CN110237127A - A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof - Google Patents
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
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- A23K20/10—Organic substances
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/30—Feeding-stuffs specially adapted for particular animals for swines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/24—Heavy metals; Compounds thereof
- A61K33/30—Zinc; Compounds thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/489—Sophora, e.g. necklacepod or mamani
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
- A61K36/718—Coptis (goldthread)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
- A61K9/1629—Organic macromolecular compounds
- A61K9/1635—Organic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polyvinyl pyrrolidone, poly(meth)acrylates
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
- A61K9/1629—Organic macromolecular compounds
- A61K9/1652—Polysaccharides, e.g. alginate, cellulose derivatives; Cyclodextrin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/12—Antidiarrhoeals
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Abstract
The invention discloses a kind of embedded micro-capsules of Chinese medicine mixed oxidization zinc of a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof, and each material composition is as follows: 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, 10 parts of kuh-seng, 90-100 parts of nano zine oxide, 10-20 parts of soluble starch, 20-30 parts of sodium carboxymethyl starch, 10-20 parts of stearic acid, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin.Beneficial effect is: being pelletized by using Chinese medicine mixed oxidization zinc powder, as the anti-diarrheal of piglet, reduces the dosage of zinc oxide, reduce the production cost of anti-diarrheal；By reducing the dosage of zinc oxide in anti-diarrheal, reduces the discharge amount of zinc in piglet excrement, reduce the pollution to soil, improve the feature of environmental protection of drug.
Description
Technical field
The present invention relates to livestock feed additive technology fields, and in particular to a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc
And preparation method thereof.
Background technique
In the prior art, young since oxidation Zinc supplementation is high for preventing baby pig diarrhea after being directly coated with using zinc oxide
Pig feed is easy to appear side effect after, influences the growth of piglet.Develop from international and domestic pharmacology, zinc oxide is in baby pig feedstuff
Additive amount will be gradually lowered to use, but in the market and the product used that can not be substituted.
Summary of the invention
The object of the invention is that providing a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc to solve the above-mentioned problems
And preparation method thereof, include can be by Chinese medicine mixing oxygen for preferred technical solution in many technical solutions provided by the invention
Change embedded micro-capsule made of zinc, treats the diarrhea of piglet, to reduce the dosage of zinc oxide, reduce the technologies such as the generation of side effect
Effect, elaboration as detailed below.
To achieve the above object, the present invention provides following technical schemes:
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc provided by the invention and preparation method thereof, each material composition is as follows:
50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, 10 parts of kuh-seng, 90-100 parts of nano zine oxide, 10-20 parts of soluble starch, carboxylic first
20-30 parts of base sodium starch, 10-20 parts of stearic acid, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin.
Preferably, 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, 10 parts of kuh-seng, 95 parts of nano zine oxide, soluble starch
15 parts, 25 parts of sodium carboxymethyl starch, 15 parts of stearic acid, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin.
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof, comprising the following steps: a, Chinese medicine semi-finished product
Preparation: by being crushed in 10 parts of 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, kuh-seng filling disintegrating apparatus to be mixed after 150-200 mesh
Uniformly, Chinese medicine semi-finished product are made；
B, 90-100 parts of 60-80 parts of Chinese medicine semi-finished product, nano zine oxide in step a, solvable the preparation of drug softwood: are taken
Property 10-20 parts of starch, 20-30 parts of sodium carboxymethyl starch, 10-20 parts of stearic acid, No. 24 parts of acrylic resin and acrylic resin 3
Numbers 6 parts are added pure water stirring after mixing, and drug softwood is made；
C, it pelletizes: drug softwood obtained in step b being added to the granulator granulation, soft strip-shaped materials grain is made；
D, ball blast: pill-rolling in shot-blasting machine is added in strip-shaped materials grain obtained in step c, and is added during pill-rolling
The uniform microspheric granula of shape is made in Zinc oxide powder；
E, microspheric granula obtained in step d drying forming: is dried to water content less than 5% to get finished product.
Preferably, the disintegrating apparatus in the step a is Ultramicro-powder machine.
Preferably, the revolving speed that granulator is pelletized in the step c is 50-70r/min.
It preferably, shot-blasting machine revolving speed adjusts shearing ball blast from low to high in the step d, and is 350- in revolving speed
Ball blast work 40-60S is carried out when 450r/min.
Preferably, using hot-air seasoning in the step e, wherein inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
To sum up, the beneficial effects of the present invention are: 1, by using Chinese medicine mixed oxidization zinc powder pelletize, as piglet
Anti-diarrheal reduces the dosage of zinc oxide, reduces the production cost of anti-diarrheal；
2, by reducing the dosage of zinc oxide in anti-diarrheal, reduce the discharge amount of zinc in piglet excrement, reduce
Pollution to soil improves the feature of environmental protection of drug.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Embodiment 1:
The present invention provides a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc, each material composition is as follows: 50 parts of hoary hair, the coptis
10 parts, 5 parts of hymsleya amabilis, 10 parts of kuh-seng, 90 parts of nano zine oxide, 10 parts of soluble starch, 20 parts of sodium carboxymethyl starch, stearic acid 10
Part, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin.
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof, comprising the following steps: a, Chinese medicine semi-finished product
Preparation: by being crushed in 10 parts of 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, kuh-seng filling disintegrating apparatus to be mixed after 150-200 mesh
Uniformly, Chinese medicine semi-finished product are made；
B, 90 parts of 60 parts of Chinese medicine semi-finished product, nano zine oxide, the soluble starch in step a the preparation of drug softwood: are taken
No. 36 parts of 10 parts, 20 parts of sodium carboxymethyl starch, 10 parts of stearic acid, No. 24 parts of acrylic resin and acrylic resin are after mixing
Pure water stirring is added, drug softwood is made；
C, it pelletizes: drug softwood obtained in step b being added to the granulator granulation, soft strip-shaped materials grain is made；
D, ball blast: pill-rolling in shot-blasting machine is added in strip-shaped materials grain obtained in step c, and is added during pill-rolling
The uniform microspheric granula of shape is made in Zinc oxide powder, and shot-blasting machine revolving speed adjusts shearing ball blast from low to high, and is in revolving speed
Ball blast work 40-60S is carried out when 350-450r/min, and Zinc oxide powder is added during ball blast, is attached to microspheric granula table
Face prevents microspheric granula adhesion；
E, microspheric granula obtained in step d drying forming: is dried to water content less than 5% to get finished product, drying side
Formula is hot-air seasoning, and controlling inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
As optional embodiment, the disintegrating apparatus in the step a is Ultramicro-powder machine；
The revolving speed that granulator is pelletized in the step c is 50-70r/min.
In the present embodiment, traditional Chinese medicine ingredients content is relatively fewer, and Zinc oxide powder content accounting is more, and capsulating material quality
Accounting is more, after pellet is made, can retain the long period in the stomach and enteron aisle of piglet, had good sustained release effect, pre- anti-diarrhea
Time it is longer.
Embodiment 2:
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc, each material composition are as follows: 50 parts of hoary hair, 10 parts of the coptis, hymsleya amabilis 5
Part, 10 parts of kuh-seng, 100 parts of nano zine oxide, 20 parts of soluble starch, 30 parts of sodium carboxymethyl starch, 20 parts of stearic acid, acrylic acid
No. 24 parts and No. 36 parts of acrylic resin of resin.
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof, comprising the following steps: a, Chinese medicine semi-finished product
Preparation: by being crushed in 10 parts of 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, kuh-seng filling disintegrating apparatus to be mixed after 150-200 mesh
Uniformly, Chinese medicine semi-finished product are made；
B, 100 parts of 80 parts of Chinese medicine semi-finished product, nano zine oxide, the soluble starch in step a the preparation of drug softwood: are taken
No. 36 parts of 20 parts, 30 parts of sodium carboxymethyl starch, 20 parts of stearic acid, No. 24 parts of acrylic resin and acrylic resin are after mixing
Pure water stirring is added, drug softwood is made；
C, it pelletizes: drug softwood obtained in step b being added to the granulator granulation, soft strip-shaped materials grain is made；
D, ball blast: pill-rolling in shot-blasting machine is added in strip-shaped materials grain obtained in step c, and is added during pill-rolling
The uniform microspheric granula of shape is made in Zinc oxide powder, and shot-blasting machine revolving speed adjusts shearing ball blast from low to high, and is in revolving speed
Ball blast work 40-60S is carried out when 350-450r/min, and Zinc oxide powder is added during ball blast, is attached to microspheric granula table
Face prevents microspheric granula adhesion；
E, microspheric granula obtained in step d drying forming: is dried to water content less than 5% to get finished product, drying side
Formula is hot-air seasoning, and controlling inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
As optional embodiment, the disintegrating apparatus in the step a is Ultramicro-powder machine；
The revolving speed that granulator is pelletized in the step c is 50-70r/min；
Hot-air seasoning is used in the step e, wherein inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
In the present embodiment, traditional Chinese medicine ingredients content is more compared in embodiment 1, reduces the weight accounting of zinc oxide, can be in piglet
After taking, the discharge of Zn-ef ficiency in excrement is reduced, to more environment-friendly.
Embodiment 3:
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc, each material composition are as follows: 50 parts of hoary hair, 10 parts of the coptis, hymsleya amabilis 5
Part, 10 parts of kuh-seng, 95 parts of nano zine oxide, 15 parts of soluble starch, 25 parts of sodium carboxymethyl starch, 15 parts of stearic acid, acrylic acid
No. 24 parts and No. 36 parts of acrylic resin of resin.
A kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof, comprising the following steps: a, Chinese medicine semi-finished product
Preparation: by being crushed in 10 parts of 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, kuh-seng filling disintegrating apparatus to be mixed after 150-200 mesh
Uniformly, Chinese medicine semi-finished product are made；
B, the preparation of drug softwood: 95 parts of 60-80 parts of Chinese medicine semi-finished product, nano zine oxide in step a, solubility is taken to form sediment
15 parts of powder, 25 parts of sodium carboxymethyl starch, 15 parts of stearic acid, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin are uniformly mixed
Pure water stirring is added afterwards, drug softwood is made；
C, it pelletizes: drug softwood obtained in step b being added to the granulator granulation, soft strip-shaped materials grain is made；
D, ball blast: pill-rolling in shot-blasting machine is added in strip-shaped materials grain obtained in step c, and is added during pill-rolling
The uniform microspheric granula of shape is made in Zinc oxide powder, and shot-blasting machine revolving speed adjusts shearing ball blast from low to high, and is in revolving speed
Ball blast work 40-60S is carried out when 350-450r/min, and Zinc oxide powder is added during ball blast, is attached to microspheric granula table
Face prevents microspheric granula adhesion；
E, microspheric granula obtained in step d drying forming: is dried to water content less than 5% to get finished product, drying side
Formula is hot-air seasoning, and controlling inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
As optional embodiment, the disintegrating apparatus in the step a is Ultramicro-powder machine；
The revolving speed that granulator is pelletized in the step c is 50-70r/min；
Hot-air seasoning is used in the step e, wherein inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
The mass fraction accounting of Chinese medicine, zinc oxide and capsulating material is balanced in the present embodiment, can play after piglet takes
While slow release effect, the discharge of Zn-ef ficiency in piglet excrement is reduced, to more environment-friendly.
It is pelletized by using Chinese medicine mixed oxidization zinc powder, as the anti-diarrheal of piglet, reduces the use of zinc oxide
Amount, reduces the production cost of anti-diarrheal；By reducing the dosage of zinc oxide in anti-diarrheal, reduce piglet excrement
The discharge amount of middle zinc reduces the pollution to soil, improves the feature of environmental protection of drug.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (7)
1. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc, which is characterized in that each material composition is as follows: 50 parts of hoary hair, the coptis 10
Part, 5 parts of hymsleya amabilis, 10 parts of kuh-seng, 90-100 parts of nano zine oxide, 10-20 parts of soluble starch, 20-30 parts of sodium carboxymethyl starch,
10-20 parts of stearic acid, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin.
2. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc according to claim 1, it is characterised in that: each material composition is such as
Under: 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, 10 parts of kuh-seng, 95 parts of nano zine oxide, 15 parts of soluble starch, carboxymethyl form sediment
25 parts of powder sodium, 15 parts of stearic acid, No. 24 parts of acrylic resin and No. 36 parts of acrylic resin.
3. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof according to claim 1, it is characterised in that: packet
It includes following steps: the preparation of a, Chinese medicine semi-finished product: 10 parts of 50 parts of hoary hair, 10 parts of the coptis, 5 parts of hymsleya amabilis, kuh-seng filling crushing being set
Standby interior crushing is uniformly mixed, obtained Chinese medicine semi-finished product after 150-200 mesh；
B, the preparation of drug softwood: 90-100 parts of 60-80 parts of Chinese medicine semi-finished product, nano zine oxide in step a, solubility is taken to form sediment
10-20 parts of powder, 20-30 parts of sodium carboxymethyl starch, 10-20 parts of stearic acid, No. 24 parts and acrylic resin No. 36 of acrylic resin
Pure water stirring is added in part after mixing, and drug softwood is made；
C, it pelletizes: drug softwood obtained in step b being added to the granulator granulation, soft strip-shaped materials grain is made；
D, ball blast: pill-rolling in shot-blasting machine is added in strip-shaped materials grain obtained in step c, and oxidation is added during pill-rolling
The uniform microspheric granula of shape is made in zinc powder；
E, microspheric granula obtained in step d drying forming: is dried to water content less than 5% to get finished product.
4. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof according to claim 3, it is characterised in that: institute
Stating the disintegrating apparatus in step a is Ultramicro-powder machine.
5. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof according to claim 3, it is characterised in that: institute
Stating the revolving speed that granulator is pelletized in step c is 50-70r/min.
6. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof according to claim 3, it is characterised in that: institute
It states shot-blasting machine revolving speed in step d and adjusts shearing ball blast from low to high, and carry out ball blast work when revolving speed is 350-450r/min
Make 40-60S.
7. a kind of embedded micro-capsule of Chinese medicine mixed oxidization zinc and preparation method thereof according to claim 3, it is characterised in that: institute
It states using hot-air seasoning in step e, wherein inlet air temperature is 120 DEG C, 45 DEG C of leaving air temp.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108653412A (en) * | 2018-07-16 | 2018-10-16 | 资兴市泰坤农林生态产业有限公司 | A kind of Chinese medicine and the preparation method and application thereof for treating rush down dysentery |
| CN109833305A (en) * | 2017-11-24 | 2019-06-04 | 珠海天成中药有限公司 | Perfume connects the preparation process of antidiarrheal enteric-coated micro-pill |
| CN109833352A (en) * | 2017-11-24 | 2019-06-04 | 珠海天成中药有限公司 | The preparation process of Erhuang antidiarrheal enteric-coated micro-pill |
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2019
- 2019-06-20 CN CN201910535903.2A patent/CN110237127A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109833305A (en) * | 2017-11-24 | 2019-06-04 | 珠海天成中药有限公司 | Perfume connects the preparation process of antidiarrheal enteric-coated micro-pill |
| CN109833352A (en) * | 2017-11-24 | 2019-06-04 | 珠海天成中药有限公司 | The preparation process of Erhuang antidiarrheal enteric-coated micro-pill |
| CN108653412A (en) * | 2018-07-16 | 2018-10-16 | 资兴市泰坤农林生态产业有限公司 | A kind of Chinese medicine and the preparation method and application thereof for treating rush down dysentery |
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