CN110240473A - 一种多功能陶瓷板及其制备方法 - Google Patents
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- 239000000919 ceramic Substances 0.000 title claims abstract description 64
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000011230 binding agent Substances 0.000 claims abstract description 18
- 229910052878 cordierite Inorganic materials 0.000 claims abstract description 18
- JSKIRARMQDRGJZ-UHFFFAOYSA-N dimagnesium dioxido-bis[(1-oxido-3-oxo-2,4,6,8,9-pentaoxa-1,3-disila-5,7-dialuminabicyclo[3.3.1]nonan-7-yl)oxy]silane Chemical compound [Mg++].[Mg++].[O-][Si]([O-])(O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2)O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2 JSKIRARMQDRGJZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 229910052863 mullite Inorganic materials 0.000 claims abstract description 18
- 238000010304 firing Methods 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 11
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
- 239000008187 granular material Substances 0.000 claims description 8
- 230000032683 aging Effects 0.000 claims description 5
- 239000000470 constituent Substances 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 9
- 238000010521 absorption reaction Methods 0.000 abstract description 6
- 239000002245 particle Substances 0.000 description 6
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 4
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 4
- 208000037656 Respiratory Sounds Diseases 0.000 description 3
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 3
- 230000003796 beauty Effects 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 229910052573 porcelain Inorganic materials 0.000 description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Inorganic materials [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- 239000000292 calcium oxide Substances 0.000 description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- QDOXWKRWXJOMAK-UHFFFAOYSA-N dichromium trioxide Chemical compound O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 239000000395 magnesium oxide Substances 0.000 description 2
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 239000011787 zinc oxide Substances 0.000 description 2
- DQMUQFUTDWISTM-UHFFFAOYSA-N O.[O-2].[Fe+2].[Fe+2].[O-2] Chemical compound O.[O-2].[Fe+2].[Fe+2].[O-2] DQMUQFUTDWISTM-UHFFFAOYSA-N 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- CSSYLTMKCUORDA-UHFFFAOYSA-N barium(2+);oxygen(2-) Chemical compound [O-2].[Ba+2] CSSYLTMKCUORDA-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 229910001950 potassium oxide Inorganic materials 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01K—ANIMAL HUSBANDRY; AVICULTURE; APICULTURE; PISCICULTURE; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
- A01K1/00—Housing animals; Equipment therefor
- A01K1/015—Floor coverings, e.g. bedding-down sheets ; Stable floors
- A01K1/0157—Mats; Sheets
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
- C04B35/185—Mullite 3Al2O3-2SiO2
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/0038—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by superficial sintering or bonding of particulate matter
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3481—Alkaline earth metal alumino-silicates other than clay, e.g. cordierite, beryl, micas such as margarite, plagioclase feldspars such as anorthite, zeolites such as chabazite
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Abstract
本发明公开了一种多功能陶瓷板及其制备方法，该多功能陶瓷板及其制备方法具体如下：所述多功能陶瓷板原料组成包括堇青石、莫来石、高铝质、粘结剂、水，所述S4中陶瓷板的烧制温度为1100℃~1400℃，烧制时间为10~12小时，所述陶瓷板的吸收率为15%~18%，所述陶瓷板的底端对称设有EV垫。本发明具有很好的吸水性能，吸水率高达18.3%，远高于国家标准规定，3组实施例的断裂模数平均值接近36，表现出较好的强度性能，散热温度在3℃左右，陶瓷板的成品率较高，易于加工推广，无刺激性异味，对动物没有伤害，具有很好的应用前景。
Description
技术领域
本发明涉及陶瓷技术领域，具体为一种多功能陶瓷板及其制备方法。
背景技术
随着社会经济的发展和城市化进程的加速，人们精神生活与物质生活不断改善，社会老龄化步伐加快，独生子女家庭普及等客观因素的突出，人们的休闲、消费和情感寄托方式也呈多样化发展。饲养宠物成为众多家庭的消遣方式，随着宠物需求数量的日益增多，宠物产业也逐渐发展壮大。20世纪90年代初，随着中国小动物保护协会成立，宜传将宠物作为伴侣，宠物市场才逐渐开始在国内兴起。相较于国外成熟的宠物市场，中国宠物市场起步虽然晚，但近20年来保持着高速发展。如今我国宠物市场正处在快速成长阶段。
日常生活中，动物在炎炎夏日或者运动后都喜欢伏在阴凉的地方休息，比较喜欢有水洼的地方，可以加速体表温度的降低，但这些环境对动物的毛皮造成一定的污染，
针对上述宠物产业中存在的技术缺陷，发明一种多功能陶瓷板及其制备方法，去解决上述问题，很有应用前景。
发明内容
本发明的目的在于提供一种多功能陶瓷板及其制备方法，该多功能陶瓷板及其制备方法具体如下：所述多功能陶瓷板原料组成包括堇青石、莫来石、高铝质、粘结剂、水，按照以下各组分质量百分比进行称量：
堇青石 15%-20%；
莫来石 35%-50%；
高铝质 20%-30%；
粘结剂 5%-10%；。
作为优选的，所述堇青石的粒度大小为30~50目，莫来石的粒度大小为50~70目，高铝质的粒度大小为70~90目，粘结剂的粒度大小为90~110目。
本发明还提供一种多功能陶瓷板及其制备方法，包括如下步骤：
S1：将堇青石、莫来石、高铝质、粘结剂分别喷雾干燥后进行颗粒粉碎，随后进行过滤、除铁，备用；
S2：将S1中的原料加水进行搅拌混合，陈腐36~64小时，备用；
S3：将S2中的混合料进行压制成型、轻压排气、重压排气、重压成型后制备成陶瓷板坯体；
S4：将S3中的坯体放在窑炉内烧制成品，最后进行抛光、封装。
作为优选的，所述S4中陶瓷板的烧制温度为1100℃~1400℃，烧制时间为10~12小时。
作为优选的，所述陶瓷板的底端对称设有EV垫。
与现有技术相比，本发明的有益效果是：
1、本发明采用该方法制备的陶瓷板具有很好的吸水率，吸水率高达18.3%，远高于国家标准规定，可以对宠物养殖过程中产生的液体及时吸收，3组实施例的断裂模数平均值接近36，表现出较好的强度性能，散热温度在3℃左右，可以给宠物带来很好的体验感，陶瓷板的成品率较高，易于加工推广，无刺激性异味，对动物没有伤害，具有很好的应用前景。
具体实施方式
为了使本发明的目的、技术方案及优点更加清楚明白，以下结合具体实施例，对本发明进行进一步详细说明。应当理解，此处所描述的具体实施例仅仅用以解释本发明，并不用于限定本发明。
实施例1
一种多功能陶瓷板，所述多功能陶瓷板原料组成包括堇青石、莫来石、高铝质、粘结剂、水，按照以下各组分质量百分比进行称量：
堇青石 15%；
莫来石 35%；
高铝质 20%；
粘结剂 5%；
本实施例的多功能陶瓷板制备方法，包括如下步骤:
S1：将堇青石、莫来石、高铝质、粘结剂分别喷雾干燥后进行颗粒粉碎，随后进行过滤可以过滤掉颗粒不均匀的杂质颗粒，除铁可以避免陶瓷板表面产生黑点，影响美观；
S2：将S1中的原料加水进行搅拌混合，陈腐36小时，可以让混合料之间混合的更加均匀，有助于保证陶瓷板的强度；
S3：将S2中的混合料进行压制成型、轻压排气、重压排气、重压成型等步骤，可以减小陶瓷板内部不必要的的空隙或裂纹，有助于保障使用寿命，最后制备成陶瓷板坯体；
S4：将S3中的坯体放在窑炉内烧制成品，最后进行抛光、封装。
所述S4中陶瓷板的烧制温度为1100℃，烧制温度为1100℃，可以避免陶瓷板上出现黑白点现象，烧制时间为10小时。
所述陶瓷板的底端对称设有EV垫。
实施例2
一种多功能陶瓷板，所述多功能陶瓷板原料组成包括堇青石、莫来石、高铝质、粘结剂、水，按照以下各组分质量百分比进行称量：
堇青石 18%；
莫来石 40%；
高铝质 25%；
粘结剂 8%；
本实施例的多功能陶瓷板制备方法，包括如下步骤:
S1：将堇青石、莫来石、高铝质、粘结剂分别喷雾干燥后进行颗粒粉碎，随后进行过滤可以过滤掉颗粒不均匀的杂质颗粒，除铁可以避免陶瓷板表面产生黑点，影响美观；
S2：将S1中的原料加水进行搅拌混合，陈腐48小时，可以让混合料之间混合的更加均匀，有助于保证陶瓷板的强度；
S3：将S2中的混合料进行压制成型、轻压排气、重压排气、重压成型等步骤，可以减小陶瓷板内部不必要的空隙或裂纹，有助于保障使用寿命，最后制备成陶瓷板坯体；
S4：将S3中的坯体放在窑炉内烧制成品，最后进行抛光、封装。
所述S4中陶瓷板的烧制温度为1200℃，烧制温度为1200℃，可以避免陶瓷板上出现黑白点现象，烧制时间为11小时。
所述陶瓷板的底端对称设有EV垫。
实施例3
一种多功能陶瓷板，所述多功能陶瓷板原料组成包括堇青石、莫来石、高铝质、粘结剂、水，按照以下各组分质量百分比进行称量：
堇青石 20%；
莫来石 50%；
高铝质 30%；
粘结剂 10%；
本实施例的多功能陶瓷板制备方法，包括如下步骤:
S1：将堇青石、莫来石、高铝质、粘结剂分别喷雾干燥后进行颗粒粉碎，随后进行过滤可以过滤掉颗粒不均匀的杂质颗粒，除铁可以避免陶瓷板表面产生黑点，影响美观；
S2：将S1中的原料加水进行搅拌混合，陈腐64小时，可以让混合料之间混合的更加均匀，有助于保证陶瓷板的强度；
S3：将S2中的混合料进行压制成型、轻压排气、重压排气、重压成型等步骤，可以减小陶瓷板内部不必要的空隙或裂纹，有助于保障使用寿命，最后制备成陶瓷板坯体；
S4：将S3中的坯体放在窑炉内烧制成品，最后进行抛光、封装。
所述S4中陶瓷板的烧制温度为1400℃，烧制温度为1400℃，可以避免陶瓷板上出现黑白点现象，烧制时间为12小时。
所述陶瓷板的底端对称设有EV垫。
对实施例1-3中所制备的陶瓷板，按照《陶瓷砖》(GBT4100-2015)“的标准测得数据如下表：
| 检测项目 | 实施例1 | 实施例2 | 实施例3 |
| 吸水率 E>3% | 17.8% | 17.6% | 18.3% |
| 断裂模数：≥28 [N/mm<sup>2</sup>(MPa)] | 35.3 | 36.6 | 36.1 |
| 成品率（%） | 98.8% | 99.2% | 99.1% |
| 散热性 （℃） | 3.2 | 3.6 | 3.3 |
| 刺激性试验 | 无刺激 | 无刺激 | 无刺激 |
由上述表格易知：采用该方法制备的陶瓷板具有很好的吸水率，3组实施例的平均吸水率为17.9%，远高于国家标准规定，3组实施例的断裂模数平均值接近36，表现出较好的强度性能，散热温度在3℃左右，陶瓷板的成品率较高，易于加工推广，无刺激性异味，对动物没有伤害，具有很好的应用前景。
对实施例1-3中所制备的陶瓷板，进行成分检测，检测成分结果如下：
| 序号 | 名称 | 含量（%） |
| 1 | SiO<sub>2</sub>(二氧化硅) | 50.70 |
| 2 | Al<sub>2</sub>O<sub>3</sub>(三氧化二铝) | 39.31 |
| 3 | Fe<sub>2</sub>O<sub>3</sub> (三氧化二铁) | 1.39 |
| 4 | CaO（氧化钙） | 0.51 |
| 5 | MgO（氧化镁） | 5.56 |
| 6 | K<sub>2</sub>O（氧化钾） | 1.14 |
| 7 | Na<sub>2</sub>O（氧化钠） | 0.41 |
| 8 | TiO<sub>2</sub>（二氧化钛） | 0.51 |
| 9 | MnO（氧化锰） | 0.06 |
| 10 | P<sub>2</sub>O<sub>5</sub>（五氧化二磷） | 0.06 |
| 11 | SO<sub>3</sub>（三氧化硫） | <0.01 |
| 12 | BaO（氧化钡） | 0.02 |
| 13 | ZnO（氧化锌） | 0.01 |
| 14 | ZrO<sub>2</sub>（二氧化锆） | 0.05 |
| 15 | Cr<sub>2</sub>O<sub>3</sub>（三氧化二镉） | 0.03 |
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。
Claims (6)
1.一种多功能陶瓷板，其特征在于，所述多功能陶瓷板原料组成包括堇青石、莫来石、高铝质、粘结剂、水，按照以下各组分质量百分比进行称量：
堇青石 15%-20%；
莫来石 35%-50%；
高铝质 20%-30%；
粘结剂 5%-10%。
2.根据权利要求1所述的一种多功能陶瓷板，其特征在于，所述堇青石的粒度大小为30~50目，莫来石的粒度大小为50~70目，高铝质的粒度大小为70~90目，粘结剂的粒度大小为90~110目。
3.根据权利要求1所述的一种多功能陶瓷板及其制备方法，其特征在于，包括如下步骤：
S1：将堇青石、莫来石、高铝质、粘结剂分别喷雾干燥后进行颗粒粉碎，随后进行过滤、除铁，备用；
S2：将S1中的原料加水进行搅拌混合，陈腐36~64小时，备用；
S3：将S2中的混合料进行压制成型、轻压排气、重压排气、重压成型后制备成陶瓷板坯体；
S4：将S3中的坯体放在窑炉内烧制成品，最后进行抛光、封装。
4.根据权利要求3所述的一种多功能陶瓷板及其制备方法，其特征在于，所述S4中陶瓷板的烧制温度为1100℃~1400℃，烧制时间为10~12小时。
5.根据权利要求1所述的一种多功能陶瓷板及其制备方法，其特征在于，所述陶瓷板的吸收率为15%~18%。
6.根据权利要求1所述的一种多功能陶瓷板及其制备方法，其特征在于，所述陶瓷板的底端对称设有EV垫。
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