CN110215095A - A kind of production technology of antibacterial, ventilating natural feather silk quilt - Google Patents
A kind of production technology of antibacterial, ventilating natural feather silk quilt Download PDFInfo
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- CN110215095A CN110215095A CN201910506727.XA CN201910506727A CN110215095A CN 110215095 A CN110215095 A CN 110215095A CN 201910506727 A CN201910506727 A CN 201910506727A CN 110215095 A CN110215095 A CN 110215095A
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G9/00—Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
- A47G9/02—Bed linen; Blankets; Counterpanes
- A47G9/0207—Blankets; Duvets
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/40—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads
- D03D15/47—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads multicomponent, e.g. blended yarns or threads
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/04—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of yarns, threads or filaments
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- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/41—Amides derived from unsaturated carboxylic acids, e.g. acrylamide
- D06M13/412—N-methylolacrylamides
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/17—Natural resins, resinous alcohols, resinous acids, or derivatives thereof
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/285—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acid amides or imides
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
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- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D06M19/00—Treatment of feathers
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- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
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- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
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Abstract
The invention discloses a kind of production technologies of antibacterial, ventilating natural feather silk quilt, including antibacterial fabric preparation → down filler pre-treatment → down filler antibiotic finish → mixing down-filling process, specifically comprise the following steps: S101, yarn selection: warp thread includes long-staple cotton fiber and bamboo charcoal fiber；S102, warp thread blending product；S103, yarn dyeing antibiotic finish；S104, face weave；S105, fabric calendering pre-treatment；S106, fabric calendering；S201, down filler selection: white goose down, silk, flaxen fiber；S202, white goose down pre-treatment；S301, down filler antibiotic finish；S302, drying sterilization；S401, mixing down-filling.Stable processing technique of the invention, eiderdown quilt produced have comfortable softness, and moisture absorption is ventilative, and the advantages of anti-microbial property high-efficient and lasting.
Description
Technical field
The present invention relates to quilt processing technique field, in particular to a kind of production technology of antibacterial, ventilating natural feather silk quilt.
Background technique
Quilt is one kind of bedding, is that area is enough to cover the rectangle cloth of human body, is typically used as guarantor when sleep
Warm, quilt usually encloses cotton-wool by quilt cover or coverlet and forms, and is called cotton-wadded quilt with the quilt that cotton is cooked.In addition to cotton-wadded quilt, it can also use
The manufacture of the staple fibres such as wool, silk or acrylic fiber.With being gradually increased for people's living standard, people are to quilt
Fabric and quilt liner material are proposed more and more functional requirements, thus conventional fabric and liner material without
Method meets the needs of market diversification.
In recent years, the high-grade material such as natural feather, silk is also gradually applied in the processing of quilt, and natural feather has matter
Gently, advantage soft, warmth retention property is good, silk softness paste skin, and sucting wet air permeability is good, but since natural feather, silk are all protein fibres
Dimension, with animal fat, bacterium easy to breed, it is therefore desirable to which safety, antibiotic property could be obtained by carrying out effective antibiotic finish
The eiderdown quilt of persistent high efficiency.
Notification number is that the Chinese patent of CN1327079C discloses a kind of plumage of mould proof deodorization health function of anti-bacteria and anti-virus
The processing method of suede, using chitin it is solvent impregnated or spray into down fiber, through chitin in conjunction with the absorption of down fiber
Make down fiber that there is certain anti-microbial property, but the binding strength of chitin and down fiber is poor under this method, with
Using the increase of time and washing times, chitin can progressively disengage down fiber and cause under down fiber anti-microbial property
Drop, therefore down fiber anti-microbial property cannot be lasting in the prior art, antibacterial effect can be also limited significantly.
Summary of the invention
The purpose of the present invention is to provide a kind of production technology of antibacterial, ventilating natural feather silk quilt, eiderdown quilt produced its
With comfortable softness, moisture absorption of breathing freely, and the advantages of anti-microbial property high-efficient and lasting.
To achieve the above object, the present invention provides the following technical scheme that a kind of production of antibacterial, ventilating natural feather silk quilt
Technique, including process: antibacterial fabric preparation → down filler pre-treatment → down filler antibiotic finish → mixing down-filling, it is main
It comprises the steps of:
(1) prepared by antibacterial fabric:
S101, yarn select: warp thread includes mass ratio for 10:(3~5) long-staple cotton fiber and bamboo charcoal fiber；Weft yarn is to wash long filament；
S102, warp thread blending product: by long-staple cotton fiber and bamboo charcoal fiber by 10:(3~5) mass ratio carry out mixed fibre, then pass through
It crosses blowing, cotton carding, drafting, rove, spinning process and blend warp yarns is made；
Warp thread, weft yarn: being impregnated in dyeing and finishing bath foam by S103, yarn dyeing antibiotic finish at room temperature, and adjusting bath foam pH to 6.5~
9.5, disperse dyes levelling agent, antibacterial agent are sequentially added, control disperse dyes levelling agent, antimicrobial agent concentration are 2~5g/L, bath raio
For 1:(10~13), dye liquor temperature is risen to 70 DEG C according to the heating rate of 1~2 DEG C/min, is then added disperse dyes, then with
Dye liquor temperature is risen to 85 DEG C by the heating rate of 2 DEG C/min, drain after 40~50min of heat preservation dyeing；
S104, face weave: the warp thread after dyeing and finishing is gone up into loom after warping, sizing, denting, according to plain weave construction
Cooperation is woven into weft yarn, completes face weave；
S105, fabric calendering pre-treatment: by calendering agent, fluorescent whitening agent be added boiling water, and stirring and dissolving formed concentration be 15~
The calendering bath foam of 30g/L is cooled to 50~55 DEG C to bath foam, woven fabric is impregnated in bath foam, bath raio be 1:(10~
12) 30~40min, is kept the temperature at a temperature of 50~55 DEG C, is then taken out fabric, is dried to water content at 80~85 DEG C after dehydration
3%~8%；
S106, fabric calendering: the fabric of S105 step is subjected to calendering by calender, antibacterial face most is made through cooling and shaping afterwards
Material；
(2) down filler pre-treatment:
S201, down filler select: filler includes mass ratio for 6:(2~4): (1~2) white goose down, silk, flaxen fiber；
S202, white goose down pre-treatment: white goose down was obstructed through the past, is removed sand, essence point, previous cleaning, washing, dehydration；
(3) down filler antibiotic finish:
S301, antibiotic finish: using the clean that beauty visitor nano silver ion antibiotic agent IM10D-L of Japan and Germany's He Te chitin antibacterial
Finishing agent SAL6680 compounds to form antibiotic finishing solution, carries out dipping antibiotic finish to white goose down, silk；
S302, drying sterilization: the white goose down of antibiotic finishing solution will be impregnated, silk carries out drying and processing, same stepping in drying course
Row ultraviolet sterilization；
(4) down-filling is mixed:
S401, according to S201 step proportion by after flaxen fiber, antibiotic finish white goose down and silk mix down-filling into S105
In the comforter batt set that step antibacterial fabric has sewed, line is seized using sealing, antibacterial, ventilating natural feather silk quilt is made in quilting.
By using above-mentioned technical proposal, cotton absorbs good permeability, flexibility height, good spinnability, and long-staple cotton is even more cotton fibre
Quality is preferably a kind of in dimension；Bamboo charcoal fiber is using moso bamboo as raw material, using pure oxygen high temperature and the new work of calcining of nitrogen barrier delay
Skill and new technology, the micropore for having bamboo charcoal innately more refines and honeycomb, then again and with honeycomb microporous structure trend
Polyester modification slice melt spinning and be made, this unique fibre structure, make bamboo charcoal fiber have moisture absorption ventilative, antibacterial anti-
Bacterium, it is cool in summer and warm in winter, environmentally protective the advantages that, by both keeping yarn for long-staple cotton fiber and the blended formation warp thread of bamboo charcoal fiber
Sucting wet air permeability has the performance for imparting yarn itself persistent high efficiency antibacterial bacteriostatic；Weft yarn washs long filament wearability using long filament is washed
Well, intensity is big, and fibre cohesion is strong, and the wrinkle resistance and durability of fabric can be improved.
Carrying out dyeing to yarn can be improved yarn color yield and dyefastness, especially disperse dyes for terylene coloring
Effect is good, so as to improve the color fastness of fabric entirety；Antibacterial agent is added in dyeing course, antibacterial agent can be with dyestuff
Fiber surface and inside are spread, adsorbed and infiltrate into together, can be preferably combined together with fiber molecule under certain temperature,
To which further its anti-microbial property is improved in time fiberfill layer face, to achieve the effect that improve fabric durable antibiotic.
It is infiltrated after face weave by calendering agent, and calendering is carried out by calender, calendering agent is made to infiltrate into fabric
Between fiber and the penetrability and anti-chiseling down of fabric can be enhanced in fibrous inside, calendering agent, to bore suede reducing fabric
Meanwhile and improve the moisture absorbing and sweat releasing property of fabric, improve the comfort level of fabric.
White goose down natural feather is fine and smooth, structurally flexible, and the humidity resistance that keeps warm is strong, may insure the pine of quilt as main filler
Soft, thermal property；Silk is most soft, fine and smooth natural fiber, and resilience is good, is not easy purse up, and filling is mixed with goose down can be with
Make goose down dispersion more evenly, is not easy to make comforter batt molding, can persistently keep the soft rebound of comforter batt, in addition, silk gas permeability pole
It is good, it is able to maintain steam free flow, is able to maintain while quilt keeps warm ventilative salubrious；Flaxen fiber is also natural fiber, green
Colour circle is protected, and is had the effect of ventilative, moisture absorption, antistatic, antibiotic and sterilizing, be can be further improved the suction of quilt as filler is palmed off as
Green permeability and anti-microbial property.
The present invention is further arranged to, and it is 1:(1~1.5 that disperse dyes levelling agent, which includes mass ratio, in the S103 step)
Anionic dispersant levelling agent, non-ionic dispersant levelling agent.
By using above-mentioned technical proposal, anionic dispersant levelling agent with nonionic dispersion levelling agent is smaller compounds, can be with
Good synergistic effect is formed, and the two can form electric double layer micelle with dyestuff, have protective effect to dyestuff crystal grain, improve
The dispersion stabilization of dyestuff also functions to slow dye, dye transfer function, further improves level-dyeing property.
The present invention is further arranged to, and antibacterial agent is silicone Quaternary Ammonium Salt Antimicrobial Agent in the S103 step.
By using above-mentioned technical proposal, organosilicon quaternary ammonium salt is the ideal antibacterial agent of a kind of comprehensive performance, finish fabric
When such antibacterial agent do not need high temperature baking, just can produce lasting antibacterial effect after general drying, the fabric after arrangement is not only
With excellent anti-microbial property, and be also equipped with good moisture absorption absorption of perspiration, flexibility, flatness, resilience, static electricity resistance and
Resistance tocrocking.
The present invention is further arranged to, and it is 5~7 parts of N- methylols third that calendering agent, which includes weight fraction, in the S105 step
Acrylamide, 1~3 part of cationic polyacrylamide, 1~3 part of lightization pentalyn.
By using above-mentioned technical proposal, N hydroxymethyl acrylamide is a kind of crosslinking agent, can be modified to fiber,
So that fiber penetrability is good, while increasing the degree of cross linking between fiber and cohesive force, increase interfibrous fine and closely woven degree, to rise
To the effect for reducing brill suede；Cationic polyacrylamide is the higher chain macromolecule compound of activity, can be formed with fiber
Hydrogen bond, improves the affinity of fiber, to further increase the cohesive force between fiber and fine and closely woven degree；Lightization rosin pentaerythrite
Ester has good cementability and anti-aging property, and the fiber anti-aging property of goose down, silk can be improved, and extends it and uses the longevity
Life.
The present invention is further arranged to, and states gathering the preparation method comprises the following steps: cation is first added into high-speed mixer for calendering agent
Acrylamide, then lightization pentalyn is dispersed in cationic polyacrylamide surface, it is eventually adding N- hydroxyl first
Base acrylamide adjusts 200~300rpm of revolving speed, is stirred 2~3min, then adjusts revolving speed to 900~1000rpmr, stirring
3~5min is mixed, then ball mill is added in the mixture after stirring, 8~10h of grinding obtains calendering agent powder body.
By using above-mentioned technical proposal, first mixed component is tentatively stirred in the slow-speed of revolution, so that mixture
Component it is tentatively uniform, then final uniform mixing is reached by high-speed stirred, avoid directly being stirred under same rotating speed and
Lead to the appearance for mixing dead zone.
Invention is further arranged to, and fluorescent whitening agent includes the fluorescent whitening agent that mass ratio is 1:3 in the S105 step
CPD, fluorescent bleaches CPS-D.
By using above-mentioned technical proposal, fluorescent whitening agent CPD is suitable for cotton, cellulose fibre brightens processing, fluorescence
Brightening agent CPS-D is suitable for terylene etc. and closes fine processing of brightening, and the two compounds the whitening effect that can preferably increase fabric.
The present invention is further arranged to, and nano silver ion antibiotic agent IM10D-L, chitin antibacterial are whole in the S301 step
The mass ratio for managing agent SAL6680 is 1:1, and the concentration of antibiotic finishing solution is 3~5g/L, and bath raio is 1:(10~12).
By using above-mentioned technical proposal, nano silver ion antibiotic agent IM10D-L, chitin antibacterial finishing agent SAL6680
All it is security performance is high, the antibacterial finishing agent that has no toxic side effect, goose down, silk can be significantly improved by the two compounding collaboration
Anti-microbial property.
The present invention is further arranged to, in the S302 step drying temperature be 100~110 DEG C, drying time be 10~
15min。
By using above-mentioned technical proposal, drying can be such that antibacterial agent preferably fixes in conjunction with goose down, silk, to reach
To the effect for improving goose down and silk durable antibiotic.
In conclusion the invention has the following advantages:
1. in the present invention eiderdown quilt fabric warp thread using long-staple cotton fiber and bamboo charcoal fiber it is blended, and while yarn dyeing into
Row antibiotic finish, to achieve the effect that significantly improve fabric anti-microbial property；
2. the present invention carries out calendering processing to fabric using calendering agent, to achieve the effect that significantly improve fabric anti-chiseling down；
3. the present invention selects white goose down, silk, flaxen fiber as down filler, reach the softness for effectively improving natural feather silk quilt
The effect of resilience, moisture retentive heat insulation and highly-breathable；
4. compounding in the present invention using nano silver ion antibiotic agent, chitin antibacterial finishing agent, antibacterial is carried out to white goose down, silk
It arranges, to achieve the effect that significantly improve down filler biocidal property.
Specific embodiment
Invention is further described in detail with reference to embodiments.
The preparation example 1-3 of calendering agent
Preparation example 1: 5kg cationic polyacrylamide, 1kg N hydroxymethyl acrylamide, 1kg are gently changed into pentalyn
High-speed mixer is sequentially added, revolving speed 200rpm is adjusted, is stirred 2min, then adjust high mixer revolving speed 900rpm, continues to stir
Mixing 3min is mixed, then ball mill is added in uniformly mixed material, 8h is ground, obtains calendering agent powder body.
Preparation example 2: 6kg cationic polyacrylamide, 2kg N hydroxymethyl acrylamide, 2kg are gently changed into rosin Ji Wusi
Alcohol ester sequentially adds high-speed mixer, adjusts revolving speed 250rpm, is stirred 2.5min, then adjust high mixer revolving speed 950rpm,
Continue to be stirred 4min, then ball mill is added in uniformly mixed material, grinds 9h, obtain calendering agent powder body.
Preparation example 3: 7kg cationic polyacrylamide, 3kg N hydroxymethyl acrylamide, 3kg are gently changed into rosin Ji Wusi
Alcohol ester sequentially adds high-speed mixer, adjusts revolving speed 300rpm, is stirred 3min, then adjust high mixer revolving speed 1000rpm, after
It is continuous to be stirred 5min, then ball mill is added in uniformly mixed material, 10h is ground, calendering agent powder body is obtained.
Embodiment
A kind of embodiment 1: production technology of antibacterial, ventilating natural feather silk quilt comprising the steps of:
S101, yarn select: warp thread includes mass ratio for 10:3 long-staple cotton fiber and bamboo charcoal fiber；Weft yarn is to wash long filament；
S102, warp thread blending product: long-staple cotton fiber and bamboo charcoal fiber are subjected to mixed fibre by the mass ratio of 10:3, using clear
Blend warp yarns are made in flower, cotton carding, drafting, rove, spinning process；
Warp thread, weft yarn: being impregnated in dyeing and finishing bath foam by S103, yarn dyeing antibiotic finish at room temperature, adjusts bath foam pH to 6.5,
Anionic dispersant levelling agent, the non-ionic dispersant levelling agent that mass ratio is 1:1 is added, is subsequently added into organosilicon quaternary ammonium salt antibacterial
Agent controls disperse dyes levelling agent, antimicrobial agent concentration 2g/L, bath raio 1:10, according to the heating rate of 1 DEG C/min by dye liquor
Temperature rises to 70 DEG C, disperse dyes is then added, then dye liquor temperature is risen to 85 DEG C with the heating rate of 2 DEG C/min, heat preservation dye
Drain after color 40min；
S104, face weave: the warp thread after dyeing and finishing is gone up into loom after warping, sizing, denting, according to plain weave construction
Cooperation is woven into weft yarn, completes face weave；
S105, fabric calendering pre-treatment: the calendering agent of preparation example 1, the fluorescent whitening agent CPD that mass ratio is 1:3 and fluorescence are increased
Boiling water is added in white dose of CPS-D, and stirring and dissolving forms the calendering bath foam that concentration is 15g/L, is cooled to 50 DEG C to bath foam, will weave
Fabric be impregnated in bath foam, bath raio 1:10 keeps the temperature 30min at 50 °C, fabric is then taken out, at 80 DEG C after dehydration
It is dried to water content 3%；
S106, fabric calendering: the fabric of S105 step is subjected to calendering by calender, antibacterial face most is made through cooling and shaping afterwards
Material；
S201, down filler select: filler includes mass ratio for 6:2:1 white goose down, silk, flaxen fiber；
S202, white goose down pre-treatment: white goose down was obstructed through the past, is removed sand, essence point, previous cleaning, washing, dehydration；
S301, antibiotic finish: use mass ratio for the clean that beauty visitor nano silver ion antibiotic agent IM10D-L of the Japan of 1:1 and Germany
He Te chitin antibacterial finishing agent SAL6680 compounds to form 3g/L antibiotic finishing solution, and it is whole to carry out dipping antibacterial to white goose down, silk
Reason；
S302, drying sterilization: by the white goose down for impregnating antibiotic finishing solution, silk in 100 DEG C of drying and processing 10min, drying course
Middle synchronous progress ultraviolet sterilization；
S401, according to S201 step proportion by after flaxen fiber, antibiotic finish white goose down and silk mix down-filling into S105
In the comforter batt set that step antibacterial fabric has sewed, the obtained antibacterial, ventilating natural feather silk quilt of line, quilting is being seized by sealing.
A kind of embodiment 2: production technology of antibacterial, ventilating natural feather silk quilt comprising the steps of:
S101, yarn select: warp thread includes mass ratio for 10:4 long-staple cotton fiber and bamboo charcoal fiber；Weft yarn is to wash long filament；
S102, warp thread blending product: long-staple cotton fiber and bamboo charcoal fiber are subjected to mixed fibre by the mass ratio of 10:4, using clear
Blend warp yarns are made in flower, cotton carding, drafting, rove, spinning process；
Warp thread, weft yarn: being impregnated in dyeing and finishing bath foam by S103, yarn dyeing antibiotic finish at room temperature, adjusts bath foam pH to 7.5,
Anionic dispersant levelling agent, the non-ionic dispersant levelling agent that mass ratio is 1:1.2 is added, it is anti-to be subsequently added into organosilicon quaternary ammonium salt
Microbial inoculum controls disperse dyes levelling agent, antimicrobial agent concentration 3g/L, and bath raio 1:11 will according to the heating rate of 1.5 DEG C/min
Dye liquor temperature rises to 70 DEG C, disperse dyes is then added, then dye liquor temperature is risen to 85 DEG C with the heating rate of 2 DEG C/min, protects
Drain after temperature dyeing 45min；
S104, face weave: the warp thread after dyeing and finishing is gone up into loom after warping, sizing, denting, according to plain weave construction
Cooperation is woven into weft yarn, completes face weave；
S105, fabric calendering pre-treatment: the calendering agent of preparation example 2, the fluorescent whitening agent CPD that mass ratio is 1:3 and fluorescence are increased
Boiling water is added in white dose of CPS-D, and stirring and dissolving forms the calendering bath foam that concentration is 20g/L, is cooled to 55 DEG C to bath foam, will weave
Fabric be impregnated in bath foam, bath raio 1:11 keeps the temperature 35min at a temperature of 55 DEG C, then takes out fabric, at 85 DEG C after dehydration
It is dried to water content 5%；
S106, fabric calendering: the fabric of S105 step is subjected to calendering by calender, antibacterial face most is made through cooling and shaping afterwards
Material；S201, down filler select: filler includes mass ratio for 6:3:2 white goose down, silk, flaxen fiber；
S202, white goose down pre-treatment: white goose down was obstructed through the past, is removed sand, essence point, previous cleaning, washing, dehydration；
S301, antibiotic finish: use mass ratio for the clean that beauty visitor nano silver ion antibiotic agent IM10D-L of the Japan of 1:1 and Germany
He Te chitin antibacterial finishing agent SAL6680 compounds to form 4g/L antibiotic finishing solution, and it is whole to carry out dipping antibacterial to white goose down, silk
Reason；
S302, drying sterilization: by the white goose down for impregnating antibiotic finishing solution, silk in 105 DEG C of drying and processing 13min, drying course
Middle synchronous progress ultraviolet sterilization；
S401, according to S201 step proportion by after flaxen fiber, antibiotic finish white goose down and silk mix down-filling into S105
In the comforter batt set that step antibacterial fabric has sewed, the obtained antibacterial, ventilating natural feather silk quilt of line, quilting is being seized by sealing.
A kind of embodiment 3: production technology of antibacterial, ventilating natural feather silk quilt comprising the steps of:
S101, yarn select: warp thread includes mass ratio for 10:5 long-staple cotton fiber and bamboo charcoal fiber；Weft yarn is to wash long filament；
S102, warp thread blending product: long-staple cotton fiber and bamboo charcoal fiber are subjected to mixed fibre by the mass ratio of 10:5, using clear
Blend warp yarns are made in flower, cotton carding, drafting, rove, spinning process；
Warp thread, weft yarn: being impregnated in dyeing and finishing bath foam by S103, yarn dyeing antibiotic finish at room temperature, adjusts bath foam pH to 8.5,
Anionic dispersant levelling agent, the non-ionic dispersant levelling agent that mass ratio is 1:1.5 is added, it is anti-to be subsequently added into organosilicon quaternary ammonium salt
Microbial inoculum, controls disperse dyes levelling agent, antimicrobial agent concentration 4g/L, and bath raio 1:12 will be contaminated according to the heating rate of 2 DEG C/min
Liquid temperature rises to 70 DEG C, disperse dyes is then added, then dye liquor temperature is risen to 85 DEG C with the heating rate of 2 DEG C/min, heat preservation
Drain after dyeing 50min；
S104, face weave: the warp thread after dyeing and finishing is gone up into loom after warping, sizing, denting, according to plain weave construction
Cooperation is woven into weft yarn, completes face weave；
S105, fabric calendering pre-treatment: the calendering agent of preparation example 3, the fluorescent whitening agent CPD that mass ratio is 1:3 and fluorescence are increased
Boiling water is added in white dose of CPS-D, and stirring and dissolving forms the calendering bath foam that concentration is 25g/L, is cooled to 55 DEG C to bath foam, will weave
Fabric be impregnated in bath foam, bath raio 1:12 keeps the temperature 40min at a temperature of 55 DEG C, then takes out fabric, at 85 DEG C after dehydration
It is dried to water content 8%；
S106, fabric calendering: the fabric of S105 step is subjected to calendering by calender, antibacterial face most is made through cooling and shaping afterwards
Material；
S201, down filler select: filler includes mass ratio for 6:4:2 white goose down, silk, flaxen fiber；
S202, white goose down pre-treatment: white goose down was obstructed through the past, is removed sand, essence point, previous cleaning, washing, dehydration；
S301, antibiotic finish: use mass ratio for the nano silver ion antibiotic agent IM10D-L of your clean beauty visitor's production of the Japan of 1:1
With German He Te production chitin antibacterial finishing agent SAL6680 compound to form 5g/L antibiotic finishing solution, to white goose down, silk into
Row dipping antibiotic finish；
S302, drying sterilization: by the white goose down for impregnating antibiotic finishing solution, silk in 110 DEG C of drying and processing 15min, drying course
Middle synchronous progress ultraviolet sterilization；
S401, according to S201 step proportion by after flaxen fiber, antibiotic finish white goose down and silk mix down-filling into S105
In the comforter batt set that step antibacterial fabric has sewed, the obtained antibacterial, ventilating natural feather silk quilt of line, quilting is being seized by sealing.
A kind of embodiment 4: production technology of antibacterial, ventilating natural feather silk quilt comprising the steps of:
S101, yarn select: warp thread includes mass ratio for 10:5 long-staple cotton fiber and bamboo charcoal fiber；Weft yarn is to wash long filament；
S102, warp thread blending product: long-staple cotton fiber and bamboo charcoal fiber are subjected to mixed fibre by the mass ratio of 10:5, using clear
Blend warp yarns are made in flower, cotton carding, drafting, rove, spinning process；
Warp thread, weft yarn: being impregnated in dyeing and finishing bath foam by S103, yarn dyeing antibiotic finish at room temperature, adjusts bath foam pH to 9.5,
Anionic dispersant levelling agent, the non-ionic dispersant levelling agent that mass ratio is 1:1.5 is added, it is anti-to be subsequently added into organosilicon quaternary ammonium salt
Microbial inoculum, controls disperse dyes levelling agent, antimicrobial agent concentration 5g/L, and bath raio 1:13 will be contaminated according to the heating rate of 2 DEG C/min
Liquid temperature rises to 70 DEG C, disperse dyes is then added, then dye liquor temperature is risen to 85 DEG C with the heating rate of 2 DEG C/min, heat preservation
Drain after dyeing 50min；
S104, face weave: the warp thread after dyeing and finishing is gone up into loom after warping, sizing, denting, according to plain weave construction
Cooperation is woven into weft yarn, completes face weave；
S105, fabric calendering pre-treatment: the calendering agent of preparation example 1, the fluorescent whitening agent CPD that mass ratio is 1:3 and fluorescence are increased
Boiling water is added in white dose of CPS-D, and stirring and dissolving forms the calendering bath foam that concentration is 30g/L, is cooled to 55 DEG C to bath foam, will weave
Fabric be impregnated in bath foam, bath raio 1:12 keeps the temperature 40min at a temperature of 55 DEG C, then takes out fabric, at 85 DEG C after dehydration
It is dried to water content 8%；
S106, fabric calendering: the fabric of S105 step is subjected to calendering by calender, antibacterial face most is made through cooling and shaping afterwards
Material；
S201, down filler select: filler includes mass ratio for 6:4:1 white goose down, silk, flaxen fiber；
S202, white goose down pre-treatment: white goose down was obstructed through the past, is removed sand, essence point, previous cleaning, washing, dehydration；
S301, antibiotic finish: use mass ratio for the clean that beauty visitor nano silver ion antibiotic agent IM10D-L of the Japan of 1:1 and Germany
He Te chitin antibacterial finishing agent SAL6680 compounds to form 5g/L antibiotic finishing solution, and it is whole to carry out dipping antibacterial to white goose down, silk
Reason；
S302, drying sterilization: by the white goose down for impregnating antibiotic finishing solution, silk in 110 DEG C of drying and processing 15min, drying course
Middle synchronous progress ultraviolet sterilization；
S401, according to S201 step proportion by after flaxen fiber, antibiotic finish white goose down and silk mix down-filling into S105
In the comforter batt set that step antibacterial fabric has sewed, the obtained antibacterial, ventilating natural feather silk quilt of line, quilting is being seized by sealing.
Comparative example
Comparative example 1: a kind of production technology of antibacterial, ventilating natural feather silk quilt, the difference from embodiment 1 is that, warp thread is not added with bamboo
Carbon fibe.
Comparative example 2: a kind of production technology of antibacterial, ventilating natural feather silk quilt, the difference from example 2 is that, yarn dyeing
When be not added with silicone Quaternary Ammonium Salt Antimicrobial Agent.
Comparative example 3: a kind of production technology of antibacterial, ventilating natural feather silk quilt, the difference with embodiment 3 be, fabric not into
Row calendering processing.
Comparative example 4: a kind of production technology of antibacterial, ventilating natural feather silk quilt, the difference with embodiment 4 be, goose down, silkworm
Nano silver ion antibiotic agent IM10D-L is not added with when silk antibiotic finish.
Comparative example 5: using notification number for the example 1 in the Chinese invention patent application file of CN1327079C as control, one
The processing method of the natural feather of the kind mould proof deodorization health function of anti-bacteria and anti-virus includes the following steps: by duck's down progress degreasing, clearly
It washes, dry, the duck's down after drying is impregnated in molecular level chitin solution, chitin molecule is made to be adsorbed on duck's down surface, and
Duck's down interior tissue is infiltrated into, after drying again, duck's down is sent into dryer with suction ventilator, is dried at a temperature of 150 DEG C.
Performance detection
According to Examples 1 to 4, the method for comparative example 1~5 makes natural feather filling sample respectively, to a embodiment, comparative example natural feather
Filling sample carries out average bacteriostasis rate test；
According to Examples 1 to 4, the method for comparative example 1~3 makes eiderdown quilt fabric sample, each embodiment and comparative example respectively
Sample fabric be cut into the consistent cloth specimen of specification, feel and pliability, average bacteriostasis rate, anti-drilling are carried out respectively to test cloth specimen
Suede, gas permeability are tested, wherein using marking system to feel and pliability, test result, full marks are 10 points, test knot
Fruit is as shown in table 1；
Wherein, average bacteriostasis rate refer to gold-coloured staphylococci, candida albicans, Escherichia coli average bacteriostasis rate.
The performance test results of sample are made in 1 the above various embodiments of table, comparative example
As can be seen that the embodiment of the present invention 1~4, the eiderdown quilt fabric of comparative example 1~3, pliability in terms of the test result of table 1
All reach 9 points or more, the test of 1 pliability of comparative example is slightly good, is primarily due to fabric warp thread in comparative example 1 and is not added with bamboo charcoal fibre
Tie up blended, pure cotton causes fabric pliability increased；The average bacteriostasis rate data of fabric show that comparative example 1~2 is average antibacterial
Rate decreases, and illustrates the antibiotic property gain of bamboo charcoal fiber, yarn antimicrobial treatment for fabric；The average bacteriostasis rate of natural feather
Test display, the decline of 4~5 numerical value of comparative example is more apparent, and the average bacteriostasis rate of comparative example 5 is lower, illustrate to add nano silver from
Sub- antibacterial agent IM10D-L promotes the bacteriostasis property of natural feather；Anti-chiseling down test display, comparative example 3 bore suede phenomenon more
Obviously, illustrate to carry out calendering processing to fabric using calendering agent in the present invention, can effectively improve the anti-chiseling down performance of fabric；Thoroughly
Gas index test shows that the fabric gas permeability of the embodiment of the present invention 1~4 is more excellent, and is not added with blended pair of bamboo charcoal fiber
1 fabric gas permeability of ratio is declined, and illustrates that bamboo charcoal fiber has a certain upgrade for the gas permeability of fabric.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art
Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this
All by the protection of Patent Law in the scope of the claims of invention.
Claims (8)
1. a kind of production technology of antibacterial, ventilating natural feather silk quilt, including process: before antibacterial fabric preparation → down filler
Reason → down filler antibiotic finish → mixing down-filling, which is characterized in that mainly comprise the steps of:
(1) prepared by antibacterial fabric:
S101, yarn select: warp thread includes mass ratio for 10:(3~5) long-staple cotton fiber and bamboo charcoal fiber；Weft yarn is to wash long filament；
S102, warp thread blending product: by long-staple cotton fiber and bamboo charcoal fiber by 10:(3~5) mass ratio carry out mixed fibre, then pass through
It crosses blowing, cotton carding, drafting, rove, spinning process and blend warp yarns is made；
Warp thread, weft yarn: being impregnated in dyeing and finishing bath foam by S103, yarn dyeing antibiotic finish at room temperature, and adjusting bath foam pH to 6.5~
9.5, disperse dyes levelling agent, antibacterial agent are sequentially added, control disperse dyes levelling agent, antimicrobial agent concentration are 2~5g/L, bath raio
For 1:(10~13), bath temperature is risen to 70 DEG C according to the heating rate of 1~2 DEG C/min, is then added disperse dyes, then with
Dye liquor temperature is risen to 85 DEG C by the heating rate of 2 DEG C/min, drain after 40~50min of heat preservation dyeing；
S104, face weave: the warp thread after dyeing and finishing is gone up into loom after warping, sizing, denting, according to plain weave construction
Cooperation is woven into weft yarn, completes face weave；
S105, fabric calendering pre-treatment: by calendering agent, fluorescent whitening agent be added boiling water, and stirring and dissolving formed concentration be 15~
The calendering bath foam of 30g/L is cooled to 50~55 DEG C to bath foam, woven fabric is impregnated in bath foam, bath raio be 1:(10~
12), keep the temperature 30~40min at a temperature of 50~55 DEG C, then take out fabric, be dried to after dehydration at 80~85 DEG C water content 3%~
8%；
S106, fabric calendering: the fabric of S105 step is subjected to calendering by calender, antibacterial face most is made through cooling and shaping afterwards
Material；
(2) down filler pre-treatment:
S201, down filler select: filler includes mass ratio for 6:(2~4): (1~2) white goose down, silk, flaxen fiber；
S202, white goose down pre-treatment: white goose down was obstructed through the past, is removed sand, essence point, previous cleaning, washing, dehydration；
(3) down filler antibiotic finish:
S301, antibiotic finish: it is produced using Japan clean your the nano silver ion antibiotic agent IM10D-L and Germany He Te of beauty visitor's production
Chitin antibacterial finishing agent SAL6680 compound to form antibiotic finishing solution, dipping antibiotic finish is carried out to white goose down, silk；
S302, drying sterilization: the white goose down of antibiotic finishing solution will be impregnated, silk carries out drying and processing, same stepping in drying course
Row ultraviolet sterilization；
(4) down-filling is mixed:
S401, according to S201 step proportion by after flaxen fiber, antibiotic finish white goose down and silk mix down-filling into S105
In the comforter batt set that step antibacterial fabric has sewed, line is seized using sealing, antibacterial, ventilating natural feather silk quilt is made in quilting.
2. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 1, it is characterised in that: the S103
In step disperse dyes levelling agent include mass ratio be 1:(1~1.5) anionic dispersant levelling agent, non-ionic dispersant level dyeing
Agent.
3. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 1, it is characterised in that: the S103
Antibacterial agent is silicone Quaternary Ammonium Salt Antimicrobial Agent in step.
4. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 1, it is characterised in that: the S105
It is 5~7 parts of cationic polyacrylamide, 1~3 part of N hydroxymethyl acrylamide, 1~3 that calendering agent, which includes weight fraction, in step
Part lightization pentalyn.
5. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 4, it is characterised in that: the calendering
Agent the preparation method comprises the following steps: cationic polyacrylamide is first added into high-speed mixer, then will gently to change pentalyn equal
It is even to be scattered in cationic polyacrylamide surface, it is eventually adding N hydroxymethyl acrylamide, 200~300rpm of revolving speed is adjusted, stirs
2~3min of mixing is mixed, then adjusts revolving speed and is stirred 3~5min to 900~1000rpmr, then the mixture after stirring is added
Enter ball mill, 8~10h of grinding obtains calendering agent powder body.
6. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 1, it is characterised in that: the S105
Fluorescent whitening agent includes fluorescent whitening agent CPD, the fluorescent whitening agent CPS-D that mass ratio is 1:3 in step.
7. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 1, it is characterised in that: the S301
Nano silver ion antibiotic agent IM10D-L in step, chitin antibacterial finishing agent SAL6680 mass ratio be 1:1, antibiotic finishing solution
Concentration be 3~5g/L, bath raio be 1:(10~12).
8. a kind of production technology of antibacterial, ventilating natural feather silk quilt according to claim 1, it is characterised in that: the S302
Drying temperature is 100~110 DEG C in step, and drying time is 10~15min.
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| CN110552214A (en) * | 2019-09-19 | 2019-12-10 | 同曦集团有限公司 | Preparation method of long-acting antibacterial fabric, product and application thereof |
| CN111945419A (en) * | 2020-08-11 | 2020-11-17 | 绍兴市柯桥区宏晟纺织品有限公司 | Production process of antibacterial rayon fabric |
| CN112252037A (en) * | 2020-11-07 | 2021-01-22 | 诸暨航丰针纺织有限公司 | Antibacterial finishing process of cotton fabric |
| CN113152082A (en) * | 2021-04-07 | 2021-07-23 | 罗莱生活科技股份有限公司 | Antibacterial home textile fabric containing sesbania fibers and preparation method thereof |
| CN113668242A (en) * | 2021-08-25 | 2021-11-19 | 江苏华实织业有限公司 | Fabric with antibacterial function and method |
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| CN115478436A (en) * | 2022-09-30 | 2022-12-16 | 建滔(清远)电子材料有限公司 | Electronic grade glass fiber cloth produced by ultralow-twist glass fiber yarn |
| CN115478436B (en) * | 2022-09-30 | 2023-05-30 | 建滔(清远)电子材料有限公司 | Electronic grade glass fiber cloth produced by ultra-low twist glass fiber yarn |
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Application publication date: 20190910 |
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