~18Kg of PURE WHEY, 8.9~15.5Kg of anhydrous butter oil, 10.0~15.4Kg of vegetable oil, 0~25.4Kg of lactose, compound dimension
Raw 0.32~0.6Kg of element, 0.64~0.96Kg of composite mineral matter, 0.075~0.115Kg of choline, taurine 0.065~
0.095Kg, 0.05~0.3Kg of carragheen, 0.05~0.25Kg of citric acid, remaining benefit are filled with water to 1000Kg；
The raw material composition of the ready-to-feed infant milk may further be enriched with the nutrient conducive to infants growth and development；The nutrient for example wraps
Include MFGM (butterfat ball film), DHA, lactoferrin；
The raw material composition of the ready-to-feed infant milk can also add other raw-food materials, emulsifier and/or stabilizer；
Other described raw-food materials are for example including other protein raw materials and/or unsaturated fatty acid, phosphatide；
The emulsifier is for example including glycerin monostearate and/or citric acid fatty glyceride.
5. the preparation method of ready-to-feed infant milk according to any one of claims 1 to 4 comprising following steps:
(1) it gets all the ready or prepares and the material and remaining raw material of polypeptide are provided, and be mixed, supply total weight with water；
(2) homogeneous is carried out to the mixed material that step (1) obtains；
(3) material after step (2) homogeneous is sterilized；
(4) cooling the ready-to-feed infant milk is carried out to the material after sterilization.
6. preparation method according to claim 5, wherein step (2) is 15~20MPa, second level in level-one homogenization pressure
Homogenization pressure carries out homogeneous under the conditions of being 3~5MPa.
7. preparation method according to claim 5 or 6, wherein sterilization processing is carried out using UHT, it is highly preferred that 130
2~5s is handled at~140 DEG C to be sterilized.
8. the preparation method according to any one of claim 5~7, wherein step (1) further includes that prepare the offer more
The material of peptide, the preparation include the following steps:
(1.1) emulsified material for being partially or wholly used for providing protein in the ready-to-feed infant milk is carried out heat treatment makes egg therein
Then the solution is cooled to the temperature for being suitable for protease hydrolytic by leucismus, and add water before cooling or after cooling, is formed
System to be hydrolyzed；
(1.2) protease is added in the system to be hydrolyzed obtained to step (1.1) to be hydrolyzed, hot inactivated proteases after hydrolysis
The material of the offer polypeptide is provided.
9. preparation method according to claim 8, in which:
Preferably, the emulsified material for being used to provide the described protein in ready-to-feed infant milk includes raw milk, desalted whey powder, concentration
One of lactalbumin or other emulsified materials containing protein are a variety of；
Preferably, protein concentration is 3.0%~20.0% in the system to be hydrolyzed；
Preferably, the mass ratio of water is advisable in system for 80%~95% or so before protease being added；
Preferably, in step (2), the protease is to meet GB2760 to one or more of eggs of protease requirements in food
The compound protease that white enzyme is mixed according to different proportion；It is highly preferred that the protease is compound protease, the compound egg
White enzyme includes the Validase FP Concentrate and Protease GBW that weight ratio is 3~8:1；The protease adds
Dosage is account for protein substrate quality 0.4%~0.9%；
Preferably, the addition protease, which is hydrolyzed, is hydrolyzed under the conditions of the optimum temperature of protease, pH；It is described
Hydrolysis time is that the content for the polypeptide for generating hydrolysis reaches content of peptides in final products ready-to-feed infant milk, is more preferably hydrolyzed
0.5~4.0h.
10. preparation method according to claim 9, wherein the preparation method of the ready-to-feed infant milk includes the following steps:
(1.1) it will be partially or wholly used for providing the emulsified material of protein and water in the ready-to-feed infant milk and be hybridly prepared into solution,
And carry out heat treatment make protein denaturation therein, then which is cooled to the temperature for being suitable for protease hydrolytic；
(1.2) to step (1.1) obtain system to be hydrolyzed in be added protease under the conditions of its optimal temperature and pH into
Row hydrolysis, heat, which inactivates the protease, after hydrolysis must provide the material of polypeptide；
(1.3) material for the offer polypeptide that step (1.2) obtain is mixed with remaining raw material, supplies total weight with water；
(2) homogeneous is carried out to the mixed material that step (1.3) obtain；It is 15~20MPa, double-stage homogenization pressure in level-one homogenization pressure
Power carries out homogeneous under the conditions of being 3~5MPa；
(3) material after step (2) homogeneous is sterilized, carries out UHT under the conditions of 2~5s is handled at 130~140 DEG C and kills
Bacterium；
(4) cooling the ready-to-feed infant milk is carried out to the material after sterilization.
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101218942A (en) * | 2008-02-02 | 2008-07-16 | 内蒙古蒙牛乳业（集团）股份有限公司 | Serum albumin added liquid condition milk for baby |
| CN101313702A (en) * | 2008-07-09 | 2008-12-03 | 内蒙古蒙牛乳业（集团）股份有限公司 | Liquid milk for baby of 6 to 12 months ages and preparation method with ejection type direct disinfection |
| CN101317597A (en) * | 2008-07-09 | 2008-12-10 | 内蒙古蒙牛乳业（集团）股份有限公司 | Liquid milk for baby of birth to 6 months age and preparation using spray type direct disinfection |
| CN102283289A (en) * | 2011-09-15 | 2011-12-21 | 澳优乳业（中国）有限公司 | Anti-inflaming infant formula milk powder and preparation process thereof |
| CN102630760A (en) * | 2012-05-11 | 2012-08-15 | 光明乳业股份有限公司 | Infant formula concentrated milk and preparation method thereof |
| CN106605709A (en) * | 2015-10-22 | 2017-05-03 | 内蒙古伊利实业集团股份有限公司 | Liquid milk suitable for children at 3-6 years old and preparation method thereof |
-
2018
- 2018-04-28 CN CN201810400000.9A patent/CN110403022B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101218942A (en) * | 2008-02-02 | 2008-07-16 | 内蒙古蒙牛乳业（集团）股份有限公司 | Serum albumin added liquid condition milk for baby |
| CN101313702A (en) * | 2008-07-09 | 2008-12-03 | 内蒙古蒙牛乳业（集团）股份有限公司 | Liquid milk for baby of 6 to 12 months ages and preparation method with ejection type direct disinfection |
| CN101317597A (en) * | 2008-07-09 | 2008-12-10 | 内蒙古蒙牛乳业（集团）股份有限公司 | Liquid milk for baby of birth to 6 months age and preparation using spray type direct disinfection |
| CN102283289A (en) * | 2011-09-15 | 2011-12-21 | 澳优乳业（中国）有限公司 | Anti-inflaming infant formula milk powder and preparation process thereof |
| CN102630760A (en) * | 2012-05-11 | 2012-08-15 | 光明乳业股份有限公司 | Infant formula concentrated milk and preparation method thereof |
| CN106605709A (en) * | 2015-10-22 | 2017-05-03 | 内蒙古伊利实业集团股份有限公司 | Liquid milk suitable for children at 3-6 years old and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112841310A (en) * | 2019-11-12 | 2021-05-28 | 东北农业大学 | Newborn formula liquid milk and preparation method thereof |
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