CN110384627A - A kind of Multidimensional protection sun water curdled milk and preparation method thereof - Google Patents
A kind of Multidimensional protection sun water curdled milk and preparation method thereof Download PDFInfo
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- CN110384627A CN110384627A CN201910619060.4A CN201910619060A CN110384627A CN 110384627 A CN110384627 A CN 110384627A CN 201910619060 A CN201910619060 A CN 201910619060A CN 110384627 A CN110384627 A CN 110384627A
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61K8/4966—Triazines or their condensed derivatives
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- A61K8/63—Steroids; Derivatives thereof
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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Abstract
The present invention discloses a kind of Multidimensional protection sun water curdled milk, including A, B, C and D component;Preparation method is heated with stirring to 80-85 DEG C comprising steps of 1) by the oily phase pot of component A investment, and homogeneous forms integrated after dissolving completely;2) B component is put into water phase pot, is heated with stirring to 80-85 DEG C, homogeneous forms gel shape network suspending medium;3) oily phase pot material is sucked in water phase pot, keeps the temperature 80-85 DEG C of homogeneous 1-3min, stir cooling after keeping the temperature 10min;4) component C is added when dropping to 60 DEG C;5) when dropping to 45 DEG C, D component is added;6) when dropping to 40 DEG C or less, discharging is examined.Sun water curdy texture of the invention is slim and graceful, water profit easily absorbs, high SPF and the anti-sweat rub resistance of waterproof, can not only effectively damage of the ultraviolet blocking-up to skin, alleviate because of sunburn caused by scytitis, moreover it is possible to the protective capacities for keeping skin wet, repairing damaged skin, overall improved skin itself.
Description
Technical field
The present invention relates to a kind of Multidimensional protection sun water curdled milks and preparation method thereof, belong to cosmetic technical field.
Background technique
Skin is the first line of defence and beautiful the first agent of appearance of human health, is possessed healthy, pale, rich
Flexible skin is the target that owner pursues.After skin receives ultraviolet light overexposure, epidermal cell can be damaged;Activation
Tyrosinase accelerates pigment synthesis, destroys the moisture-keeping functions of skin, skin is made to become drying, allows elastic fibers in skin corium
It is impaired, generate microgroove.Under acute irradiation, skin inflammation, equivalent damage of burning also will cause.When having abnormal case, then it can become
At pigmentosa cutaneum carcinoma etc..So sun-proof not just blackening in order to prevent, can also delay senescence, pigmentation, resistance
DNA damage and cuticle loss caused by ultraviolet, therefore sun-proof be very important.With the development of social economy, Ren Minsheng
The flat raising of running water and environmental pollution and atmosphere are destroyed the aggravation of degree, and the sun-proof consciousness of people is also increasingly stronger.
Ultraviolet light in sunlight by its physiological effect can be divided into UVC (short wave ultraviolet, 200nm-290nm), UVB (in
Wave ultraviolet light, 290nm-320nm) and UVA (long wave ultraviolet, 320nm-400nm).The UVC on ground is reached very after ozone layer
Faint, UVB only has part and is absorbed by ozone layer, and UVA is not absorbed completely.Therefore, the ultraviolet light on ground is mainly by 10 parts
UVB and 90 part of UVA composition.UVB is most strong to skin ability to function, can be irradiated to corium surface, makes dermal vascular expansion in redness
Shape, epidermal cell nucleic acid or protein denaturation will appear oedema, blister, erythema, decortication, skin aging after permanent irradiation, very
Cutaneum carcinoma can extremely be caused.UVA penetration power is strong, reaches dermis of skin depths, has accumulation to skin effect, permanent irradiation can draw
Skin brown, collagenous fibres fracture, flexibility decrease, wrinkle generation are played, and increases damage of the UVB to skin.It can be seen that
UVB and UVA should be the main object of protectiving ultraviolet injury.
Sun-proof high magnification numbe at present on the market is mostly water-in-oil system or cream system, and the sense of water-in-oil system skin is mostly
Greasy, bellding light, poor air permeability, and cream system is then more sticky, waterproof sweat resistance is poor.
Summary of the invention
The purpose of the present invention is to provide a kind of quality is slim and graceful, water profit easily absorbs, high SPF and the anti-sweat antifriction of waterproof
The Multidimensional protection sun water curdled milk of wiping, can effectively damage of the ultraviolet blocking-up to skin, alleviate because of sunburn caused by scytitis,
The protective capacities for being also able to maintain skin wet, repairing damaged skin, overall improved skin itself.
Invention also provides the preparation methods of the Multidimensional protection sun water curdled milk.
To achieve the goals above, a kind of Multidimensional protection sun water curdled milk that the present invention uses, by weight, including group
Point:
Component A: 5-10 parts of ethylhexyl methoxy cinnamate, own ester 1-5 parts of diethylamino oxybenzene formylbenzoate, ethyl
1-5 parts of hexyl triazinone, titanium dioxide/silica/1-5 parts of dimethyl silicone polymer, bis-ethylhexoxyphenol methoxyphenyl triazine
0.5-1 parts, 1-5 parts of dimethyl silicone polymer, 0.5-3 parts of C12-13 alcohol lactate, 0.1-0.5 parts of emulsifier;
B component: 30-70 parts of deionized water, 5-20 parts of moisturizer, 1-5 parts of skin sense regulator, acrylate/C10-C30 alkane
0.1-0.5 parts of base acrylate crosspolymers, ammonium acryloyldime-thyltaurate/- 25 methacrylate of docosyl alcohol polyethers
It is 0.1-0.5 parts of cross-linked polymer, 0.01-0.1 parts of EDETATE SODIUM salt, 0.1-0.5 parts of allantoin, 0.1-0.5 parts of dipotassium glycyrrhizinate, sweet
Oily caprylate 0.1-0.5 parts, 0.1-0.5 parts of pH adjusting agent;
Component C: 0.01-0.02 parts of citric acid;
D component: 0.1-1 parts of preservative, bisabolol/0.05-0.5 parts of ginger-root extract, acrophyta extract 0.1-1
Part, 0.05-0.5 parts of essence.
The emulsifier is the smooth isostearate of sorb, polysorbate -60, the smooth oleate of sorb, Phosphoric acid monohexadecyl ester
One or more mixing of potassium.
The moisturizer is glycerol, 1,3-BDO, 1,3-PD, sorbierite, one of trehalose or a variety of
Mixing.
The EDETATE SODIUM salt is tetra- sodium of EDETATE SODIUM or EDTA.
The pH adjusting agent is the mixing of one or both of arginine, triethanolamine.
The preservative is one in Phenoxyethanol, Sensiva SC50,1,2- hexylene glycol, methyl hydroxybenzoate or Nipasol
Kind or a variety of mixing.
The acrophyta extract is HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Roots of Panax Notoginseng
The mixing of extract, tomonea extract, Chinese herbaceous peony root extract.
The skin sense regulator is silica, polymethylsilsesquioxane, methyl methacrylate cross-linked polymer, vinyl
One of dimethyl silicone polymer/polymethyl siloxane silsesquioxane cross-linked polymer or a variety of mixing.
In addition, the present invention also provides the preparation methods of the Multidimensional protection sun water curdled milk, specifically includes the following steps:
1) component A is put into oily phase pot, is heated with stirring to 80-85 DEG C, make the own ester of diethylamino oxybenzene formylbenzoate,
After Uvinul T 150, bis-ethylhexoxyphenol methoxyphenyl triazine dissolution completely, homogeneous is formed integrally;
2) B component is put into water phase pot, is heated with stirring to 80-85 DEG C, stirring homogeneous forms gel after dissolving completely
Shape network suspending medium;
3) oily phase pot material is sucked in water phase pot, keeps 80-85 DEG C of homogeneous 1-3min of temperature, stirred after keeping the temperature 10min
Cooling;
4) component C is added when temperature drops to 60 DEG C, continues stirring cooling after carrying out appropriate sour regurgitation;
5) when temperature drops to 45 DEG C, D component is added;
6) when temperature drops to 40 DEG C or less, it is qualified to examine, filtering and discharging.
The performance or the mechanism of action of part primary raw material are as follows in inventive formulation:
Acrophyta extract: in the Yunnan genunie medicinal materials such as plant HERBA DENDROBII, Radix Angelicae Sinensis, Radix Notoginseng from Yunnan composition
Skin makeup side is cured, is compounded according to the prescription thought of Traditional Chinese Medicine " monarch, minister, help, make ", there is good antioxidant activity and suppression
Tyrosinase activity processed, and have the function of good improvement skin microcirculation, good moist skin, balanced pigment can be played
The effect of with skin is nourished.
Allantoin is nontoxic one kind, tasteless and nonirritant, without hypersensitive white powder, mainly makees skin conditioning agent, prevents
It protects agent to use, can help that skin is anti-inflammatory, releives and promotes cell repair.Allantoin can reduce the adhesion strength of corneocyte,
Epidermal cell is accelerated to update.It is some containing tartaric acid, vitamin A to there are irritating cosmetics or the after-sun restorative of anti-inflammatory calmness to produce
Product, which can all add allantoin, enhances its repair ability.
Dipotassium glycyrrhizinate is skin conditioning agent use, predominantly glycyrrhizin (glycyrrhizic acid) ingredient of Radix Glycyrrhizae root and stem
It is suitble to anaphylaxis skin, anti-irritant and oil-control, moves back red and swollen antiphlogistic healing effect.Can effectively prevent skin it is stimulated when sensitivity inflammation
Phenomenon.Inflammation caused by counterglow has anti-inflammatory sedation, is commonly used for antiallergy and repairs in cosmetics.
Bisabolol/ginger (ZINGIBER OFFICINALE) root extract: bisabolol is extracted from spirea, is had
Anti-inflammatory antibacterial effect, the ingredient stability is good and skin has good compatibility, reduces scytitis, mitigates acne,
It prevents dark sore from generating, improves the anti-irritant ability of skin, repair the skin for having inflammation injury, spf value is improved in sunscreen product.
Bisabolol has apparent anti-inflammatory and anti-convulsion effect, and herein functionally, the effect of natural bisabolol is two times of composite, is had
Analgesic mitigates stimulation and antianaphylaxis function, has skin care effect to allergic skin or child skin.Bisabolol have it is calm and
Anti- perspiration effect is usually used in sunscreen and treats the ointment of sunburn and burn;Ginger-root extract can enhance the activity of skin,
Cucumber Extract has anti-oxidant, anti-ageing effect;It can also promote the growth of hair, hairdo promotor;Simultaneously have moisturizing and
Inhibit the effect of stink.
Compared with prior art, the beneficial effects of the present invention are:
1) Multidimensional protection sun water curdled milk of the invention uses chemically and physically sun-proof with different UV absorption wave bands
Agent combines, and realizes that UVA/UVB all band covered protection, various dimensions ultraviolet protection, SPF of the invention reach SPF30PA
+++, daily solarization protection requirements can be met.
2) Multidimensional protection sun water curdled milk of the invention selects special composition (acrylate/C10-C30 alkyl
Acid esters cross-linked polymer, ammonium acryloyldime-thyltaurate/- 25 Methacrylate Crosspolymer of docosyl alcohol polyethers, dioxy
Change titanium/silica/dimethyl silicone polymer) according to special ratios formed can be stable containing a small amount of table work cross-linked network suspended substance
Water is clearly changed in system, skin sense, and spreadability is excellent;Physics, chemical sun are evenly dispersed to be suspended in the network structure of crosslinking, is smeared
When quick continuous film forming, keep elasticity, maintain film shape, resist the outer frictions (rub resistances of conventional sunscreen product such as clothing
The mechanism of action is shown in Fig. 1, the rub resistance mechanism of action of water-setting of the present invention cream is shown in Fig. 2);Sun-screening agent uniform fold not discontinue improves anti-
Benefit is shone, and there is the anti-sweat of waterproof and naturally element Yan Xiaoguo.
3) Multidimensional protection sun water curdled milk of the invention is especially added with dipotassium glycyrrhizinate, bisabolol/ginger-root extract etc.
With anti-inflammatory antiallergic active constituent, effectively inflammation after inhibition UVA, UVB light injury stimulation and mitigation solarization;In addition acrophyta is added
Extract (gold fork Herba Dendrobii extract, angelica extract, Herba Verbenae, Notogineng Extract, wild rose extract, RADIX PAEONIAE RUBRA
Extract), the penetration of hydrolyzate is extremely strong, can quickly penetrate into skin matter layer after being applied to skin surface, through cuticula with
Skin epidermal cells combine, and by cell as nutrient absorption, participate in and promote cell metabolism, moreover it is possible to repair the skin damaged
Skin promotes skin cell regeneration, the protective capacities of overall improved skin itself.
Detailed description of the invention
Fig. 1 is the rub resistance mechanism of action of conventional sunscreen product;
Fig. 2 is the rub resistance mechanism of action of the invention;
Fig. 3 is the micro- image of 10*10 times of water-setting cream of the embodiment of the present invention 2;
Fig. 4 is the micro- image of 10*20 times of water-setting cream of the embodiment of the present invention 2;
Fig. 5 is the micro- image of 10*40 times of water-setting cream of the embodiment of the present invention 2;
Fig. 6 is that the skin sensing of sun water curdled milk of the present invention comments figure.
Specific embodiment
In order to make the objectives, technical solutions and advantages of the present invention clearer, below by embodiment, to the present invention into
Row is further described.However, it should be understood that the specific embodiments described herein are merely illustrative of the present invention, and do not have to
In limiting the scope of the invention.
Example 1
A kind of Multidimensional protection sun water curdled milk specifically includes following components by weight:
Component A: 9 parts of ethylhexyl methoxy cinnamate, 3 parts of the own ester of diethylamino oxybenzene formylbenzoate, ethylhexyl
1.3 parts of triazinone, titanium dioxide/2 parts of silica/dimethyl silicone polymer, 0.5 part of bis-ethylhexoxyphenol methoxyphenyl triazine,
2.5 parts of dimethyl silicone polymer, 1 part of C12-13 alcohol lactate, 0.2 part of emulsifier;
B component: 65.63 parts of deionized water, 9 parts of moisturizer, 4 parts of skin sense regulator, acrylate/C10-C30 alkyl third
0.2 part of olefin(e) acid ester cross-linked polymer, -25 methacrylate cross-linked polymeric of ammonium acryloyldime-thyltaurate/docosyl alcohol polyethers
0.4 part of object, 0.02 part of EDETATE SODIUM salt, 0.15 part of allantoin, 0.1 part of dipotassium glycyrrhizinate, 0.1 part of glycerol caprylate, pH adjusting agent
0.2 part;
Component C: 0.01 part of citric acid;
D component: 0.5 part of preservative, 0.1 part of root extract of bisabolol/ginger (ZINGIBER OFFICINALE), high mountain
0.3 part of plant extracts, 0.1 part of essence.
The emulsifier is the smooth isostearate of sorb;The moisturizer is the mixed of 1,3 butylene glycol and 1,3- propylene glycol
It closes;
The EDETATE SODIUM salt is EDETATE SODIUM;The pH adjusting agent is triethanolamine;The preservative be Phenoxyethanol and
The mixing of Sensiva SC50.
The acrophyta extract is HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Roots of Panax Notoginseng
The mixing of extract, tomonea extract, Chinese herbaceous peony root extract;
The skin sense regulator is that silica and polymethylsilsesquioxane are mixed according to 2:1.
The preparation method of the Multidimensional protection sun water curdled milk, comprising the following specific steps
1) component A is put into oily phase pot, is heated with stirring to 80 DEG C, makes crystal sun-screening agent (diethylamino hydroxyl Benzoylbenzene
Hexyl formate, Uvinul T 150, bis-ethylhexoxyphenol methoxyphenyl triazine) dissolution completely after, homogeneous forms uniform
Body;
2) B component is put into water phase pot, is heated with stirring to 80 DEG C, stirring homogeneous forms gel shape net after dissolving completely
Network suspending medium;
3) oily phase pot material is sucked in water phase pot, keeps 80 DEG C of homogeneous 1min of temperature, stir cooling after keeping the temperature 10min;
4) component C is added when temperature drops to 60 DEG C, continues stirring cooling after carrying out appropriate sour regurgitation;
5) when temperature drops to 45 DEG C, D component is added;
6) when temperature drops to 40 DEG C or less, it is qualified to examine, filtering and discharging.
Example 2
A kind of Multidimensional protection sun water curdled milk specifically includes following components by weight:
Component A: 8 parts of ethylhexyl methoxy cinnamate, 3.5 parts of the own ester of diethylamino oxybenzene formylbenzoate, ethyl hexyl
1.5 parts of base triazinone, titanium dioxide/3 parts of silica/dimethyl silicone polymer, bis-ethylhexoxyphenol methoxyphenyl triazine 0.8
Part, 3 parts of dimethyl silicone polymer, 1.5 parts of C12-13 alcohol lactate, 0.4 part of emulsifier;
B component: 62.79 parts of deionized water, 10 parts of moisturizer, 3 parts of skin sense regulator, acrylate/C10-C30 alkyl third
0.3 part of olefin(e) acid ester cross-linked polymer, -25 methacrylate cross-linked polymeric of ammonium acryloyldime-thyltaurate/docosyl alcohol polyethers
0.3 part of object, 0.05 part of EDETATE SODIUM salt, 0.2 part of allantoin, 0.2 part of dipotassium glycyrrhizinate, 0.15 part of glycerol caprylate, pH adjusting agent
0.3 part;
Component C: 0.02 part of citric acid;
D component: 0.6 part of preservative, 0.2 part of root extract of bisabolol/ginger (ZINGIBER OFFICINALE), high mountain
0.5 part of plant extracts, 0.2 part of essence;
The emulsifier is the smooth isostearate of sorb;The moisturizer is 1,3 butylene glycol, 1,3- propylene glycol and seaweed
The mixing of sugar;The pH adjusting agent is arginine;The EDETATE SODIUM salt is EDETATE SODIUM;The preservative is Phenoxyethanol, second
The mixing of base hexyl glycerol, methyl hydroxybenzoate and Nipasol.
The acrophyta extract is HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Roots of Panax Notoginseng
The mixing of extract, tomonea extract, Chinese herbaceous peony root extract;The skin sense regulator is methyl methacrylate cross-linked polymeric
Object and the mixing of vinyldimethicone/polymethyl siloxane silsesquioxane cross-linked polymer.
The preparation method of the Multidimensional protection sun water curdled milk, comprising the following specific steps
1) component A is put into oily phase pot, is heated with stirring to 85 DEG C, makes crystal sun-screening agent (diethylamino hydroxyl Benzoylbenzene
Hexyl formate, Uvinul T 150, bis-ethylhexoxyphenol methoxyphenyl triazine) dissolution completely after, homogeneous forms uniform
Body;
2) B component is put into water phase pot, is heated with stirring to 85 DEG C, stirring homogeneous forms gel shape net after dissolving completely
Network suspending medium;
3) oily phase pot material is sucked in water phase pot, keeps 85 DEG C of homogeneous 2min of temperature, heat preservation stirring cooling after ten minutes;
4) component C is added when temperature drops to 60 DEG C, continues stirring cooling after carrying out appropriate sour regurgitation;
5) when temperature drops to 45 DEG C, D component is added;
6) when temperature drops to 40 DEG C or less, it is qualified to examine, filtering and discharging.
Example 3
A kind of Multidimensional protection sun water curdled milk, by weight, the sun water curdled milk specifically include following components:
Component A: 7 parts of ethylhexyl methoxy cinnamate, 2 parts of the own ester of diethylamino oxybenzene formylbenzoate, ethylhexyl
1.8 parts of triazinone, titanium dioxide/3.5 parts of silica/dimethyl silicone polymer, 1 part of bis-ethylhexoxyphenol methoxyphenyl triazine,
3.5 parts of dimethyl silicone polymer, 2 parts of C12-13 alcohol lactate, 0.6 part of emulsifier;
B component: 62.76 parts of deionized water, 11 parts of moisturizer, 2 parts of skin sense regulator, acrylate/C10-C30 alkyl third
0.4 part of olefin(e) acid ester cross-linked polymer, -25 methacrylate cross-linked polymeric of ammonium acryloyldime-thyltaurate/docosyl alcohol polyethers
0.2 part of object, 0.07 part of EDETATE SODIUM salt, 0.25 part of allantoin, 0.3 part of dipotassium glycyrrhizinate, 0.2 part of glycerol caprylate, pH adjusting agent
0.40 part;
Component C: 0.02 part of citric acid;
D component: 0.4 part of preservative, 0.3 part of root extract of bisabolol/ginger (ZINGIBER OFFICINALE), high mountain
0.7 part of plant extracts, 0.3 part of essence.
The emulsifier is polysorbate -60;The moisturizer is 1,3 butylene glycol, 1,3- propylene glycol and sorbierite
3 kinds of mixing;The pH adjusting agent is arginine;The EDETATE SODIUM salt is EDETATE SODIUM;The preservative is methyl hydroxybenzoate and hydroxyl
The mixing of phenylpropyl alcohol ester.
The acrophyta extract is HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Roots of Panax Notoginseng
The mixing of extract, tomonea extract, Chinese herbaceous peony root extract;The skin sense regulator is silica and vinylpolydimethyl silicon
Oxygen alkane/polymethyl siloxane silsesquioxane cross-linked polymer foodstuff mixture.
The preparation method of the Multidimensional protection sun water curdled milk, specific preparation process the following steps are included:
1) component A is put into oily phase pot, is heated with stirring to 83 DEG C, makes crystal sun-screening agent (diethylamino hydroxyl Benzoylbenzene
Hexyl formate, Uvinul T 150, bis-ethylhexoxyphenol methoxyphenyl triazine) dissolution completely after, homogeneous forms uniform
Body;
2) B component is put into water phase pot, is heated with stirring to 83 DEG C, stirring homogeneous forms gel shape net after dissolving completely
Network suspending medium;
3) oily phase pot material is sucked in water phase pot, keeps 83 DEG C of homogeneous 3min of temperature, stir cooling after keeping the temperature 10min;
4) component C is added when temperature drops to 60 DEG C, continues stirring cooling after carrying out appropriate sour regurgitation;
5) when temperature drops to 45 DEG C, D component is added;
6) when temperature drops to 40 DEG C or less, it is qualified to examine, filtering and discharging.
Microorganism is carried out to sun water curdled milk made from above-described embodiment 1-3 and service check, specific inspection result are as follows
Shown in table 1, table 2.
The Micro biological Tests result of 1 sun water curdled milk of table
Analytical table 1 carries out Micro biological Tests it is found that examining according to the wholesomeness of " cosmetics health specification ", the present invention
The total plate count of sun water curdled milk, mould and yeast sum, fecal coliform class, staphylococcus aureus and pseudomonas aeruginosa
Etc. the inspections of projects meet the requirements, illustrate that sun water curdled milk of the invention is safe and reliable.
The detection performance result of 2 sun water curdled milk of table
Analytical table 2 is it is found that the pH value of sun water curdled milk of the invention is 6.96-7.03 (standard 4.5-8.5), viscosity
It can be 4530-4840 (standard 3000-6000cps) that relative density is 0.994-0.996 (standard 0.98-1.02), separately
Outside, appearance, odor type comply with standard, and cold-resistant, resistance to Thermal test, centrifugation test are without exception.
To above-mentioned skin sense relatively preferably sun water curdled milk liquid made from embodiment 2 carry out displaing microstructure observing and skin sense and
Waterproof performance test;
1) different amplification displaing microstructure observing: is carried out to sun water curdled milk using Olympus BX-53 microscope
Displaing microstructure observing, imaging show that ultra light sun block lotion of the invention may eventually form uniform suspension structure, sun-proof agent solution partial size
It is uniformly distributed, is conducive to improve sun-proof effect, specific imaging results are shown in attached drawing 3,4,5;
2) skin sense and waterproof performance test:
Test position volunteer without skin lesion of 30 ages between 18~40 is looked for, at 20 ± 2 DEG C of temperature, relative humidity
In 50 ± 10% indoor environment, the spreadability for the normal process test sun water curdled milk commented according to skin sensing, changes water at salubrious degree
Sense, greasy feeling and heavy feeling, residual film, waterproofness, with rear comfort, with rear pliability and plain face natural sense;
Skin sense evaluating result: as shown in fig. 6, clearly to change water, spreadability good for Multidimensional protection sun water curdled milk of the invention,
Greasy feeling and heavy feeling are lower, have certain residual film and waterproofness, preferable with rear soft feeling and comfort, plain face is imitated naturally
Fruit is preferable, is the sunscreen product that a skin sense is good and waterproof antiwear is wiped.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modification, equivalent replacement or improvement etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (9)
1. a kind of Multidimensional protection sun water curdled milk, which is characterized in that by weight, including following components:
Component A: 5-10 parts of ethylhexyl methoxy cinnamate, own ester 1-5 parts of diethylamino oxybenzene formylbenzoate, ethylhexyl
1-5 parts of triazinone, titanium dioxide/silica/1-5 parts of dimethyl silicone polymer, bis-ethylhexoxyphenol methoxyphenyl triazine 0.5-
1 part, 1-5 parts of dimethyl silicone polymer, 0.5-3 parts of C12-13 alcohol lactate, 0.1-0.5 parts of emulsifier;
B component: 30-70 parts of deionized water, 5-20 parts of moisturizer, 1-5 parts of skin sense regulator, acrylate/C10-C30 alkyl third
0.1-0.5 parts of olefin(e) acid ester cross-linked polymer, ammonium acryloyldime-thyltaurate/- 25 methacrylate of docosyl alcohol polyethers crosslinking
0.1-0.5 parts of polymer, 0.01-0.1 parts of EDETATE SODIUM salt, 0.1-0.5 parts of allantoin, 0.1-0.5 parts of dipotassium glycyrrhizinate, caprylic
0.1-0.5 parts of acid esters, 0.1-0.5 parts of pH adjusting agent;
Component C: 0.01-0.02 parts of citric acid;
D component: 0.1-1 parts of preservative, bisabolol/0.05-0.5 parts of ginger-root extract, 0.1-1 parts of acrophyta extract,
0.05-0.5 parts of essence.
2. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the emulsifier is that sorb is smooth
One or more mixing of the smooth oleate of isostearate, polysorbate -60, sorb, Phosphoric acid monohexadecyl ester potassium.
3. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the moisturizer is sweet
Oil, 1,3-BDO, 1,3-PD, sorbierite, one of trehalose or a variety of mixing.
4. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the EDETATE SODIUM salt is EDTA
Tetra- sodium of disodium or EDTA.
5. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the pH adjusting agent is smart ammonia
The mixing of one or both of acid, triethanolamine.
6. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the preservative is benzene oxygen second
One of alcohol, Sensiva SC50,1,2- hexylene glycol, methyl hydroxybenzoate or Nipasol or a variety of mixing.
7. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the acrophyta extract
For HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Radix Notoginseng root extract, tomonea extract, Peony Root
The mixing of extract.
8. a kind of Multidimensional protection sun water curdled milk according to claim 1, which is characterized in that the skin sense regulator is silicon
Stone, polymethylsilsesquioxane, methyl methacrylate cross-linked polymer, vinyldimethicone/methyl polysilicone
One of alkane silsesquioxane cross-linked polymer or a variety of mixing.
9. a kind of preparation method of any one of claim 1-8 Multidimensional protection sun water curdled milk, which is characterized in that including with
Lower specific steps:
1) component A is put into oily phase pot, is heated with stirring to 80-85 DEG C, makes the own ester of diethylamino oxybenzene formylbenzoate, ethyl
After hexyl triazinone, bis-ethylhexoxyphenol methoxyphenyl triazine dissolution completely, homogeneous is formed integrally;
2) B component is put into water phase pot, is heated with stirring to 80-85 DEG C, stirring homogeneous forms gel shape net after dissolving completely
Network suspending medium;
3) oily phase pot material is sucked in water phase pot, keeps 80-85 DEG C of homogeneous 1-3min of temperature, stir cooling after keeping the temperature 10min;
4) component C is added when temperature drops to 60 DEG C, continues stirring cooling after carrying out appropriate sour regurgitation;
5) when temperature drops to 45 DEG C, D component is added;
6) when temperature drops to 40 DEG C or less, it is qualified to examine, filtering and discharging.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112370406A (en) * | 2020-11-30 | 2021-02-19 | 广东丸美生物技术股份有限公司 | Low-irritation sunscreen lotion and preparation method thereof |
CN113925791A (en) * | 2021-09-29 | 2022-01-14 | 广州卓芬化妆品有限公司 | Waterproof sunscreen composition and preparation method thereof |
CN116585210A (en) * | 2023-04-12 | 2023-08-15 | 深圳市亮而彩科技有限公司 | Hydrogel cream and preparation method thereof |
-
2019
- 2019-07-10 CN CN201910619060.4A patent/CN110384627A/en not_active Withdrawn
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112370406A (en) * | 2020-11-30 | 2021-02-19 | 广东丸美生物技术股份有限公司 | Low-irritation sunscreen lotion and preparation method thereof |
CN113925791A (en) * | 2021-09-29 | 2022-01-14 | 广州卓芬化妆品有限公司 | Waterproof sunscreen composition and preparation method thereof |
CN116585210A (en) * | 2023-04-12 | 2023-08-15 | 深圳市亮而彩科技有限公司 | Hydrogel cream and preparation method thereof |
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