CN107599531A - A kind of silk and preparation method - Google Patents
A kind of silk and preparation method Download PDFInfo
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- CN107599531A CN107599531A CN201710748793.9A CN201710748793A CN107599531A CN 107599531 A CN107599531 A CN 107599531A CN 201710748793 A CN201710748793 A CN 201710748793A CN 107599531 A CN107599531 A CN 107599531A
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Abstract
The invention discloses outer layer silk is provided with the top of a kind of silk, including the real silk, bottom is provided with basic unit's silk, intermediate layer silk is provided with inside real silk, and be provided with sheared edge in edge；The outside of the outer layer silk is provided with rendering layer, and bottom is provided with antistatic silk fabric；Chemical fibre layer is provided with the top of the intermediate layer silk, the outer surface of the chemical fibre layer is provided with antistatic backing.The preparation process of the inventive method includes：Dyestuff, winder, warping plus print opening, dry；Energy of the invention is dust-proof, the electrostatic being enriched with clothes can be eliminated in time, so as to keep the cleaning of clothes and ensure that the health of human body, with the function such as antistatic, warming, simultaneously by waterproof layer, it is easy to waterproof, is easy to by rendering layer antifouling, pass through nanometer silver antimicrobial particle, it is easy to that there is certain anti-microbial property, and by sheared edge, facilitates the shearing of silk, it is scientific and efficient and preparation method is simple and convenient.
Description
Technical field
The present invention relates to silk technical field, specially a kind of silk and preparation method.
Background technology
Silk, a kind of textile, it is made into silk or synthetic fibers, staple fibre, long filament;Knitted with silk or artificial silk are pure
Or the general name for the fabric being interwoven.In ancient times, silk be exactly silk (based on mulberry silk, also including a small amount of tussah silk and
Cassava silkwormsilk) woven textile.Modern times, it is fine that every warp employs artificial or thread due to the extension of textile raw material
Woven textile is tieed up, the silk of broad sense can be referred to as.And the woven silk of pure mulberry silk institute, " silk is especially referred to as again
Silk fabric ".Silk also refers in particular to the woven textile of mulberry silk institute.Silk is the special product of China.Han nationality working people is to invent and advise greatly
Mould production silk fabrics is even more to open large-scale commerce and trade exchange between east and west for the first time in world history, is called the Silk Road in history.
From Han dynasty, Chinese silk constantly transports foreign countries in force, turns into world-famous product.Gone at that time from China to west
Main road, once it was referred to as in " Silk Road " by European, China is also referred to as " silk state ", but existing silk can not be dust-proof, no
The electrostatic being enriched with clothes can be eliminated in time, and inconvenient waterproof, inconvenience is antifouling, without certain anti-microbial property, and inconvenience
The shearing of silk, and preparation method is complicated, producing efficiency is low.
The content of the invention
The present invention provides a kind of silk and preparation method, can be dust-proof, the electrostatic being enriched with clothes can be eliminated in time, so as to protect
Hold the cleaning of clothes and ensure that the health of human body, there is the function such as antistatic, warming, while by waterproof layer, be easy to waterproof,
It is easy to by rendering layer antifouling, by nanometer silver antimicrobial particle, is easy to that there is certain anti-microbial property, and by sheared edge,
Facilitate the shearing of silk, and preparation method is simple and convenient, it is scientific and efficient, can effectively solve the problems, such as in above-mentioned background technology.
To achieve the above object, the invention provides a kind of silk, including real silk top to be provided with outer layer silk,
Bottom is provided with basic unit's silk, intermediate layer silk is provided with inside real silk, and be provided with sheared edge in edge；The outer layer silk
The outside of silk fabric is provided with rendering layer, and bottom is provided with antistatic silk fabric；Chemical fibre layer, the chemistry are provided with the top of the intermediate layer silk
The outer surface of fibrous layer is provided with antistatic backing, and the intermediate layer silk is internally provided with nanometer silver antimicrobial particle, described anti-
Conductive fiber line is provided with electrostatic layer, the conductive fiber line is interweaved by warp and parallel to be formed；Have at the top of the rendering layer
Waterproof layer, the bottom of rendering layer is provided with layers of chrome.
Further, connected between the chemical fibre layer and antistatic backing by binding agent.
Further, the preparation process of the binding agent is specially under agitation, to take 50-73 percentage by weights
Water, and polyvinyl alcohol, mixing, are warming up to 88-95 degree so that polyvinyl alcohol is completely dissolved, and 1 hour is incubated under 70-80 degree, is adjusted
Section pH is 8-9, obtains solution A；Then the compound emulsifying agent of 30-40 percentage by weights is taken, under stirring condition, by the Composite Milk
Agent and remaining water are added in solution A, then are slowly added into the vinylacetate and 40-50 weight of 40-50 percentage by weights
The composite initiator of percentage, 88-95 degree is warming up to, is incubated 0.3-0.5 hours；It is cooled to 60-70 degree；It is slowly added into again afterwards
Remaining vinylacetate and remaining composite initiator；88-95 degree is warming up to, is incubated 0.2-0.4 hours；Add 30-40%
The compound emulsifying agent of percentage by weight, and polyvinyl acetate, 0.2-0.4 hours are incubated under 88-95 degree, are subsequently cooled to
40-50 degree；Again under agitation, addition sodium acid carbonate, dibutyl phthalate, diethylene glycol dibenzoate, octanol are different
Propyl alcohol, it is well mixed, obtains solution B；Remaining compound emulsifying agent, allyl methacrylate, double methyl-props are added into solution B
Olefin(e) acid glycol ester, toluene di-isocyanate(TDI), NMA, waxy corn starch, sodium hypochlorite, it is well mixed, 40-
50 degree of insulation 0.1-0.3 hours, room temperature is cooled to, produces the binding agent.
According to above-mentioned technical proposal, the mosquito proof auxiliary agent layer is internally provided with mosquito proof auxiliary agent, and mosquito proof auxiliary agent is logical
Cross made from after pest repellant and bonding agent uniform stirring.
According to above-mentioned technical proposal, the antistatic backing is as made from antistatic material, and wherein antistatic material is by such as
The raw material composition of lower parts by weight：Epoxy resin 50-100 parts, polybutylene terephthalate (PBT) 1-50 parts, potassium titanate 0.7-10
Part, -13 parts of silica 1, magnesium hydroxide 1-40 parts, anhydrous calcium chloride 1-12 parts, ferrous sulfate 0.1-3 parts, are added to stirring
Uniform stirring is made in device.
According to above-mentioned technical proposal, the rendering layer is made up of the raw material of following parts by weight：Glutinous rice starch 25-40 parts, carboxylic
Sodium carboxymethylcellulose pyce 15-25 parts, cyclodextrin 2-9 parts, polyvinyl acetate 0.02-1.0 parts, nanometer titanium dioxide 0.2-1.5 parts, plant
Fibres 10-20 parts, surfactant 0.04-0.2 parts, preservative 0.02-0.15 parts, antioxidant 0.01-0.1 parts.
Present invention also offers a kind of silk preparation method, including dyestuff, winder, batch warping plus print to be open, dry,
Comprise the following steps：
1）Dyestuff：Coloring agent is added, coloring agent and water, uniform stirring are added in staining jar, heats up and maintains the temperature at 40-50
DEG C, add carbonic acid and adjust the PH of dye liquor between 4-6；Immersion, 1.5-3.5 hours in staining jar are immersed in by textile raw material,
Then low temperature rapid dyeing auxiliary agent immersion 10-50min is added, is then heated up with 2-3 DEG C/min speed, is warming up to 80-90 DEG C
And keep 45-60min；Drying, the textile raw material after immersion is dried in the environment of 80-90 DEG C；Rinsing, after taking out drying
Textile raw material, which immerses, rinses 35-55 minutes in clear water, and adds purificant；Dry, take out the textile raw material after rinsing and dry in the air naturally
It is dry.
2）Winder：Using automatic winder winder, technique is：Short slub：DS1.9-2.9cm, LS1.2-1.8cm；It is long thick
Section：DL1.2-1.5cm, LL20-50cm；Details：D16%-30%, L16-60cm；Cotton knot：N3.8-5；Relative humidity in workshop：
68%-78%, temperature：20-28℃；
3）Warping：Warping is carried out to conductive fiber line, warp and weft, tension scheme is the floor of 4th areas, three Ceng Huo, 3rd areas three, single
Warp tension is 35cN-55cN, and side warp thread line tension increases 20%-25%, speed：200-350 ms/min；Rolling density：0.5-
0.7g/cm3；
4）Print is added to be open：Add print outer layer silk, intermediate layer silk in silk broadcloth layer surface, basic unit's silk, layers of chrome, waterproof layer, receive
The silver-colored antibacterial granule of rice, antistatic silk fabric, rendering layer, chemical fibre layer, antistatic backing；Then opened at the marginal position of silk broadcloth layer
If sheared edge；Then baked；
5）Dry：Silk after baking is produced after room temperature is dried.
According to above-mentioned technical proposal, it is characterised in that：The step 5）The humidity that middle room temperature is dried to be maintained at 10% with
Under.
According to above-mentioned technical proposal, the step 4）Stoving temperature be 40-60 DEG C.
Compared with prior art, beneficial effects of the present invention：Can be dust-proof, the electrostatic being enriched with clothes can be eliminated in time, from
And keep the cleaning of clothes and ensure that the health of human body, there is the function such as antistatic, warming, while by waterproof layer, be easy to
Waterproof, is easy to antifouling by rendering layer, by nanometer silver antimicrobial particle, is easy to have certain anti-microbial property, and by cutting
Otch, facilitate the shearing of silk, and preparation method is simple and convenient, it is scientific and efficient.
Brief description of the drawings
Accompanying drawing is used for providing a further understanding of the present invention, and a part for constitution instruction, the reality with the present invention
Apply example to be used to explain the present invention together, be not construed as limiting the invention.
In the accompanying drawings：
Fig. 1 is the overall structure diagram of the present invention；
Fig. 2 is the structural representation of the antistatic backing of the present invention；
Fig. 3 is the Making programme figure of the present invention；
Label in figure：1st, silk broadcloth layer；2nd, outer layer silk；3rd, intermediate layer silk；4th, basic unit's silk；5th, layers of chrome；6th, waterproof layer；7、
Nanometer silver antimicrobial particle；8th, antistatic silk fabric；9th, rendering layer；10th, conductive fiber line；11st, parallel；12nd, warp；13rd, chemical fibre
Layer；14th, antistatic backing；15th, sheared edge.
Embodiment
The preferred embodiments of the present invention are illustrated below in conjunction with accompanying drawing, it will be appreciated that described herein preferred real
Apply example to be merely to illustrate and explain the present invention, be not intended to limit the present invention.
Embodiment 1
As Figure 1-3, the invention provides a kind of silk, the real silk top to be provided with outer layer silk 2, and bottom is provided with base
Layer silk 4, is provided with intermediate layer silk 3, and be provided with sheared edge 15 in edge inside real silk 1；The outer layer silk
Outside is provided with rendering layer 9, and bottom is provided with antistatic silk fabric 8；The top of intermediate layer silk 3 is provided with chemical fibre layer 13, describedization
The outer surface for learning fibrous layer 13 is provided with antistatic backing 14, and the intermediate layer silk 3 is internally provided with nanometer silver antimicrobial particle
7, the antistatic backing 14 is interior to be provided with conductive fiber line 10, and the conductive fiber line 10 is interweaved by warp 12 and parallel 11 to be formed；
Waterproof layer 6 is arranged at the top of the rendering layer 9, and the bottom of rendering layer 9 is provided with layers of chrome 5.
According to above-mentioned technical proposal, connected between the chemical fibre layer 13 and antistatic backing 14 by binding agent.
According to above-mentioned technical proposal, the preparation process of the binding agent is specially under agitation, to take 50 weight percents
The water of ratio, and polyvinyl alcohol, mixing, are warming up to 88 degree so that polyvinyl alcohol is completely dissolved, insulation 1 hour under 70 degree, regulation
PH is 8, obtains solution A；Then take the compound emulsifying agent of 30 percentage by weights, under stirring condition, by the compound emulsifying agent and
Remaining water is added in solution A, then be slowly added into 40 percentage by weights vinylacetate and 40 percentage by weights it is compound
Initiator, 88 degree are warming up to, are incubated 0.3 hour；It is cooled to 60 degree；It is slowly added into remaining vinylacetate and residue again afterwards
Composite initiator；88 degree are warming up to, is incubated 0.2 hour；Add the compound emulsifying agent of 30 percentage by weights, and poly-vinegar acid second
Alkene ester, 88 degree are incubated 0.2 hour down, are subsequently cooled to 40 degree；Again under agitation, sodium acid carbonate, phthalic acid are added
Dibutyl ester, diethylene glycol dibenzoate, octanol, isopropanol, it is well mixed, obtains solution B；Added into solution B remaining compound
Emulsifying agent, allyl methacrylate, ethyleneglycol dimethyacrylate, toluene di-isocyanate(TDI), NMA, wax
Matter cornstarch, sodium hypochlorite, it is well mixed, 40 degree are incubated 0.1 hour, are cooled to room temperature, produce the binding agent.
According to above-mentioned technical proposal, the mosquito proof auxiliary agent layer 10 is internally provided with mosquito proof auxiliary agent, and mosquito proof auxiliary agent is
By obtained after pest repellant and bonding agent uniform stirring.
According to above-mentioned technical proposal, the antistatic backing 8 is as made from antistatic material, and wherein antistatic material is by such as
The raw material composition of lower parts by weight：50 parts of epoxy resin, 1 part of polybutylene terephthalate (PBT), 0.7 part of potassium titanate, titanium dioxide
1 part of silicon, 1 part of magnesium hydroxide, 1 part of anhydrous calcium chloride, 0.1 part of ferrous sulfate, are added to uniform stirring in agitator and are made.
According to above-mentioned technical proposal, the rendering layer 9 is made up of the raw material of following parts by weight：25 parts of glutinous rice starch, carboxylic first
15 parts of base sodium cellulosate, 2 parts of cyclodextrin, 0.02 part of polyvinyl acetate, 0.2 part of nanometer titanium dioxide, 10 parts of string, surface
0.04 part of activating agent, 0.02 part of preservative, 0.01 part of antioxidant.
A kind of silk preparation method, including dyestuff, winder, batch warping plus print opening, drying, comprise the following steps：
1）Dyestuff：Coloring agent is added, coloring agent and water, uniform stirring are added in staining jar, heats up and maintains the temperature at 40 DEG C,
Carbonic acid is added by the PH regulations of dye liquor to 4；Immersion, textile raw material is immersed in staining jar 1.5 hours, it is fast then to add low temperature
Fast dyeing assistant soaks 10min, is then heated up with 2 DEG C/min speed, is warming up to 80-90 DEG C and keeps 45min；Drying, will
Textile raw material after immersion is dried in the environment of 80 DEG C；Rinsing, take out in the immersion clear water of the textile raw material after drying and rinse 35
Minute, and add purificant；Dry, take out the textile raw material naturally dry after rinsing.
2）Winder：Using automatic winder winder, technique is：Short slub：DS1.9cm, LS1.2cm；Long slubbing：
DL1.2cm, LL20cm；Details：D16%, L16cm；Cotton knot：N3.8；Relative humidity in workshop：68%th, temperature：20℃；
3）Warping：Warping is carried out to conductive fiber line, warp and weft, tension scheme is the floor of 4th areas, three Ceng Huo, 3rd areas three, single
Warp tension is 35cN, and side warp thread line tension increases by 20%, speed：200 ms/min；Rolling density：0.5g/cm3；
4）Print is added to be open：Add print outer layer silk, intermediate layer silk in silk broadcloth layer surface, basic unit's silk, layers of chrome, waterproof layer, receive
The silver-colored antibacterial granule of rice, antistatic silk fabric, rendering layer, chemical fibre layer, antistatic backing；Then opened at the marginal position of silk broadcloth layer
If sheared edge；Then baked；
5）Dry：Silk after baking is produced after room temperature is dried.
According to above-mentioned technical proposal, the step 5）The humidity that middle room temperature is dried will be maintained at less than 10%.
According to above-mentioned technical proposal, the step 4）Stoving temperature be 40 DEG C.
Embodiment 2
As Figure 1-3, the invention provides a kind of silk, the real silk top to be provided with outer layer silk 2, and bottom is provided with base
Layer silk 4, is provided with intermediate layer silk 3, and be provided with sheared edge 15 in edge inside real silk 1；The outer layer silk
Outside is provided with rendering layer 9, and bottom is provided with antistatic silk fabric 8；The top of intermediate layer silk 3 is provided with chemical fibre layer 13, describedization
The outer surface for learning fibrous layer 13 is provided with antistatic backing 14, and the intermediate layer silk 3 is internally provided with nanometer silver antimicrobial particle
7, the antistatic backing 14 is interior to be provided with conductive fiber line 10, and the conductive fiber line 10 is interweaved by warp 12 and parallel 11 to be formed；
Waterproof layer 6 is arranged at the top of the rendering layer 9, and the bottom of rendering layer 9 is provided with layers of chrome 5.
According to above-mentioned technical proposal, connected between the chemical fibre layer 13 and antistatic backing 14 by binding agent.
Further, the preparation process of the binding agent is specially under agitation, to take the water of 60 percentage by weights, with
And polyvinyl alcohol, mixing, it is warming up to 88-95 degree so that polyvinyl alcohol is completely dissolved, insulation 1 hour under 75 degree, and regulation pH is
8.5, obtain solution A；Then the compound emulsifying agent of 35 percentage by weights is taken, under stirring condition, by the compound emulsifying agent and surplus
Remaining water is added in solution A, then is slowly added into the vinylacetate of 45 percentage by weights and the compound of 45 percentage by weights is drawn
Agent is sent out, is warming up to 90 degree, is incubated 0.4 hour；It is cooled to 65 degree；It is slowly added into remaining vinylacetate and remaining again afterwards
Composite initiator；90 degree are warming up to, is incubated 0.3 hour；Add the compound emulsifying agent of 35% percentage by weight, and poly-vinegar acid second
Alkene ester, 90 degree are incubated 0.3 hour down, are subsequently cooled to 45 degree；Again under agitation, sodium acid carbonate, phthalic acid are added
Dibutyl ester, diethylene glycol dibenzoate, octanol, isopropanol, it is well mixed, obtains solution B；Added into solution B remaining compound
Emulsifying agent, allyl methacrylate, ethyleneglycol dimethyacrylate, toluene di-isocyanate(TDI), NMA, wax
Matter cornstarch, sodium hypochlorite, it is well mixed, 45 degree are incubated 0.2 hour, are cooled to room temperature, produce the binding agent.
According to above-mentioned technical proposal, the mosquito proof auxiliary agent layer is internally provided with mosquito proof auxiliary agent, and mosquito proof auxiliary agent is logical
Cross made from after pest repellant and bonding agent uniform stirring.
According to above-mentioned technical proposal, the antistatic backing is as made from antistatic material, and wherein antistatic material is by such as
Under parts by weight raw material composition：75 parts of epoxy resin, 25 parts of polybutylene terephthalate (PBT), 6 parts of potassium titanate, silica
6 parts, 23 parts of magnesium hydroxide, 7 parts of anhydrous calcium chloride, 1.5 parts of ferrous sulfate, be added to uniform stirring in agitator and be made.
According to above-mentioned technical proposal, the rendering layer is made up of the raw material of following parts by weight：33 parts of glutinous rice starch, carboxymethyl
20 parts of sodium cellulosate, 6 parts of cyclodextrin, 0.06 part of polyvinyl acetate, 0.8 part of nanometer titanium dioxide, 15 parts of string, surface are lived
0.1 part of agent of property, 0.1 part of preservative, 0.06 part of antioxidant.
Present invention also offers a kind of silk preparation method, including dyestuff, winder, batch warping plus print to be open, dry,
Comprise the following steps：
1）Dyestuff：Coloring agent is added, coloring agent and water, uniform stirring are added in staining jar, heats up and maintains the temperature at 45 DEG C,
Carbonic acid is added by the PH regulations of dye liquor to 5；Immersion, textile raw material is immersed in staining jar 2 hours, it is quick then to add low temperature
Dyeing assistant soaks 30min, is then heated up with 2.5 DEG C/min speed, is warming up to 85 DEG C and keeps 50min；Drying, will soak
Textile raw material afterwards is dried in the environment of 85 DEG C；Rinsing, take out in the immersion clear water of the textile raw material after drying and rinse 40 minutes,
And add purificant；Dry, take out the textile raw material naturally dry after rinsing.
2）Winder：Using automatic winder winder, technique is：Short slub：DS2cm, LS1.5cm；Long slubbing：DL1.3cm,
LL30cm；Details：D20%, L40cm；Cotton knot：N4.3；Relative humidity in workshop：73%th, temperature：25℃；
3）Warping：Warping is carried out to conductive fiber line, warp and weft, tension scheme is the floor of 4th areas, three Ceng Huo, 3rd areas three, single
Warp tension is 45cN, and side warp thread line tension increases by 23%, speed：300 ms/min；Rolling density：0.6g/cm3；
4）Print is added to be open：Add print outer layer silk, intermediate layer silk in silk broadcloth layer surface, basic unit's silk, layers of chrome, waterproof layer, receive
The silver-colored antibacterial granule of rice, antistatic silk fabric, rendering layer, chemical fibre layer, antistatic backing；Then opened at the marginal position of silk broadcloth layer
If sheared edge；Then baked；
5）Dry：Silk after baking is produced after room temperature is dried.
According to above-mentioned technical proposal, it is characterised in that：The step 5）The humidity that middle room temperature is dried to be maintained at 10% with
Under.
According to above-mentioned technical proposal, the step 4）Stoving temperature be 50 DEG C.
Embodiment 3
As Figure 1-3, the invention provides a kind of silk, the real silk top to be provided with outer layer silk 2, and bottom is provided with base
Layer silk 4, is provided with intermediate layer silk 3, and be provided with sheared edge 15 in edge inside real silk 1；The outer layer silk
Outside is provided with rendering layer 9, and bottom is provided with antistatic silk fabric 8；The top of intermediate layer silk 3 is provided with chemical fibre layer 13, describedization
The outer surface for learning fibrous layer 13 is provided with antistatic backing 14, and the intermediate layer silk 3 is internally provided with nanometer silver antimicrobial particle
7, the antistatic backing 14 is interior to be provided with conductive fiber line 10, and the conductive fiber line 10 is interweaved by warp 12 and parallel 11 to be formed；
Waterproof layer 6 is arranged at the top of the rendering layer 9, and the bottom of rendering layer 9 is provided with layers of chrome 5.
According to above-mentioned technical proposal, connected between the chemical fibre layer 13 and antistatic backing 14 by binding agent.
Further, the preparation process of the binding agent is specially under agitation, to take the water of 73 percentage by weights, with
And polyvinyl alcohol, mixing, it is warming up to 95 degree so that polyvinyl alcohol is completely dissolved, and insulation 1 hour under 80 degree, regulation PH is 9, is obtained
To solution A；Then the compound emulsifying agent of 40 percentage by weights is taken, under stirring condition, by the compound emulsifying agent and remaining water
It is added in solution A, then is slowly added into the vinylacetate of 50 percentage by weights and the composite initiator of 50 percentage by weights, rises
Temperature is incubated 0.5 hour to 95 degree；It is cooled to 70 degree；It is slowly added into remaining vinylacetate again afterwards and remaining compound draws
Send out agent；95 degree are warming up to, is incubated 0.4 hour；Add the compound emulsifying agent of 40 percentage by weights, and polyvinyl acetate, 95
The lower insulation of degree 0.4 hour, is subsequently cooled to 50 degree；Again under agitation, addition sodium acid carbonate, dibutyl phthalate,
Diethylene glycol dibenzoate, octanol, isopropanol, it is well mixed, obtains solution B；Remaining compound emulsifying agent is added into solution B,
Allyl methacrylate, ethyleneglycol dimethyacrylate, toluene di-isocyanate(TDI), NMA, waxy corn
Starch, sodium hypochlorite, it is well mixed, 50 degree are incubated 0.3 hour, are cooled to room temperature, produce the binding agent.
According to above-mentioned technical proposal, the mosquito proof auxiliary agent layer is internally provided with mosquito proof auxiliary agent, and mosquito proof auxiliary agent is logical
Cross made from after pest repellant and bonding agent uniform stirring.
According to above-mentioned technical proposal, the antistatic backing is as made from antistatic material, and wherein antistatic material is by such as
The raw material composition of lower parts by weight：100 parts of epoxy resin, 50 parts of polybutylene terephthalate (PBT), 10 parts of potassium titanate, titanium dioxide
13 parts of silicon, 40 parts of magnesium hydroxide, 12 parts of anhydrous calcium chloride, 3 parts of ferrous sulfate, are added to uniform stirring in agitator and are made.
According to above-mentioned technical proposal, the rendering layer is made up of the raw material of following parts by weight：40 parts of glutinous rice starch, carboxylic first
25 parts of base sodium cellulosate, 9 parts of cyclodextrin, 1.0 parts of polyvinyl acetate, 1.5 parts of nanometer titanium dioxide, 20 parts of string, surface
0.2 part of activating agent, 0.15 part of preservative, 0.1 part of antioxidant.
Present invention also offers a kind of silk preparation method, including dyestuff, winder, batch warping plus print to be open, dry,
Comprise the following steps：
1）Dyestuff：Coloring agent is added, coloring agent and water, uniform stirring are added in staining jar, heats up and maintains the temperature at 50 DEG C,
Carbonic acid is added by the PH regulations of dye liquor to 6；Immersion, textile raw material is immersed in staining jar 3.5 hours, it is fast then to add low temperature
Fast dyeing assistant soaks 50min, is then heated up with 3 DEG C/min speed, is warming up to 90 DEG C and keeps 60min；Drying, will soak
Textile raw material afterwards is dried in the environment of 90 DEG C；Rinsing, take out in the immersion clear water of the textile raw material after drying and rinse 55 minutes,
And add purificant；Dry, take out the textile raw material naturally dry after rinsing.
2）Winder：Using automatic winder winder, technique is：Short slub：DS2.9cm, LS1.8cm；Long slubbing：DL1.5,
LL50cm；Details：D30%, L60cm；Cotton knot：N5；Relative humidity in workshop：78%th, temperature： 28℃；
3）Warping：Warping is carried out to conductive fiber line, warp and weft, tension scheme is the floor of 4th areas, three Ceng Huo, 3rd areas three, single
Warp tension is 55cN, and side warp thread line tension increases by 25%, speed：350 ms/min；Rolling density： 0.7g/cm3；
4）Print is added to be open：Add print outer layer silk, intermediate layer silk in silk broadcloth layer surface, basic unit's silk, layers of chrome, waterproof layer, receive
The silver-colored antibacterial granule of rice, antistatic silk fabric, rendering layer, chemical fibre layer, antistatic backing；Then opened at the marginal position of silk broadcloth layer
If sheared edge；Then baked；
5）Dry：Silk after baking is produced after room temperature is dried.
According to above-mentioned technical proposal, it is characterised in that：The step 5）The humidity that middle room temperature is dried to be maintained at 10% with
Under.
According to above-mentioned technical proposal, the step 4）Stoving temperature be 60 DEG C.
Energy of the invention is dust-proof, the electrostatic being enriched with clothes can be eliminated in time, so as to keep the cleaning of clothes and ensure that people
The health of body, has a function such as antistatic, warming, while by waterproof layer, is easy to waterproof, is easy to by rendering layer antifouling, leads to
Nanometer silver antimicrobial particle is crossed, is easy to that there is certain anti-microbial property, and by sheared edge, facilitates the shearing of silk, and prepare
Method is simple and convenient, scientific and efficient.
The preferred embodiment of the present invention is the foregoing is only, is not intended to limit the invention, although with reference to foregoing implementation
The present invention is described in detail example, and for those skilled in the art, it still can be to foregoing embodiments
Described technical scheme is modified, or carries out equivalent substitution to which part technical characteristic.All spirit in the present invention
Within principle, any modification, equivalent substitution and improvements made etc., it should be included in the scope of the protection.
Claims (9)
1. a kind of silk, including silk broadcloth layer（1）, it is characterised in that it is provided with outer layer silk at the top of the real silk（2）, bottom
Portion is provided with basic unit's silk（4）, in real silk（1）Inside is provided with intermediate layer silk（3）, and it is provided with sheared edge in edge
（15）；The outside of the outer layer silk is provided with rendering layer（9）, bottom is provided with antistatic silk fabric（8）；The intermediate layer silk（3）Top
Portion is provided with chemical fibre layer（13）, the chemical fibre layer（13）Outer surface be provided with antistatic backing（14）, the intermediate layer
Silk（3）Be internally provided with nanometer silver antimicrobial particle（7）, the antistatic backing（14）It is interior to be provided with conductive fiber line（10）, institute
State conductive fiber line（10）By warp（12）And parallel（11）Interweave composition；The rendering layer（9）Top have waterproof layer（6）,
In rendering layer（9）Bottom be provided with layers of chrome（5）.
A kind of 2. silk according to claim 1, it is characterised in that：The chemical fibre layer（13）And antistatic backing（14）
Between connected by binding agent.
A kind of 3. silk according to claim 2, it is characterised in that：The preparation process of the binding agent is specially to stir
Under the conditions of, the water of 50-73 percentage by weights, and polyvinyl alcohol are taken, mixing, is warming up to 88-95 degree so that polyvinyl alcohol is complete
Dissolve, be incubated 1 hour under 70-80 degree, regulation PH is 8-9, obtains solution A；Then the composite emulsifying of 30-40 percentage by weights is taken
Agent, under stirring condition, the compound emulsifying agent and remaining water are added in solution A, then be slowly added into 40-50 weight percents
The vinylacetate of ratio and the composite initiator of 40-50 percentage by weights, 88-95 degree is warming up to, is incubated 0.3-0.5 hours；It is cold
But to 60-70 degree；It is slowly added into remaining vinylacetate and remaining composite initiator again afterwards；88-95 degree is warming up to, is protected
Warm 0.2-0.4 hours；The compound emulsifying agent of 30-40 percentage by weights, and polyvinyl acetate are added, is incubated under 88-95 degree
0.2-0.4 hours, it is subsequently cooled to 40-50 degree；Again under agitation, addition sodium acid carbonate, dibutyl phthalate, two
Glycol dibenzoate, octanol, isopropanol, it is well mixed, obtains solution B；Remaining compound emulsifying agent, first are added into solution B
Base allyl acrylate, ethyleneglycol dimethyacrylate, toluene di-isocyanate(TDI), NMA, waxy corn form sediment
Powder, sodium hypochlorite, it is well mixed, 40-50 degree insulation 0.1-0.3 hours, is cooled to room temperature, produces the binding agent.
A kind of 4. silk according to claim 1, it is characterised in that：The mosquito proof auxiliary agent layer（10）It is internally provided with anti-
Mosquito auxiliary agent, mosquito proof auxiliary agent are by obtained after pest repellant and bonding agent uniform stirring.
A kind of 5. silk according to claim 1, it is characterised in that：The antistatic backing（8）It is made by antistatic material
, wherein antistatic material is made up of the raw material of following parts by weight：Epoxy resin 50-100 parts, poly terephthalic acid fourth two
Alcohol ester 1-50 parts, potassium titanate 0.7-10 parts, -13 parts of silica 1, magnesium hydroxide 1-40 parts, anhydrous calcium chloride 1-12 parts, sulfuric acid
Ferrous 0.1-3 parts, it is added to uniform stirring in agitator and is made.
A kind of 6. silk according to claim 1, it is characterised in that：The rendering layer（9）By the original of following parts by weight
Material composition：Glutinous rice starch 25-40 parts, sodium carboxymethylcellulose 15-25 parts, cyclodextrin 2-9 parts, polyvinyl acetate 0.02-1.0
Part, nanometer titanium dioxide 0.2-1.5 parts, string 10-20 parts, surfactant 0.04-0.2 parts, preservative 0.02-0.15
Part, antioxidant 0.01-0.1 parts.
7. a kind of silk preparation method for described in claim 1, including dyestuff, winder, warping plus print opening, drying, its
It is characterised by：Comprise the following steps：
1）Dyestuff：Coloring agent is added, coloring agent and water, uniform stirring are added in staining jar, heats up and maintains the temperature at 40-
50 °C, add carbonic acid and adjust the pH of dye liquor between 4-6；Immersion, it is small to be immersed in 1.5-3.5 in staining jar by textile raw material
When, low temperature rapid dyeing auxiliary agent immersion 10-50min is then added, is then heated up with 2-3 DEG C/min speed, is warming up to 80-90
DEG C and keep 45-60min；Drying, the textile raw material after immersion is dried in the environment of 80-90 DEG C；Rinsing, after taking out drying
Textile raw material immerse 35-55 minutes rinsed in clear water, and add purificant；Dry, it is natural to take out the textile raw material after rinsing
Dry；
2）Winder：Using automatic winder winder, technique is：Short slub：DS1.9-2.9cm, LS1.2-1.8cm；Long slubbing：
DL1.2-1.5cm, LL20-50cm；Details：D16%-30%, L16-60cm；Cotton knot：N3.8-5；Relative humidity in workshop：68%-
78%th, temperature：20-28℃；
3）Warping：Warping is carried out to conductive fiber line, warp and weft, tension scheme is the floor of 4th areas, three Ceng Huo, 3rd areas three, single
Warp tension is 35cN-55cN, and side warp thread line tension increases 20%-25%, speed：200-350 ms/min；Rolling density：0.5-
0.7g/cm3；
4）Print is added to be open：Add print outer layer silk, intermediate layer silk in silk broadcloth layer surface, basic unit's silk, layers of chrome, waterproof layer, receive
The silver-colored antibacterial granule of rice, antistatic silk fabric, rendering layer, chemical fibre layer, antistatic backing；Then opened at the marginal position of silk broadcloth layer
If sheared edge；Then baked；
5）Dry：Silk after baking is produced after room temperature is dried.
A kind of 8. silk preparation method according to claim 7, it is characterised in that：The step 5）Middle room temperature is dried wet
Degree will be maintained at less than 10%.
A kind of 9. silk preparation method according to claim 7, it is characterised in that：The step 4）Stoving temperature be
40-60℃。
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108859313A (en) * | 2018-08-01 | 2018-11-23 | 湖州卓豪丝绸有限公司 | A kind of antibacterial silk composite material |
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| CN103171363A (en) * | 2013-03-02 | 2013-06-26 | 淄博海润丝绸发展有限公司 | Silk specially used for painting and calligraphy and manufacturing method thereof |
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| CN105237953A (en) * | 2015-10-16 | 2016-01-13 | 文雪烽 | Antistatic material |
| CN106884341A (en) * | 2017-03-24 | 2017-06-23 | 合肥云都棉花有限公司 | A kind of colouring method of textile raw material |
| CN107009708A (en) * | 2017-05-17 | 2017-08-04 | 荆门千年健医疗保健科技有限公司 | A kind of novel antistatic cloth |
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| CN103171363A (en) * | 2013-03-02 | 2013-06-26 | 淄博海润丝绸发展有限公司 | Silk specially used for painting and calligraphy and manufacturing method thereof |
| CN103334199A (en) * | 2013-06-14 | 2013-10-02 | 山西绿洲纺织有限责任公司 | Cannabis textile fabric and textile technology thereof |
| CN104650777A (en) * | 2015-01-28 | 2015-05-27 | 海安县紫石涂料有限公司 | Binder composition |
| CN105237953A (en) * | 2015-10-16 | 2016-01-13 | 文雪烽 | Antistatic material |
| CN106884341A (en) * | 2017-03-24 | 2017-06-23 | 合肥云都棉花有限公司 | A kind of colouring method of textile raw material |
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| CN108859313A (en) * | 2018-08-01 | 2018-11-23 | 湖州卓豪丝绸有限公司 | A kind of antibacterial silk composite material |
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