CN110004500A - A kind of sun-proof Wear-resistant Treatment technology of silk production - Google Patents
A kind of sun-proof Wear-resistant Treatment technology of silk production Download PDFInfo
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- CN110004500A CN110004500A CN201910055822.2A CN201910055822A CN110004500A CN 110004500 A CN110004500 A CN 110004500A CN 201910055822 A CN201910055822 A CN 201910055822A CN 110004500 A CN110004500 A CN 110004500A
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- silk
- wear
- submissive
- degreasing
- treatment technology
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B7/00—Obtaining silk fibres or filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B7/00—Obtaining silk fibres or filaments
- D01B7/04—Reeling silk
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
- D01C3/02—De-gumming silk
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- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Husbandry (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of silks to make sun-proof Wear-resistant Treatment technology, and step 1: silkworm chrysalis is killed using hot-air or electromagnetic wave etc., and removes suitable moisture by pupa killing, to reinforce Wen ﹑ humid control in silk cocoon storage and take the measure of protection；Step 2: filature, will be dry in step 1 after silk cocoon side through solution silk degreaser spray solution silk, while degreasing silk gum, which is made, through spinning machine still adheres to sheet silk on silk；Step 3: it impregnates, the present invention relates to silk manufacture technology fields.The silk makes sun-proof Wear-resistant Treatment technology, by solve silk degreaser be by mass fraction be 92-98% defatting enzyme and water by weight 1:150-1:400 ratio, the destruction using akaline liquid to the natural elastic and wear-resisting property of silk is avoided using defatting enzyme, it can maintain the natural performance of silk, existing cicada silk is avoided since chemical agent destroys its surface fiber, so that the appearance of the sun-proof reduced performance problem in surface of cicada silk.
Description
Technical field
The present invention relates to silk manufacture technology field, specially a kind of silk makes sun-proof Wear-resistant Treatment technology.
Background technique
Silk is a kind of textile, is made into silk or synthetic fibers, staple fibre, short silk etc.；With silk or artificial silk
The general name of the pure fabric knitted or be interwoven.In ancient times, it (also includes a small amount of tussah based on mulberry silk that silk, which is exactly silk,
Silk and cassava silkwormsilk) woven textile.Modern times, all warps were using artificial or natural length due to the extension of textile raw material
The woven textile of silk fiber, can be known as the silk of broad sense.And the woven silk of pure mulberry silk institute, and it is especially referred to as " true
Silk ".Silk is the specialty of China.Ancient times working people invents and is mass produced silk fabrics, more opens world history
Upper first time large-scale commerce and trade exchange between east and west, is called the Silk Road in history.From ancient times, silk just constantly transports state in force
Outside, become world-famous product.The main road gone at that time to west is known as " Silk Road " by westerner.Staple fibre refers to
The non-natural fibers as made from physicochemical method are divided into regenerated fiber and two kinds of chemical fibre.Regenerated fiber is to use certain
A little natural polymers or derivatives thereof do raw material, weaving solution are made after dissolving, then spinneret is spun into threadiness
Material；Chemical fibre is to make synthetic fibers made of raw material using petroleum, natural gas, coal and agricultural and sideline product.It is added in silk
Staple fibre, primarily to making the crease-resistant contracting of silk, Anti-moth-eating, more easy to maintain etc..Staple fibre only has 100 years history,
Before this, the mankind depend on the natural fibers such as cotton, hair, silk, fiber crops applied to textile garment and other production fields.50 years 20th century
In generation, later various synthetic fibers successively came out, and amount is big inexpensive, had greatly enriched textile fabric total output and use scope, had become day
The rival of right fiber.
In existing silk manufacturing process, mostly impregnated using silk boiling or using chemical reagent in existing silk reeling process
Method raw silk is removed from cocoon, the process of this silk production reduces the natural elastic of silk and wear-resisting property, reduces
The performance of silk, and existing cicada silk destroys its surface fiber due to chemical agent, so that the surface of cicada silk is sun protection
It can reduce.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of silks to make sun-proof Wear-resistant Treatment technology, solves existing
Mostly raw silk is removed from cocoon using silk boiling or using the method that chemical reagent is impregnated in some silk reeling process, it is this true
The process of silk production reduces the natural elastic of silk and wear-resisting property, reduces the performance of silk, and existing cicada silk by
Its surface fiber is destroyed in chemical agent, so that the problem of the sun-proof reduced performance in surface of cicada silk.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs: a kind of sun-proof wear-resisting place of silk production
Reason technology, specifically comprises the following steps:
Step 1: silkworm chrysalis is killed using hot-air or electromagnetic wave etc., and removes suitable moisture by pupa killing, is store in silk cocoon
To reinforce Wen ﹑ humid control when hiding and take the measure of protection；
Step 2: filature, by the silk cocoon side in step 1 after drying through solution silk degreaser spray solution silk, while through the mechanism of reeling off raw silk from cocoons
The sheet silk on silk is still adhered at degreasing silk gum；
Step 3: impregnating, and takes out obtained degreasing silk gum in step 2 and still adheres to the sheet silk on silk, be placed in wash it is clean
It is impregnated in liquid 25-30 hours, the weight ratio that degreasing silk gum has still adhered to sheet silk and detergent liquid on silk is 1:35, is impregnated
Cheng Zhong stirred once every 2.5 hours, the sheet silk that degreasing silk gum has still adhered on silk is allowed to be thoroughly impregnated in detergent liquid,
It separates the silk gum adhered on silk with silk, obtains soaked silk；
Step 4: cleaning, after the soaked silk that step 3 is obtained is cleaned with clear water, then it is small with clear water bubble 7-10
When, obtain the silk of degreasing；
Step 5: it is submissive, the silk of the degreasing obtained in step 4 is de- dry, it is subsequently placed in submissive liquid and impregnates 0.2-
0.4 hour, the silk of degreasing and the weight ratio of submissive liquid were 1:15, the silk after immersion, after acquisition is submissive；
Step 6: adding anti-wear agent, by obtained in step 5 it is submissive after silk be added de- dry, be subsequently placed in wear-resisting base fluid
Middle immersion 0.5-1 hours, it is submissive after silk and wear-resisting base fluid weight ratio be 1:20, after immersion, obtain it is wear-resisting after
Silk；
Step 7: drying, by step 6 obtain it is submissive after silk it is de- do, dry, that is, obtain the silk prepared；
Step 8；It examines, by the silk prepared obtained in step 7 with 5 to be a collection of, extraction sample silk 25 is twisted, big to twist
Silk every batch of extracts 13 and twists, and long hank knotting every batch of extracts 10 and twists, and inspection project includes weight and quality two major classes, and quality restriction is divided into again
Appearance test and testing of apparatus, testing of apparatus include that item is examined in cutting, evenness, fiber number, cleaning, cleaning, strong sandstorm and obvolvent etc.
Mesh.
Preferably, spinning machine is metal cylinder drum-type structure in the step 2.
Preferably, the solution silk degreaser in the step 2 be by mass fraction be 92-98% defatting enzyme and water by weight
Measure the ratio than 1:150-1:400,1 DEG C -25 DEG C of aqueous solution being prepared at normal temperature.
Preferably, the detergent liquid in the processing step three is hydrogen peroxide, the solid phosphinylidyne for being 15-20% by mass fraction
Amine, dish washing liquid and water, by weight the ratio of 2:1:1:110-400,1 DEG C -25 DEG C of aqueous solution being prepared at normal temperature.
Preferably, the submissive liquid in the processing step five is that mass fraction is soft for hydrogen peroxide, the spun silk of 15-20%
Agent TF-404A and water by weight the ratio of 1:3:500, prepare at normal temperature and 1 DEG C -30 DEG C of aqueous solution.
Preferably, the anti-wear agent in the processing step six is to mention the dry and wet crock fastness that mass fraction is 80-95%
Agent 713 and silicone oil and water are risen by weight the ratio of 1:2:400, prepare at normal temperature and 1 DEG C -30 DEG C of aqueous solution.
(3) beneficial effect
The present invention provides a kind of silks to make sun-proof Wear-resistant Treatment technology.Have compared with prior art following beneficial to effect
Fruit: the silk makes sun-proof Wear-resistant Treatment technology, and by step 1: pupa killing is killed silkworm chrysalis using hot-air or electromagnetic wave etc.
Extremely, and suitable moisture is removed, reinforces Wen ﹑ humid control in silk cocoon storage and takes the measure of protection；Step 2: reel silk from cocoons
Silk, by the silk cocoon side in step 1 after drying through solution silk degreaser spray solution silk, while it is still viscous that degreasing silk gum is made through spinning machine
Sheet silk on attached silk；Step 3: impregnating, and takes out obtained degreasing silk gum in step 2 and still adheres to the sheet silkworm on silk
Silk is placed in detergent liquid and impregnates 25-30 hours, and degreasing silk gum still adheres to the weight ratio of sheet silk and detergent liquid on silk and is
1:35 in soaking process, stirred primary every 2.5 hours, degreasing silk gum is allowed still to adhere to the sheet silk on silk in detergent liquid
Middle full penetration separates the silk gum adhered on silk with silk, obtains soaked silk；Step 4: cleaning obtains step 3
After the soaked silk obtained is cleaned with clear water, then with clear water bubble 7-10 hours, obtain the silk of degreasing；Step 5: it is submissive,
The silk of the degreasing obtained in step 4 is de- dry, it is subsequently placed in submissive liquid and impregnates 0.2-0.4 hours, the silk of degreasing
Weight ratio with submissive liquid is 1:15, the silk after immersion, after acquisition is submissive；Step 6: adding anti-wear agent, will be in step 5
Obtain it is submissive after silk be added de- dry, be subsequently placed in wear-resisting base fluid and impregnate 0.5-1 hours, it is submissive after silk with it is resistance to
The weight ratio for grinding base fluid is 1:20, the silk after immersion, after acquisition is wear-resisting；Step 7: drying, and step 6 is obtained soft
Silk along after, which takes off, to be done, dries, that is, obtains the silk prepared；Step 8；It examines, the silkworm prepared that will be obtained in step 7
Silk is a batch with 5, extracts sample silk 25 and twists, and mosses every batch of extracts 13 and twists, and long hank knotting every batch of extracts 10 and twists, and inspection project includes
Weight and quality two major classes, quality restriction are divided into appearance test and testing of apparatus again, testing of apparatus include cutting, evenness, fiber number,
Project is examined in cleaning, clean, strong sandstorm and obvolvent etc., is solved in existing silk reeling process mostly using silk boiling or using chemistry
The method that reagent is impregnated removes raw silk from cocoon, is easy to make raw silk to damage natural performance, by solve silk degreaser be by
The defatting enzyme and water that mass fraction is 92-98% are avoided using defatting enzyme using alkali by weight the ratio of 1:150-1:400
Property destruction of the liquid to the natural elastic and wear-resisting property of silk, the natural performance of silk can be maintained, avoid existing cicada silk
Since chemical agent destroys its surface fiber, so that the appearance of the sun-proof reduced performance problem in surface of cicada silk.
Specific embodiment
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is only
It is a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, ordinary skill people
Member's every other embodiment obtained without making creative work, shall fall within the protection scope of the present invention.
The embodiment of the present invention provides a kind of technical solution: a kind of silk makes sun-proof Wear-resistant Treatment technology, specifically include as
Lower step:
Step 1: silkworm chrysalis is killed using hot-air or electromagnetic wave etc., and removes suitable moisture by pupa killing, is store in silk cocoon
To reinforce Wen ﹑ humid control when hiding and take the measure of protection；
Step 2: filature, by the silk cocoon side in step 1 after drying through solution silk degreaser spray solution silk, while through the mechanism of reeling off raw silk from cocoons
The sheet silk on silk is still adhered at degreasing silk gum；Spinning machine is metal cylinder drum-type structure；Solving silk degreaser is by matter
Amount score is the ratio of the defatting enzyme and water of 92-98% by weight 1:150-1:400,1 DEG C -25 be prepared at normal temperature
DEG C aqueous solution；
Step 3: impregnating, and takes out obtained degreasing silk gum in step 2 and still adheres to the sheet silk on silk, be placed in wash it is clean
It is impregnated in liquid 25-30 hours, the weight ratio that degreasing silk gum has still adhered to sheet silk and detergent liquid on silk is 1:35, is impregnated
Cheng Zhong stirred once every 2.5 hours, the sheet silk that degreasing silk gum has still adhered on silk is allowed to be thoroughly impregnated in detergent liquid,
It separates the silk gum adhered on silk with silk, obtains soaked silk；Detergent liquid is the dioxygen for being 15-20% by mass fraction
Water, solid carbamide, dish washing liquid and water, by weight the ratio of 2:1:1:110-400, be prepared at normal temperature 1 DEG C -25
DEG C aqueous solution；
Step 4: cleaning, after the soaked silk that step 3 is obtained is cleaned with clear water, then it is small with clear water bubble 7-10
When, obtain the silk of degreasing；
Step 5: it is submissive, the silk of the degreasing obtained in step 4 is de- dry, it is subsequently placed in submissive liquid and impregnates 0.2-
0.4 hour, the silk of degreasing and the weight ratio of submissive liquid were 1:15, the silk after immersion, after acquisition is submissive；Submissive liquid
Be by mass fraction be 15-20% hydrogen peroxide, spun silk softening agent TF-404A and water by weight 1:3:500 ratio, normal
The lower preparation of temperature and 1 DEG C -30 DEG C of aqueous solution；
Step 6: adding anti-wear agent, by obtained in step 5 it is submissive after silk be added de- dry, be subsequently placed in wear-resisting base fluid
Middle immersion 0.5-1 hours, it is submissive after silk and wear-resisting base fluid weight ratio be 1:20, after immersion, obtain it is wear-resisting after
Silk；Anti-wear agent is the dry wet friction fastness improving agent 713 and silicone oil and water by weight 1 by mass fraction for 80-95%:
The ratio of 2:400, prepare at normal temperature and 1 DEG C -30 DEG C of aqueous solution；
Step 7: drying, by step 6 obtain it is submissive after silk it is de- do, dry, that is, obtain the silk prepared；
Step 8；It examines, by the silk prepared obtained in step 7 with 5 to be a collection of, extraction sample silk 25 is twisted, big to twist
Silk every batch of extracts 13 and twists, and long hank knotting every batch of extracts 10 and twists, and inspection project includes weight and quality two major classes, and quality restriction is divided into again
Appearance test and testing of apparatus, testing of apparatus include that item is examined in cutting, evenness, fiber number, cleaning, cleaning, strong sandstorm and obvolvent etc.
Mesh.
It is mostly soaked using silk boiling or using chemical reagent in conclusion the present invention solves in existing silk reeling process
The method of bubble removes raw silk from cocoon, is easy that raw silk is made to damage natural performance, is to be by mass fraction by solution silk degreaser
The defatting enzyme and water of 92-98% is avoided using akaline liquid using defatting enzyme to silkworm by weight the ratio of 1:150-1:400
The destruction of the natural elastic and wear-resisting property of silk, can maintain the natural performance of silk, avoid existing cicada silk due to chemical drugs
Agent destroys its surface fiber, so that the appearance of the sun-proof reduced performance problem in surface of cicada silk.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of silk makes sun-proof Wear-resistant Treatment technology, it is characterised in that: specifically comprise the following steps: step 1: pupa killing, benefit
Silkworm chrysalis is killed with hot-air or electromagnetic wave etc., and removes suitable moisture, silk cocoon storage when to reinforce Wen ﹑ humid control and
Take the measure of protection；
Step 2: filature, by the silk cocoon side in step 1 after drying through solution silk degreaser spray solution silk, while being made through spinning machine
Degreasing silk gum still adheres to the sheet silk on silk；
Step 3: impregnating, and takes out obtained degreasing silk gum in step 2 and still adheres to the sheet silk on silk, is placed in detergent liquid
It impregnates 25-30 hours, it is 1:35, soaking process that degreasing silk gum, which has still adhered to the weight ratio of sheet silk and detergent liquid on silk,
In, it was stirred every 2.5 hours once, allows the sheet silk that degreasing silk gum has still adhered on silk to be thoroughly impregnated in detergent liquid, make
Silk gum on adherency silk is separated with silk, obtains soaked silk；
Step 4: cleaning after the soaked silk for obtaining step 3 is cleaned with clear water, then with clear water bubble 7-10 hours, obtains
Obtain the silk of degreasing；
Step 5: it is submissive, the silk of the degreasing obtained in step 4 is de- dry, it is subsequently placed in submissive liquid and impregnates 0.2-0.4
Hour, the weight ratio of the silk of degreasing and submissive liquid is 1:15, the silk after immersion, after acquisition is submissive；
Step 6: adding anti-wear agent, by obtained in step 5 it is submissive after silk be added de- dry, be subsequently placed in wear-resisting base fluid and soak
Bubble 0.5-1 hour, it is submissive after silk and wear-resisting base fluid weight ratio be 1:20, after immersion, acquisition it is wear-resisting after silkworm
Silk；
Step 7: drying, by step 6 obtain it is submissive after silk it is de- do, dry, that is, obtain the silk prepared；
Step 8；It examines, by the silk prepared obtained in step 7 with 5 to be a collection of, extraction sample silk 25 is twisted, and mosses is every
It criticizes and extracts 13 strands, long hank knotting every batch of extracts 10 and twists, and inspection project includes weight and quality two major classes, and quality restriction is divided into appearance again
It examines and testing of apparatus, testing of apparatus includes that project is examined in cutting, evenness, fiber number, cleaning, cleaning, strong sandstorm and obvolvent etc..
2. a kind of silk according to claim 1 makes sun-proof Wear-resistant Treatment technology, it is characterised in that: in the step 2
Spinning machine is metal cylinder drum-type structure.
3. a kind of silk according to claim 1 makes sun-proof Wear-resistant Treatment technology, it is characterised in that: in the step 2
Solution silk degreaser be by mass fraction be 92-98% defatting enzyme and water by weight 1:150-1:400 ratio, in room temperature
Under 1 DEG C -25 DEG C of aqueous solution being prepared.
4. a kind of silk according to claim 1 makes sun-proof Wear-resistant Treatment technology, it is characterised in that: the processing step
Detergent liquid in three is hydrogen peroxide, solid carbamide, dish washing liquid and the water for being 15-20% by mass fraction, by weight 2:1:
The ratio of 1:110-400,1 DEG C -25 DEG C of aqueous solution being prepared at normal temperature.
5. a kind of silk according to claim 1 makes sun-proof Wear-resistant Treatment technology, it is characterised in that: the processing step
Submissive liquid in five be by mass fraction be 15-20% hydrogen peroxide, spun silk softening agent TF-404A and water by weight 1:3:
500 ratio, prepare at normal temperature and 1 DEG C -30 DEG C of aqueous solution.
6. a kind of silk according to claim 1 makes sun-proof Wear-resistant Treatment technology, it is characterised in that: the processing step
Anti-wear agent in six is the dry wet friction fastness improving agent 713 and silicone oil and water by weight 1 by mass fraction for 80-95%:
The ratio of 2:400, prepare at normal temperature and 1 DEG C -30 DEG C of aqueous solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910055822.2A CN110004500A (en) | 2019-01-21 | 2019-01-21 | A kind of sun-proof Wear-resistant Treatment technology of silk production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910055822.2A CN110004500A (en) | 2019-01-21 | 2019-01-21 | A kind of sun-proof Wear-resistant Treatment technology of silk production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110004500A true CN110004500A (en) | 2019-07-12 |
Family
ID=67165433
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910055822.2A Withdrawn CN110004500A (en) | 2019-01-21 | 2019-01-21 | A kind of sun-proof Wear-resistant Treatment technology of silk production |
Country Status (1)
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| CN (1) | CN110004500A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113564730A (en) * | 2021-08-31 | 2021-10-29 | 冯志伟 | Cold water spinning formula |
-
2019
- 2019-01-21 CN CN201910055822.2A patent/CN110004500A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113564730A (en) * | 2021-08-31 | 2021-10-29 | 冯志伟 | Cold water spinning formula |
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Application publication date: 20190712 |