CN110367507A - A kind of durian essence and preparation method thereof - Google Patents

A kind of durian essence and preparation method thereof Download PDF

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Publication number
CN110367507A
CN110367507A CN201910814377.3A CN201910814377A CN110367507A CN 110367507 A CN110367507 A CN 110367507A CN 201910814377 A CN201910814377 A CN 201910814377A CN 110367507 A CN110367507 A CN 110367507A
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China
Prior art keywords
disulfide
ethyl
methyl
durian
ether
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关宇龙
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Guangdong Xinjie Biochemical Technology Co Ltd
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Guangdong Xinjie Biochemical Technology Co Ltd
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Priority to CN201910814377.3A priority Critical patent/CN110367507A/en
Publication of CN110367507A publication Critical patent/CN110367507A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/105Natural spices, flavouring agents or condiments; Extracts thereof obtained from liliaceae, e.g. onions, garlic
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/202Aliphatic compounds
    • A23L27/2022Aliphatic compounds containing sulfur
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/202Aliphatic compounds
    • A23L27/2024Aliphatic compounds having oxygen as the only hetero atom
    • A23L27/2026Hydroxy compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/202Aliphatic compounds
    • A23L27/2024Aliphatic compounds having oxygen as the only hetero atom
    • A23L27/2028Carboxy compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/204Aromatic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/205Heterocyclic compounds
    • A23L27/2052Heterocyclic compounds having oxygen or sulfur as the only hetero atoms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Seasonings (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of durian essence and preparation method thereof.Durian essence, including following components: propanethiol, dimethyl disulfide, dipropyl disulfide, methyl propyl disulfide, 3- hydroxyl-butanone, ethyl butyrate, ethyl acetate, ethyl hexanoate, methyl cyclopentenyl ketone, vanillic aldehyde, ethyl thioacetate, delta-decalactone, NSC 97324, diisopropyl disulfide ether, 3- sulfydryl -2- methyl anyl alcohol, butanethiol, caproic acid, onion oil, propenyl propyl disulfide ether, ethyl 2-methylbutyrate and propylene glycol.The subjective appreciation of durian essence of the invention is close to natural durian fragrance, and its smell coordination is stable, fidelity is high, characteristic is strong, can be obviously improved flavor quality using durian essence of the invention.The present invention also provides a kind of durian essence preparation methods.

Description

A kind of durian essence and preparation method thereof
Technical field
The present invention relates to edible essence fields, more particularly to a kind of durian essence and preparation method thereof.
Background technique
Currently, using predominantly direct processing and eating or preparing extract for durian.Since durian growing environment is severe It carves, and is difficult to ensure and deposits after maturation, loss late of rotting in storing and sales process is high, and direct processing and eating unavoidably faces raw material Storage period short, perishable drawback, and extract has application effect difference because the missing of ingredient leads to its flavor serious distortion Disadvantage.
Some durian essence in the market naturally feel poor, and fidelity is insufficient, and lasting is poor.
Summary of the invention
Based on this, the object of the present invention is to provide a kind of durian essence and preparation method thereof.
Durian essence of the invention, including following components: propanethiol, dimethyl disulfide, dipropyl disulfide, methyl-prop Base disulfide, 3- hydroxyl-butanone, ethyl butyrate, ethyl acetate, ethyl hexanoate, methyl cyclopentenyl ketone, vanillic aldehyde, thio second Acetoacetic ester, delta-decalactone, NSC 97324, diisopropyl disulfide ether, 3- sulfydryl -2- methyl anyl alcohol, butanethiol, caproic acid, Onion oil, propenyl propyl disulfide ether, ethyl 2-methylbutyrate and propylene glycol.
It is further preferred that by weight percentage, comprising: propanethiol 0.1%-1%, dimethyl disulfide 0.01%- 0.1%, dipropyl disulfide 0.02%-0.2%, methyl propyl disulfide 0.05%-0.5%, 3- hydroxyl-butanone 0.15%- 1.5%, ethyl butyrate 0.5%-5%, ethyl acetate 0.1%-1%, ethyl hexanoate 0.3%-3%, methyl cyclopentenyl ketone 0.1%-1%, vanillic aldehyde 0.2%-2%, ethyl thioacetate 0.05%-0.5%, delta-decalactone 0.2%-2%, dimethyl Trithioether 0.01%-0.1%, diisopropyl disulfide ether 0.02%-0.2%, 3- sulfydryl -2- methyl anyl alcohol 0.01%-0.1%, Butanethiol 0.02%-0.2%, caproic acid 0.05%-0.5%, onion oil 0.02%-0.2%, propenyl propyl disulfide ether 0.01%-0.1%, ethyl 2-methylbutyrate 0.2%-2% and propylene glycol 78.8%-97.88%.
It is further preferred that by weight percentage, comprising: propanethiol 0.25%, dimethyl disulfide 0.05%, dipropyl Base disulfide 0.02%, methyl propyl disulfide 0.15%, 3- hydroxyl-butanone 0.75%, ethyl butyrate 2%, ethyl acetate 0.75%, ethyl hexanoate 1.2%, methyl cyclopentenyl ketone 0.25%, vanillic aldehyde 0.6%, ethyl thioacetate 0.15%, Ding Wei Decalactone 0.65%, NSC 97324 0.05%, diisopropyl disulfide ether 0.1%, 3- sulfydryl -2- methyl anyl alcohol 0.02%, Butanethiol 0.05%, caproic acid 0.2%, onion oil 0.08%, propenyl propyl disulfide ether 0.05%, ethyl 2-methylbutyrate 1.8% and propylene glycol 90.83%.
The subjective appreciation of durian essence of the invention is close to natural durian fragrance, and its smell coordination is stable, true to nature Degree is high, characteristic is strong, can be obviously improved flavor quality using durian essence of the invention.
The present invention still further provides a kind of durian essence preparation method, comprising: with propylene glycol dissolve by heating vanillic aldehyde, After methyl cyclopentenyl ketone, propanethiol, dimethyl disulfide, dipropyl disulfide, methyl propyl disulfide, 3- hydroxyl-is added Butanone, ethyl butyrate, ethyl acetate, ethyl hexanoate, ethyl thioacetate, delta-decalactone, NSC 97324, diisopropyl Disulfide, 3- sulfydryl -2- methyl anyl alcohol, butanethiol, caproic acid, onion oil, propenyl propyl disulfide ether, ethyl 2-methylbutyrate, It stirs evenly, obtains durian essence.
Durian essence preparation method preparation process of the invention is simple, and raw material is simple and easy to get, and production cost is low, is preparing Fragrance component can utmostly be retained in the process, avoid fragrance loss, be adapted for the popularization and application of durian essence preparation.
Specific embodiment
Embodiment described in following exemplary embodiment does not represent all embodiment party consistent with this disclosure Formula.On the contrary, they are only the examples of the method consistent with some aspects as detailed in the attached claim, the disclosure Son.
It is only to be not intended to be limiting the disclosure merely for for the purpose of describing particular embodiments in the term that the disclosure uses. The "an" of the singular used in disclosure and the accompanying claims book, " described " and "the" are also intended to including majority Form, unless the context clearly indicates other meaning.It is also understood that term "and/or" used herein refers to and wraps It may be combined containing one or more associated any or all of project listed.
Durian essence of the invention, including following components: propanethiol, dimethyl disulfide, dipropyl disulfide, methyl-prop Base disulfide, 3- hydroxyl-butanone, ethyl butyrate, ethyl acetate, ethyl hexanoate, methyl cyclopentenyl ketone, vanillic aldehyde, thio second Acetoacetic ester, delta-decalactone, NSC 97324, diisopropyl disulfide ether, 3- sulfydryl -2- methyl anyl alcohol, butanethiol, caproic acid, Onion oil, propenyl propyl disulfide ether, ethyl 2-methylbutyrate and propylene glycol.
Durian essence of the invention carries out fragrance sense organ according to GBT14454.2-2008 " fragrance aroma assessment method " and comments Valence.
Sensory evaluation method are as follows: invite 8 to durian fragrance than more sensitive sensory evaluation person, for all sensory evaluation people Member provides the top durian essence (obtaining by commercially available mode) of one kind as control sample, asks sensory evaluation personnel according to each reality The fragrance degree of closeness of the durian essence and control sample of applying example offer scores within the scope of 1-9 points, and calculates average mark, It is higher closer to score with the fragrance of control sample, have that peculiar smell, fragrance are sharp or the flat then score of fragrance is low.
Lower mask body combines five embodiments to illustrate durian essence of the invention.
Embodiment one
The durian essence of the present embodiment, by weight percentage, comprising: propanethiol 0.1%, dimethyl disulfide 0.01%, dipropyl disulfide 0.02%, methyl propyl disulfide 0.05%, 3- hydroxyl-butanone 0.15%, ethyl butyrate 0.5%, ethyl acetate 0.1%, ethyl hexanoate 0.3%, methyl cyclopentenyl ketone 0.1%, vanillic aldehyde 0.2%, thioacetic acid second Ester 0.05%, delta-decalactone 0.2%, NSC 97324 0.01%, diisopropyl disulfide ether 0.02%, 3- sulfydryl -2- first Base amylalcohol 0.01%, butanethiol 0.02%, caproic acid 0.05%, onion oil 0.02%, propenyl propyl disulfide ether 0.01%, 2- first Base ethyl butyrate 0.2% and propylene glycol 97.88%.
The durian essence sensory evaluation scoring of the present embodiment is 8.425 points.
Embodiment two
The durian essence of the present embodiment, by weight percentage, comprising: propanethiol 1%, dimethyl disulfide 0.1%, two Dipropyl disulfide 0.2%, methyl propyl disulfide 0.5%, 3- hydroxyl-butanone 1.5%, ethyl butyrate 5%, ethyl acetate 1%, Ethyl hexanoate 3%, methyl cyclopentenyl ketone 1%, vanillic aldehyde 2%, ethyl thioacetate 0.5%, delta-decalactone 2%, diformazan Base trithioether 0.1%, diisopropyl disulfide ether 0.2%, 3- sulfydryl -2- methyl anyl alcohol 0.1%, butanethiol 0.2%, caproic acid 0.5%, onion oil 0.2%, propenyl propyl disulfide ether 0.1%, ethyl 2-methylbutyrate 2% and propylene glycol 78.8%.
The durian essence sensory evaluation scoring of the present embodiment is 8.675 points.
Embodiment three
The durian essence of the present embodiment, by weight percentage, comprising: propanethiol 0.3%, dimethyl disulfide 0.04%, dipropyl disulfide 0.12%, methyl propyl disulfide 0.32%, 3- hydroxyl-butanone 1.1%, ethyl butyrate 2%, Ethyl acetate 0.8%, ethyl hexanoate 2.2%, methyl cyclopentenyl ketone 0.7%, vanillic aldehyde 0.15%, ethyl thioacetate 0.33%, delta-decalactone 1.6%, NSC 97324 0.09%, diisopropyl disulfide ether 0.08%, 3- sulfydryl -2- methyl Amylalcohol 0.08%, butanethiol 0.17%, caproic acid 0.42%, onion oil 0.11%, propenyl propyl disulfide ether 0.04%, 2- methyl Ethyl butyrate 0.17% and propylene glycol 89.18%.
The durian essence sensory evaluation scoring of the present embodiment is 8.725 points.
Example IV
The durian essence of the present embodiment, by weight percentage, comprising: propanethiol 0.85%, dimethyl disulfide 0.05%, dipropyl disulfide 0.06%, methyl propyl disulfide 0.26%, 3- hydroxyl-butanone 1.36%, ethyl butyrate 4.3%, ethyl acetate 0.68%, ethyl hexanoate 2.6%, methyl cyclopentenyl ketone 0.3%, vanillic aldehyde 1.4%, thioacetic acid second Ester 0.35%, delta-decalactone 1.6%, NSC 97324 0.06%, diisopropyl disulfide ether 0.17%, 3- sulfydryl -2- first Base amylalcohol 0.09%, butanethiol 0.13%, caproic acid 0.39%, onion oil 0.18%, propenyl propyl disulfide ether 0.03%, 2- first Base ethyl butyrate 0.9% and propylene glycol 84.24%.
The durian essence sensory evaluation scoring of the present embodiment is 8.625 points.
Embodiment five
The durian essence of the present embodiment, by weight percentage, comprising: propanethiol 0.25%, dimethyl disulfide 0.05%, dipropyl disulfide 0.02%, methyl propyl disulfide 0.15%, 3- hydroxyl-butanone 0.75%, ethyl butyrate 2%, Ethyl acetate 0.75%, ethyl hexanoate 1.2%, methyl cyclopentenyl ketone 0.25%, vanillic aldehyde 0.6%, ethyl thioacetate 0.15%, delta-decalactone 0.65%, NSC 97324 0.05%, diisopropyl disulfide ether 0.1%, 3- sulfydryl -2- methyl Amylalcohol 0.02%, butanethiol 0.05%, caproic acid 0.2%, onion oil 0.08%, propenyl propyl disulfide ether 0.05%, 2- methyl Ethyl butyrate 1.8% and propylene glycol 90.83%.
The durian essence sensory evaluation scoring of the present embodiment is 8.875 points.
Embodiment one to embodiment five durian essence subjective appreciation close to natural durian fragrance, and its fragrance is assisted It adjusts stable, fidelity height, characteristic strong, can be obviously improved flavor quality using the durian essence of each embodiment.
The sensory evaluation scoring highest of the durian essence of embodiment five, by the proportion of the above-mentioned weight percent of the embodiment For optimal proportion mode, the fragrance of durian essence can be made naturally to feel, stability, fidelity and flavor quality reach best.
Durian essence of the invention can be used as food additives for beverage, juice production etc., can significantly improve pomegranate The flavor and taste of beverage contg. lotus, fruit juice.
Durian essence preparation method of the present invention can be used for preparing the durian essence of embodiment one to embodiment five, comprising: Dissolve by heating vanillic aldehyde, after methyl cyclopentenyl ketone with propylene glycol, be added propanethiol, dimethyl disulfide, dipropyl disulfide, Methyl propyl disulfide, 3- hydroxyl-butanone, ethyl butyrate, ethyl acetate, ethyl hexanoate, ethyl thioacetate, in the last of the ten Heavenly stems of fourth position Ester, NSC 97324, diisopropyl disulfide ether, 3- sulfydryl -2- methyl anyl alcohol, butanethiol, caproic acid, onion oil, acrylic third Base disulfide, ethyl 2-methylbutyrate, stir evenly, and obtain durian essence.
Durian essence preparation method preparation process of the invention is simple, and raw material is simple and easy to get, and production cost is low, is preparing Fragrance component can utmostly be retained in the process, avoid fragrance loss, be adapted for the popularization and application of durian essence preparation.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention Range.

Claims (4)

1. a kind of durian essence, which is characterized in that including following components: propanethiol, dimethyl disulfide, dipropyl disulfide, Methyl propyl disulfide, 3- hydroxyl-butanone, ethyl butyrate, ethyl acetate, ethyl hexanoate, methyl cyclopentenyl ketone, vanillic aldehyde, Ethyl thioacetate, delta-decalactone, NSC 97324, diisopropyl disulfide ether, 3- sulfydryl -2- methyl anyl alcohol, butanethiol, Caproic acid, onion oil, propenyl propyl disulfide ether, ethyl 2-methylbutyrate and propylene glycol.
2. durian essence according to claim 1, which is characterized in that by weight percentage, comprising: propanethiol 0.1%- 1%, dimethyl disulfide 0.01%-0.1%, dipropyl disulfide 0.02%-0.2%, methyl propyl disulfide 0.05%- 0.5%, 3- hydroxyl-butanone 0.15%-1.5%, ethyl butyrate 0.5%-5%, ethyl acetate 0.1%-1%, ethyl hexanoate 0.3%-3%, methyl cyclopentenyl ketone 0.1%-1%, vanillic aldehyde 0.2%-2%, ethyl thioacetate 0.05%-0.5%, fourth Position decalactone 0.2%-2%, NSC 97324 0.01%-0.1%, diisopropyl disulfide ether 0.02%-0.2%, 3- sulfydryl- 2- methyl anyl alcohol 0.01%-0.1%, butanethiol 0.02%-0.2%, caproic acid 0.05%-0.5%, onion oil 0.02%- 0.2%, propenyl propyl disulfide ether 0.01%-0.1%, ethyl 2-methylbutyrate 0.2%-2% and propylene glycol 78.8%- 97.88%.
3. durian essence according to claim 2, which is characterized in that by weight percentage, comprising: propanethiol 0.25%, dimethyl disulfide 0.05%, dipropyl disulfide 0.02%, methyl propyl disulfide 0.15%, 3- hydroxyl-butanone 0.75%, ethyl butyrate 2%, ethyl acetate 0.75%, ethyl hexanoate 1.2%, methyl cyclopentenyl ketone 0.25%, vanillic aldehyde 0.6%, ethyl thioacetate 0.15%, delta-decalactone 0.65%, NSC 97324 0.05%, diisopropyl disulfide ether 0.1%, 3- sulfydryl -2- methyl anyl alcohol 0.02%, butanethiol 0.05%, caproic acid 0.2%, onion oil 0.08%, acrylic propyl Disulfide 0.05%, ethyl 2-methylbutyrate 1.8% and propylene glycol 90.83%.
4. a kind of durian essence preparation method characterized by comprising dissolve by heating vanillic aldehyde, methyl cyclopentene with propylene glycol After alcohol ketone, propanethiol, dimethyl disulfide, dipropyl disulfide, methyl propyl disulfide, 3- hydroxyl-butanone, butyric acid second is added Ester, ethyl acetate, ethyl hexanoate, ethyl thioacetate, delta-decalactone, NSC 97324, diisopropyl disulfide ether, 3- mercapto Base -2- methyl anyl alcohol, butanethiol, caproic acid, onion oil, propenyl propyl disulfide ether, ethyl 2-methylbutyrate, stir evenly, obtain To durian essence.
CN201910814377.3A 2019-08-30 2019-08-30 A kind of durian essence and preparation method thereof Pending CN110367507A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110897141A (en) * 2019-11-27 2020-03-24 苏州禾田香料有限公司 Durian type edible essence containing 2-propanethiol

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CN101014586A (en) * 2004-09-10 2007-08-08 西姆莱斯有限责任两合公司 Disubstituted tetrathianes as fragrances or flavourings
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110897141A (en) * 2019-11-27 2020-03-24 苏州禾田香料有限公司 Durian type edible essence containing 2-propanethiol

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