CN103891890B - A kind of decompression short sleep liquid diary product and preparation method thereof - Google Patents

A kind of decompression short sleep liquid diary product and preparation method thereof Download PDF

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CN103891890B
CN103891890B CN201210573986.2A CN201210573986A CN103891890B CN 103891890 B CN103891890 B CN 103891890B CN 201210573986 A CN201210573986 A CN 201210573986A CN 103891890 B CN103891890 B CN 103891890B
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milk
liquid diary
diary product
product
cow
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CN103891890A (en
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王艳萍
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Inner Mongolia Yili Industrial Group Co Ltd
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Inner Mongolia Yili Industrial Group Co Ltd
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Abstract

The invention provides a kind of decompression short sleep liquid diary product and preparation method thereof, is described liquid diary product containing, for example the composition of lower weight portion: 35 ~ 98.89 parts, cow's milk, Lactium? 0.01 ~ 1 part, stabilizing agent 0.11 part, flavoring essence 0 ~ 0.5 part, sugar 0 ~ 0.5 part, lactase 0 ~ 0.5 part, add water to 100 parts; Wherein stabilizing agent to be weight ratio be 7: 3: 1 single bi-tristearin, sucrose fatty ester and gellan gum.Liquid diary product of the present invention not only meets the nutritional need of human body, improves the quality of dairy products simultaneously, has enriched dairy market.

Description

A kind of decompression short sleep liquid diary product and preparation method thereof
Technical field
The invention relates to a kind of decompression short sleep liquid diary product and preparation method thereof.
Background technology
Operating pressure is large, mood easily impatient, to being busy with work, feeling worn out mentally and physically, a lot of modern lives under certain pressure, be unemployed, promote, adjust firewood, office's relation etc.According to statistics, the disease of relevant to operating pressure psychology, physiology aspect has become the main cause causing employee's absence from duty, shut-down, contingency.
The pressure energy of appropriateness makes people's self-challenge, exploits potentialities, is rich in efficiency, evoke creativeness, and bad pressure, no matter what its source is, is all serious to the consequence of employee and tissue.Operating pressure can cause anxiety, the consequence such as dejected, angry, causes the disease of various physiology aspect, as angiocardiopathy, headache, or causes operating irregularity etc., and to organizing the loss also brought economically.The World Health Organization claims operating pressure to be " worldwide epidemic disease ".
The source of operating pressure mainly contains two: environmental factor and individual factor.First, many external environmental factors directly can cause operating pressure, as job schedule, operating rate, job security etc.But, do not have two people can make same reaction to same work, because individual factor also can cause pressure.Everyone is different to the reaction of pressure, if process bad, can cause pressure-dependent imbalance, as insomnia etc.Data show, and the adult of about 30% suffers from intermittent insomnia, and 10% suffers from chronic insomnia.Hypnotic and tranquillizer are widely used, and a kind of pure natural solution of market in urgent need.
Lactium is that the one obtained from the casein hydrolysis cow's milk can contribute to alleviating mood, promotes the peptide class with better nutritivity value of sleep.It is containing 10 amino acid whose three-dimensional structure polypeptide.Its amino acid sequence is: Tyr-Leu-Gly-Tyr-Leu-Glu-Gln-Leu-Leu-Arg.Its technological process of production is: skim milk, and---centrifugation casein---------------concentrated------sieving,---dispatch from the factory spraying dry in pasteurize in acid treatment (HCl) in casease hydrolysis in NaOH alkalization by packaging---inspection---.Lactium is non-toxic, have no side effect.Security and regulation see the following form one and table two.Simultaneously Lactium efficacy validation its have: improving water flood (1 zoopery+2 human clinicals), body weight control (2 zooperies+1 human clinical) and effects such as (4 human clinicals) of releasing the pressure.
But with the addition of the liquid diary product poor stability of Lactium, also can affect products taste, the liquid diary product prepared can not be preserved for a long time, greatly limit the marketing of this dairy products.Therefore, how to improve the stability containing Lactium liquid diary product, become the problem that need solve at present.
Summary of the invention
One object of the present invention is to provide a kind of decompression short sleep liquid diary product.
Another object of the present invention is to the preparation method that a kind of above-mentioned liquid diary product is provided.
For reaching above-mentioned purpose, on the one hand, the invention provides a kind of decompression short sleep liquid diary product, described liquid diary product is containing, for example the composition of lower weight portion: 35 ~ 98.89 parts, cow's milk, Lactium0.01 ~ 1 part, stabilizing agent 0.11 part, flavoring essence 0 ~ 0.5 part, sugar 0 ~ 0.5 part, lactase 0 ~ 0.5 part, add water to 100 parts; Wherein stabilizing agent to be weight ratio be 7: 3: 1 single bi-tristearin, sucrose fatty ester and gellan gum.
Lactium of the present invention is commercially available prod known in the field, is that the one obtained from the casein hydrolysis cow's milk can contribute to alleviating mood, promotes the peptide class with better nutritivity value of sleep.It is containing 10 amino acid whose three-dimensional structure polypeptide.Its amino acid sequence is: Tyr-Leu-Gly-Tyr-Leu-Glu-Gln-Leu-Leu-Arg.Lactium of the present invention is this area conventional commercial product, and it can by commercially available, and its quality standard also dawn known in the art, only need buy the Lactium meeting corresponding conventional quality standard.For example purchased from PharmachemLaboratoriesInc. company.
In addition, in the present invention, milk refers to the sweet milk or recombined milk that meet China Fresh Milk acquisition criteria GB6914, comprises full-cream, degreasing and half degreasing; Or with the recombined milk that other components of the milk powder be processed into, grease, protein hydrolysate, whey powder or liquid breast configure.
Single bi-tristearin is wherein a kind of mixture, it is this area typical additives, described in for example in " food additives use sanitary standard " (GB2760), be purchased the single bi-tristearin meeting respective quality standard and namely can be used for the present invention.
The present invention with the addition of Lactium especially, and the stability of invention product and mouthfeel are adjusted, distinctive stabiliser system: single bi-tristearin, sucrose fatty ester and gellan gum rationally composite, ensure that invention product stability does not produce precipitation, do not flocculate in shelf life, and it is pure in mouth feel, strong, be not mingled with peculiar smell, this product can also play the effect promoting sleep, control body weight, release the pressure simultaneously.
The further preferred described liquid diary product of the present invention is flavored milk.
In the present invention, described starting milk (cow's milk) should be understood to: Fresh Milk, comprises full-cream, degreasing and half degreasing; Or with the recombined milk that other components of milk powder, cream, protein hydrolysate, whey powder or milk configure.
Liquid diary product of the present invention can conventionally be prepared by ordinary liquid dairy product preparation method, and after simply mixing by liquid diary product composition of the present invention, conveniently dairy products processing method is processed.But in order to improve liquid diary product quality of the present invention further, present invention also offers a kind of preferred preparation method of described liquid diary product, described method comprises the steps:
(1) cow's milk pretreatment: sterilize after cow's milk removal of impurities;
(2) preparation of liquid diary product: by cow's milk, stabilizing agent and the Lactium mixing after sterilization, mix 15 ~ 30min at 60 ~ 70 DEG C;
(3) homogeneous of liquid diary product: the liquid diary product mixed is warming up to 55 ~ 75 DEG C, homogeneous under pressure 100 ~ 250bar, constant volume;
(4) sterilizing of liquid diary product: by the liquid diary product sterilizing after homogeneous, after cooling, namely sterile filling obtains liquid diary product of the present invention.
According to method of the present invention, the removal of impurities described in step (1) can be this area any except miscellaneous operation, this concrete removal of impurities is operating as conventionally known to one of skill in the art;
And the sterilization of step (1) also can be the sterilization method of this area routine, the present invention preferably carries out the pasteurize of 5 ~ 15s at 72 ~ 90 DEG C.
In order to improve liquid diary product quality of the present invention further, the present invention is also preferred after step (1) sterilization, and the liquid state breast after sterilization, by before liquid state breast and the mixing of other compositions, is cooled to less than 8 DEG C by step (2).
According to method of the present invention, if batching in containing sugar, essence, lactase and or other compositions, can add according to the routine operation in affiliated field.Usually, sugar be with stabilizing agent premix after join in milk, essence can add before constant volume, and lactase adds after UHT.
According to method of the present invention, described in step (3), homogeneous is this area customary means, and according to the record of description of the present invention, conventionally conventional homogenizing method carries out homogeneous.
According to method of the present invention, step (4) described sterilizing can be carried out according to this area conventional sterilization procedures, this sterilizing methods by this area usual, and the present invention preferably sterilizing 4 ~ 15s at 121 ~ 150 DEG C.
In order to improve liquid diary product quality of the present invention further again, the further preferred steps of the present invention (4) described sterile filling carries out sterile filling being less than at 20 DEG C.
According to method of the present invention, it can be more specifically:
A temperature is no more than the raw material milk of 8 DEG C by (), by the mechanical admixture in clean newborn technique removing raw material milk;
B raw material milk after clean breast is carried out the raw material milk after by clean breast at 72 ~ 90 DEG C by (), carry out the pasteurize of 5 ~ 15 seconds, and the raw material milk after pasteurize is cooled to less than 8 DEG C;
(c) preparation milk composition; Raw material milk and other compositions are prepared, and temperature is 60-70 DEG C, and the time is 15-30min;
D () homogeneous, is warming up to 55 ~ 75 DEG C by above-mentioned milk composition, homogenization pressure 100 ~ 250bar.
E the above-mentioned milk composition prepared was carried out sterilizing at 121 ~ 150 DEG C/4 ~ 15 seconds by (), and the milk composition after sterilizing is cooled to less than 25 DEG C;
F () sterile filling, carries out sterile filling under the condition of temperature≤20 DEG C.
In sum, the invention provides a kind of decompression short sleep liquid diary product and preparation method thereof.The present invention does not also see like product in existing market, and liquid diary product advantage of the present invention and remarkable result are:
(1), this product extends the shelf life of product, reaches more than six months, expands sales range and sales cycle.
(2), with the addition of functional component Lactium, energy improving water flood (1 zoopery+2 human clinicals), body weight control (2 zooperies+1 human clinical) and effects such as (4 human clinicals) of releasing the pressure.
(3), this product without any peculiar smell, have pure milk fragrance, the collocation of rational stabilizing agent makes final finished mouthfeel strong, pure.
This product not only meets the nutritional need of human body, improves the quality of dairy products simultaneously, has enriched dairy market, along with the development of society, people are to life and healthy pay attention to day by day, and to the cognition degree of natural, healthy goods, this product will hold out broad prospects.
Detailed description of the invention
Describe the beneficial effect of implementation process of the present invention and generation below by way of specific embodiment in detail, be intended to help reader to understand essence of the present invention and feature better, not as can the restriction of practical range to this case.
Embodiment 1
Modulation breast containing Lactium and production method thereof
One, the breast of the modulation containing Lactium of the present embodiment is prepared according to following material rate:
Milk 99.83 weight portion
Lactium0.06 weight portion
Stabilizing agent 0.11 weight portion
Wherein stabilizing agent to be weight ratio be 7: 3: 1 single bi-tristearin, sucrose fatty ester and gellan gum.
Raw material standard:
Milk: meet GB6914 standard
Each material performance index meets related quality criterion requirement.
Two, the production method of the liquid milk product of the present embodiment comprises the following steps successively:
(1) raw material milk temperature being no more than 8 DEG C, by clean newborn technique removing mechanical admixture wherein, then carries out the pasteurize of 10 seconds at 72 DEG C, be cooled to afterwards less than 8 DEG C for subsequent use;
(2) pasteurize milk is warming up to 60 ~ 65 DEG C, add stabilizing agent and Lactium, stirring is mixed, and obtains the milk fluid composition prepared;
(3) by the milk fluid composition for preparing in step (2) at about 65 DEG C, homogeneous under 200bar condition;
(4) the milk fluid composition after homogeneous carried out sterilizing at 121 DEG C/4 seconds, was cooled to less than 25 DEG C afterwards
(5) carry out sterile filling at the temperature below 20 DEG C, the product after filling can dispatch from the factory after heat insulation experiment (being generally 30 ~ 40 DEG C to place 5 ~ 7 days) is qualified.
The present embodiment is the modulation breast containing Lactium, and in liquid dairy product per ton, Lactium addition is 600g
Embodiment 2
Diabetic milk containing Lactium and preparation method thereof
One, the liquid milk containing Lactium of the present embodiment is prepared according to following material rate:
Wherein stabilizing agent to be weight ratio be 7: 3: 1 single bi-tristearin, sucrose fatty ester and gellan gum.
Raw material standard:
Milk: meet GB6914 standard
Each material performance index meets related quality criterion requirement.
Two, the present embodiment is that the production method of low-lactose milk beverage containing Lactium comprises step successively:
(1) raw material milk temperature being no more than 8 DEG C, by clean newborn technique removing mechanical admixture wherein, then carries out the pasteurize of 5 seconds at 85 DEG C, be cooled to afterwards less than 8 DEG C for subsequent use;
(2) heated up 60 ~ 65 DEG C by the raw material milk after pasteurize, add stabilizing agent and Lactium, stirring is mixed, and obtains the milk fluid composition prepared;
(3) by the milk fluid composition for preparing in step (2) at about 70 DEG C, homogeneous under 220bar condition;
(4) the milk fluid composition after homogeneous, after being settled to 100 parts, stirs with water, superhigh temperature (UHT) sterilizing is carried out at 137 DEG C/4 seconds, be cooled to less than 25 DEG C afterwards, add sterilized lactase preparation online, at lower than 20 DEG C, carry out sterile filling.Namely obtain the low-lactose product containing Lactium of the present embodiment, this product can dispatch from the factory after heat insulation experiment (placing 5 ~ 7 days for 30 ~ 40 DEG C) is qualified.
The present embodiment is the milk beverage containing Lactium, and in liquid dairy product per ton, Lactium addition is 1000g.
In the present embodiment, also measure the lactose hydrolysis ratio of this product in heat insulation experiment process, in insulation placement after 1,2,3,4 days, the lactose hydrolysis ratio in product is respectively 64.36%, 82.25%, 97.1%, 100%.Product lactose hydrolysis ratio when dispatching from the factory of this embodiment reaches 100%, is particularly suitable for lactose intolerance drunk by people, is the nutrition that it provides cow's milk, promotes absorbing calcium.
Embodiment 3:
Milk beverage containing Lactium and preparation method thereof
One, the liquid milk containing Lactium of the present embodiment is prepared according to following material rate:
Wherein stabilizing agent to be weight ratio be 7: 3: 1 single bi-tristearin, sucrose fatty ester and gellan gum.
Raw material standard:
Milk: meet GB6914 standard
Each material performance index meets related quality criterion requirement.
Two, the present embodiment is that the production method of milk beverage containing Lactium comprises step successively:
(1) raw material milk temperature being no more than 8 DEG C, by clean newborn technique removing mechanical admixture wherein, then carries out the pasteurize of 5 seconds at 80 DEG C, be cooled to afterwards less than 8 DEG C for subsequent use;
(2) heated up 60 ~ 65 DEG C by the raw material milk after pasteurize, add stabilizing agent and Lactium, stirring is mixed, and obtains the milk fluid composition prepared;
(3) by the milk fluid composition for preparing in step (2) at about 70 DEG C, homogeneous under 220bar condition;
(4) the milk fluid composition after homogeneous, after being settled to 100 parts, stirs with water, carries out superhigh temperature (UHT) sterilizing, is cooled to less than 25 DEG C afterwards, carry out sterile filling at 137 DEG C/4 seconds.
Test example 1
Containing the mouthfeel evaluation experimental of the liquid milk product of Lactium
Example 1, embodiment 2 and embodiment 3 and common plain chocolate are as taste tests sample, and carry out taste flavor and taste experiment, carry out the contrast of sample taste flavor every other month, the time is six months.
Table 1: products taste local flavor is investigated
Time Embodiment 1 Embodiment 2 Embodiment 3 Common plain chocolate
One month Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour
Two months Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour
Three months Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour
Four months Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour
Five months Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour Milk is strong, free from extraneous odour There are milk, free from extraneous odour
Six months There are milk, free from extraneous odour There are milk, free from extraneous odour There are milk, free from extraneous odour Milk is not enough, have activated flavour
Observation experiment result as can be seen from table 1, the product containing Lactium of the present invention can preserve more than 6 months in normal temperature, does not occur any peculiar smell, is beneficial to product promotion and sale.
Test example 2
The functional investigation experiment of the liquid milk product containing Lactium
Embodiment 1 is for the Efficacy experiments of the people of dyssomnias or poor sleeping quality
Tested number is 50 people, and efficiently individual quantity is 48 people, and the age is 40-45 year crowd, and ratio of age is 1: 1; Experimental period is: the wash-out phase in 30 days+1 weeks.Dosage is: wrap 250ml embodiment 1 product every day one.After taking surrounding: Sleep efficiency increases by 75.6%, Sleep latency shortens 24.8%, and daytime function obstacle reduces 22.3%, and global PSQI index (Pittsburg Sleep Quality Index) reduces by 34.1%.
Test example 3
This test example has investigated stabilizing agent of the present invention for the stablizing effect containing Lactium liquid milk:
One, the different proportion first investigating stabilizer element affects for product stability:
Patent list bi-tristearin of the present invention, sucrose fatty ester and gellan gum rational proportion are 0.07%: 0.03%: 0.01% that is 7: 3: 1.In whole product, all to adopt this ratio to carry out composite for stabilizing agent, in the composite stabilising system of this ratio significantly better than other products.
Product I: 998.3 parts, milk, Lactium0.6 part, single bi-tristearin 0.7 part, sucrose fatty ester 0.3 part, gellan gum 0.1 part (their ratios are 7: 3: 1);
Product I I: 996.4 parts, milk, Lactium0.6 part, single hard fatty acids glyceride 1 part, sucrose fatty ester 1 part, gellan gum 1 part;
Product I II: 970.4 parts, milk, Lactium0.6 part, sucrose fatty ester 15 parts, polyglyceryl fatty acid ester 10 parts, gellan gum 4 parts.
Table 2 is that three kinds of product stability observed results are as follows:
Table 2: product stability is observed
As can be seen from the table, by the product of 7: 3: 1 proportions, significantly better than the product of other compound stabilizers.
Two, the impact of stabilizing agent heterogeneity for product stability has secondly been investigated:
Patent of the present invention adds single bi-tristearin and sucrose fatty ester all can improve products taste, gives the sense of product milk.
Product I: 998.3 parts, milk, Lactium0.6 part, single bi-tristearin 0.7 part, sucrose fatty ester 0.3 part, gellan gum 0.1 part (their ratios are 7: 3: 1);
Product V: 998.3 parts, milk, Lactium0.6 part, single hard fatty acids glyceride 0.6 part, sucrose fatty ester 0.3, gellan gum 0.2 part;
Product VI: 999 parts, milk, Lactium0.6 part, sucrose fatty ester 0.3 part, gellan gum 0.1 part.
The said goods I ~ VI difference is only that stabilizer component ratio is different, and other compositions composition according to embodiment 1 identical with preparation method and preparation method carry out, to get rid of the impact that other factors may cause product stability.
Table 3 is that three kinds of product stability observed results are as follows:
Table 3: product stability is observed
As can be seen from the table, the arranging effect of three kinds of stabilizing agents, significantly better than the product of other compound stabilizers.
Three, the impact for products taste of stabilizing agent heterogeneity and ratio has finally also been investigated, in table 4.
Table 4: product sensory and taste flavor are investigated
As can be seen from the table, single bi-tristearin and sucrose fatty ester can promote the mouthfeel of milk, give milk fragrance.

Claims (7)

1. a decompression short sleep liquid diary product, it is characterized in that, described liquid diary product is containing, for example the composition of lower weight portion: 35 ~ 98.89 parts, cow's milk, Lactium0.01 ~ 1 part, stabilizing agent 0.11 part, flavoring essence 0 ~ 0.5 part, sugar 0 ~ 0.5 part, lactase 0 ~ 0.5 part, add water to 100 parts; Wherein single bi-tristearin of stabilizing agent to be weight ratio be 7:3:1, sucrose fatty ester and gellan gum.
2. liquid diary product according to claim 1, is characterized in that, described liquid diary product is flavored milk.
3. the preparation method of liquid diary product described in claim 1 or 2, is characterized in that, described method comprises the steps:
(1) cow's milk pretreatment: sterilize after cow's milk removal of impurities;
(2) preparation of liquid diary product: by cow's milk, stabilizing agent and the Lactium mixing after sterilization, mix 15 ~ 30min at 60 ~ 70 DEG C;
(3) homogeneous of liquid diary product: the liquid diary product mixed is warming up to 55 ~ 75 DEG C, homogeneous under pressure 100 ~ 250bar, constant volume;
(4) sterilizing of liquid diary product: by the liquid diary product sterilizing after homogeneous, after cooling, namely sterile filling obtains liquid diary product of the present invention;
If batching in containing sugar, essence, lactase and or other compositions, can add according to the routine operation in affiliated field; Sugar be with stabilizing agent premix after join in milk, essence added before constant volume, and lactase adds after UHT.
4. method according to claim 3, is characterized in that, step (1) described sterilization is the pasteurize carrying out 5 ~ 15s at 72 ~ 90 DEG C.
5. method according to claim 3, is characterized in that, after step (1) sterilization, step (2), by before cow's milk and the mixing of other compositions, also comprises the step that the cow's milk after by sterilization cools to less than 8 DEG C.
6. method according to claim 3, is characterized in that, step (4) described sterilizing is sterilizing 4 ~ 15s at 121 ~ 150 DEG C.
7. method according to claim 3, is characterized in that, step (4) described sterile filling carries out sterile filling being less than at 20 DEG C.
CN201210573986.2A 2012-12-26 2012-12-26 A kind of decompression short sleep liquid diary product and preparation method thereof Active CN103891890B (en)

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CN107467647B (en) * 2016-06-07 2022-07-15 内蒙古伊利实业集团股份有限公司 Functional composition capable of improving sleep and application thereof
CN108714208A (en) * 2018-06-21 2018-10-30 北京斯利安药业有限公司 Composition, preparation method, using and relieve stress, improve sleep product
CN112868792A (en) * 2019-11-29 2021-06-01 内蒙古蒙牛乳业(集团)股份有限公司 Liquid dairy product and preparation method thereof

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