CN110170289A - A kind of high throughput coprecipitation device - Google Patents
A kind of high throughput coprecipitation device Download PDFInfo
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- CN110170289A CN110170289A CN201910561992.8A CN201910561992A CN110170289A CN 110170289 A CN110170289 A CN 110170289A CN 201910561992 A CN201910561992 A CN 201910561992A CN 110170289 A CN110170289 A CN 110170289A
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- 238000000975 co-precipitation Methods 0.000 title claims abstract description 79
- 238000009826 distribution Methods 0.000 claims abstract description 92
- 238000006243 chemical reaction Methods 0.000 claims abstract description 69
- 239000007788 liquid Substances 0.000 claims abstract description 56
- 239000000523 sample Substances 0.000 claims description 40
- 238000004140 cleaning Methods 0.000 claims description 24
- 238000001816 cooling Methods 0.000 claims description 17
- 239000002826 coolant Substances 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 14
- 238000012937 correction Methods 0.000 claims description 10
- 238000002347 injection Methods 0.000 claims description 9
- 239000007924 injection Substances 0.000 claims description 9
- 238000007789 sealing Methods 0.000 claims description 9
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 7
- 238000013019 agitation Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 abstract description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 20
- 239000000243 solution Substances 0.000 description 11
- 238000001802 infusion Methods 0.000 description 6
- 238000010586 diagram Methods 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 238000007711 solidification Methods 0.000 description 4
- 230000008023 solidification Effects 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 230000010412 perfusion Effects 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000012482 calibration solution Substances 0.000 description 2
- 238000006757 chemical reactions by type Methods 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention belongs to automate high-throughput techniques field, a kind of high-throughput coprecipitation device is disclosed, comprising: main body frame, liquid pump, switching distribution valve group, distribution needle group, coprecipitation reaction module and central control system；The liquid pump is fixed on the main body frame, and the switching distribution valve group is connected by liquid feeding pipeline with the liquid pump, and the switching distribution valve group is connected by distribution circuit with the distribution needle group；The distribution needle group is removably attached in the coprecipitation reaction module, and the coprecipitation reaction module is fixed on the main body frame；The liquid pump, switching distribution valve group and the coprecipitation reaction module are connected with the central control system respectively.High throughput coprecipitation device provided by the invention is able to ascend assignment accuracy and efficiency.
Description
Technical field
The present invention relates to automation high-throughput techniques field, in particular to a kind of high-throughput coprecipitation device.
Background technique
It is that precipitating reagent is added in metal salt solution or adds in precipitating reagent that coprecipitation, which prepares composite oxide catalysts,
Enter metal salt solution, generate slightly solubility metal salt or metal hydrate, be precipitated out from solution, then it is aged, filter, wash
It the programs such as washs, dry, roasting, forming, activating and catalyst or catalyst carrier is made.Existing high throughput coprecipitation device
Have higher the degree of automation, distributes needle, PH probe and perfusion tube by the distribution that mechanical arm carries fluid dispensing system
The reciprocation cycle operation that the realizations such as road automatically control, completes reagent addition.But in operation, it may appear that reagent addition
Assignment accuracy is low, sendout it is unstable it is easy fluctuate, infusion pipeline leak the defects of.
Summary of the invention
The present invention provides a kind of high-throughput coprecipitation device, solves high-throughput coprecipitation device in the prior art
The technical issues of reagent assignment accuracy is low, and sendout is unstable, and perfusion tube Louis leaks.
In order to solve the above technical problems, the present invention provides a kind of high-throughput coprecipitation devices, comprising: body frame
Frame, liquid pump, switching distribution valve group, distribution needle group, coprecipitation reaction module and central control system；
The liquid pump is fixed on the main body frame, and the switching distribution valve group passes through liquid feeding pipeline and the liquid
Pump is connected, and the switching distribution valve group is connected by distribution circuit with the distribution needle group；
The distribution needle group is removably attached in the coprecipitation reaction module, and the coprecipitation reaction module is fixed
On the main body frame；
The liquid pump, switching distribution valve group and the coprecipitation reaction module are with the center control respectively
System is connected.
Further, high-throughput coprecipitation device further include: two axis robots and PH probe；
Two axis robot is fixed on the main body frame, and the PH probe is fixed in two axis robot；
Two axis robot and the PH probe are connected with the central control system respectively.
Further, two axis robot includes: X-axis system, Z axis system and cantilever；
The X-axis system is fixed on the main body frame, and the Z axis system is fixed on the mobile terminal of the X-axis system
On, the cantilever is fixed on the mobile terminal of the Z axis system；
The X-axis system and the Z axis system are connected with the central control system respectively.
Further, high-throughput coprecipitation device further include: PH probe cleans calibration module；
PH probe cleaning calibration module is fixed on the main body frame.
Further, the PH probe correction module includes: probe cleaning assembly, probe dry component, probe correction appearance
Device and the calibration solution being arranged in the probe correction container.
Further, the high-throughput coprecipitation device further include: distribution needle cleaning module；
The distribution needle cleaning module is fixed on the main body frame；
Wherein, the distribution needle cleaning module is provided between two of the arbitrary neighborhood coprecipitation reaction modules.
Further, high-throughput coprecipitation device is stated further include: reaction kettle keeps in support；
The reaction kettle is kept in support and is fixed on the main body frame.
Further, the switching distribution valve group includes: switching valve and distributing valve；
The input terminal of the switching valve is connected by the liquid feeding pipeline with the liquid pump, the output end of the switching valve
It is connected with the input terminal of the distributing valve, the output end of the distributing valve passes through the distribution circuit and the distribution needle group phase
Even.
Further, the coprecipitation reaction module include: top cover, coolant seal lid, understructure, heating structure and
Electromagnetic agitation structure；
The distribution needle group is fixed on the top cover, and the top cover is removably fastened on the coolant seal and covers；
The understructure includes: pedestal and the reaction kettle that is arranged in the pedestal；
The coolant seal lid fixation seals the reaction kettle on the base, and is provided with and the distribution needle group pair
The liquid injection port answered；
The heating structure is fixed on the base, and is connected with the central control system；
The electromagnetic agitation structure setting on the base, and is connected with the central control system.
Further, the coolant seal lid includes: sealing cover, heat insulating mattress and cooling system；
The liquid injection port is arranged on the sealing cover, is located above the reaction kettle；
The heat insulating mattress is arranged on the bottom face of the sealing cover；
Wherein, the cooling system includes: cooling tube；
The cooling tube is fixed on the top cover bottom face, is located at right above the reaction kettle, and is controlled with the center
System processed is connected；
The matched hole of kettle mouth with the reaction kettle is opened up on the heat insulating mattress；
The liquid injection port is connected to the hole that the heat insulating mattress opens up, and the cooling tube that is staggered is distributed on the top cover.
One or more technical solutions provided in the embodiments of the present application have at least the following technical effects or advantages:
The high-throughput coprecipitation device provided in the embodiment of the present application carries liquid pump, switching on main body frame
It distributes valve group, distribution needle group, coprecipitation reaction module and central control system and constitutes Fully automated synthesis device；Specifically,
The distribution network based on liquid pump, switching distribution valve group and distribution needle group is established, and distribution needle group is corresponded into co-precipitation instead
Answer the one-to-one arrangement of module, by liquid pump and switching distribution valve group realize each coprecipitation reaction module reagent quantitative addition and
Type switching；That is, forming the solidification distribution structure for corresponding to coprecipitation reaction module, needed to switch reagent according to reaction
Type and quantity promote the stability of assignment accuracy and sendout.In compared with the existing technology, by distribution needle group and infusion pipeline
The solidification distribution network of the mode of operation of the fixed fixed point addition that moves in circles on the robotic arm, the application can be avoided mechanical reciprocating
Addition precision deterioration caused by the vibration and pipeline deformation of movement squeeze, additive amount is unstable and infusion pipeline service life is bad
The problem of change.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of high-throughput coprecipitation device provided in an embodiment of the present invention；
Fig. 2 is the structural schematic diagram of coprecipitation reaction module provided in an embodiment of the present invention；
Fig. 3 is the structural schematic diagram of PH probe correction module provided in an embodiment of the present invention；
Fig. 4 is the structural schematic diagram of switching distribution valve group provided in an embodiment of the present invention.
Specific embodiment
The embodiment of the present application is solved high-throughput coprecipitated in the prior art by providing a kind of high-throughput coprecipitation device
The technical issues of shallow lake synthesizer reagent assignment accuracy is low, and sendout is unstable, and perfusion tube Louis leaks.
In order to better understand the above technical scheme, in conjunction with appended figures and specific embodiments to upper
It states technical solution to be described in detail, it should be understood that the specific features in the embodiment of the present invention and embodiment are to the application skill
The detailed description of art scheme, rather than the restriction to technical scheme, in the absence of conflict, the embodiment of the present application
And the technical characteristic in embodiment can be combined with each other.
Referring to Fig. 1, a kind of high throughput coprecipitation device, comprising: main body frame 1, liquid pump 2, switching distribution valve group
11, needle group, coprecipitation reaction module 9 and central control system are distributed.
It is specifically described below.
The liquid pump 2 is fixed on the main body frame 1, switching distribution valve group 11 by liquid feeding pipeline with it is described
Liquid pump 2 is connected, and the switching distribution valve group 11 is connected by distribution circuit with the distribution needle group；To form distribution net
Network.
That is, the reagent that liquid pump 2 exports is sent to the switching via the liquid feeding pipeline and distributes valve group 11, lead to
It crosses the switching distribution valve group 11 and carries out type switching and flow adjusting, corresponding distribution needle is then assigned to by distribution circuit
Group is added to corresponding coprecipitation reaction module 9.
It is worth noting that in general, the quantity of the fixed coprecipitation reaction module 9 on the main body frame 1
It is 8 in the present embodiment to be multiple；Each coprecipitation reaction module 9 corresponding distribution needle group in the present embodiment, is total to
Needle group is distributed described in being provided with 8 groups；Distributing valve group 11 by the switching, quantitative be connected corresponds to liquid pump 2 on demand, realizes a certain
The quantitative addition of reagent.To avoid carrying distribution needle group in the prior art by mechanical arm and draw in reagent storage module
Reagent is then moved to the Complicated Flow that a certain coprecipitation reaction module 9 discharges reagent, greatly improves operating efficiency；It is more important
, avoid reagent and draw, shift, during release, made since pipeline residual, vibration and pipeline deformation squeeze overflow etc.
At reagent loss, thus ensure that reagent addition precision and quantity stability and reliability.
On the other hand, control structure is also simplified, the requirement of positioning accuracy is reduced；Meanwhile also avoiding infusion pipeline
The problems such as friction in the operation to move in circles, tubing caused by extruding etc. is damaged, and reagent leaks.
In general, the distribution needle group is removably attached in the coprecipitation reaction module 9, and the co-precipitation is anti-
Module 9 is answered to be fixed on the main body frame 1；So as to realize convenient taking-up and investment in operation.
The liquid pump 2, switching distribution valve group 11 and the coprecipitation reaction module 9 are controlled with the center respectively
System processed is connected；It is uniformly controlled to realize, promotes mutually coordinated property and operating efficiency.
Further, high-throughput coprecipitation device further include: two axis robots and PH probe 5；The two axis machine
Tool hand is fixed on the main body frame 1, and the PH probe is fixed in two axis robot；So as to follow described two
Axis robot adjusts upward the position of PH probe 5 in two axis, so that fixed point monitoring corresponds to the PH in coprecipitation reaction module 9
Value.Two axis robot and the PH probe 5 are connected with the central control system respectively, and realization is uniformly controlled, and coordinate each
The operation of module.
It is worth noting that the shift motion of two axis robots described in the present embodiment be it is laterally and vertical, i.e., according to three
Coordinate system is tieed up, is X-direction and Z-direction.
Further, two axis robot includes: X-axis system, Z axis system 3 and cantilever 4；The X-axis system is fixed
On the main body frame 1, X-direction, the Z axis system are set generally along the arrangement mode of multiple coprecipitation reaction modules 9
System 3 is fixed on the mobile terminal of the X-axis system, and the cantilever 4 is fixed on the mobile terminal of the Z axis system 3；To realize
The selection of multiple coprecipitation reaction modules 9.
The X-axis system and the Z axis system 3 are connected with the central control system respectively, realize and are uniformly coordinated control
System.
Further, high-throughput coprecipitation device further include: PH probe cleans calibration module 8；PH probe cleans school
Quasi-mode block 8 is fixed on the main body frame 1, the cleaning, drying and calibration for PH probe 5.
Referring to Fig. 3, the PH probe correction module 8 includes: the probe cleaning assembly 8- being fixed on the main body frame 1
2, probe dry component 8-3, probe correction container 8-1 and the calibration solution to set within it.PH probe 5 cleans group by probe
Part 8-2 cleaning, then dry via probe dry component 8-3, probe correction container 8-1 carries out calibration operation.
In general, the cavity for being provided with cleaning solution can be used in probe cleaning assembly 8-2, and probe dry component 8-3 can be adopted
It is dry with sky, air drying structure can also be used.
Further, the high-throughput coprecipitation device further include: distribution needle cleaning module 10；The distribution needle is clear
Mold cleaning block 10 is fixed on the main body frame 1；Wherein, it is all provided between two of the arbitrary neighborhood coprecipitation reaction modules 9
It is equipped with the distribution needle cleaning module 10, consequently facilitating distributing the cleaning of needle group and keeping in.It can certainly be described total with two
Precipitation reaction module 9 is one group of reaction module, and a distribution needle cleaning module 10 is arranged between adjacent two sufficient reaction modules,
While to guarantee use demand, simplify platform layout.
The distribution needle cleaning module 10 is mainly the cleaning solution cavity being arranged on main body frame, built-in cleaning solution.
Further, high-throughput coprecipitation device is stated further include: reaction kettle keeps in support 7；The reaction kettle is temporary
Support 7 is fixed on the main body frame 1, for temporarily temporary reaction kettle.
Referring to Fig. 3, the switching distribution valve group includes: switching valve 11-2 and distributing valve 11-1；The switching valve 11-2's
Input terminal is connected by the liquid feeding pipeline with the liquid pump 2, the output end of the switching valve 11-2 and the distributing valve 11-
1 input terminal is connected, and the output end of the distributing valve 11-1 is connected by the distribution circuit with the distribution needle group.
To first pass through switching valve 11-2 gating liquid pump 2 and corresponding coprecipitation reaction module when executing reagent addition
9, flow is then adjusted by distributing valve 11-1.
It should be noted that each liquid distribution passage is using the control of liquid pump 2 (such as 48 according to enough pumps
Channel need to use 48 liquid pumps), then it can also be without using switching distribution valve group 11.But such situation installation cost and complexity
It will sharply increase, simultaneously, during actual use can be reduced by the adjustment of experimental technique to each channel independent control
It is required that.To reduce installation cost and complexity, this example controls multiple groups liquid distribution passage scheme using a liquid pump 2.
Switching distribution valve group 11 integrates seven switching valve 11-2 and eight distributing valve 11-1.Distributing valve 11-1 can be realized all the way to six road liquid
Body assignment channel evenly distributes；Switching valve 11-2, which can be realized, all the way switches the liquid distribution passage on eight tunnels.Six of them is cut
It changes valve 11-2 to connect with six liquid pumps 2, and connects simultaneously with the independent distribution fluid passage in eight groups of coprecipitation reaction modules 9
It is logical.One of switching valve 11-2 is connect with a liquid pump 2, while passing through eight distributing valve 11-1 and eight groups of coprecipitation reactions
Equivalent distribution fluid passage connection in module 9.
Referring to fig. 2, the coprecipitation reaction module 9 includes: top cover 9-1, coolant seal lid 9-2, understructure, heating knot
Structure 9-3 and electromagnetic agitation structure 9-4.
The distribution needle group is fixed on the top cover 9-1, and the top cover 9-1 is removably fastened on the coolant seal
It covers on 9-2；That is, fixed structure of the top cover 9-1 as the distribution needle group, on the one hand realizes consolidating for distribution needle group
It is fixed, it on the other hand also can be convenient for operation distribution needle group.
In general, the groove with top cover 9-1 cooperation is opened up at the top of the coolant seal lid 9-2, convenient for fixing
It fastens.
The understructure includes: pedestal and the reaction kettle 9-5 being arranged in the pedestal；The pedestal is fixed on institute
It states in main body frame 1.
The coolant seal lid 9-2 fixation seals the reaction kettle 9-5 on the base, and is provided with and the distribution
The corresponding liquid injection port of needle group；It is additionally provided with the through-hole passed through for the PH probe 5, and the note is sealed by rubber sealing film etc.
Liquid mouth and the through-hole.
The heating structure 9-3 is fixed on the base, and is connected with the central control system, guarantees reaction temperature
Degree；The bottom of heating structure 9-3, for being heated to reaction kettle 9-5.Heating cushion can be used to be heated, oil can also be used
Bath is heated.Heating structure 9-3 accurately controls heating temperature at 40~100 DEG C.It should be noted that heating structure 9-3
It is heated according to heating pad mode, heating cushion may also set up two sides or surrounding in reaction kettle 9-5, to realize to reaction kettle
9-5 and experimental solutions therein carry out quick heating as uniform as possible.
The electromagnetic agitation structure 9-4 setting on the base, and is connected with the central control system, realizes electromagnetism
Stirring, is generally arranged stirrer in the reaction kettle 9-5.
Further, the coolant seal lid 9-2 includes: sealing cover, heat insulating mattress and cooling system；The liquid injection port is set
It sets on the sealing cover, is located above the reaction kettle 9-5；The heat insulating mattress is arranged on the bottom face of the sealing cover；
Wherein, the cooling system includes: cooling tube；The cooling tube is fixed on the top cover bottom face, is located at the reaction kettle
Right above 9-5, and it is connected with the central control system；It opens up on the heat insulating mattress and is matched with the kettle mouth of the reaction kettle 9-5
Hole；The liquid injection port is connected to the hole that the heat insulating mattress opens up, and the cooling tube that is staggered is distributed on the top cover.
The cooling tube can be realized condensing reflux function, to guarantee coprecipitation reaction solution vapor in a heated state
It does not escape out；Cooling medium is filled in cooling tube.
One or more technical solutions provided in the embodiments of the present application have at least the following technical effects or advantages:
The high-throughput coprecipitation device provided in the embodiment of the present application carries liquid pump, switching on main body frame
It distributes valve group, distribution needle group, coprecipitation reaction module and central control system and constitutes Fully automated synthesis device；Specifically,
The distribution network based on liquid pump, switching distribution valve group and distribution needle group is established, and distribution needle group is corresponded into co-precipitation instead
Answer the one-to-one arrangement of module, by liquid pump and switching distribution valve group realize each coprecipitation reaction module reagent quantitative addition and
Type switching；That is, forming the solidification distribution structure for corresponding to coprecipitation reaction module, needed to switch reagent according to reaction
Type and quantity promote the stability of assignment accuracy and sendout.In compared with the existing technology, by distribution needle group and infusion pipeline
The solidification distribution network of the mode of operation of the fixed fixed point addition that moves in circles on the robotic arm, the application can be avoided mechanical reciprocating
Addition precision deterioration caused by the vibration and pipeline deformation of movement squeeze, additive amount is unstable and infusion pipeline service life is bad
The problem of change.
It should be noted last that the above specific embodiment is only used to illustrate the technical scheme of the present invention and not to limit it,
Although being described the invention in detail referring to example, those skilled in the art should understand that, it can be to the present invention
Technical solution be modified or replaced equivalently, without departing from the spirit and scope of the technical solution of the present invention, should all cover
In the scope of the claims of the present invention.
Claims (10)
1. a kind of high throughput coprecipitation device characterized by comprising main body frame, liquid pump, switching distribution valve group,
Distribute needle group, coprecipitation reaction module and central control system；
The liquid pump is fixed on the main body frame, and the switching distribution valve group passes through liquid feeding pipeline and the liquid pump phase
Even, the switching distribution valve group is connected by distribution circuit with the distribution needle group；
The distribution needle group is removably attached in the coprecipitation reaction module, and the coprecipitation reaction module is fixed on institute
It states on main body frame；
The liquid pump, the switching distribution valve group and the coprecipitation reaction module respectively with the central control system phase
Even.
2. high throughput coprecipitation device as described in claim 1, which is characterized in that high-throughput coprecipitation device is also
It include: two axis robots and PH probe；
Two axis robot is fixed on the main body frame, and the PH probe is fixed in two axis robot；
Two axis robot and the PH probe are connected with the central control system respectively.
3. high throughput coprecipitation device as claimed in claim 2, which is characterized in that two axis robot includes: X-axis
System, Z axis system and cantilever；
The X-axis system is fixed on the main body frame, and the Z axis system is fixed on the mobile terminal of the X-axis system, institute
Cantilever is stated to be fixed on the mobile terminal of the Z axis system；
The X-axis system and the Z axis system are connected with the central control system respectively.
4. high throughput coprecipitation device as claimed in claim 2, which is characterized in that high-throughput coprecipitation device is also
It include: PH probe cleaning calibration module；
PH probe cleaning calibration module is fixed on the main body frame.
5. high throughput coprecipitation device as claimed in claim 4, which is characterized in that the PH probe correction module packet
It includes: probe cleaning assembly, probe dry component, probe correction container and the calibration being arranged in the probe correction container
Liquid.
6. high throughput coprecipitation device as described in claim 1, which is characterized in that the high throughput coprecipitation dress
It sets further include: distribution needle cleaning module；
The distribution needle cleaning module is fixed on the main body frame；
Wherein, the distribution needle cleaning module is provided between two of the arbitrary neighborhood coprecipitation reaction modules.
7. high throughput coprecipitation device as described in claim 1, which is characterized in that state high-throughput coprecipitation device
Further include: reaction kettle keeps in support；
The reaction kettle is kept in support and is fixed on the main body frame.
8. high throughput coprecipitation device as described in any one of claims 1 to 7, which is characterized in that the switching distribution
Valve group includes: switching valve and distributing valve；
The input terminal of the switching valve is connected by the liquid feeding pipeline with the liquid pump, the output end of the switching valve and institute
The input terminal for stating distributing valve is connected, and the output end of the distributing valve is connected by the distribution circuit with the distribution needle group.
9. high throughput coprecipitation device as claimed in claim 8, which is characterized in that the coprecipitation reaction module packet
It includes: top cover, coolant seal lid, understructure, heating structure and electromagnetic agitation structure；
The distribution needle group is fixed on the top cover, and the top cover is removably fastened on the coolant seal and covers；
The understructure includes: pedestal and the reaction kettle that is arranged in the pedestal；
The coolant seal lid fixation seals the reaction kettle on the base, and is provided with corresponding with the distribution needle group
Liquid injection port；
The heating structure is fixed on the base, and is connected with the central control system；
The electromagnetic agitation structure setting on the base, and is connected with the central control system.
10. high throughput coprecipitation device as claimed in claim 9, which is characterized in that the coolant seal lid includes: close
Capping, heat insulating mattress and cooling system；
The liquid injection port is arranged on the sealing cover, is located above the reaction kettle；
The heat insulating mattress is arranged on the bottom face of the sealing cover；
Wherein, the cooling system includes: cooling tube；
The cooling tube is fixed on the top cover bottom face, is located at right above the reaction kettle, and is with the center control
System is connected；
The matched hole of kettle mouth with the reaction kettle is opened up on the heat insulating mattress；
The liquid injection port is connected to the hole that the heat insulating mattress opens up, and the cooling tube that is staggered is distributed on the top cover.
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| WO2013044454A1 (en) * | 2011-09-27 | 2013-04-04 | 深圳市亚辉龙生物科技有限公司 | Full-automatic immunity analyzer and detection method thereof |
| CN106574267A (en) * | 2014-08-15 | 2017-04-19 | 考希尔股份有限公司 | High-throughput sample processing systems and methods of use |
| CN204556649U (en) * | 2015-03-24 | 2015-08-12 | 江苏华爵检测技术股份有限公司 | A kind of gas analysis cabinet |
| CN207703559U (en) * | 2017-11-23 | 2018-08-07 | 中国大唐集团科学技术研究院有限公司西北分公司 | A kind of selective-catalytic-reduction denitrified system entrance flue gas multi-point sampling device |
| CN109226766A (en) * | 2018-08-07 | 2019-01-18 | 北京科技大学 | A kind of device and method that high throughput prepares metal-base composites |
| CN210252274U (en) * | 2019-06-26 | 2020-04-07 | 浙江优通自动化技术有限公司 | High-flux coprecipitation synthesizer |
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