CN110195267A - A kind of fruit vinegar fiber and preparation method thereof - Google Patents
A kind of fruit vinegar fiber and preparation method thereof Download PDFInfo
- Publication number
- CN110195267A CN110195267A CN201810157048.1A CN201810157048A CN110195267A CN 110195267 A CN110195267 A CN 110195267A CN 201810157048 A CN201810157048 A CN 201810157048A CN 110195267 A CN110195267 A CN 110195267A
- Authority
- CN
- China
- Prior art keywords
- acetone
- cellulose diacetate
- sodium hyaluronate
- quality
- fiber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/24—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives
- D01F2/28—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives from organic cellulose esters or ethers, e.g. cellulose acetate
Abstract
A kind of fruit vinegar fiber and preparation method thereof, the fruit vinegar fiber includes cellulose diacetate, acetone, tartaric acid and sodium hyaluronate, the mass ratio of cellulose diacetate and acetone is 20-30%, the quality of tartaric acid is the 3-10% of cellulose diacetate and acetone quality summation, and the quality of sodium hyaluronate is the 0.05-0.5% of cellulose diacetate and acetone quality summation；Cellulose diacetate is mixed with acetone, slurries are made, pure slurries are obtained by filtration；Lactic acid or malic acid are added in pure slurries, while sodium hyaluronate is added, is uniformly mixed, mixed serum is made；To the molten spray of mixed serum or spinning, fruit vinegar fiber is obtained.The present invention in cellulose diacetate by adding tartaric acid and sodium hyaluronate, the special efficacy of tartaric acid and sodium hyaluronate can be played, it acts synergistically with the advantages of original moisture absorption of fiber itself, excellent adsorption, so that fibre bundle has fruit aroma, can be widely applied to beauty daily use chemicals industry.
Description
Technical field
The present invention relates to a kind of acetate fibers, belong to fibre technology field.
Background technique
Fruit vinegar acid cellulose is a kind of staple fibre being easy to get very much, at low cost, has good knitting property, compares table
Area is big, nontoxic, anti-mildew；Feel, comfort, hydrophily and good permeability are all fine；It may be used as mixed fertilizer or burn
Burn-up, can paint, can dry-clean or wash, and not shrink usually.Cellulose acetate has selection as porous film material
Property it is high, permeable amount is big, the processing is simple the features such as.Cellulose diacetate can be processed into the materials such as fiber and film, diacetate fiber
Plain tow is a kind of regenerated cellulose, has the characteristics that moisture absorption, excellent adsorption.
In terms of acetate fiber is widely used in cigarette filter at present, expanded in terms of other application less.Also have with
Other materials are mixed and made into mixed yarn, as disclosed in Chinese patent literature CN103243437A " a kind of bamboo fibre, flax fiber and
The mixed yarn of acetate fiber ", including following ingredients: bamboo fibre 30-40 parts by weight, flax fiber 30-40 parts by weight and acetic acid are fine
Tie up 20-30 parts by weight.But acetate fiber yet there are no all document reports in the application of beauty daily use chemicals industry.
Summary of the invention
The present invention is directed to existing acetate fiber deficiency existing for application aspect, and providing one kind can be applied to beauty daily use chemicals
The fruit vinegar fiber of industry, while a kind of preparation method of fruit vinegar fiber being provided.
Fruit vinegar fiber of the invention, including cellulose diacetate, acetone, tartaric acid and sodium hyaluronate, cellulose diacetate and third
The mass ratio of ketone is 20-30%, and the quality of tartaric acid is the 3-10% of cellulose diacetate and acetone quality summation, the matter of sodium hyaluronate
Amount is the 0.05-0.5% of cellulose diacetate and acetone quality summation.
The preparation method of above-mentioned fruit vinegar fiber, comprising the following steps:
(1) cellulose diacetate, acetone, tartaric acid and sodium hyaluronate are weighed, wherein the mass ratio of cellulose diacetate and acetone
For 20-30%, the quality of tartaric acid is the 3-10% of cellulose diacetate and acetone quality summation, and the quality of sodium hyaluronate is two acetic acid
The 0.05-0.5% of cellulose and acetone quality summation；
(2) cellulose diacetate is mixed with acetone, and the impurity filtered in removal slurries is (miscellaneous in diacetate fiber
The impurity that matter and hemicellulose therein etc., the impurity that acetone etc. is brought into, and charging are brought into the process), obtain pure slurry
Liquid；
(3) lactic acid or malic acid are added in pure slurries, while sodium hyaluronate is added, is uniformly mixed, mixed serum is made；
(4) to the molten spray of mixed serum or spinning, fruit vinegar fibrous finished product is obtained.
Above-mentioned fruit vinegar fiber can be processed into the materials such as fiber and film (such as facial mask, wet tissue etc.), with moisture absorption, absorption
Property good cellulose diacetate in tartaric acid and sodium hyaluronate is added after, enhance the moisture-keeping functions of diacetate fiber, tartaric acid it is tiny
Molecule has superpower penetration, can rapid osmotic skin.It is effectively anti-using tartaric acid to the good action of human epidermal and corium
Only pore blocks, and increases the water content of skin, and it is flexible that skin becomes consolidation, and microgroove and wrinkle also can be reduced and then, improvement
Acne, nti-freckle smoothing wrinkle.Because of the water conservation of sodium hyaluronate, water lock ability, skin elasticity can be enhanced, skin is allowed to be maintained at wet shape for a long time
In state, enhance the water holding capacity of skin.
The present invention can play the special of tartaric acid and sodium hyaluronate by adding tartaric acid and sodium hyaluronate in cellulose diacetate
Effect acts synergistically with the advantages of original moisture absorption of fiber itself, excellent adsorption, so that fibre bundle has fruit aroma, it can
To be widely used in beauty daily use chemicals industry.
Specific embodiment
Embodiment 1
The mass ratio of cellulose diacetate and acetone is 20% in the fruit vinegar fiber of the present embodiment, and the quality of malic acid is two
The 5% of cellulose acetate and acetone quality summation, the quality of sodium hyaluronate are cellulose diacetate and acetone quality summation
0.1%.Its preparation process, comprising the following steps:
(1) cellulose diacetate is mixed with acetone, solid content (quality percentage of the cellulose diacetate in slurries is made
Than) be 20% slurries, through filtering removal slurries in impurity, obtain purer slurries；
(2) malic acid and sodium hyaluronate are added in slurries after filtration, is uniformly mixed, mixed serum is made；
(3) it to the molten spray of mixed serum, obtains and has fruity fruit vinegar fiber.
Cellulose diacetate can be processed into the materials such as fiber and film, and Celluloseacetate cigarette filter tow is a kind of regenerated fiber
Element has the characteristics that moisture absorption, excellent adsorption.On the basis of cellulose diacetate original function, after tartaric acid and sodium hyaluronate is added,
The moisture-keeping functions of diacetate fiber are enhanced, the tiny molecule of tartaric acid has superpower penetration, can rapid osmotic skin.
Effect of the tartaric acid between epidermis: the speed of epithelial cell metabolism is promoted in the desmosome connection reducing horn cell,
Aging cutin cell detachment is accelerated, skin is promoted to update, the epithelial cell arrangement also made is more neat, and cuticula then becomes
It is smooth and careful.Meanwhile tartaric acid can also allow the angling embolism around pore easy to fall off, and unimpeded follicular canal, effectively prevent hair
Hole obstruction.Effect of the tartaric acid to corium: sodium hyaluronate, glutinous polysaccharide, the hyperplasia of collagen and elastic fibers can be stimulated and arranged again
Column, increase the water content of skin, and it is flexible that skin becomes consolidation, and microgroove and wrinkle also can and then reductions.Tartaric acid is for skin
These functions be primarily used to improve acne, nti-freckle smoothing wrinkle.
Skin elasticity can be enhanced because of the water conservation of sodium hyaluronate, water lock ability using the facial mask containing sodium hyaluronate, make skin long-term
It is maintained in wet state, enhances the water holding capacity of skin.
Embodiment 2
In the fruit vinegar fiber of the present embodiment, the mass ratio of cellulose diacetate and acetone be 30% (, the quality of lactic acid is two
The 3% of cellulose acetate and acetone quality summation, the quality of sodium hyaluronate are cellulose diacetate and acetone quality summation
0.5%.
Cellulose diacetate is mixed with acetone, the slurries that solid content is 30% are made, pure slurries are obtained by filtration；?
Lactic acid and sodium hyaluronate are added in slurries, is uniformly mixed, mixed serum is made；To mixed serum spinning, fruit vinegar fiber is obtained.
Embodiment 3
In the fruit vinegar fiber of the present embodiment, the mass ratio of cellulose diacetate and acetone is 25%, and the quality of malic acid is
The 10% of cellulose diacetate and acetone quality summation, the quality of sodium hyaluronate are cellulose diacetate and acetone quality summation
0.05%.
The slurries that solid content is 25% are made in cellulose diacetate and acetone, pure slurries are obtained by filtration；In slurries
Malic acid and sodium hyaluronate is added, is uniformly mixed, mixed serum is made；To the molten spray of mixed serum, fruit vinegar fiber is obtained.
Embodiment 4
In the present embodiment, the mass ratio of cellulose diacetate and acetone is 28%, and the quality of lactic acid is cellulose diacetate
With the 7% of acetone quality summation, the quality of sodium hyaluronate is the 0.3% of cellulose diacetate and acetone quality summation.
Cellulose diacetate is mixed with acetone, the slurries that solid content is 28% are made, pure slurries are obtained after filtering；?
Lactic acid and sodium hyaluronate are added in slurries, is uniformly mixed, mixed serum is made；To mixed serum spinning, fruit vinegar fiber is obtained.
Claims (2)
1. a kind of fruit vinegar fiber and preparation method thereof, it is characterized in that: including cellulose diacetate, acetone, tartaric acid and sodium hyaluronate, two
The mass ratio of cellulose acetate and acetone is 20-30%, and the quality of tartaric acid is the 3- of cellulose diacetate and acetone quality summation
10%, the quality of sodium hyaluronate is the 0.05-0.5% of cellulose diacetate and acetone quality summation.
2. a kind of a kind of fruit vinegar fiber described in claim 1 and preparation method thereof, it is characterized in that: the following steps are included:
(1) cellulose diacetate, acetone, tartaric acid and sodium hyaluronate are weighed, wherein the mass ratio of cellulose diacetate and acetone is 20-
30%, the quality of tartaric acid is the 3-10% of cellulose diacetate and acetone quality summation, and the quality of sodium hyaluronate is diacetate fiber
The 0.05-0.5% of element and acetone quality summation；
(2) cellulose diacetate is mixed with acetone, and filter removal slurries in impurity (impurity in diacetate fiber, and
The impurity that hemicellulose therein etc., the impurity that acetone etc. is brought into, and charging are brought into the process), obtain pure slurries；
(3) lactic acid or malic acid are added in pure slurries, while sodium hyaluronate is added, is uniformly mixed, mixed serum is made；
(4) to the molten spray of mixed serum or spinning, fruit vinegar fibrous finished product is obtained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810157048.1A CN110195267A (en) | 2018-02-24 | 2018-02-24 | A kind of fruit vinegar fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810157048.1A CN110195267A (en) | 2018-02-24 | 2018-02-24 | A kind of fruit vinegar fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110195267A true CN110195267A (en) | 2019-09-03 |
Family
ID=67744008
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810157048.1A Withdrawn CN110195267A (en) | 2018-02-24 | 2018-02-24 | A kind of fruit vinegar fiber and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110195267A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115335025A (en) * | 2020-03-02 | 2022-11-11 | Elc管理有限责任公司 | Delivery of cosmetic agents, compositions and uses thereof |
-
2018
- 2018-02-24 CN CN201810157048.1A patent/CN110195267A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115335025A (en) * | 2020-03-02 | 2022-11-11 | Elc管理有限责任公司 | Delivery of cosmetic agents, compositions and uses thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190903 |