CN110269139A - Performance animal protein sources extracting process - Google Patents
Performance animal protein sources extracting process Download PDFInfo
- Publication number
- CN110269139A CN110269139A CN201810420862.8A CN201810420862A CN110269139A CN 110269139 A CN110269139 A CN 110269139A CN 201810420862 A CN201810420862 A CN 201810420862A CN 110269139 A CN110269139 A CN 110269139A
- Authority
- CN
- China
- Prior art keywords
- animal protein
- extract liquor
- organic solvent
- polar organic
- protein source
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000021120 animal protein Nutrition 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 30
- 230000008569 process Effects 0.000 title claims abstract description 17
- 238000000605 extraction Methods 0.000 claims abstract description 15
- 239000003495 polar organic solvent Substances 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 12
- 238000002156 mixing Methods 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 230000000740 bleeding effect Effects 0.000 claims abstract description 8
- 239000010775 animal oil Substances 0.000 claims abstract description 7
- 239000004519 grease Substances 0.000 claims abstract description 6
- 238000004821 distillation Methods 0.000 claims abstract description 4
- 239000011259 mixed solution Substances 0.000 claims abstract description 4
- 239000007921 spray Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims abstract description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 4
- 235000019441 ethanol Nutrition 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 239000003208 petroleum Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 238000005516 engineering process Methods 0.000 abstract description 9
- 238000000746 purification Methods 0.000 abstract description 3
- 150000001413 amino acids Chemical class 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 7
- 235000018102 proteins Nutrition 0.000 description 7
- 108090000623 proteins and genes Proteins 0.000 description 7
- 102000004169 proteins and genes Human genes 0.000 description 7
- 239000000047 product Substances 0.000 description 5
- 241000287828 Gallus gallus Species 0.000 description 3
- 239000012454 non-polar solvent Substances 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000003895 organic fertilizer Substances 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 241000272525 Anas platyrhynchos Species 0.000 description 1
- 241000272814 Anser sp. Species 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- 108010052285 Membrane Proteins Proteins 0.000 description 1
- 102000018697 Membrane Proteins Human genes 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 125000003275 alpha amino acid group Chemical group 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- -1 heptan Alkane Chemical class 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000001863 plant nutrition Effects 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
- A23K10/26—Animal feeding-stuffs from material of animal origin from waste material, e.g. feathers, bones or skin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
- A23K20/147—Polymeric derivatives, e.g. peptides or proteins
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
Abstract
The present invention relates to a kind of performance animal protein sources extracting process, belong to feed processing technology.Specifically comprise the following steps: 1) to crush animal protein source；2) polar organic solvent and non-polar organic solvent are mixed in the ratio of 1:1 ~ 1:2, it is added in agitator tank simultaneously, wherein the dosage of polar organic solvent is the 40% ~ 60% of animal protein source total weight, whipping temp controls within 70Co, mixing speed is controlled in 250 ~ 500rpm/min, mixing time stands 1h after 1 ~ 2h, stirring；3) mixed solution using animal oil extract liquor for step 2 is extracted, and removes the grease and moisture contained in mixture, and OT bleeding agent is added in extraction process, and bleeding agent dosage is animal protein source total weight 0.2 ~ 0.5%, obtains extraction mixture；4) the extraction mixture for obtaining step 3) obtains extract liquor using vacuum non-pressure process；5) extract liquor that step 4) is obtained, using distillation technique, the semiarid albumen powder of acquisition；6) the partial desiccation albumen powder for obtaining step 5), is dried using spray dried form, is encapsulated.This method uses extraction process, and purification rate is high, at low cost, meets environmentally friendly related request.
Description
Technical field
The present invention relates to feed industries to produce performance animal protein sources method, belongs to feed processing technology.
Background technique
With the development and raising of living standards of the people, high-quality subsidiary food supply is constantly reinforced.Performance animal albumen
Source plays the role of the cultivation of pig, poultry (chicken, duck, goose) and aquatic products (fish, shrimp etc.) very important, and expectation is with relatively small in the industry
Amount, reach best culture efficiency.
The application amount of domestic animals protein sources increases year by year at present, most of by external import.The prior art is to use
Fried technology production of albumen powder, amino acid, process flow are as follows: animal protein source (pluck, chicken bone etc.) is using fried
→ squeezing oil removing → dead color powdery finished product.Fried method is equivalent to chemical method, has the following deficiencies: that (1) is oily with a batch, repeatedly,
What is be recycled is multiple batches of fried, and because the acid value of oil is raw high, oil quality decline generates certain toxicity, leads to the production of the production technology
Quality cannot be guaranteed；(2) it is proved by Maillard reaction, eventually leads to albumen powder in product, the structure of amino acid becomes
Change, content is unstable to be gradually decreased (in 60%-40% range), and albumen powder, amino acid content are reduced.(3) it generates brown
Discoloration element shows inoxidizability to grease type autoxidation, generates the reproducibilities intermediate products such as aldehyde, ketone in brown stain reflection, causes
The generation of noxious material.(4) energy consumption is high when heating, and causes product cost height.If obtaining animal protein source using cooking process, though
So better than fried method, but sewage discharge generates pollution to environment, and taste is larger, does not meet environmental requirement.
Summary of the invention
In order to solve above-mentioned technical problem, the present invention provides a kind of performance animal protein sources extracting process, should
Method uses extraction process, and purification rate is high, at low cost, meets environmentally friendly related request.
The purpose of the present invention is what is be achieved through the following technical solutions: a kind of performance animal protein sources extracting process,
It is characterized in that, includes the following steps:
1) animal protein source is crushed；
2) polar organic solvent and non-polar organic solvent are mixed in the ratio of 1:1 ~ 1:2, while are added in agitator tank,
The dosage of middle polar organic solvent is the 40% ~ 60% of animal protein source total weight, and whipping temp controls within 70Co, mixing speed
In 250 ~ 500rpm/min, mixing time stands 1h after 1 ~ 2h, stirring for control；
3) mixed solution using animal oil extract liquor for step 2 is extracted, and removes the grease and water contained in mixture
Point, OT bleeding agent is added in extraction process, bleeding agent dosage is animal protein source total weight 0.2 ~ 0.5%, obtains extraction mixing
Object；
4) the extraction mixture for obtaining step 3) obtains extract liquor using vacuum non-pressure process；
5) extract liquor that step 4) is obtained, using distillation technique, the semiarid albumen powder of acquisition；
6) the partial desiccation albumen powder for obtaining step 5), is dried, then encapsulate using spray dried form.
The polar organic solvent chooses ethyl alcohol or glycerine.
The nonpolar solvent chooses ether or petroleum ether or light oil.
The animal oil extract liquor chooses hexane or heptane, and dosage is the 5% ~ 10% of animal protein source total weight.
Beneficial effects of the present invention: the present invention is mentioned with animal protein source (pluck, skeleton, offal etc. is raw materials)
Protein (albumen powder, chicken meal), amino acid are refined, realizes industrialized production.Using organic solvent extraction, purification of protein
(amino acid) method, protein, amino acid structure are not destroyed, and keep ecosystem, and make protein (amino acid) total amount content
20% or more is improved than traditional processing technology；Thick protein (amino acid) content reaches 65%.Low energy consumption in production process, does not give up
Water discharge, without environmental pollution, extractant can be reused, and water is as organic fertilizer.The process stabilizing, easy to control, technology
Maturation, product safety environmental protection, long shelf-life；A variety of total amino acid contents are up to 65.72%.It is raw that the technique can also be used for pluck
Produce the production technology of functional intestine membrane protein.The water distilled out, which contains a small amount of protein, can be used as plant nutrition liquid, quite organic
Fertilizer uses；Distilling off solvent is recyclable to be recycled；Grease is distilled out for industrial application.The performance animal protein sources are using extraction
The production technology of mode, fill the domestic gaps technology.
Specific embodiment
A kind of performance animal protein sources extracting process, includes the following steps: 1) to crush animal protein source；
2) polar organic solvent and non-polar organic solvent are mixed in the ratio of 1:1 ~ 1:2, while are added in agitator tank,
The dosage of middle polar organic solvent is the 40% ~ 60% of animal protein source total weight, and whipping temp controls within 70Co, mixing speed
In 250 ~ 500rpm/min, mixing time stands 1h after 1 ~ 2h, stirring for control；3) step is directed to using animal oil extract liquor
2) mixed solution is extracted, and the grease and moisture contained in mixture is removed, and OT bleeding agent is added in extraction process, is seeped
Saturating agent dosage is animal protein source total weight 0.1%, obtains extraction mixture；4) the extraction mixture for obtaining step 3) uses
Vacuum non-pressure process obtains extract liquor；5) extract liquor that step 4) is obtained, using distillation technique, the semiarid albumen of acquisition
Powder；6) the partial desiccation albumen powder for obtaining step 5), is dried, then encapsulate using spray dried form.Wherein, polar organic solvent
Choose ethyl alcohol or glycerine.Nonpolar solvent chooses ether or petroleum ether or light oil.Animal oil extract liquor chooses hexane or heptan
Alkane, dosage are the 5% ~ 10% of animal protein source total weight.
Extract liquor is shown in Table 1 with scale
Each component ratio by weight provides in table
| Animal protein source | Polar solvent | Nonpolar solvent | OT bleeding agent | Total amino acid content (%) |
| 500 parts | 200 ~ 300 parts | 100 ~ 200 parts | 1 ~ 3 part | 63~65 |
Claims (4)
1. a kind of performance animal protein sources extracting process, which comprises the steps of:
1) animal protein source is crushed；
2) polar organic solvent and non-polar organic solvent are mixed in the ratio of 1:1 ~ 1:2, while are added in agitator tank,
The dosage of middle polar organic solvent is the 40% ~ 60% of animal protein source total weight, and whipping temp controls within 70Co, mixing speed
In 250 ~ 500rpm/min, mixing time stands 1h after 1 ~ 2h, stirring for control；
3) mixed solution using animal oil extract liquor for step 2 is extracted, and removes the grease and water contained in mixture
Point, OT bleeding agent is added in extraction process, bleeding agent dosage is animal protein source total weight 0.2 ~ 0.5%, obtains extraction mixing
Object；
4) the extraction mixture for obtaining step 3) obtains extract liquor using vacuum non-pressure process；
5) extract liquor that step 4) is obtained, using distillation technique, the semiarid albumen powder of acquisition；
6) the partial desiccation albumen powder for obtaining step 5), is dried, then encapsulate using spray dried form.
2. a kind of performance animal protein sources extracting process according to claim 1, which is characterized in that the polarity has
Solvent chooses ethyl alcohol or glycerine.
3. a kind of performance animal protein sources extracting process according to claim 1, which is characterized in that the nonpolarity
Solvent chooses ether or petroleum ether or light oil.
4. a kind of performance animal protein sources extracting process according to claim 1, which is characterized in that the animal oil
Extract liquor chooses hexane or heptane, and dosage is the 5% ~ 10% of animal protein source total weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810420862.8A CN110269139A (en) | 2018-05-04 | 2018-05-04 | Performance animal protein sources extracting process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810420862.8A CN110269139A (en) | 2018-05-04 | 2018-05-04 | Performance animal protein sources extracting process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110269139A true CN110269139A (en) | 2019-09-24 |
Family
ID=67958806
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810420862.8A Pending CN110269139A (en) | 2018-05-04 | 2018-05-04 | Performance animal protein sources extracting process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110269139A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113831389A (en) * | 2021-10-26 | 2021-12-24 | 重庆望业生物制药有限公司 | Method for preparing compound protein amino acid product by using waste liquid from animal viscera extraction |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB835813A (en) * | 1956-09-04 | 1960-05-25 | Wasagchemie Ag | A method of producing protein of low fat content from marine sources |
| CH500670A (en) * | 1969-01-16 | 1970-12-31 | Corn Products Co | Improved powdered yolk with reduced - contents of fat and cholesterol |
| US4330463A (en) * | 1978-12-22 | 1982-05-18 | Internationale Octrooi Maatschappij "Octropa" B.V. | Process of preparing blood cell protein from hemoglobin |
| CN1314089A (en) * | 2001-02-20 | 2001-09-26 | 上海通诚生化科技开发研究所 | Natural full protein additive and its producing method and use |
| CN102265961A (en) * | 2010-06-07 | 2011-12-07 | 天津宝迪农业科技股份有限公司 | Method for decoloring and deodorization of animal plasma protein powder |
| US20140272045A1 (en) * | 2013-03-15 | 2014-09-18 | Advance International, Inc. | Automated method and system for recovering protein powder meal, pure omega 3 oil and purified distilled water from animal tissue |
| CN105124131A (en) * | 2015-10-27 | 2015-12-09 | 武汉科技大学 | Light-yellow odourless degreasing silkworm pupa protein power and preparation method thereof |
| CN105941837A (en) * | 2016-05-31 | 2016-09-21 | 东莞市林氏生物技术股份有限公司 | High-protein fish meal and preparation method thereof |
-
2018
- 2018-05-04 CN CN201810420862.8A patent/CN110269139A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB835813A (en) * | 1956-09-04 | 1960-05-25 | Wasagchemie Ag | A method of producing protein of low fat content from marine sources |
| CH500670A (en) * | 1969-01-16 | 1970-12-31 | Corn Products Co | Improved powdered yolk with reduced - contents of fat and cholesterol |
| US4330463A (en) * | 1978-12-22 | 1982-05-18 | Internationale Octrooi Maatschappij "Octropa" B.V. | Process of preparing blood cell protein from hemoglobin |
| CN1314089A (en) * | 2001-02-20 | 2001-09-26 | 上海通诚生化科技开发研究所 | Natural full protein additive and its producing method and use |
| CN102265961A (en) * | 2010-06-07 | 2011-12-07 | 天津宝迪农业科技股份有限公司 | Method for decoloring and deodorization of animal plasma protein powder |
| US20140272045A1 (en) * | 2013-03-15 | 2014-09-18 | Advance International, Inc. | Automated method and system for recovering protein powder meal, pure omega 3 oil and purified distilled water from animal tissue |
| CN105124131A (en) * | 2015-10-27 | 2015-12-09 | 武汉科技大学 | Light-yellow odourless degreasing silkworm pupa protein power and preparation method thereof |
| CN105941837A (en) * | 2016-05-31 | 2016-09-21 | 东莞市林氏生物技术股份有限公司 | High-protein fish meal and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113831389A (en) * | 2021-10-26 | 2021-12-24 | 重庆望业生物制药有限公司 | Method for preparing compound protein amino acid product by using waste liquid from animal viscera extraction |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190924 |