CN110255899A - A kind of formula and its production method of high temperature decoration firing glass container - Google Patents
A kind of formula and its production method of high temperature decoration firing glass container Download PDFInfo
- Publication number
- CN110255899A CN110255899A CN201910522138.0A CN201910522138A CN110255899A CN 110255899 A CN110255899 A CN 110255899A CN 201910522138 A CN201910522138 A CN 201910522138A CN 110255899 A CN110255899 A CN 110255899A
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- CN
- China
- Prior art keywords
- glass container
- temperature
- decoration firing
- high temperature
- production method
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C1/00—Processes, not specifically provided for elsewhere, for producing decorative surface effects
- B44C1/16—Processes, not specifically provided for elsewhere, for producing decorative surface effects for applying transfer pictures or the like
- B44C1/165—Processes, not specifically provided for elsewhere, for producing decorative surface effects for applying transfer pictures or the like for decalcomanias; sheet material therefor
- B44C1/175—Transfer using solvent
- B44C1/1756—Decalcomanias applied under heat and pressure, e.g. provided with a heat activable adhesive
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B1/00—Preparing the batches
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses the formulas and its production method of a kind of high temperature decoration firing glass container, including following percentage raw material: colourless cullet 20%, soda ash 12%, aluminium hydroxide 5.2%, ice crystal 4.5%, borax 8%, potassium carbonate 6%, dolomite 16%, calcite 12%, barium sulfate 4.14%, sodium nitrate 2%, cobalt oxide 0.01%, boron oxide 3.15%, toughener 7%, the formula and its production method of this high temperature decoration firing glass container, by sufficiently being cleaned to colourless cullet, simultaneously during glass container production, successively glass is cleaned, to which effectively the impurity on glass container is purged, and then improve the decoration firing quality of glass container, toughener by addition is polyester epoxy resin, it was being prepared to effectively raise glass container Toughness in journey, is effectively reduced the breakage rate of glass container, while improving the intensity that glass container uses.
Description
Technical field
The present invention relates to glass container production technical field, the formula of specially a kind of high temperature decoration firing glass container and its life
Production method.
Background technique
Glass is fused together and is formed by silica and other chemical substances.The earliest glass manufacturer in the world is
Ancient Egyptian, and with the development of science and technology, the progress of social productive forces, in today's society, the glass made of glass holds
Device is widely used in our life, and with the difference of application environment, the surface meeting of some crown glass containers
It is set to become more beautiful beautiful by adding decorative pattern.
Currently, existing decoration firing glass container is in high temperature decoration firing, usually due to containing impurity on glass container, thus shadow
The decoration firing quality of glass container is rung, and during the processing of existing glass container, usually due to colliding between glass, and
The intensity of glass container is smaller, and then large batch of glass container disrepair phenomenon occurs for this purpose, it is proposed that a kind of high temperature decoration firing
The formula and its production method of glass container.
Summary of the invention
It is above-mentioned to solve the purpose of the present invention is to provide the formula and its production method of a kind of high temperature decoration firing glass container
The problem of being proposed in background technique.
To achieve the above object, the invention provides the following technical scheme: a kind of formula of high temperature decoration firing glass container and its
Production method, including following percentage raw material: colourless cullet 20%, soda ash 12%, aluminium hydroxide 5.2%, ice crystal
4.5%, borax 8%, potassium carbonate 6%, dolomite 16%, calcite 12%, barium sulfate 4.14%, sodium nitrate 2%, cobalt oxide
0.01%, boron oxide 3.15%, toughener 7%.
(1) cleaning: the colourless cullet come will be collected and carried out after sufficiently cleaning, then dry simultaneously natural drying；
(2) mixed grinding: above-mentioned resulting raw material being put into and is ground into ball mill, and by the raw material after grinding into
Row refilters mixing, and high-purity mixed powder is made；
(3) high temperature melting: powder obtained in step (1) is sent into high-temperature smelting pot, and adjusts high-temperature smelting pot temperature and is
It is melted at a temperature of 1500-1550 DEG C, and keeping temperature is 10-12 hours, obtains uniform glass stoste；
(4) adjusting molding machine temperature is 1100-1300 DEG C, and the glass stoste that temperature is reduced to 1250 DEG C is sent into molding machine
Inside forms Semi-finished glass container；
(5) it when the temperature of Semi-finished glass container made from step (4) being down to 800-820 DEG C, then is sent into conveyer belt
In annelaing pot, and annelaing pot internal temperature is 780-810 DEG C, makes Semi-finished glass container retention time 4- inside annelaing pot
4.5 hours, after temperature is reduced to 100 DEG C, Semi-finished glass container taking-up natural room temperature is dried；
(6) Semi-finished glass container made from step (5) cleaned, dried, polish, polish after cleaned again simultaneously
It is dry；
(7) marble paper needed for glass container decoration firing is drawn a design, and after marble paper is impregnated, marble paper is fitted tightly over
It needs on the glass container of decoration firing, carries out naturally dry；
(8) glass container for being stained with marble paper is fed through in oven and is toasted, and glass container successively passes through in oven
Heat-flash section, firing section, slow cooling section, rapid cooling section, are adjusted to 200-590 DEG C by the temperature of oven；
(9) glass container after decoration firing cooling down carries out wiping detection, obtains qualified glass container.
Preferably, the toughener is polyester epoxy resin.
Preferably, a length of 4 hours when the ball mill grinding, and ratio of grinding media to material is 7:1, revolving speed 240-280r/min.
Preferably, the step (3) high temperature temperature of smelting furnace is 1520 DEG C, while keeping temperature is 11 hours.
Preferably, molding machine temperature is 1200 DEG C in the step (4).
Preferably, in the step (8), the maximum temperature of oven is 560 DEG C, and when glass container is placed in oven
Between be 1-1.5 hours.
Compared with prior art, the beneficial effects of the present invention are:
1, of the invention by sufficiently being cleaned to colourless cullet, while during glass container production, successively
Glass is cleaned, to effectively be purged the impurity on glass container, and then improves the decoration firing of glass container
Quality is polyester epoxy resin by the toughener of addition, to effectively raise glass container during the preparation process tough
Property, it is effectively reduced the breakage rate of glass container, while improving the intensity that glass container uses.
2, the present invention slowly persistently rises to maximum temperature by the way that glass container to be placed in oven, and in oven, then
Slow cooling improves the baking efficiency of glass container to effectively carry out marble paper to examine print to minimum temperature.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The present invention provides a kind of technical solution: a kind of formula and its production method of high temperature decoration firing glass container, including with
Lower percentage raw material: colourless cullet 20%, soda ash 12%, aluminium hydroxide 5.2%, ice crystal 4.5%, borax 8%, potassium carbonate
6%, dolomite 16%, calcite 12%, barium sulfate 4.14%, sodium nitrate 2%, cobalt oxide 0.01%, boron oxide 3.15%, increasing
Tough dose 7%.
(1) cleaning: the colourless cullet come will be collected and carried out after sufficiently cleaning, then dry simultaneously natural drying；
(2) mixed grinding: above-mentioned resulting raw material being put into and is ground into ball mill, and by the raw material after grinding into
Row refilters mixing, and high-purity mixed powder is made；
(3) high temperature melting: powder obtained in step (1) is sent into high-temperature smelting pot, and adjusts high-temperature smelting pot temperature and is
It is melted at a temperature of 1500-1550 DEG C, and keeping temperature is 10-12 hours, obtains uniform glass stoste；
(4) adjusting molding machine temperature is 1100-1300 DEG C, and the glass stoste that temperature is reduced to 1250 DEG C is sent into molding machine
Inside forms Semi-finished glass container；
(5) it when the temperature of Semi-finished glass container made from step (4) being down to 800-820 DEG C, then is sent into conveyer belt
In annelaing pot, and annelaing pot internal temperature is 780-810 DEG C, makes Semi-finished glass container retention time 4- inside annelaing pot
4.5 hours, after temperature is reduced to 100 DEG C, Semi-finished glass container taking-up natural room temperature is dried；
(6) Semi-finished glass container made from step (5) cleaned, dried, polish, polish after cleaned again simultaneously
It is dry；
(7) marble paper needed for glass container decoration firing is drawn a design, and after marble paper is impregnated, marble paper is fitted tightly over
It needs on the glass container of decoration firing, carries out naturally dry；
(8) glass container for being stained with marble paper is fed through in oven and is toasted, and glass container successively passes through in oven
Heat-flash section, firing section, slow cooling section, rapid cooling section, are adjusted to 200-590 DEG C by the temperature of oven；
(9) glass container after decoration firing cooling down carries out wiping detection, obtains qualified glass container.
The toughener is polyester epoxy resin.
It is 4 hours a length of when the described ball mill grinding, and ratio of grinding media to material is 7:1, revolving speed 240-280r/min.
Step (3) the high temperature temperature of smelting furnace is 1520 DEG C, while keeping temperature is 11 hours.
Molding machine temperature is 1200 DEG C in the step (4).
In the step (8), the maximum temperature of oven is 560 DEG C, and glass container standing time in oven is 1-
1.5 hour.
Working principle: by sufficiently being cleaned to colourless cullet, while during glass container production, successively
Glass is cleaned, to effectively be purged the impurity on glass container, and then improves the decoration firing of glass container
Quality is polyester epoxy resin by the toughener of addition, to effectively raise glass container during the preparation process tough
Property, it is effectively reduced the breakage rate of glass container, while improving the intensity that glass container uses, by putting glass container
It sets in oven, and slowly persistently rises to maximum temperature, then slow cooling to minimum temperature, to will effectively spend in oven
Paper carries out examining print, improves the baking efficiency of glass container
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of formula and its production method of high temperature decoration firing glass container, which is characterized in that including following percentage raw material: nothing
Color cullet 20%, soda ash 12%, aluminium hydroxide 5.2%, ice crystal 4.5%, borax 8%, potassium carbonate 6%, dolomite 16%,
Calcite 12%, barium sulfate 4.14%, sodium nitrate 2%, cobalt oxide 0.01%, boron oxide 3.15%, toughener 7%.
(1) cleaning: the colourless cullet come will be collected and carried out after sufficiently cleaning, then dry simultaneously natural drying；
(2) mixed grinding: above-mentioned resulting raw material being put into and is ground into ball mill, and the raw material after grinding is carried out again
Filtering mixing, is made high-purity mixed powder；
(3) high temperature melting: powder obtained in step (1) is sent into high-temperature smelting pot, and adjusting high-temperature smelting pot temperature is 1500-
It is melted at a temperature of 1550 DEG C, and keeping temperature is 10-12 hours, obtains uniform glass stoste；
(4) adjusting molding machine temperature is 1100-1300 DEG C, and the glass stoste that temperature is reduced to 1250 DEG C is sent into molding machine
Portion forms Semi-finished glass container；
(5) it when the temperature of Semi-finished glass container made from step (4) being down to 800-820 DEG C, then is sent into and is annealed with conveyer belt
In case, and annelaing pot internal temperature is 780-810 DEG C, makes Semi-finished glass container retention time 4-4.5 inside annelaing pot
Hour, after temperature is reduced to 100 DEG C, Semi-finished glass container taking-up natural room temperature is dried；
(6) it is cleaned and is done again after being cleaned, dried by Semi-finished glass container made from step (5), being polished, polish
It is dry；
(7) marble paper needed for glass container decoration firing is drawn a design, and after marble paper is impregnated, marble paper is fitted tightly over needs
On the glass container of decoration firing, naturally dry is carried out；
(8) glass container for being stained with marble paper is fed through in oven and is toasted, and glass container successively passes through heat-flash in oven
Section, firing section, slow cooling section, rapid cooling section, are adjusted to 200-590 DEG C by the temperature of oven；
(9) glass container after decoration firing cooling down carries out wiping detection, obtains qualified glass container.
2. the formula and its production method of a kind of high temperature decoration firing glass container according to claim 1, it is characterised in that: institute
Stating toughener is polyester epoxy resin.
3. the formula and its production method of a kind of high temperature decoration firing glass container according to claim 1, it is characterised in that: institute
A length of 4 hours when the ball mill grinding stated, and ratio of grinding media to material is 7:1, revolving speed 240-280r/min.
4. the formula and its production method of a kind of high temperature decoration firing glass container according to claim 1, it is characterised in that: institute
The step of stating (3) high temperature temperature of smelting furnace is 1520 DEG C, while keeping temperature is 11 hours.
5. the formula and its production method of a kind of high temperature decoration firing glass container according to claim 1, it is characterised in that: institute
Molding machine temperature is 1200 DEG C in the step of stating (4).
6. the formula and its production method of a kind of high temperature decoration firing glass container according to claim 1, it is characterised in that: institute
In the step of stating (8), the maximum temperature of oven is 560 DEG C, and glass container standing time in oven is 1-1.5 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910522138.0A CN110255899A (en) | 2019-06-17 | 2019-06-17 | A kind of formula and its production method of high temperature decoration firing glass container |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910522138.0A CN110255899A (en) | 2019-06-17 | 2019-06-17 | A kind of formula and its production method of high temperature decoration firing glass container |
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| CN110255899A true CN110255899A (en) | 2019-09-20 |
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| CN201910522138.0A Pending CN110255899A (en) | 2019-06-17 | 2019-06-17 | A kind of formula and its production method of high temperature decoration firing glass container |
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2019
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Application publication date: 20190920 |