CN110230184A - A kind of polyester fabric preparation method - Google Patents
A kind of polyester fabric preparation method Download PDFInfo
- Publication number
- CN110230184A CN110230184A CN201910546151.XA CN201910546151A CN110230184A CN 110230184 A CN110230184 A CN 110230184A CN 201910546151 A CN201910546151 A CN 201910546151A CN 110230184 A CN110230184 A CN 110230184A
- Authority
- CN
- China
- Prior art keywords
- polyester fabric
- mosquito repellent
- raw material
- repellent liquid
- polyester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 229920000728 polyester Polymers 0.000 title claims abstract description 105
- 239000004744 fabric Substances 0.000 title claims abstract description 94
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 80
- 239000000077 insect repellent Substances 0.000 claims abstract description 77
- 239000002994 raw material Substances 0.000 claims abstract description 41
- 241001251949 Xanthium sibiricum Species 0.000 claims abstract description 25
- 235000007516 Chrysanthemum Nutrition 0.000 claims abstract description 21
- 239000001771 mentha piperita Substances 0.000 claims abstract description 21
- 240000004784 Cymbopogon citratus Species 0.000 claims abstract description 15
- 235000017897 Cymbopogon citratus Nutrition 0.000 claims abstract description 15
- 238000009954 braiding Methods 0.000 claims abstract description 13
- 238000001035 drying Methods 0.000 claims abstract description 9
- 239000000284 extract Substances 0.000 claims abstract 3
- 239000010632 citronella oil Substances 0.000 claims description 40
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 34
- 238000002156 mixing Methods 0.000 claims description 33
- 239000000919 ceramic Substances 0.000 claims description 29
- 239000012528 membrane Substances 0.000 claims description 28
- 238000004061 bleaching Methods 0.000 claims description 26
- 239000007789 gas Substances 0.000 claims description 25
- 238000000034 method Methods 0.000 claims description 24
- 241000723353 Chrysanthemum Species 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 18
- 229920004934 Dacron® Polymers 0.000 claims description 16
- 238000007654 immersion Methods 0.000 claims description 15
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 14
- 238000001771 vacuum deposition Methods 0.000 claims description 13
- 229920001971 elastomer Polymers 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 238000000855 fermentation Methods 0.000 claims description 8
- 230000004151 fermentation Effects 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 8
- JSYPRLVDJYQMAI-ODZAUARKSA-N (z)-but-2-enedioic acid;prop-2-enoic acid Chemical compound OC(=O)C=C.OC(=O)\C=C/C(O)=O JSYPRLVDJYQMAI-ODZAUARKSA-N 0.000 claims description 7
- 230000002708 enhancing effect Effects 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 159000000000 sodium salts Chemical class 0.000 claims description 7
- WUUHFRRPHJEEKV-UHFFFAOYSA-N tripotassium borate Chemical compound [K+].[K+].[K+].[O-]B([O-])[O-] WUUHFRRPHJEEKV-UHFFFAOYSA-N 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- 150000002500 ions Chemical class 0.000 claims description 6
- 239000002759 woven fabric Substances 0.000 claims description 6
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical class NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 5
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 5
- 238000001755 magnetron sputter deposition Methods 0.000 claims description 5
- 238000004544 sputter deposition Methods 0.000 claims description 5
- 238000001256 steam distillation Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 4
- 238000000576 coating method Methods 0.000 claims description 4
- -1 methylene phosphonic acid Chemical compound 0.000 claims description 4
- 241001589086 Bellapiscis medius Species 0.000 claims description 3
- 239000004831 Hot glue Substances 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000004033 diameter control Methods 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 claims description 3
- 230000005021 gait Effects 0.000 claims description 3
- 238000007731 hot pressing Methods 0.000 claims description 3
- 229920002635 polyurethane Polymers 0.000 claims description 3
- 239000004814 polyurethane Substances 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 239000004753 textile Substances 0.000 claims description 3
- 238000005477 sputtering target Methods 0.000 claims description 2
- 230000005540 biological transmission Effects 0.000 claims 1
- 229910052573 porcelain Inorganic materials 0.000 claims 1
- 241000255925 Diptera Species 0.000 abstract description 19
- 230000000694 effects Effects 0.000 abstract description 14
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 abstract description 14
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 abstract description 8
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 abstract description 7
- 229930182470 glycoside Natural products 0.000 abstract description 6
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 abstract description 6
- 239000001941 cymbopogon citratus dc and cymbopogon flexuosus oil Substances 0.000 abstract description 5
- 241000233866 Fungi Species 0.000 abstract description 4
- 241000134874 Geraniales Species 0.000 abstract description 4
- 239000005792 Geraniol Substances 0.000 abstract description 4
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 abstract description 4
- ZHYZQXUYZJNEHD-VQHVLOKHSA-N geranic acid Chemical compound CC(C)=CCC\C(C)=C\C(O)=O ZHYZQXUYZJNEHD-VQHVLOKHSA-N 0.000 abstract description 4
- 229930008392 geranic acid Natural products 0.000 abstract description 4
- 229940113087 geraniol Drugs 0.000 abstract description 4
- 230000002401 inhibitory effect Effects 0.000 abstract description 4
- ZHYZQXUYZJNEHD-UHFFFAOYSA-N trans-geranic acid Natural products CC(C)=CCCC(C)=CC(O)=O ZHYZQXUYZJNEHD-UHFFFAOYSA-N 0.000 abstract description 4
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 abstract description 3
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 abstract description 3
- 239000007844 bleaching agent Substances 0.000 abstract description 3
- WTEVQBCEXWBHNA-YFHOEESVSA-N citral B Natural products CC(C)=CCC\C(C)=C/C=O WTEVQBCEXWBHNA-YFHOEESVSA-N 0.000 abstract description 3
- 238000007689 inspection Methods 0.000 abstract description 3
- 229930007744 linalool Natural products 0.000 abstract description 3
- 244000189548 Chrysanthemum x morifolium Species 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 229920004933 Terylene® Polymers 0.000 description 15
- 239000004615 ingredient Substances 0.000 description 11
- 238000005406 washing Methods 0.000 description 11
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 9
- 238000002474 experimental method Methods 0.000 description 9
- 239000000341 volatile oil Substances 0.000 description 8
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 6
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 6
- 238000000605 extraction Methods 0.000 description 6
- 238000004140 cleaning Methods 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 239000003599 detergent Substances 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 125000004185 ester group Chemical group 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 230000001846 repelling effect Effects 0.000 description 4
- 229920002994 synthetic fiber Polymers 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 241000256059 Culex pipiens Species 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 229920000139 polyethylene terephthalate Polymers 0.000 description 3
- 238000004007 reversed phase HPLC Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 2
- 208000036142 Viral infection Diseases 0.000 description 2
- 239000012675 alcoholic extract Substances 0.000 description 2
- 229930013930 alkaloid Natural products 0.000 description 2
- 150000003797 alkaloid derivatives Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 244000145845 chattering Species 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
- 150000003009 phosphonic acids Chemical class 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- 229910021655 trace metal ion Inorganic materials 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- ZBMRKNMTMPPMMK-UHFFFAOYSA-N 2-amino-4-[hydroxy(methyl)phosphoryl]butanoic acid;azane Chemical compound [NH4+].CP(O)(=O)CCC(N)C([O-])=O ZBMRKNMTMPPMMK-UHFFFAOYSA-N 0.000 description 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- LLLVZDVNHNWSDS-UHFFFAOYSA-N 4-methylidene-3,5-dioxabicyclo[5.2.2]undeca-1(9),7,10-triene-2,6-dione Chemical compound C1(C2=CC=C(C(=O)OC(=C)O1)C=C2)=O LLLVZDVNHNWSDS-UHFFFAOYSA-N 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 208000035473 Communicable disease Diseases 0.000 description 1
- 241000256113 Culicidae Species 0.000 description 1
- 208000001490 Dengue Diseases 0.000 description 1
- 206010012310 Dengue fever Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000010242 baoji Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 208000025729 dengue disease Diseases 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 150000002430 hydrocarbons Chemical group 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 201000005630 leukorrhea Diseases 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000008149 soap solution Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- 206010046901 vaginal discharge Diseases 0.000 description 1
- 230000010148 water-pollination Effects 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/12—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/13—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/227—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of hydrocarbons, or reaction products thereof, e.g. afterhalogenated or sulfochlorinated
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to polyester fabric technical field, specifically a kind of polyester fabric preparation method；Five steps such as dry, impregnate drying, braiding, plated film aperture including selecting and checking that raw material, the raw material qualified to inspection bleach；The present invention passes through using lemongrass oil as constituent main in mosquito repellent liquid, lemongrass oil will be by geranial, neral, geraniol, geranic acid and linalool, flower mosquito can effectively be driven, simultaneously using chrysanthemum, dried peppermint leaf and Siberian cocklebur as the auxiliary element of mosquito repellent liquid, wherein the sub- glycosides in Siberian cocklebur has slight or moderate inhibiting effect to the fungi in air, lemon-grass extract can be prevented mouldy in air, improve the effect duration of lemon-grass extract.
Description
Technical field
The invention belongs to polyester fabric technical field, specifically a kind of polyester fabric preparation method.
Background technique
Terylene is an important species in synthetic fibers, is the product name of China's polyester fiber, is with poly- to benzene two
Formic acid (PTA) or dimethyl terephthalate (DMT) (DMT) and ethylene glycol (MEG) be raw material through esterification or transesterification and polycondensation reaction and
Fiber-forming polymer obtained --- polyethylene terephthalate (PET) through spinning and post-processes manufactured fiber, terylene point
Minor be HO-H2C-H2C-O [- OC-Ph-COOCH2CH2O-] n, because on strand there are a large amount of ester groups thus claim polyester fiber
(PET), the chemical structural formula of long-chain molecule is H (OCH2CCOCO) NOCH2CH2OH, the polyester relative molecular weight for fiber
Generally in 18000-25000 or so, Wool-Like Polyester molecular weight is lower, and industrial terylene molecular weight is higher；In fact, wherein there are also few
The monomer and oligomer of amount exist；The degree of polymerization of these oligomer is lower, and exists with annular form；Poly terephthalic acid second two
Ester can produce ethylene terephthalate 9BHET by direct esterification by terephthalic acid (TPA) (PTA) and ethylene glycol (EG)) retraction
Poly- to form, from the point of view of terylene molecular composition, it is made of short fat hydrocarbon chain, ester group, phenyl ring, end alcoholic extract hydroxyl group, in terylene
Except having no other polar groups there are in addition to two end alcoholic extract hydroxyl groups, thus polyester fiber hydrophily is very poor.About contain in terylene molecule
Hydrolysis, thermal cracking can occur at 200 DEG C or more for 46% ester group, ester group, meet highly basic then soap solution, reduce the degree of polymerization, 100 DEG C with
The detergent washing powder of common dosage has no effect to terylene down；Also contain aliphatic hydrocarbon chain in terylene molecule, it can make to wash
Synthetic fibre molecule has certain flexibility, but due in terylene molecule also cannot in the phenyl ring that rotates, therefore terylene macromolecular is essentially
Rigid molecule, strand are easy to keep line style, and therefore, terylene macromolecular is readily formed crystallization under this condition, therefore terylene
Crystallinity and orientation it is higher.
With the development of society, the function of people's endowing terylene fabric is more and more, for example, polyester fabric has mosquito repellent function
Can, although having existed the polyester fabric of the function in the prior art, the polyester fabric during use there are still
Two problems: first, the duration that mosquito repellent polyester fabric uses is limited, such as application No. is 20141034887 China is special
Benefit, although can achieve the effect that mosquito repellent using Mozzie buster, after multiple washing, the ingredient almost all of expelling parasite grass disappears
It loses；Second, existing mosquito repellent polyester fabric can only drive common mosquito, and (flower mosquito refers to medium and small for toxic flower mosquito
Type black mosquito kind, there is silvery white speckle, there is a center white longitudinal grin on mesoscutum, is stretched backward from front end up to wing base level
Bifurcated before escutcheon, rear instep 1-4 section have base white ring, and minor details are entirely white, and belly back side 2-6 section has base leukorrhea, distributed more widely, north
Up to Shenyang, Tibet Autonomous Region is arrived in northwest to Baoji, southwest, but be on the south 34 ° of north latitude it is common, multiply in residential area and its week more
In the small-sized ponding such as the container and container for plants that enclose and stone cave, mainly to suck blood on daytime, afternoon, activity peak was more obvious than the morning,
Female mosquito is very active and violent blood sucker, at the same time it can also propagate the mosquitos matchmaker such as dengue fever infectious disease), in the prior art not
Occur for the polyester fabric of colored mosquito is driven, therefore, how to accomplish the duration that can extend mosquito repellent polyester fabric mosquito repellent and
It can effectively be driven for toxic flower mosquito, be those skilled in the art's technical issues that need to address.
Summary of the invention
In order to make up for the deficiencies of the prior art, to solve the duration of polyester fabric mosquito repellent in the prior art and drive mosquito kind
The problem of class cannot get both, the invention proposes a kind of polyester fabric preparation methods.
The technical solution adopted by the present invention to solve the technical problems is: a kind of polyester fabric preparation side of the present invention
Method, comprising the following steps:
S1: selecting and checks raw material: selecting 30D/12F semi-gloss polyester filament as organizine, selects 40D/36F polyester filament
It as tram, selects 50D/72F polyester filament as undrawn yarn, and checks that the item of raw material is dry whether uniformly, whether color fastness accords with
Close national textile industry quality index；If meeting, continue following operation；If not meeting, continue to choose raw material, Zhi Daofu
It is combined into only；The correct selection and inspection of raw material help to improve the yield rate that terylene polyester fabric is manufactured, and the present invention selects
The dacron thread of 30D/12F, 40D/36F and 50D/72F is the reason is that facilitate bleaching liquid to bleach it, and fluffy degree after its bleaching
Height is easy to mosquito repellent liquid in conjunction with fabric；
S2: it is dried to examining qualified raw material to carry out bleaching: qualified raw material will be examined to be put into bleaching liquid first and carried out
Bleaching, is dried, and bleaching liquid is made of following components by mass parts: 0.2-0.6 parts of potassium borate, diethylidene three after bleaching
0.5-1.5 parts of seven sodium salt of amine pentamethylene phosphonic acids, 0.5-1.5 parts of acrylic acid maleic acid, 1,5- anhydrous grape sugar alcohol
0.5-1.5 parts, 1.5-7.5 parts of sodium hydroxide, 2-8 parts of hydrogen peroxide and 1000 parts of water；
Potassium borate, accession number: 1332-77-0；Molecular structural formula, as follows:
Five subunit phosphonic acids of diethylenetriamines, seven sodium salt, No. CAS: 68155-78-2, molecular structural formula is as follows:
Acrylic acid maleic acid, abbreviation AA/MA, No. CAS: 26677-99-6；Molecular structural formula, as follows:
1,5- anhydrous grape sugar alcohol, alias: 1,5- acid anhydride-D- D-sorbite, CAS accession number: 154-58-5, molecular structure
Formula is as follows:
By potassium borate, seven sodium salt of diethylenetriamine pentamethylenophosphonic acid, acrylic acid maleic acid and 1,5- without
The synergistic effect such as water glucitol, can act in hydrogen peroxide and free metal, capture trace metal ion, improve bleaching
The stability of hydrogen peroxide in the solution in the process, so as to improve bleaching effect of the invention to a greater degree, and to original
While material damage is small, it is fluffy to facilitate raw material, and mosquito repellent liquid is sufficiently sufficiently combined with raw material；
S3: impregnate drying: the raw material after bleaching is dried, which is put into mosquito repellent liquid, to be impregnated and dries, the temperature summer control of immersion
At 30-35 degrees Celsius, winter controls at 20-25 degrees Celsius system；The mosquito repellent liquid is by 40%~42% citronella oil, 10%~12%
Chrysanthemum, 15%~17% dried peppermint leaf and 35%~37% Siberian cocklebur composition；It is impregnated by the way that raw material to be put into mosquito repellent liquid, can allow original
Containing the ingredient of mosquito repellent liquid in material, so that the polyester fabric that raw material is fabricated to has the function of mosquito repellent, and contain in the mosquito repellent liquid
Lemongrass oil component is particularly helpful to drive colored mosquito；And Siberian cocklebur main component is sub- glycosides, resin, fat oil, alkaloid, dimension life
Element and pigment etc., and sub- glycosides has slight or moderate inhibiting effect to the fungi in air, can prevent citronella oil from sending out in air
It is mould, improve the effect duration of citronella oil；
S4: braiding: after raw material soaking drying after, to tri- kinds of different dacron threads of 30D/12F, 40D/36F and 50D/72F into
Row doubling, reeling, double twisting, be formed and gait naturally after, by the polyester filament of the 50D/72F after gaiting pass through up- coiler wind
On 30D/12F organizine and 40D/36F tram, the speed of up- coiler wrapping wire is that 100-200 turns/min, and 30D/12F, 40D/
The twist of two kinds of dacron thread double twistings on two-for-one twister of 36F is 300~900T/m；50D/72F dacron thread will be finally wound with
Two kinds of dacron threads of 30D/12F and 40D/36F are placed on loom, open the power supply of loom, of the loom in woven fabric
Power control is in 250Kg, and the woven fabric form of loom is staggered form braiding；By by the dacron thread of 50D/72F wound on 30D/
On 12F organizine and 40D/36F tram, the ingredient of the mosquito repellent liquid contained on 30D/12F organizine and 40D/36F tram can be lockked,
Help to extend its repelling effect；
S5: plated film aperture: the polyester fabric after braiding is subjected to vacuum coating processing, the vacuum coating processing is using true
Empty magnetron sputtering membrane process, material used are TiO2, and the adhesive of hot pressing is EVA hot-melt adhesive and polyurethane binding；
After the completion of vacuum coating processing, several micro-holes are offered on vacuum coating, the diameter control of micro-hole is in 0.1-
0.5mm；By the vacuum coating on the polyester fabric of braiding, it can more extend lost, the raising of mosquito repellent liquid on polyester fabric
The repelling effect of its polyester fabric；
Preferably, it is that first mosquito repellent liquid is put into ultrasonic wave fermentation vat to carry out that the raw material, which is put into immersion way in mosquito repellent liquid,
It impregnates, the power control of ultrasonic wave fermentation vat is in 5-8kHZ, and in 80-100min, the number of immersion is controlled for the time control of immersion
At 3-5 times, the temperature of immersion is controlled at 25-35 degrees Celsius；Mosquito repellent liquid and raw material are combined using ultrasonic wave fermentation vat, it can
To improve rate of the mosquito repellent liquid in conjunction with raw material, while it can also improve the rate of polyester fabric production；
Preferably, the production method of the mosquito repellent liquid is to take 10%~12% chrysanthemum, 15%~17% dried peppermint leaf and 35%
~37% Siberian cocklebur is put into centrifuge, centrifuge work 15-20min, and the preferred 300-500W of power of centrifuge, centrifuge work
After standing 10min after the completion, takes out chrysanthemum, dried peppermint leaf and the mixture of Siberian cocklebur and be put into high speed disperser, and in high speed dispersion
It is put into 40%~42% citronella oil in machine, persistently emulsifies 10-15min, shape under conditions of high speed disperser 8000-10000rpm
At uniform emulsion liquid to get arrive mosquito repellent liquid；By cooperating for centrifuge and high speed disperser, can quickly be driven
Mosquito liquid；
Wherein, the high speed disperser includes support base and motor switch；The side of the support base is connected with branch
Dagger, motor is welded at the top of support column, and motor passes through motor switch control and opens；Side of the support column far from motor
Equipped with stirring rod, it is driven between stirring rod and motor by being placed on the belt inside support column；It is put below the stirring rod
It is equipped with mixing drum, connection anchor ear is equipped between mixing drum and support column, and it is detachable to connect anchor ear；The mixing drum inner wall package
There is layer of ceramic film, ceramic membrane is for preventing citronella oil from adhering to；Space between the mixing drum and ceramic membrane passes through external gas
Source is connected with air；Make ceramic membrane global shape waist type, and the position of external gas source by placing rubber slab in the ceramic membrane
It is mutually close with rubber slab；Chrysanthemum, dried peppermint leaf and the mixture of Siberian cocklebur at work, are put into mixing drum first by the high speed disperser
It is interior, then citronella oil is also placed in mixing drum, the rotation of motor switch stirring rod is opened, makes chrysanthemum, dried peppermint leaf, Siberian cocklebur and lemongrass
Oil mixing, during the mixing of chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil, ceramic membrane can prevent citronella oil from adhering to, to reduce
The waste of citronella oil；In the mixing of chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil, by external gas source to mixing drum and ceramic membrane
Between ventilate, increase the frequency shaken in the horizontal direction of ceramic membrane, adhered on ceramic membrane to be further reduced citronella oil,
The rate that chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil mix is improved, and because is placed with rubber slab, and rubber slab in ceramic membrane
Mutually close with the position of external gas source, therefore, in external gas source to when ventilating between ceramic membrane and mixing drum, ceramic membrane can be generated
Shake on vertical direction improves the mixing efficiency between mixture to improve the chattering frequency of mixture in mixing drum.
Preferably, the citronella oil is extracted from lemon-grass, and the preferred Hainan of the lemon-grass produces lemon-grass, the citronella oil
Extracting method uses steam distillation；Extraction of essential oil is carried out to lemon-grass using steam distillation, extraction of essential oil rate is
The dry lemon-grass of 0.09%~1.06%, 50g long 2cm are in aqueous solution of the 1400mL-1500mL containing 8gNaCl, extraction time 3h
When essential oil oil yield highest, up to 1.06%, and citronella oil is mainly by for geranial, neral, geraniol, geranic acid and fragrant camphor tree
Alcohol composition, the quality of five kinds of main components accounts for about the 86%~96% of essential oil gross mass, and five kinds of ingredients are to drive colored mosquito
The main component of son.
Preferably, the vacuum magnetron sputtering coating film need using: vacuum chamber 1~12, each indoor magnetic control of vacuum splashes
Shooting at the target is 1~3, and auxiliary enhancing ion source is 1~2；The auxiliary enhancing ion source is pure N2 or O2, is sputtering gas with Ar
The flow-rate ratio of body, the sputter gas and auxiliary enhancing ionized gas is 1:3；Vacuum degree is 210-300Pa, sputtering in reaction chamber
Power is 1800~2600W, and gas pressure intensity is 1.0~2.0Pa；It, can be on the surface of polyester fabric by this kind of plated film mode
Adhere to one layer of ionic membrane, helps to slow down scattering and disappearing for mosquito repellent liquid ingredient on polyester fabric, when improving the use of polyester fabric mosquito repellent
Between.
Preferably, the polyester fabric is suitable for production tent, curtain and field work clothes etc.；Pass through the above method
The polyester fabric being made can drive common mosquito and drive with virose colored mosquito, so that the polyester fabric system
At finished product, can be used for making the tent of field survivorship, curtain used in the resident of mountain area and the work clothes in field dress
Deng.
Beneficial effects of the present invention are as follows:
1. a kind of polyester fabric preparation method of the present invention, by using citronella oil as composition main in mosquito repellent liquid
Ingredient, citronella oil mainly by geranial, neral, geraniol, geranic acid and linalool, can effectively drive flower mosquito,
Simultaneously using chrysanthemum, dried peppermint leaf and Siberian cocklebur as the auxiliary element of mosquito repellent liquid, wherein the sub- glycosides in Siberian cocklebur has the fungi in air
Slight or moderate inhibiting effect, can prevent citronella oil mouldy in air, improve the effect duration of citronella oil.
2. a kind of polyester fabric preparation method of the present invention, is dried by bleaching, impregnates drying, braiding, plated film are opened
The methods of hole step produces polyester fabric, can slow down the volatilization duration of mosquito repellent liquid in polyester fabric, improve the drive of polyester fabric
Mosquito uses the time, and the mosquito repellent liquid ingredient, to crowd's fanout free region, environment protection health can be widely applied to production and living reality
In.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is the line chart of embodiment 1 in the present invention；
Fig. 2 is the line chart of embodiment 2 in the present invention；
Fig. 3 is the line chart of embodiment 3 in the present invention；
Fig. 4 is the schematic perspective view of high speed dispersion machine of the present invention；
Fig. 5 is the cross-sectional view of mixing drum in high speed dispersion machine of the present invention；
Fig. 6 is the cross-sectional view of A-A in Fig. 5；
In figure: support base 1, motor switch 2, support column 3, motor 4, stirring rod 5, mixing drum 6, connection anchor ear 7, ceramics
Film 8, external gas source 9, rubber slab 10.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As shown in Figures 1 to 6, a kind of polyester fabric preparation method of the present invention, comprising the following steps:
S1: selecting and checks raw material: selecting 30D/12F semi-gloss polyester filament as organizine, selects 40D/36F polyester filament
It as tram, selects 50D/72F polyester filament as undrawn yarn, and checks that the item of raw material is dry whether uniformly, whether color fastness accords with
Close national textile industry quality index；If meeting, continue following operation；If not meeting, continue to choose raw material, Zhi Daofu
It is combined into only；The correct selection and inspection of raw material help to improve the yield rate that terylene polyester fabric is manufactured, and the present invention selects
The dacron thread of 30D/12F, 40D/36F and 50D/72F is the reason is that facilitate bleaching liquid to bleach it, and fluffy degree after its bleaching
Height is easy to mosquito repellent liquid in conjunction with fabric；
S2: it is dried to examining qualified raw material to carry out bleaching: qualified raw material will be examined to be put into bleaching liquid first and carried out
Bleaching, is dried, and bleaching liquid is made of following components by mass parts: 0.2-0.6 parts of potassium borate, diethylidene three after bleaching
0.5-1.5 parts of seven sodium salt of amine pentamethylene phosphonic acids, 0.5-1.5 parts of acrylic acid maleic acid, 1,5- anhydrous grape sugar alcohol
0.5-1.5 parts, 1.5-7.5 parts of sodium hydroxide, 2-8 parts of hydrogen peroxide and 1000 parts of water；
Potassium borate, accession number: 1332-77-0；Molecular structural formula, as follows:
Five subunit phosphonic acids of diethylenetriamines, seven sodium salt, No. CAS: 68155-78-2, molecular structural formula is as follows:
Acrylic acid maleic acid, abbreviation AA/MA, No. CAS: 26677-99-6；Molecular structural formula, as follows:
1,5- anhydrous grape sugar alcohol, alias: 1,5- acid anhydride-D- D-sorbite, CAS accession number: 154-58-5, molecular structure
Formula is as follows:
By potassium borate, seven sodium salt of diethylenetriamine pentamethylenophosphonic acid, acrylic acid maleic acid and 1,5- without
The synergistic effect such as water glucitol, can act in hydrogen peroxide and free metal, capture trace metal ion, improve bleaching
The stability of hydrogen peroxide in the solution in the process, so as to improve bleaching effect of the invention to a greater degree, and to original
While material damage is small, it is fluffy to facilitate raw material, and mosquito repellent liquid is sufficiently sufficiently combined with raw material；
S3: impregnate drying: the raw material after bleaching is dried, which is put into mosquito repellent liquid, to be impregnated and dries, the temperature summer control of immersion
At 30-35 degrees Celsius, winter controls at 20-25 degrees Celsius system；The mosquito repellent liquid is by 40%~42% citronella oil, 10%~12%
Chrysanthemum, 15%~17% dried peppermint leaf and 35%~37% Siberian cocklebur composition；It is impregnated by the way that raw material to be put into mosquito repellent liquid, can allow original
Containing the ingredient of mosquito repellent liquid in material, so that the polyester fabric that raw material is fabricated to has the function of mosquito repellent, and contain in the mosquito repellent liquid
Lemongrass oil component is particularly helpful to drive colored mosquito；And Siberian cocklebur main component is sub- glycosides, resin, fat oil, alkaloid, dimension life
Element and pigment etc., and sub- glycosides has slight or moderate inhibiting effect to the fungi in air, can prevent citronella oil from sending out in air
It is mould, improve the effect duration of citronella oil；
S4: braiding: after raw material soaking drying after, to tri- kinds of different dacron threads of 30D/12F, 40D/36F and 50D/72F into
Row doubling, reeling, double twisting, be formed and gait naturally after, by the polyester filament of the 50D/72F after gaiting pass through up- coiler wind
On 30D/12F organizine and 40D/36F tram, the speed of up- coiler wrapping wire is that 100-200 turns/min, and 30D/12F, 40D/
The twist of two kinds of dacron thread double twistings on two-for-one twister of 36F is 300~900T/m；50D/72F dacron thread will be finally wound with
Two kinds of dacron threads of 30D/12F and 40D/36F are placed on loom, open the power supply of loom, of the loom in woven fabric
Power control is in 250Kg, and the woven fabric form of loom is staggered form braiding；By by the dacron thread of 50D/72F wound on 30D/
On 12F organizine and 40D/36F tram, the ingredient of the mosquito repellent liquid contained on 30D/12F organizine and 40D/36F tram can be lockked,
Help to extend its repelling effect；
S5: plated film aperture: the polyester fabric after braiding is subjected to vacuum coating processing, the vacuum coating processing is using true
Empty magnetron sputtering membrane process, material used are TiO2, and the adhesive of hot pressing is EVA hot-melt adhesive and polyurethane binding；
After the completion of vacuum coating processing, several micro-holes are offered on vacuum coating, the diameter control of micro-hole is in 0.1-
0.5mm；By the vacuum coating on the polyester fabric of braiding, it can more extend lost, the raising of mosquito repellent liquid on polyester fabric
The repelling effect of its polyester fabric；
As a kind of specific embodiment of the invention, it is first by mosquito repellent liquid that the raw material, which is put into immersion way in mosquito repellent liquid,
It is put into ultrasonic wave fermentation vat and is impregnated, in 5-8kHZ, the time of immersion controls in 80- the power control of ultrasonic wave fermentation vat
100min, the number of immersion are controlled at 3-5 times, and the temperature of immersion is controlled at 25-35 degrees Celsius；It will be driven using ultrasonic wave fermentation vat
Mosquito liquid is combined with raw material, and rate of the mosquito repellent liquid in conjunction with raw material can be improved, while can also improve polyester fabric production
Rate.
As a kind of specific embodiment of the invention, the production method of the mosquito repellent liquid be take 10%~12% chrysanthemum,
15%~17% dried peppermint leaf and 35%~37% Siberian cocklebur are put into centrifuge, centrifuge work 15-20min, and the power of centrifuge
It is preferred that 300-500W, after standing 10min after the completion of centrifuge work, takes out chrysanthemum, dried peppermint leaf and the mixture of Siberian cocklebur and is put into height
In fast dispersion machine, and 40%~42% citronella oil is put into high speed disperser, in the item of high speed disperser 8000-10000rpm
10-15min is persistently emulsified under part, forms uniform emulsion liquid to get mosquito repellent liquid is arrived；Pass through centrifuge and high speed disperser
It cooperates, can quickly obtain mosquito repellent liquid；
Wherein, the high speed disperser includes support base 1 and motor switch 2；The side of the support base 1 is connected with
Support column 3, the top of support column 3 are welded with motor 4, and motor 4 is opened by the control of motor switch 2；The support column 3 is far from electricity
The side of machine 4 is equipped with stirring rod 5, is driven between stirring rod 5 and motor 4 by being placed on the belt inside support column 3；It is described to stir
The lower section for mixing bar 5 is placed with mixing drum 6, connection anchor ear 7 is equipped between mixing drum 6 and support column 3, and it is detachable to connect anchor ear 7；
6 inner wall of mixing drum is enclosed with layer of ceramic film 8, and ceramic membrane 8 is for preventing citronella oil from adhering to；The mixing drum 6 and ceramics
Space between film 8 is connected with air by external gas source 9；Keep ceramic membrane 8 whole by placing rubber slab 10 in the ceramic membrane 8
Shape is waist type, and the position of external gas source 9 and rubber slab 10 are mutually close；The high speed disperser at work, first by chrysanthemum,
Dried peppermint leaf and the mixture of Siberian cocklebur are put into mixing drum 6, and then citronella oil is also placed in mixing drum 6, are opened motor switch 2 and are stirred
The rotation of bar 5 is mixed, makes chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil mixing, in the process of chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil mixing
In, ceramic membrane 8 can prevent citronella oil from adhering to, to reduce the waste of citronella oil；In chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil
It when mixing, is ventilated by external gas source 9 between mixing drum 6 and ceramic membrane 8, increases what ceramic membrane 8 was shaken in the horizontal direction
Frequency adheres on ceramic membrane 8 to be further reduced citronella oil, improves the speed that chrysanthemum, dried peppermint leaf, Siberian cocklebur and citronella oil mix
Rate, and because be placed with rubber slab 10 in ceramic membrane 8, and rubber slab 10 and the position of external gas source 9 are mutually close, therefore,
External gas source 9 between ceramic membrane 8 and mixing drum 6 to when ventilating, and ceramic membrane 8 can generate the shake on vertical direction, to improve
The chattering frequency of mixture in mixing drum 6 improves the mixing efficiency between mixture.
As a kind of specific embodiment of the invention, the citronella oil is extracted from lemon-grass, and the lemon-grass is preferred
Hainan produces lemon-grass, and the citronella oil extracting method uses steam distillation；Lemon-grass is carried out using steam distillation
Extraction of essential oil, extraction of essential oil rate are 0.09%~1.06%, and the dry lemon-grass of 50g long 2cm contains 8gNaCl in 1400mL-1500mL
Aqueous solution in, essential oil oil yield highest when extraction time 3h, up to 1.06%, and citronella oil is mainly by for geranial, flores aurantii
Aldehyde, geraniol, geranic acid and linalool composition, the quality of five kinds of main components account for about the 86%~96% of essential oil gross mass,
And five kinds of ingredients are the main component for driving colored mosquito.
As a kind of specific embodiment of the invention, the vacuum magnetron sputtering coating film needs to use vacuum chamber 1~12
A, each indoor magnetic controlled sputtering target of vacuum is 1~3, and auxiliary enhancing ion source is 1~2；The auxiliary enhances ion source
For pure N2 or O2, using Ar as sputter gas, the flow-rate ratio of the sputter gas and auxiliary enhancing ionized gas is 1:3；Reaction chamber
Interior vacuum degree is 210-300Pa, and sputtering power is 1800~2600W, and gas pressure intensity is 1.0~2.0Pa；Pass through this kind of plated film side
Formula can adhere to one layer of ionic membrane on the surface of polyester fabric, help to slow down scattering and disappearing for mosquito repellent liquid ingredient on polyester fabric, mention
High polyester fabric mosquito repellent uses the time.
As a kind of specific embodiment of the invention, the polyester fabric is suitable for production tent, curtain and field
With work clothes etc.；The polyester fabric being made by the above method can drive common mosquito and drive with virose
Flower mosquito, so that finished product made of the polyester fabric, can be used for making the tent of field survivorship, curtain used in the resident of mountain area
And the work clothes etc. in field dress.
To verify specifically used effect of the invention, related application personnel of the present invention have carried out the reality of following 1-3 embodiment
Test operation:
The polyester fabric that table 1 is manufactured by the method for the invention drives in its polyester fabric after different washing times
Mosquito liquid hold-up
Above-described embodiment experimental conditions are as follows: selecting the polyester fabric of the method for the invention production, and labeled as experiment
Group 1, experimental group 2, experimental group 3, experimental group 4, experimental group 5 are to reduce experimental error, then by experimental group 1, experimental group 2, experiment
After group 3, experimental group 4, the polyester fabric in experimental group 5 wash 10,20,30,40,50 times respectively, washed using the measurement of RP-HPLC method
The content of mosquito repellent liquid in synthetic fibre fabric, to obtain the content of mosquito repellent liquid in above table.(note: the content of mosquito repellent liquid is equal in upper table
For approximation, and when polyester fabric cleans in experimental group 1, experimental group 2, experimental group 3, experimental group 4, experimental group 5, needs
Using under identical mode of washing, identical washing facility, identical liquid detergent, identical wash temperature and identical environment
Sunning mode, to reduce the error of experiment).
Experimental result: can be obtained by upper table analysis, experimental group 1, experimental group 2, experimental group 3, experimental group 4, in experimental group 5
Polyester fabric after cleaning 50, inside the mosquito repellent liquid content loss that contains it is less, therefore polyester fabric produced by the present invention has
There is good using effect and longer using the time.
The polyester fabric and lack in the present invention manufactured by S2 step that table 2 is manufactured by the method for the invention
Polyester fabric mosquito repellent liquid content balance in its polyester fabric after different washing times
Above-described embodiment experimental conditions are as follows: adhering to the shadow of content to mosquito repellent liquid on fabric for S2 step in the verifying present invention
It rings, selects three groups of polyester fabrics for not lacking the manufacturing of S2 step, and be labeled as control group 1, control group 2 and control group 3, together
The polyester fabric that tri- groups of the method for the invention of Shi Xuanyong are manufactured, and labelling experiment group 1, experimental group 2 and experimental group 3, so
The polyester fabric in control group 1, control group 2, control group 3, experimental group 1, experimental group 2 and experimental group 3 is washed 10 respectively afterwards,
20, after 30,40 times, using the content of mosquito repellent liquid in RP-HPLC method measurement polyester fabric, to obtain mosquito repellent liquid in above table
Content.(note: the content of mosquito repellent liquid is approximation in upper table, and to control group 1, control group 2, control group 3, experimental group
1, identical mode of washing, identical washing facility, phase need to be used when polyester fabric is cleaned in experimental group 2 and experimental group 3
With liquid detergent, the sunning mode under identical wash temperature and identical environment, to reduce the error of experiment).
Experimental result: can be obtained by upper table analysis, and control group 1,2 control group 3 of control group are after cleaning 40 times, polyester fabric
On mosquito repellent liquid loss it is more than half, and the polyester fabric in experimental group 1, experimental group 2 and experimental group 3 cleaning 40 after, inside contain
Some mosquito repellent liquid content loss are less, therefore S2 step has large effect to the use duration of polyester fabric in the present invention,
Therefore, it can be obtained by above-mentioned experiment, S2 step can be such that mosquito repellent liquid and polyester fabric sufficiently combines in the present invention, improve polyester fabric
The use duration and using effect of mosquito repellent.
The polyester fabric and lack in the present invention manufactured by S5 step that table 3 is manufactured by the method for the invention
Polyester fabric mosquito repellent liquid content balance in its polyester fabric after different washing times
Above-described embodiment experimental conditions are as follows: adhering to the shadow of content to mosquito repellent liquid on fabric for S5 step in the verifying present invention
It rings, selects three groups of polyester fabrics for not lacking the manufacturing of S5 step, and be labeled as control group 1, control group 2 and control group 3, together
The polyester fabric that tri- groups of the method for the invention of Shi Xuanyong are manufactured, and labelling experiment group 1, experimental group 2 and experimental group 3, so
The polyester fabric in control group 1, control group 2, control group 3, experimental group 1, experimental group 2 and experimental group 3 is washed 10 respectively afterwards,
20, after 30,40 times, using the content of mosquito repellent liquid in RP-HPLC method measurement polyester fabric, to obtain mosquito repellent liquid in above table
Content.(note: the content of mosquito repellent liquid is approximation in upper table, and to control group 1, control group 2, control group 3, experimental group
1, identical mode of washing, identical washing facility, phase need to be used when polyester fabric is cleaned in experimental group 2 and experimental group 3
With liquid detergent, the sunning mode under identical wash temperature and identical environment, to reduce the error of experiment).
Experimental result: can be obtained by upper table analysis, and control group 1,2 control group 3 of control group are after cleaning 40 times, polyester fabric
On mosquito repellent liquid excessive loss, and the polyester fabric in experimental group 1, experimental group 2 and experimental group 3 cleaning 40 after, inside contain
Some mosquito repellent liquid content loss are less, therefore S5 step has a very big impact the use duration of polyester fabric in the present invention,
Therefore, it can be obtained by above-mentioned experiment, S5 step can effectively slow down the volatilization of mosquito repellent liquid in the present invention, improve polyester fabric mosquito repellent
Use duration and using effect.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the above embodiments and description only describe originals of the invention
Reason, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes and improvements
It all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appended claims and its equivalent circle
It is fixed.
Claims (6)
1. a kind of polyester fabric preparation method, it is characterised in that: the following steps are included:
S1: selecting and checks raw material: selecting 30D/12F semi-gloss polyester filament as organizine, selects the conduct of 40D/36F polyester filament
Tram selects 50D/72F polyester filament as undrawn yarn, and checks that the item of raw material is dry whether uniformly, and whether color fastness meets state
Family's textile industry quality index；If meeting, continue following operation；If not meeting, continue choose raw material, until meet for
Only；
S2: drying to examining qualified raw material to carry out bleaching: qualified raw material will be examined to be put into bleaching liquid first and bleached,
It is dried after bleaching, and bleaching liquid is made of following components by mass parts: 0.2-0.6 parts of potassium borate, diethylenetriamines five
0.5-1.5 parts of seven sodium salt of methylene phosphonic acid, 0.5-1.5 parts of acrylic acid maleic acid, 1,5- anhydrous grape sugar alcohol 0.5-1.5
Part, 1.5-7.5 parts of sodium hydroxide, 2-8 parts of hydrogen peroxide and 1000 parts of water；
S3: impregnate drying: the raw material after bleaching is dried, which is put into mosquito repellent liquid, to be impregnated and dries, and the temperature summer control of immersion exists
30-35 degrees Celsius, winter controls at 20-25 degrees Celsius；The mosquito repellent liquid is by 40%~42% citronella oil, 10%~12% chrysanthemum
Flower, 15%~17% dried peppermint leaf and 35%~37% Siberian cocklebur composition；
S4: braiding: after raw material soaking drying, tri- kinds of 30D/12F, 40D/36F and 50D/72F different dacron threads are carried out simultaneously
Yarn, reeling, double twisting, be formed and gait naturally after, by the polyester filament of the 50D/72F after gaiting by up- coiler wound on
On 30D/12F organizine and 40D/36F tram, the speed of up- coiler wrapping wire is that 100-200 turns/min, and 30D/12F, 40D/36F
The twist of two kinds of dacron thread double twistings on two-for-one twister is 300~900T/m；The 30D/ of 50D/72F dacron thread will be finally wound with
Two kinds of dacron threads of 12F and 40D/36F are placed on loom, open the power supply of loom, tension control of the loom in woven fabric
System is in 250Kg, and the woven fabric form of loom is staggered form braiding；
S5: plated film aperture: the polyester fabric after braiding is subjected to vacuum coating processing, the vacuum coating processing uses Vacuum Magnetic
Sputter coating process is controlled, material used is TiO2, and the adhesive of hot pressing is EVA hot-melt adhesive and polyurethane binding；To true
After the completion of empty coating film treatment, several micro-holes are offered on vacuum coating, the diameter control of micro-hole is in 0.1-0.5mm.
2. a kind of polyester fabric preparation method according to claim 1, it is characterised in that: the raw material is put into mosquito repellent liquid
Immersion way is that first mosquito repellent liquid is put into ultrasonic wave fermentation vat to impregnate, and the power control of ultrasonic wave fermentation vat is in 5-
8kHZ, in 80-100min, the number of immersion is controlled at 3-5 times for the time control of immersion, and the temperature control of immersion is taken the photograph in 25-35
Family name's degree.
3. a kind of polyester fabric preparation method according to claim 2, it is characterised in that: the production method of the mosquito repellent liquid
To take 10%~12% chrysanthemum, 15%~17% dried peppermint leaf and 35%~37% Siberian cocklebur to be put into centrifuge, centrifuge work 15-
20min, and the power preferred 300-500W of centrifuge take out chrysanthemum, dried peppermint leaf after standing 10min after the completion of centrifuge work
It is put into high speed disperser with the mixture of Siberian cocklebur, and is put into 40%~42% citronella oil in high speed disperser, in high speed point
10-15min is persistently emulsified under conditions of scattered machine 8000-10000rpm, forms uniform emulsion liquid to get mosquito repellent liquid is arrived；
Wherein, the high speed disperser includes support base (1) and motor switch (2)；The side of the support base (1) is affixed
Have support column (3), be welded at the top of support column (3) motor (4), motor (4) is opened by motor switch (2) control；It is described
Support column (3) is equipped with stirring rod (5) far from the side of motor (4), by being placed on support between stirring rod (5) and motor (4)
The internal belt transmission of column (3)；Be placed with mixing drum (6) below the stirring rod (5), mixing drum (6) and support column (3) it
Between be equipped with connection anchor ear (7), and it is detachable to connect anchor ear (7)；Mixing drum (6) inner wall is enclosed with layer of ceramic film (8), pottery
Porcelain film (8) is for preventing citronella oil from adhering to；Space between the mixing drum (6) and ceramic membrane (8) is logical by external gas source (9)
There is air；Make ceramic membrane (8) global shape waist type, and external gas source by placing rubber slab (10) in the ceramic membrane (8)
(9) position and rubber slab (10) are mutually close.
4. a kind of polyester fabric preparation method according to claim 3, it is characterised in that: the citronella oil is from lemon-grass
It extracts, and the preferred Hainan of the lemon-grass produces lemon-grass, the citronella oil extracting method is based on steam distillation.
5. a kind of polyester fabric preparation method according to claim 1, it is characterised in that: the vacuum magnetron sputtering coating film
Need using: vacuum chamber 1~12, each indoor magnetic controlled sputtering target of vacuum be 1~3, auxiliary enhancing ion source be 1~2；
The auxiliary enhancing ion source is pure N2 or O2, and using Ar as sputter gas, the sputter gas and auxiliary enhance ionized gas
Flow-rate ratio is 1:3；In reaction chamber vacuum degree be 210-300Pa, sputtering power be 1800~2600W, gas pressure intensity be 1.0~
2.0Pa。
6. a kind of polyester fabric preparation method according to claim 1, it is characterised in that: the polyester fabric is suitable for system
Make tent, curtain and field work clothes etc..
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Application publication date: 20190913 |