CN110250482A - A kind of root of Dahurain angelica and its infusion technology - Google Patents
A kind of root of Dahurain angelica and its infusion technology Download PDFInfo
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- CN110250482A CN110250482A CN201910592536.XA CN201910592536A CN110250482A CN 110250482 A CN110250482 A CN 110250482A CN 201910592536 A CN201910592536 A CN 201910592536A CN 110250482 A CN110250482 A CN 110250482A
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- root
- dahurain angelica
- extracting solution
- angelica
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- 235000001287 Guettarda speciosa Nutrition 0.000 title claims abstract description 125
- 238000005516 engineering process Methods 0.000 title claims abstract description 17
- 238000001802 infusion Methods 0.000 title claims abstract description 17
- 244000061520 Angelica archangelica Species 0.000 title 1
- 241000125175 Angelica Species 0.000 claims abstract description 124
- 238000000034 method Methods 0.000 claims abstract description 35
- 230000008569 process Effects 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 17
- 239000000341 volatile oil Substances 0.000 claims abstract description 15
- PQMOXTJVIYEOQL-UHFFFAOYSA-N Cumarin Natural products CC(C)=CCC1=C(O)C(C(=O)C(C)CC)=C(O)C2=C1OC(=O)C=C2CCC PQMOXTJVIYEOQL-UHFFFAOYSA-N 0.000 claims abstract description 9
- FSOGIJPGPZWNGO-UHFFFAOYSA-N Meomammein Natural products CCC(C)C(=O)C1=C(O)C(CC=C(C)C)=C(O)C2=C1OC(=O)C=C2CCC FSOGIJPGPZWNGO-UHFFFAOYSA-N 0.000 claims abstract description 9
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims abstract description 6
- 235000010241 potassium sorbate Nutrition 0.000 claims abstract description 6
- 239000004302 potassium sorbate Substances 0.000 claims abstract description 6
- 229940069338 potassium sorbate Drugs 0.000 claims abstract description 6
- 150000003839 salts Chemical class 0.000 claims abstract description 6
- CIWBSHSKHKDKBQ-DUZGATOHSA-N D-araboascorbic acid Natural products OC[C@@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-DUZGATOHSA-N 0.000 claims abstract description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 5
- 235000010350 erythorbic acid Nutrition 0.000 claims abstract description 5
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 5
- DINKXUCRJBUQAZ-UHFFFAOYSA-N tert-butyl 5-bromopyridine-3-carboxylate Chemical compound CC(C)(C)OC(=O)C1=CN=CC(Br)=C1 DINKXUCRJBUQAZ-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000000605 extraction Methods 0.000 claims abstract description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 24
- 239000010935 stainless steel Substances 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000001914 filtration Methods 0.000 claims description 12
- 239000002994 raw material Substances 0.000 claims description 12
- 238000000746 purification Methods 0.000 claims description 11
- 241000213006 Angelica dahurica Species 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 9
- 239000011344 liquid material Substances 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 7
- 235000019441 ethanol Nutrition 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 6
- 239000006071 cream Substances 0.000 claims description 6
- 238000010025 steaming Methods 0.000 claims description 6
- 235000013373 food additive Nutrition 0.000 claims description 5
- 239000002778 food additive Substances 0.000 claims description 5
- 201000010099 disease Diseases 0.000 claims description 4
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 241000607479 Yersinia pestis Species 0.000 claims description 3
- 230000009471 action Effects 0.000 claims description 3
- 229910000278 bentonite Inorganic materials 0.000 claims description 3
- 239000000440 bentonite Substances 0.000 claims description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 238000005352 clarification Methods 0.000 claims description 3
- 238000011049 filling Methods 0.000 claims description 3
- 239000012530 fluid Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000007781 pre-processing Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 235000020097 white wine Nutrition 0.000 claims description 3
- 230000037237 body shape Effects 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 11
- 235000011194 food seasoning agent Nutrition 0.000 abstract description 8
- 239000003814 drug Substances 0.000 abstract description 7
- 239000003795 chemical substances by application Substances 0.000 abstract description 5
- 238000010411 cooking Methods 0.000 abstract description 5
- 239000004615 ingredient Substances 0.000 abstract description 5
- 230000007721 medicinal effect Effects 0.000 abstract description 5
- 239000003963 antioxidant agent Substances 0.000 abstract description 3
- 230000003078 antioxidant effect Effects 0.000 abstract description 3
- 229940079593 drug Drugs 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 239000004283 Sodium sorbate Substances 0.000 abstract 1
- 235000019250 sodium sorbate Nutrition 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 241000272525 Anas platyrhynchos Species 0.000 description 2
- 241000287828 Gallus gallus Species 0.000 description 2
- 208000002193 Pain Diseases 0.000 description 2
- 235000013409 condiments Nutrition 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000035772 mutation Effects 0.000 description 2
- 241000272814 Anser sp. Species 0.000 description 1
- 206010017553 Furuncle Diseases 0.000 description 1
- 244000299452 Gouania lupuloides Species 0.000 description 1
- 235000000292 Gouania lupuloides Nutrition 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 206010022000 influenza Diseases 0.000 description 1
- 201000005630 leukorrhea Diseases 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 230000001114 myogenic effect Effects 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 206010039083 rhinitis Diseases 0.000 description 1
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium erythorbate Chemical compound [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 description 1
- 235000010352 sodium erythorbate Nutrition 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 208000004371 toothache Diseases 0.000 description 1
- 206010046901 vaginal discharge Diseases 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/115—Natural spices, flavouring agents or condiments; Extracts thereof obtained by distilling, stripping, or recovering of volatiles
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3508—Organic compounds containing oxygen containing carboxyl groups
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/358—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention discloses a kind of root of Dahurain angelica and its infusion technologies, are related to extract Technique of Chinese Medicine Efficacious Ingredient field.T passes through the root of Dahurain angelica and its infusion technology, it being capable of the medicinal ingredients such as volatile oil, cumarin and its derivative in the high efficiency extraction root of Dahurain angelica, root of Dahurain angelica mixed concentrated liquid is made, it can further improve the medical value and seasoning value of the root of Dahurain angelica, when medicinal, later period pharmaceutical processing process can be reduced, guarantees its medicinal effects；When cooking flavouring, its root of Dahurain angelica mixed concentrated liquid can be cooked directly together with food materials, while reaching its ideal seasoning value, and influence to food materials quality or mouthfeel can be reduced, root of Dahurain angelica herbal cuisine function greatly is optimized, improves the herbal cuisine Land use systems of the root of Dahurain angelica, by the way that the additives such as salt, D-araboascorbic acid sodium and potassium sorbate are added in root of Dahurain angelica mixed concentrated liquid as antioxidant fresh-keeping agent, it is able to extend the pot-life of its product, realizes more stable practical application value.
Description
Technical field
The present invention relates to extract Technique of Chinese Medicine Efficacious Ingredient field, specially a kind of root of Dahurain angelica and its infusion technology.
Background technique
The root of Dahurain angelica, Chinese medicine name are perennial tall and big draft, and 1-2.5 meters high, root is cylindrical, 2-5 centimetres of basal part of stem diameter, and base is raw
Leaf one returns pinnation, and universal umbel basidixed or side are raw, fruit oblong to oval.Main mutation has Radix angelicae dahuricae, Qi Bai
The root of Dahurian angelica, the root of Dahurain angelica (former mutation), Taiwan Radix Angelicae Pubescentis.It is used as medicine with root, the functions such as the dehumidifying that gets rid of illness, apocenosis myogenic, promoting blood circulation and stopping pain.Cure mainly wind
Cold flu, headache, rhinitis, toothache.The diseases such as leukorrhea with reddish discharge, pain furuncle poison.The root of Dahurain angelica is both medicinal material and fragrance condiment, purposes
It extensively, is the important member in perfumery family as one of " Thirteen Spice " raw material, taste fragrance, slight bitter have and remove peculiar smell, increases
Fragrance, flavor adjustment, orectic effect.The root of Dahurain angelica makees chafing dish bottom flavorings, halogen material, has the function render palatable, is fresh-keeping, preventing corruption
Effect.Baoshang or cooking beef and mutton add the root of Dahurain angelica, can make fine and tender taste except fresh adding of having a strong smell.The root of Dahurain angelica has the effect of convergence, roast chicken, duck, meat
It when class, can prevent water from running off, chicken, duck, the goose baked is moistened fresh and tender, and Jiao Bugan is not dry.The root of Dahurain angelica is at it as fragrance condiment
While, the medical value of its own is also played, and health-care effect can be reached, it is quite popular.
The medical value and seasoning value of the root of Dahurain angelica are all very high, and the brewing method of the root of Dahurain angelica is usually to pick impurity at present, use water
Clean, impregnate, pull out and moisturize, slightly smile to crust without soapy feeling when, then after bored profit, dry medicine materical crude slice is made in chip drying.It is in medicine
Used time, process is tedious for later period pharmaceutical processing, difficulty is big, and its effective component is not easy to extract, and influences medicinal effects；It is used as
When cooking flavouring, needs angelica dahurica powder or root of Dahurain angelica slice to cook together with food materials, the quality or mouthfeel of food materials finished product are caused
Very big influence.
Summary of the invention
In view of the above problems, the present invention provides a kind of root of Dahurain angelica and its infusion technology, it can high efficiency extraction it is white
The medicinal ingredients such as volatile oil, cumarin and its derivative in the root of Dahurian angelica, are made root of Dahurain angelica mixed concentrated liquid, when medicinal, after can reducing
Phase pharmaceutical processing process, guarantees its medicinal effects；When cooking flavouring, root of Dahurain angelica mixed concentrated liquid can be directly together with food materials
Culinary art while reaching its ideal seasoning value, and can reduce the influence to food materials quality or mouthfeel, very big to optimize
Root of Dahurain angelica herbal cuisine function.
The present invention is in order to solve the above technical problems, provide the following technical solutions:
A kind of root of Dahurain angelica, the root of Dahurain angelica are the root of triennial Radix angelicae dahuricae, which is located in advance by following steps
Reason:
(a), it chooses sturdy, smooth in appearance no disease and pests harm the extra dry white wine root of Dahurian angelica of individual to be placed in container, 40 DEG C of left sides is then added
Right warm water impregnates 5 minutes, then pulls out and drain away the water after being stirred cleaning；
(b), the root of Dahurain angelica after cleaning is put into porous steaming tray, high fire is stewing in steamer steams 30 points -60 minutes, then stops working
It is stewing to steam -150 minutes 120 minutes, it operates 3-5 times repeatedly, during this period, the root of Dahurain angelica must be avoided to contact with the boiling water in steamer,
The root of Dahurain angelica is set to reach certain humidity under the action of vapor, until root of Dahurain angelica section quality softens, losing mealiness can be sliced
Processing；
(c), slice processing is carried out to the root of Dahurain angelica after stewing steaming, slice thickness control is arrived between 1 millimeter -2 millimeters
Thickness root of Dahurain angelica between 1 millimeter -2 millimeters is sliced.
A kind of infusion technology of the root of Dahurain angelica, the infusion technology include following operation:
(d), the root of Dahurain angelica after pre-processing in claim 1 is put into stainless steel bubble bucket, is subsequently poured into identical as the root of Dahurain angelica
The ethyl alcohol of mass fraction, then by stainless steel bubble bucket sealing, stainless steel bubble bucket is rocked, the feed distribution for keeping it internal is uniform, so
Brewed 2-3 days afterwards；
(e), stainless steel bubble bucket is heated in brew process, constant temperature, the temperature for keeping it internal maintains 54 DEG C -60
Between DEG C, once inside out work is carried out to stainless steel bubble bucket every 7-8 hour, the raw material for keeping it internal is uniformly impregnated；
(f), when brewed process closes to an end, stainless steel bubble bucket is heated, its internal temperature is made to maintain 90
It DEG C -100 DEG C, is kept for 20 minutes, so that it is naturally cooled to 45 DEG C -50 DEG C, then carried out to the raw material in stainless steel bubble bucket
Filter operation, obtains root of Dahurain angelica extracting solution.
Preferably, the purity of the ethyl alcohol is between 62%-75%.
Preferably, the detailed steps of filter operation are as follows: first by stainless steel steep bucket in 200 mesh of raw material gauze into
Row filters for the first time, isolated solid feed and liquid material, then will for the first time filtered solid feed with 200
Purpose gauze package, then by centrifugal separation, the liquid material being further separated out in solid feed, then dividing twice
The liquid material mixing separated out, carries out second and filters, filter the gauze of -400 mesh of 300 mesh for the second time, obtain after filtering white
Root of Dahurian angelica extracting solution.
Preferably, which also includes concentration purifying technique, is completed by following process:
(g), root of Dahurain angelica extracting solution is subjected to bentonite clarification, then obtains the pure root of Dahurain angelica after carrying out diatomite filtering, film filtering
Extracting solution；
(h), pure root of Dahurain angelica extracting solution is realized by way of distillation to volatile oil, the cumarin in root of Dahurain angelica extracting solution
And its purification of derived material, purification process are that the root of Dahurain angelica concentrate for being rich in volatile essential oil is obtained using condensing unit, are steamed
The step of evaporating purification is divided into three phases: a length of 4-6 hour, temperature are maintained at 72 DEG C -80 DEG C when the first stage；Second-order
A length of 3-4 hour, temperature are maintained at 90 DEG C -95 DEG C when section；Phase III makes root of Dahurain angelica extracting solution keep fluidized state, continues
- 30 minutes 20 minutes；
(i), it after volatile substance purification such as volatile oil in root of Dahurain angelica extracting solution, then is remained in distillation equipment
Remaining root of Dahurain angelica extracting solution carries out receipts water, and the root of Dahurain angelica condensed cream rich in cumarin and its derived material that concentration is in fluid is made,
It receives water process and water law is received using heating, so that the temperature of root of Dahurain angelica extracting solution is maintained at 72 DEG C -78 DEG C, until root of Dahurain angelica extracting solution becomes
Thick is in flow-like；
(j), made of being rich in obtained in above-mentioned operation (h) in the root of Dahurain angelica concentrate and process (i) of volatile essential oil
Root of Dahurain angelica condensed cream is uniformly mixed, and is added food additives and is uniformly mixed to get root of Dahurain angelica mixed concentrated liquid, the food additive is arrived
Adding agent includes salt 0.5%, D-araboascorbic acid sodium 0.02% and potassium sorbate 0.02%；
(K), root of Dahurain angelica mixed concentrated liquid is filling, be sealed.
Compared with prior art, the root of Dahurain angelica and its infusion technology have it is following the utility model has the advantages that
It according to the technical solution of the present invention, being capable of the medicines such as volatile oil, cumarin and its derivative in the high efficiency extraction root of Dahurain angelica
With ingredient, root of Dahurain angelica mixed concentrated liquid is made, when medicinal, later period pharmaceutical processing process can be reduced, guarantee its medicinal effects；?
When cooking flavouring, root of Dahurain angelica mixed concentrated liquid can be cooked directly together with food materials, reach the same of its ideal seasoning value
When, and the influence to food materials quality or mouthfeel can be reduced, it is very big to optimize root of Dahurain angelica herbal cuisine function, improve the herbal cuisine benefit of the root of Dahurain angelica
With mode, the medical value and seasoning value of the root of Dahurain angelica are further increased, by the way that salt, D- are added in root of Dahurain angelica mixed concentrated liquid
The additives such as sodium isoascorbate and potassium sorbate are able to extend the pot-life of its product as antioxidant fresh-keeping agent, realize more
Add stable practical application value.
Specific embodiment is handed over flat
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described, it is clear that described embodiments are only a part of the embodiments of the present invention, and
The embodiment being not all of.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creative work
Under the premise of every other embodiment obtained, shall fall within the protection scope of the present invention.
The lower present invention provides a kind of technical solution:
A kind of root of Dahurain angelica, the root of Dahurain angelica select the root of triennial Radix angelicae dahuricae, are then pre-processed by following steps:
(a), it chooses sturdy, smooth in appearance no disease and pests harm the extra dry white wine root of Dahurian angelica of individual to be placed in container, 40 DEG C of left sides is then added
Right warm water impregnates 5 minutes, then pulls out and drain away the water after being stirred cleaning；
(b), the root of Dahurain angelica after cleaning is put into porous steaming tray, high fire is stewing in steamer steams 30 points -60 minutes, then stops working
It is stewing to steam -150 minutes 120 minutes, it operates 3-5 times repeatedly, during this period, the root of Dahurain angelica must be avoided to contact with the boiling water in steamer,
The root of Dahurain angelica is set to reach certain humidity under the action of vapor, until root of Dahurain angelica section quality softens, losing mealiness can be sliced
Processing；
(c), slice processing is carried out to the root of Dahurain angelica after stewing steaming, slice thickness control is arrived between 1 millimeter -2 millimeters
Thickness root of Dahurain angelica between 1 millimeter -2 millimeters is sliced.
A kind of infusion technology of the root of Dahurain angelica, the infusion technology include following operation:
(d), the root of Dahurain angelica after pre-processing in claim 1 is put into stainless steel bubble bucket, is subsequently poured into identical as the root of Dahurain angelica
The ethyl alcohol of mass fraction, then by stainless steel bubble bucket sealing, stainless steel bubble bucket is rocked, the feed distribution for keeping it internal is uniform, so
Brewed 2-3 days afterwards；
(e), stainless steel bubble bucket is heated in brew process, constant temperature, the temperature for keeping it internal maintains 54 DEG C -60
Between DEG C, once inside out work is carried out to stainless steel bubble bucket every 7-8 hour, the raw material for keeping it internal is uniformly impregnated；
(f), when brewed process closes to an end, stainless steel bubble bucket is heated, its internal temperature is made to maintain 90
It DEG C -100 DEG C, is kept for 20 minutes, so that it is naturally cooled to 45 DEG C -50 DEG C, then carried out to the raw material in stainless steel bubble bucket
Filter operation, obtains root of Dahurain angelica extracting solution.
Preferably, the purity of the ethyl alcohol in process (d) is between 62%-75%.The ethyl alcohol of this concentration is more suitable for dissolution simultaneously
The effective component in the root of Dahurain angelica is extracted, the concentration purifying technique in later period is more advantageous to.
Preferably, in process (f) filter operation detailed steps are as follows: first by stainless steel steep bucket in 200 purposes of raw material
Gauze carries out first time filtering, and isolated solid feed and liquid material then will first time filtered solid feeds
It is wrapped up with the gauze of 200 mesh, then passes through centrifugal separation, the liquid material being further separated out in solid feed, then two
The secondary liquid material mixing isolated, carries out second and filters, filter the gauze of -400 mesh of 300 mesh for the second time, after filtering
To root of Dahurain angelica extracting solution.This scheme can realize the efficient utilization to root of Dahurain angelica raw material, reduce the waste to root of Dahurain angelica raw material material, go forward side by side
The quality of one step raising root of Dahurain angelica extracting solution.
Preferably, which also includes concentration purifying technique, is completed by following process:
(g), root of Dahurain angelica extracting solution is subjected to bentonite clarification, then obtains the pure root of Dahurain angelica after carrying out diatomite filtering, film filtering
Extracting solution；
(h), pure root of Dahurain angelica extracting solution is realized by way of distillation to volatile oil, the cumarin in root of Dahurain angelica extracting solution
And its purification of derived material, purification process are that the root of Dahurain angelica concentrate for being rich in volatile essential oil is obtained using condensing unit, are steamed
The step of evaporating purification is divided into three phases: a length of 4-6 hour, temperature are maintained at 72 DEG C -80 DEG C when the first stage；Second-order
A length of 3-4 hour, temperature are maintained at 90 DEG C -95 DEG C when section；Phase III makes root of Dahurain angelica extracting solution keep fluidized state, continues
- 30 minutes 20 minutes；
(i), it after volatile substance purification such as volatile oil in root of Dahurain angelica extracting solution, then is remained in distillation equipment
Remaining root of Dahurain angelica extracting solution carries out receipts water, and the root of Dahurain angelica condensed cream rich in cumarin and its derived material that concentration is in fluid is made,
It receives water process and water law is received using heating, so that the temperature of root of Dahurain angelica extracting solution is maintained at 72 DEG C -78 DEG C, until root of Dahurain angelica extracting solution becomes
Thick is in flow-like；
(j), made of being rich in obtained in above-mentioned operation (h) in the root of Dahurain angelica concentrate and process (i) of volatile essential oil
Root of Dahurain angelica condensed cream is uniformly mixed, and is added food additives and is uniformly mixed to get root of Dahurain angelica mixed concentrated liquid, food addition is arrived
Agent includes salt 0.5%, D-araboascorbic acid sodium 0.02% and potassium sorbate 0.02%；Wherein salt, D-araboascorbic acid sodium
It is used as antioxidant fresh-keeping agent with potassium sorbate, can be extended the shelf life.
(K), root of Dahurain angelica mixed concentrated liquid is filling, be sealed.The root of Dahurain angelica mixed concentrated liquid can be directly used for pharmacy, can
The pharmaceutical processing process for reducing the later period, guarantees its medicinal effects；Also it can be directly used for seasoning, food materials be added and cook together, are reaching
While value to its ideal seasoning, and the influence to food materials quality or mouthfeel can be reduced.
In the description of the present invention, the terms "include", "comprise" or its any other variant are intended to nonexcludability
Include so that include a series of elements process, method, article or equipment not only include those elements, but also
Including other elements that are not explicitly listed, or further include for this process, method, article or equipment it is intrinsic
Element.In the absence of more restrictions, the element limited by sentence " including a reference structure ", it is not excluded that wrapping
Include in the process, method, article or equipment of the element that there is also other identical elements.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (5)
1. a kind of root of Dahurain angelica, the root of Dahurain angelica is the root of triennial Radix angelicae dahuricae, it is characterised in that: the root of Dahurain angelica by following steps into
Row pretreatment:
(a), it chooses sturdy, smooth in appearance no disease and pests harm the extra dry white wine root of Dahurian angelica of individual to be placed in container, is then added 40 DEG C or so
Warm water impregnates 5 minutes, then pulls out and drain away the water after being stirred cleaning；
(b), the root of Dahurain angelica after cleaning is put into porous steaming tray, high fire is stewing in steamer steams 30 points -60 minutes, stewing steam of then stopping working
It -150 minutes 120 minutes, operates 3-5 times repeatedly, during this period, the root of Dahurain angelica must be avoided to contact with the boiling water in steamer, made white
The root of Dahurian angelica reaches certain humidity under the action of vapor, and until root of Dahurain angelica section quality softens, slice processing can be carried out by losing mealiness
?；
(c), slice processing is carried out to the root of Dahurain angelica after stewing steaming, slice thickness control exists between 1 millimeter -2 millimeters to get to thickness
The root of Dahurain angelica is sliced between 1 millimeter -2 millimeters.
2. a kind of infusion technology of the root of Dahurain angelica, it is characterised in that: the infusion technology includes following operation:
(d), the root of Dahurain angelica after pre-processing in claim 1 is put into stainless steel bubble bucket, is subsequently poured into and root of Dahurain angelica phase homogenous quantities
The ethyl alcohol of number, then by stainless steel bubble bucket sealing, stainless steel bubble bucket is rocked, the feed distribution for keeping it internal is uniform, then steeps
2-3 days processed；
(e), stainless steel bubble bucket is heated in brew process, constant temperature, the temperature for keeping it internal maintain 54 DEG C -60 DEG C it
Between, once inside out work is carried out to stainless steel bubble bucket every 7-8 hour, the raw material for keeping it internal is uniformly impregnated；
(f), when brewed process closes to an end, stainless steel bubble bucket is heated, its internal temperature is made to maintain 90 DEG C -100
DEG C, it is kept for 20 minutes, so that it is naturally cooled to 45 DEG C -50 DEG C, then be filtered operation to the raw material in stainless steel bubble bucket,
Obtain root of Dahurain angelica extracting solution.
3. a kind of root of Dahurain angelica infusion technology according to claim 2, it is characterised in that: the purity of the ethyl alcohol is in 62%-
Between 75%.
4. a kind of root of Dahurain angelica infusion technology according to claim 2, it is characterised in that: the detailed steps of its filter operation are as follows:
Stainless steel is first steeped into the raw material in bucket and carries out first time filtering with the gauze of 200 mesh, isolated solid feed and liquid are former
Then material wraps up the gauze of 200 mesh of filtered solid feed for the first time, then by centrifugal separation, further separate
Then liquid material in solid feed out mixes the liquid material isolated twice, carry out second and filter, second of mistake
The gauze for filtering -400 mesh of 300 mesh, obtains root of Dahurain angelica extracting solution after filtering.
5. a kind of root of Dahurain angelica infusion technology according to claim 2, it is characterised in that: the root of Dahurain angelica infusion technology also includes concentration
Purifying technique is completed by following process:
(g), root of Dahurain angelica extracting solution is subjected to bentonite clarification, then obtains pure root of Dahurain angelica extraction after carrying out diatomite filtering, film filtering
Liquid；
(h), pure root of Dahurain angelica extracting solution is by way of distillation, realize in root of Dahurain angelica extracting solution volatile oil, cumarin and its
The purification of derived material, purification process are that the root of Dahurain angelica concentrate for being rich in volatile essential oil is obtained using condensing unit, and distillation mentions
Pure step is divided into three phases: a length of 4-6 hour, temperature are maintained at 72 DEG C -80 DEG C when the first stage；Second stage duration
For 3-4 hour, temperature is maintained at 90 DEG C -95 DEG C；Phase III make root of Dahurain angelica extracting solution keep fluidized state, continue 20 minutes-
30 minutes；
(i), after volatile substance purification such as volatile oil in root of Dahurain angelica extracting solution, then to remaining white in distillation equipment
Root of Dahurian angelica extracting solution carries out receipts water, and concentration is made in the root of Dahurain angelica condensed cream rich in cumarin and its derived material of fluid, receives water mistake
Water law is received in Cheng Caiyong heating, and the temperature of root of Dahurain angelica extracting solution is made to be maintained at 72 DEG C -78 DEG C, until root of Dahurain angelica extracting solution becomes thick in stream
Body shape；
(j), the manufactured root of Dahurain angelica in the root of Dahurain angelica concentrate and process (i) of volatile essential oil will be rich in obtained in above-mentioned operation (h)
Condensed cream is uniformly mixed, and is added food additives and is uniformly mixed to get root of Dahurain angelica mixed concentrated liquid, the food additives packet is arrived
Include salt 0.5%, D-araboascorbic acid sodium 0.02% and potassium sorbate 0.02%；
(K), root of Dahurain angelica mixed concentrated liquid is filling, be sealed.
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Citations (2)
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|---|---|---|---|---|
| US20070172531A1 (en) * | 2006-01-20 | 2007-07-26 | Desheng Tao | Chinese traditional medicine composition for treatment of avian influenza, method for preparation, and application thereof |
| CN101062069A (en) * | 2007-06-18 | 2007-10-31 | 石任兵 | Whole coumarins extract from root of dahuriae angelica and the preparing method thereof |
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2019
- 2019-07-03 CN CN201910592536.XA patent/CN110250482A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070172531A1 (en) * | 2006-01-20 | 2007-07-26 | Desheng Tao | Chinese traditional medicine composition for treatment of avian influenza, method for preparation, and application thereof |
| CN101062069A (en) * | 2007-06-18 | 2007-10-31 | 石任兵 | Whole coumarins extract from root of dahuriae angelica and the preparing method thereof |
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| Title |
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| 任星宇等: "白芷挥发油提取方法及药理作用的研究进展", 《中国药房》 * |
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Application publication date: 20190920 |