CN110117913A - A kind of dyeing liquid and preparation method thereof of natural herb drug - Google Patents
A kind of dyeing liquid and preparation method thereof of natural herb drug Download PDFInfo
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- CN110117913A CN110117913A CN201910429331.XA CN201910429331A CN110117913A CN 110117913 A CN110117913 A CN 110117913A CN 201910429331 A CN201910429331 A CN 201910429331A CN 110117913 A CN110117913 A CN 110117913A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
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Abstract
The present invention relates in a kind of dyeing liquid and preparation method thereof of natural herb drug, including production wormwood dye liquor step, extracts wormwood essential oil step and prepare dyeing liquor step；Production wormwood dye liquor step includes: cleaning wormwood leaf step, crushes wormwood leaf step, impregnates wormwood leaf step, wormwood pigment coarse extraction step, the thin extraction step of wormwood pigment.Extracting wormwood essential oil step includes: that wormwood leaf is dried step, wormwood leaf pulverization process step, it prepares dyeing liquor step: the wormwood dye liquor and the wormwood essential oil being taken and mixed according to the ratio of 10:1, is sufficiently stirred to obtain dyeing liquor after preservative and mordant is added.The stin of thickness that dyeing liquid and preparation method thereof according to above-mentioned natural herb drug obtains is moderate, yield is high.It is appropriate comprising wormwood dye liquor and wormwood essential oil ratio in dyeing liquor, it ensure that the excellent medicinal efficacy of dyeing liquor while guaranteeing that dyeing liquor pigment is pure.
Description
Technical field
The present invention relates to the fields that herbal drug extracts essential oil, more particularly to a kind of dyeing liquor system of natural herb drug
Preparation Method.
Background technique
Wormwood is a kind of herbaceos perennial, and plant has enhanced aroma.Wormwood can be used as medicine, and have Wen Jing, dry, dissipate
Tremble with fear, hemostasis, anti-inflammatory, relieving asthma, cough-relieving, miscarriage prevention, antiallergy the effects of.Wormwood essential oil is extracted from the leaf of wormwood, stalk
A kind of volatile flavor, generally pale yellow or green-yellow have warming and activating meridian, qi and activate blood circulation, cold-dispelling pain-relieving, improve part
Circulation, the effect for increasing immunity are usually used in smearing acupuncture point or affected part, and rubbing extremely absorbs repeatedly.The ingredient of wormwood essential oil is with small
Based on molecule volatility terpenoid, in addition there are aliphatic compounds, small molecule aromatic compound.
Using the characteristic of wormwood essential oil, wormwood essential oil can be applied in life, the textile fabric such as containing wormwood essential oil can
To play the role of mosquito repellent, clearing damp, antiallergy, increase immunity.
However, essential oil yield that the extracting method of existing wormwood essential oil obtains is lower, purity is lower and to wormwood
Utilization rate is low.And the combination of the wormwood essential oil and textile fabric in the existing textile fabric containing wormwood essential oil is not close, Sojourn times
Between it is short, volatile, the textile fabric containing wormwood essential oil easily loses effect.
Summary of the invention
Based on this, it is necessary to for wormwood essential oil and textile fabric combination is close, residence time is short, volatile, volatile
The problem of going effect provides a kind of dyeing liquid and preparation method thereof and preparation method thereof of natural herb drug.
A kind of dyeing liquid and preparation method thereof of natural herb drug, the dyeing liquid and preparation method thereof of the natural herb drug include system
Make wormwood dye liquor step, extracts wormwood essential oil step, prepares dyeing liquor step and soaking and dyeing step；
Making wormwood dye liquor step includes:
Wormwood leaf step is cleaned, fresh wormwood Ye Bingyong cleaning solution is taken to clean up；
Wormwood leaf step is crushed, clean fresh wormwood leaf is shredded；
Wormwood leaf step is impregnated, by the wormwood leaf crushed according to small in immersion 5 in the ratio addition cleaning solution of material-water ratio 1:15
Up to 8 hours, and 60 degrees Celsius to 90 degrees Celsius are heated to, obtain soak；
Soak is placed in ultrasonic extractor and handles 0.5 hour to 1 hour by wormwood pigment coarse extraction step, using
100 mesh screens obtain crude wormwood pigment solution；
Sodium bicarbonate is added to crude wormwood pigment solution with the ratio of 2g/L, after being sufficiently stirred in the thin extraction step of wormwood pigment
Purification wormwood pigment is obtained by 460 mesh screens, concentration purification wormwood pigment solution obtains the wormwood that concentration is 50g/L and contaminates
Liquid；
Extracting wormwood essential oil step includes:
Wormwood leaf is dried step, and clean fresh wormwood leaf is carried out processing of drying in the shade；
Wormwood leaf pulverization process step obtains wormwood leaf powder by the wormwood leaf pulverization process dried in the shade and by 10 meshes；
Wormwood leaf powder step is extracted, sodium-chloride water solution will be added in wormwood leaf powder and repeatedly after diacolation, lead in percolator
Crossing soxhlet extraction, extracting obtains obtained by crude extractions liquid repeatedly by the progress of the mixture of filtrate and filter residue, dehydrated alcohol is added crude
In extracting solution, and the obtained by crude extractions liquid that dehydrated alcohol is added is placed in ultrasonic extractor and is handled 0.5 hour to 1 hour,
By treated, obtained by crude extractions liquid obtains refining extracting solution by 460 mesh screens；
Purification extracting solution is added centrifugal filtration in refrigerated centrifuge, obtains wormwood essential oil by extracting solution filtration treatment step；
It prepares dyeing liquor step: the wormwood dye liquor and the wormwood essential oil being taken and mixed according to the ratio of 10:1, anti-corrosion is added
It is sufficiently stirred to obtain dyeing liquor after agent and mordant.
The wormwood leaf crushed is added in cleaning solution according to the ratio of material-water ratio 1:15 in one of the embodiments,
It impregnates 6 hours to 7 hours, and is heated to 70 degrees Celsius to 80 degrees Celsius, obtain soak.
The wormwood leaf crushed is added in cleaning solution according to the ratio of material-water ratio 1:15 in one of the embodiments,
It impregnates 7 hours, and is heated to 75 degrees Celsius, obtain soak.
It, will be in the filter residue fallen by 100 mesh screens in one of the embodiments, in wormwood pigment coarse extraction step
The cleaning solution that 3 times of quality are added boils 1 hour to 2 hours in pressure cooker, is during which stirred 3 to 5 times with no bacteria stick, the filter that will be obtained
Slag solution passes through 100 mesh screens at high temperature and obtains wormwood filter residue pigment, obtains crude wormwood pigment solution after cooling.
In one of the embodiments, before being cleaned using cleaning liquid to fresh wormwood leaf, first removed using wax
Liquid carries out wax removal to fresh wormwood leaf.
The wax removal liquid includes following component by weight percentage: percarbonic acid in one of the embodiments,
Sodium 60%~80%, neopelex 2%~5%, sodium alkyl sulfonate 1%~3%, fatty acid methyl ester sulfonate 1%
~4%, fat alcohol polyethylene ether sulfate 1%~5%, manganese sulfate 0.2%~1%, anhydrous sodium sulfate 10%~15%, peppermint
Alcohol 0.5%~1%；Wherein, the carbon atom number of alkyl is 5~15 in sodium alkyl sulfonate, and surplus is water.
Carbon atom number fatty acid-based in fatty acid methyl ester sulfonate is 5~12 in one of the embodiments,.
The carbon atom number of fatty alcohol radical is 5~12 in fat alcohol polyethylene ether sulfate in one of the embodiments,.
Dyeing liquor pH value step is adjusted in one of the embodiments: by the pH value adjustment of dyeing liquor to 6 to 6.5.
The concentration of the sodium bicarbonate solution is 0.3mol/L in one of the embodiments,.
The dyeing liquid and preparation method thereof of above-mentioned natural herb drug is high to the utilization rate of wormwood, according to above-mentioned natural herb drug
The obtained stin of thickness of dyeing liquid and preparation method thereof is moderate, yield is high.It include wormwood dye liquor and wormwood essential oil ratio in dyeing liquor
Example is appropriate, ensure that the excellent medicinal efficacy of dyeing liquor while guaranteeing that dyeing liquor pigment is pure.The dye of natural herb drug
The textile that the dyeing liquor that color liquid and preparation method thereof obtains dyes, color is excellent, has mosquito repellent, clearing damp, antiallergy, increases immunity
Effect.Also, the dyeing liquor that the dyeing liquid and preparation method thereof of natural herb drug obtains and textile fabric are tightly combined, residence time
Long, not volatile.
Detailed description of the invention
Fig. 1 is the flow diagram of the dyeing liquid and preparation method thereof of natural herb drug in one embodiment；
Fig. 2 is the flow diagram that wormwood dye liquor step is made in one embodiment；
Fig. 3 is the flow diagram that wormwood essential oil step is extracted in another embodiment.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to the accompanying drawings and embodiments, right
The present invention is further elaborated.It should be appreciated that specific embodiment described herein is only used to explain the present invention, not
For limiting the present invention.
Also referring to Fig. 1 to Fig. 3, the present invention provides a kind of dyeing liquid and preparation method thereof 10 of natural herb drug, the day
The dyeing liquid and preparation method thereof 10 of right herbal drug includes production wormwood dye liquor step 100, extracts wormwood essential oil step 200, preparation
Dyeing liquor step 300 and soaking and dyeing step 400.
Making wormwood dye liquor step 100 includes:
Step 101: cleaning wormwood leaf, specifically, fresh wormwood Ye Bingyong cleaning solution is taken to clean up.
It should be noted that fresh wormwood leaf is cleaned up the wormwood dye liquor for avoiding and extracting, to adulterate other miscellaneous
Matter.As the raw material of wormwood dye liquor, the wormwood plant big using fresh branch fertilizer leaf is needed.Blade on healthy and strong wormwood plant
In chlorophyll content it is more abundant, to guarantee the yield of wormwood dye liquor, guarantee the wormwood dye liquor extracted have bright-coloured color
Pool.In order to guarantee generation redox reaction few as far as possible in the chlorophyll extraction process in wormwood blade, in the present embodiment,
Cleaning solution is deionized water.Deionized water is the pure water eliminated in after ionic species impurity.Without chemically in deionized water
Matter active anion and cation, the chlorophyll further avoided in wormwood blade occur redox reaction, guarantee
Chlorophyll in wormwood blade has more bright-coloured color.
In a further embodiment, first wormwood blade is cleaned with wax removal liquid, in the Chinese mugwort that will remove wax
Blade of grass piece is cleaned with deionized water.It includes following component by weight percentage: SODIUM PERCARBONATE 60% that wax, which removes liquid,
~80%, neopelex 2%~5%, sodium alkyl sulfonate 1%~3%, fatty acid methyl ester sulfonate 1%~4%,
Fat alcohol polyethylene ether sulfate 1%~5%, manganese sulfate 0.2%~1%, anhydrous sodium sulfate 10%~15%, menthol
0.5%~1%, surplus is water；Wherein, the carbon atom number of alkyl is 5~15 in sodium alkyl sulfonate, in fatty acid methyl ester sulfonate
Fatty acid-based carbon atom number is 5~12, and the carbon atom number of fatty alcohol radical is 5~12 in fat alcohol polyethylene ether sulfate.Wax
Matter removal liquid disinfectant biocidal efficacies are high, environmentally protective, easy to use, and the organophosphorus pesticide of wormwood blade surface can be made fast
Prompt drop solution eliminates efficiency up to 99% or more；There are surface active function abundant and disinfection and sterilization effect simultaneously, can wash simultaneously
Net greasy residues sufficiently remove wax, remove effectively the impurity and pesticide residue of wormwood blade surface, ensure that wormwood contaminates
Liquid it is hygienic and healthy and safe.
Step 103: wormwood leaf is crushed, specifically, clean fresh wormwood leaf is shredded.
It should be noted that by clean fresh wormwood leaf chopping so that carrying out immersion and color to fresh wormwood leaf
When plain coarse extraction, the chlorophyll in fresh wormwood leaf can smoothly be overflowed from blade, improve the effect of the extraction to wormwood dye liquor
Rate.Specifically, being crushed using sterile knife to fresh wormwood blade during crushing wormwood leaf, to guarantee extracting Chinese mugwort
Wormwood blade not will receive the infection of fungi and bacterium during careless dye liquor, avoid being treated in journey to wormwood blade
Wormwood blade is putrid and deteriorated.Further, the size for the fragment that fresh wormwood blade is ground into is less than 1 square centimeter.Another
In outer embodiment, cutting and grinding are carried out to fresh wormwood blade using the careless machine that chops after disinfection.Chop careless machine to fresh wormwood leaf
Piece is cut high-efficient, and the leaf blade size cut out is uniform.
Step 105: wormwood leaf is impregnated, specifically, the wormwood leaf crushed is added clearly according to the ratio of material-water ratio 1:15
It is being impregnated 5 hours to 8 hours in washing lotion, and is being heated to 60 degrees Celsius to 90 degrees Celsius, obtaining soak.
It should be noted that the wormwood leaf crushed is heated immersion in cleaning solution to be further convenient for fresh wormwood
Chlorophyll in leaf can be smoothly diffused into cleaning solution from blade, be prepared for the pigment coarse extraction of next step wormwood.Another
In one embodiment, by the wormwood leaf crushed according to 6 hours to 7 small in immersion in the ratio addition cleaning solution of material-water ratio 1:15
When, and 70 degrees Celsius to 80 degrees Celsius are heated to, obtain soak.In other embodiments, by the wormwood leaf crushed according to
The ratio of material-water ratio 1:15, which is added in cleaning solution, is impregnating 7 hours, and is heated to 75 degrees Celsius, obtains soak.
Step 107: wormwood pigment coarse extraction is handled 0.5 hour specifically, soak is placed in ultrasonic extractor
To 1 hour, using 100 mesh screens, crude wormwood pigment solution is obtained.
It should be noted that ultrasonic extractor can produce consumingly mechanical oscillation to destroy the group of wormwood leaf fragment
Knitting structure is diffused into chlorophyll in cleaning solution from blade.By concussion treated soak using 100 meshes
The crude wormwood pigment solution obtained after filtering can fall the wormwood leaf residue filter of the overwhelming majority.In other embodiment
In, it will treated that soak obtains crude wormwood pigment solution after 120 mesh screens by concussion.In other embodiments
In, it will treated that soak obtains crude wormwood pigment solution after 80 mesh screens by concussion.A reality wherein
It applies in example, in wormwood pigment coarse extraction step, the every processing of ultrasonic extractor five minutes is stirred 1 minute with no bacteria stick, to increase
Add ultrasonic extractor to the demolition effect of the institutional framework of wormwood leaf fragment, improves the utilization rate to wormwood leaf fragment.It improves
The pigment concentration of crude wormwood pigment solution.
In order to further improve the utilization rate to wormwood leaf fragment, the yield of crude wormwood pigment solution is improved, at it
In middle one embodiment, in wormwood pigment coarse extraction step, 3 times of quality will be added in the filter residue fallen by 100 mesh screens
Cleaning solution boil 1 hour to 2 hours in pressure cooker, during which stirred 3 to 5 times with no bacteria stick, by obtained filter residue solution in height
Temperature is lower to obtain wormwood filter residue pigment by 100 mesh screens, obtains crude wormwood pigment solution after cooling.In this way, to passing through 100
The filter residue that mesh screen falls further is utilized, and extracts crude wormwood pigment in the filter residue fallen by 100 mesh screens
Solution further increases the utilization rate to wormwood leaf fragment, improves the yield of crude wormwood pigment solution.
Step 109: wormwood pigment carefully extracts, specifically, carbonic acid is added to crude wormwood pigment solution with the ratio of 2g/L
Hydrogen sodium, obtains purification wormwood pigment by 460 mesh screens after being sufficiently stirred, and concentration purification wormwood pigment solution obtains concentration
For the wormwood dye liquor of 50g/L.
It should be noted that being analyzed by spectrophotometer crude wormwood pigment solution, being carried out to dyeing quality
Comparison, shows to extract wormwood pigment using sodium bicarbonate solution as extractant more appropriate.It is molten using sodium bicarbonate
Liquid is easier to extract wormwood pigment as extractant, and the pigment of obtained dye liquor is deeper, firmness is more preferable.Wherein one
In a embodiment, the concentration of the sodium bicarbonate solution is 0.25mol/L to 0.35mol/L.In another embodiment, institute
The concentration for stating sodium bicarbonate solution is 0.28mol/L to 0.32mol/L.In the present embodiment, the sodium bicarbonate solution is dense
Degree is 0.3mol/L.The purification wormwood pigment obtained by 460 mesh screens eliminates remaining wormwood residue, will refine wormwood
Pigment is concentrated to get the wormwood dye liquor that concentration is 50g/L.With the wormwood dye liquor of 50g/L to textile dyeing, the color of textile fabric
It is bright-coloured, firmness is good.
Extracting wormwood essential oil step 200 includes:
Step 201: wormwood leaf is dried, specifically, clean fresh wormwood leaf is carried out processing of drying in the shade.
It should be noted that the raw material as wormwood essential oil, needs the wormwood plant big using fresh branch fertilizer leaf.It is healthy and strong
Wormwood plant on blade in essential oil content it is more abundant, to guarantee the yield of wormwood essential oil.To fresh wormwood leaf into
Row dries in the shade before processing, needs to clean up fresh wormwood leaf with cleaning solution.In order to guarantee the wormwood essential oil in wormwood blade
Generation redox reaction few as far as possible in extraction process, in the present embodiment, cleaning solution is deionized water.Deionized water be except
It has gone in the pure water after ionic species impurity.Without the anion and cation that chemical property is active in deionized water, further
Redox reaction occurs for the derived essential oil avoided in wormwood blade.Clean fresh wormwood leaf is subjected to processing of drying in the shade, more
Protect to big degree the institutional framework and structural constituent of fresh wormwood leaf.
Step 203: wormwood leaf pulverization process, specifically, being obtained by the wormwood leaf pulverization process dried in the shade and by 10 meshes
Wormwood leaf powder.
It should be noted that the wormwood leaf to dry in the shade is in withered state, so the pole after by external force due to drying out
Easily crush, it is in the present embodiment, using stone roll that the wormwood leaf spreading dried in the shade is broken.Wormwood leaf is constantly stirred during spreading
Fragment.The wormwood fragment that spreading obtains is obtained wormwood leaf powder by 10 meshes to easily facilitate in the next steps from wormwood leaf
Middle extraction wormwood essential oil.
Step 205: extraction wormwood leaf powder, specifically, sodium-chloride water solution is added into wormwood leaf powder in percolator
In repeatedly after diacolation, the mixture of filtrate and filter residue is carried out by extracting repeatedly by soxhlet extraction and obtains obtained by crude extractions liquid, will
Dehydrated alcohol is added in obtained by crude extractions liquid, and the obtained by crude extractions liquid that dehydrated alcohol is added is placed in ultrasonic extractor and is handled
0.5 hour to 1 hour, by treated, obtained by crude extractions liquid obtained refining extracting solution by 460 mesh screens.
Become it should be noted that sodium-chloride water solution can be effectively prevented wormwood leaf powder corruption during diacolation
Matter.Using percolator to the mixture of sodium-chloride water solution and wormwood leaf powder repeatedly diacolation so that Chinese mugwort in wormwood leaf powder
Careless essential oil can pass through soxhlet extraction and extract.The mixture of filtrate and filter residue is carried out instead by soxhlet extraction
The yield and concentration of wormwood essential oil can be improved in multiple extracting.Obtained by crude extractions liquid is handled in ultrasonic extractor makes obtained by crude extractions
Blade residue in liquid can discharge wormwood essential oil as much as possible.Dehydrated alcohol is the fine solvent of wormwood essential oil, using nothing
It is more consummate that water-ethanol does the essential oil that extractant is extracted from obtained by crude extractions liquid.Through ultrasonic extractor treated obtained by crude extractions
Liquid can filter out most of folium artemisiae argyi residues by 460 meshes and obtain purification extracting solution.
Step 207: extracting solution filtration treatment obtains specifically, centrifugal filtration in refrigerated centrifuge is added in purification extracting solution
To wormwood essential oil；
It should be noted that in the present embodiment, centrifugal filtration in high speed freezing centrifuge is added in purification extracting solution.High speed cold
Freezing centrifuge can be by the big cell in purification extracting solution in remaining wormwood cell, wormwood cell fragment or wormwood cell
Device is all filtered out to obtain pure wormwood essential oil.
It prepares dyeing liquor step 300: the wormwood dye liquor and the wormwood essential oil being taken and mixed according to the ratio of 10:1, is added
It is sufficiently stirred to obtain dyeing liquor after entering preservative and mordant.
It is mixed it should be noted that taking the wormwood dye liquor and the wormwood essential oil according to what the ratio of 10:1 was mixed to get
Closing liquid both ensure that dyeing liquor had preferable depth of color, in turn ensure that dyeing liquor has sufficient medicinal ingredient.In this reality
It applies in example, for the preservative used for calcium propionate, calcium propionate is also highly stable to the property under strong light and under high temperature, is soluble in
Water, convenient for being sufficiently mixed, having a safety feature with dyeing liquor, guarantee dyeing liquor it is safe and healthy while to mould have it is excellent
Inhibiting effect.Mordant is used to increase the combination fastness of dyeing liquor Yu textile to be dyed.In the present embodiment, using acetic acid
Copper makees mordant, and copper acetate can kill virus while increasing the combination fastness of dyeing liquor and textile to be dyed, expelling parasite.
The dyeing liquid and preparation method thereof of above-mentioned natural herb drug is high to the utilization rate of wormwood, according to above-mentioned natural herb drug
The obtained stin of thickness of dyeing liquid and preparation method thereof is moderate, yield is high.It include wormwood dye liquor and wormwood essential oil ratio in dyeing liquor
Example is appropriate, ensure that the excellent medicinal efficacy of dyeing liquor while guaranteeing that dyeing liquor pigment is pure.Pass through above-mentioned natural herb
The textile containing natural herb drug that the dyeing liquid and preparation method thereof of drug obtains, color is excellent, has mosquito repellent, clearing damp, resists
Allergy, the effect for increasing immunity.Also, the dyeing liquor on the textile containing natural herb drug is tight in conjunction with textile fabric
Close, residence time long, it is not volatile, it is ensured that the textile containing natural herb drug has drug effect for a long time.
Each technical characteristic of above embodiments can be combined arbitrarily, for simplicity of description, not to above-described embodiment
In each technical characteristic it is all possible combination be all described, as long as however, the combination of these technical characteristics be not present lance
Shield all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of dyeing liquid and preparation method thereof of natural herb drug the method includes production wormwood dye liquor step, extracts wormwood
Essential oil step and prepare dyeing liquor step；
Making wormwood dye liquor step includes:
Wormwood leaf step is cleaned, fresh wormwood Ye Bingyong cleaning solution is taken to clean up；
Wormwood leaf step is crushed, clean fresh wormwood leaf is shredded；
Wormwood leaf step is impregnated, by the wormwood leaf crushed according to small in immersion 5 in the ratio addition cleaning solution of material-water ratio 1:15
Up to 8 hours, and 60 degrees Celsius to 90 degrees Celsius are heated to, obtain soak；
Soak is placed in ultrasonic extractor and handles 0.5 hour to 1 hour by wormwood pigment coarse extraction step, using
100 mesh screens obtain crude wormwood pigment solution；
Sodium bicarbonate is added to crude wormwood pigment solution with the ratio of 2g/L, after being sufficiently stirred in the thin extraction step of wormwood pigment
Purification wormwood pigment is obtained by 460 mesh screens, concentration purification wormwood pigment solution obtains the wormwood that concentration is 50g/L and contaminates
Liquid；
Extracting wormwood essential oil step includes:
Wormwood leaf is dried step, and clean fresh wormwood leaf is carried out processing of drying in the shade；
Wormwood leaf pulverization process step obtains wormwood leaf powder by the wormwood leaf pulverization process dried in the shade and by 10 meshes；
Wormwood leaf powder step is extracted, sodium-chloride water solution will be added in wormwood leaf powder and repeatedly after diacolation, lead in percolator
Crossing soxhlet extraction, extracting obtains obtained by crude extractions liquid repeatedly by the progress of the mixture of filtrate and filter residue, dehydrated alcohol is added crude
In extracting solution, and the obtained by crude extractions liquid that dehydrated alcohol is added is placed in ultrasonic extractor and is handled 0.5 hour to 1 hour,
By treated, obtained by crude extractions liquid obtains refining extracting solution by 460 mesh screens；
Purification extracting solution is added centrifugal filtration in refrigerated centrifuge, obtains wormwood essential oil by extracting solution filtration treatment step；
It prepares dyeing liquor step: the wormwood dye liquor and the wormwood essential oil being taken and mixed according to the ratio of 10:1, anti-corrosion is added
It is sufficiently stirred to obtain dyeing liquor after agent and mordant.
2. the dyeing liquid and preparation method thereof of natural herb drug according to claim 1, which is characterized in that the Chinese mugwort that will be crushed
Blade of grass is added in cleaning solution according to the ratio of material-water ratio 1:15 to be impregnated 6 hours to 7 hours, and is heated to 70 degrees Celsius to 80 and is taken the photograph
Family name's degree, obtains soak.
3. the dyeing liquid and preparation method thereof of natural herb drug according to claim 1, which is characterized in that the Chinese mugwort that will be crushed
Blade of grass is added in cleaning solution according to the ratio of material-water ratio 1:15 to be impregnated 7 hours, and is heated to 75 degrees Celsius, obtains soak.
4. the dyeing liquid and preparation method thereof of natural herb drug according to claim 1, which is characterized in that thick in wormwood pigment
In extraction step, the cleaning solution that 3 times of quality are added in the filter residue fallen by 100 mesh screens is boiled 1 hour to 2 in pressure cooker
Hour, it is during which stirred 3 to 5 times with no bacteria stick, obtained filter residue solution is passed through into 100 mesh screens at high temperature and obtains wormwood filter
Slag pigment obtains crude wormwood pigment solution after cooling.
5. the dyeing liquid and preparation method thereof of natural herb drug according to claim 1, which is characterized in that using cleaning liquid
Before cleaning to fresh wormwood leaf, wax removal first is carried out to fresh wormwood leaf using wax removal liquid.
6. the dyeing liquid and preparation method thereof of natural herb drug according to claim 5, which is characterized in that the wax removal
Liquid includes following component by weight percentage: SODIUM PERCARBONATE 60%~80%, neopelex 2%~5%, alkane
Base sodium sulfonate 1%~3%, fatty acid methyl ester sulfonate 1%~4%, fat alcohol polyethylene ether sulfate 1%~5%, manganese sulfate
0.2%~1%, anhydrous sodium sulfate 10%~15%, menthol 0.5%~1%, surplus is water；Wherein, alkane in sodium alkyl sulfonate
The carbon atom number of base is 5~15.
7. the dyeing liquid and preparation method thereof of natural herb drug according to claim 6, which is characterized in that fatty acid methyl ester sulphur
Fatty acid-based carbon atom number is 5~12 in hydrochlorate.
8. the dyeing liquid and preparation method thereof of natural herb drug according to claim 6, which is characterized in that fatty alcohols polyethylene
The carbon atom number of fatty alcohol radical is 5~12 in ether sulfate.
9. the dyeing liquid and preparation method thereof of natural herb drug according to claim 1, which is characterized in that adjust dyeing liquor PH
It is worth step: by the pH value adjustment of dyeing liquor to 6 to 6.5.
10. special according to claim 1 to the dyeing liquid and preparation method thereof of natural herb drug described in any claim in 9
Sign is that the concentration of the sodium bicarbonate solution is 0.3mol/L.
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Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08109346A (en) * | 1994-10-07 | 1996-04-30 | Yuki Soken:Kk | Ink using natural dye |
| CN102422875A (en) * | 2011-11-22 | 2012-04-25 | 江南大学 | Method for preprocessing Asiatic wormwood to preserve color in combination with quick-freezing and unfreezing for keeping quality |
| CN102505533A (en) * | 2011-09-27 | 2012-06-20 | 通亿（泉州）轻工有限公司 | Dyeing and finishing method of dyed knitted cotton underwear fabric with tarragon delicate fragrance and mosquito-repelling and cleaning functions |
| CN105586445A (en) * | 2015-12-22 | 2016-05-18 | 广州番禺职业技术学院 | Real leather manufacturing method |
| CN106835769A (en) * | 2017-01-23 | 2017-06-13 | 湖南工程学院 | Folium artemisiae argyi colouring substance is in cellulose fibre with the application in bath mordant dyeing technique |
| CN106967514A (en) * | 2017-04-13 | 2017-07-21 | 河南骏化发展股份有限公司 | A kind of SODIUM PERCARBONATE powdered cleanser and its preparation method and application |
| CN107028859A (en) * | 2016-12-19 | 2017-08-11 | 哈尔滨灵草舒生物科技有限公司 | A kind of orchid skin protection bath cream and preparation method thereof |
| CN108456594A (en) * | 2018-05-07 | 2018-08-28 | 南召留山岭南艾叶制品有限公司 | A kind of extracting method of high yield wormwood essential oil |
| CN108486917A (en) * | 2018-04-19 | 2018-09-04 | 际华三五四三针织服饰有限公司 | Organic cotton fabrics Chinese mugwort liquid dyeing |
-
2019
- 2019-05-22 CN CN201910429331.XA patent/CN110117913A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08109346A (en) * | 1994-10-07 | 1996-04-30 | Yuki Soken:Kk | Ink using natural dye |
| CN102505533A (en) * | 2011-09-27 | 2012-06-20 | 通亿（泉州）轻工有限公司 | Dyeing and finishing method of dyed knitted cotton underwear fabric with tarragon delicate fragrance and mosquito-repelling and cleaning functions |
| CN102422875A (en) * | 2011-11-22 | 2012-04-25 | 江南大学 | Method for preprocessing Asiatic wormwood to preserve color in combination with quick-freezing and unfreezing for keeping quality |
| CN105586445A (en) * | 2015-12-22 | 2016-05-18 | 广州番禺职业技术学院 | Real leather manufacturing method |
| CN107028859A (en) * | 2016-12-19 | 2017-08-11 | 哈尔滨灵草舒生物科技有限公司 | A kind of orchid skin protection bath cream and preparation method thereof |
| CN106835769A (en) * | 2017-01-23 | 2017-06-13 | 湖南工程学院 | Folium artemisiae argyi colouring substance is in cellulose fibre with the application in bath mordant dyeing technique |
| CN106967514A (en) * | 2017-04-13 | 2017-07-21 | 河南骏化发展股份有限公司 | A kind of SODIUM PERCARBONATE powdered cleanser and its preparation method and application |
| CN108486917A (en) * | 2018-04-19 | 2018-09-04 | 际华三五四三针织服饰有限公司 | Organic cotton fabrics Chinese mugwort liquid dyeing |
| CN108456594A (en) * | 2018-05-07 | 2018-08-28 | 南召留山岭南艾叶制品有限公司 | A kind of extracting method of high yield wormwood essential oil |
Non-Patent Citations (5)
| Title |
|---|
| 中国科学技术协会主编: "《纺织科学技术学科发展报告 2016-2017》", 31 March 2018, 中国科学技术出版社 * |
| 冯胜: "《精细化工新配方》", 30 April 2011, 广东科技出版社 * |
| 周启澄 等: "《中国传统植物染料现代研发与生态纺织技术》", 31 March 2015, 东华大学出版社 * |
| 尹卫平 等: "《精细化工产品及工艺》", 31 August 2009, 华东理工大学出版社 * |
| 柯贵珍 等: ""天然植物艾叶对毛织物的染色研究"", 《毛纺科技》 * |
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