CN103767026B - Method for preparing beverage by using peony root pigment - Google Patents
Method for preparing beverage by using peony root pigment Download PDFInfo
- Publication number
- CN103767026B CN103767026B CN201410019505.2A CN201410019505A CN103767026B CN 103767026 B CN103767026 B CN 103767026B CN 201410019505 A CN201410019505 A CN 201410019505A CN 103767026 B CN103767026 B CN 103767026B
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- Prior art keywords
- pigment
- peony root
- tree peony
- beverage
- subsequent use
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- 239000000049 pigment Substances 0.000 title claims abstract description 69
- 235000013361 beverage Nutrition 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims abstract description 17
- 241000736199 Paeonia Species 0.000 title abstract description 15
- 235000006484 Paeonia officinalis Nutrition 0.000 title abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 239000000706 filtrate Substances 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 230000032683 aging Effects 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims abstract description 13
- 238000002360 preparation method Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000002791 soaking Methods 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 5
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 62
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 62
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- 239000000284 extract Substances 0.000 claims description 9
- 238000011049 filling Methods 0.000 claims description 6
- 241000143437 Aciculosporium take Species 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 4
- 238000004108 freeze drying Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 238000002390 rotary evaporation Methods 0.000 claims description 4
- MZZSDCJQCLYLLL-UHFFFAOYSA-N Secalonsaeure A Natural products COC(=O)C12OC3C(CC1=C(O)CC(C)C2O)C(=CC=C3c4ccc(O)c5C(=O)C6=C(O)CC(C)C(O)C6(Oc45)C(=O)OC)O MZZSDCJQCLYLLL-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 3
- 238000004134 energy conservation Methods 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000000047 product Substances 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 238000007873 sieving Methods 0.000 abstract 2
- 238000009924 canning Methods 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 abstract 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 18
- UILPJVPSNHJFIK-UHFFFAOYSA-N Paeonol Chemical compound COC1=CC=C(C(C)=O)C(O)=C1 UILPJVPSNHJFIK-UHFFFAOYSA-N 0.000 description 10
- 230000001105 regulatory effect Effects 0.000 description 6
- YLTGFGDODHXMFB-UHFFFAOYSA-N isoacetovanillon Natural products COC1=CC=C(C(C)=O)C=C1O YLTGFGDODHXMFB-UHFFFAOYSA-N 0.000 description 5
- MLIBGOFSXXWRIY-UHFFFAOYSA-N paeonol Natural products COC1=CC=C(O)C(C(C)=O)=C1 MLIBGOFSXXWRIY-UHFFFAOYSA-N 0.000 description 5
- 230000036541 health Effects 0.000 description 4
- 208000004880 Polyuria Diseases 0.000 description 3
- 230000035619 diuresis Effects 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 230000036592 analgesia Effects 0.000 description 2
- 230000000879 anti-atherosclerotic effect Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000001754 anti-pyretic effect Effects 0.000 description 2
- 230000000767 anti-ulcer Effects 0.000 description 2
- 239000002221 antipyretic Substances 0.000 description 2
- 238000010959 commercial synthesis reaction Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 229930182478 glucoside Natural products 0.000 description 2
- 150000008131 glucosides Chemical class 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 231100000957 no side effect Toxicity 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000000469 ethanolic extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 235000002864 food coloring agent Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000401 methanolic extract Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/58—Colouring agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention mainly relates to a method for preparing beverage by using a peony root pigment. The method comprises the following steps: step one. preparing the peony root pigment, to be specific, drying obtained peony roots, crushing the peony roots so as to obtain peony root powder, then soaking and extracting by using ethyl alcohol, filtering, concentrating filtrate and drying so as to obtain the peony root pigment; and step two. preparing the beverage by using the peony root pigment, to be specific, adding water to the peony root pigment so as to dissolve the peony root pigment, adjusting PH value, sieving by using a 200-mesh screen so as to obtain pigment liquid for later use, adding the obtained pigment liquid to prepared beverage raw material liquid, mixing, uniformly stirring, adjusting PH, then ageing for 36-48 hours, sieving, homogenizing two times, and canning, thus finishing the preparation of the beverage, wherein the weight ratio of the beverage raw material liquid to the pigment liquid is (30-80): 1. According to the method, the peony root pigment is added to the beverage, so that the obtained beverage is right in color and good in safety without side effects and is a non-industrial synthetic product. Due to adoption of a full-ecological technology in a preparation process, the method has the advantages of energy conservation, environmental protection, healthcare and the like.
Description
Technical field
The present invention relates to the application of pigment, particularly relate to a kind of method applied tree peony root pigment and prepare beverage.
Background technology
Currently used pigment mostly is synthetic dyestuff and belongs to tar dyestuff, and not only also harmful without nutritive value, Long-Time Service can endanger the health of people, easily carcinogenic, and therefore vegetable colour dyeing is mentioned again.And natural colouring matter more and more causes the concern of scientific research field, and there is the trend replacing synthetic food color.
Tree peony whole body is precious, and its root skin, leaf, flower, fruit all have good using value.Moutan bark, autumn excavates root, and removing radicula, strips root skin, dry, and life is used or fried and uses.Compendium of Material Medica: " nourishing Yin and falling fire, separate spot poison, throat, diuresis stasis.Descendant specially controls fire mutually with yellow tiller, does not know that the merit of the root bark of tree peony more wins also.Red colored person's profit, the person of spending in vain mends, and people also seldom realizes, and should distinguish it." modern study, contained paeonol and glucosides constituents in addition thereof all have antiinflammatory action; The methanolic extract of moutan bark has suppression Platelet; Paeonol has the effects such as central inhibitory action and antiatherosclerosis, diuresis, antiulcer such as calmness, cooling, antipyretic, analgesia, spasmolysis.
Summary of the invention
The object of this invention is to provide a kind of method applied tree peony root pigment and prepare beverage, join in beverage by tree peony root pigment, the beverage of gained is bright in colour, and non-commercial synthesis product, has no side effect, and security is good; Preparation process is full ecological technique, has energy-conservation, environmental protection, the advantages such as health care.
The technical scheme that the present invention realizes above-mentioned purpose employing is: a kind of method applied tree peony root pigment and prepare beverage, comprises the following steps:
Step one, prepare tree peony root pigment
A. take fresh tree peony root, clean up with water, the laggard row airing of removing impurity, airing is not more than 10% to moisture content, namely obtains dry tree peony root, is pulverized by the tree peony root of drying, crosses 20 mesh sieves, obtains tree peony root powder, for subsequent use;
B. the ethanolic solution adding its weight 5 times in the tree peony root powder obtained to step a soaks, and the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, for subsequent use; Add the ethanolic solution of its weight 5 times in the filter residue obtained after filtration, the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, then merges twice filtrate, for subsequent use;
C. the filtrate after the merging obtained by step b is placed in rotary evaporation devices, concentrates and obtains medicinal extract, medicinal extract is placed in freeze drier, under-60 DEG C of conditions, carries out freeze drying, and the dry pressed powder terminating to obtain is tree peony root pigment, for subsequent use;
Step 2, application tree peony root pigment prepare beverage
Get the tree peony root pigment prepared, the ratio being 1:10 according to solid-liquid ratio is dissolved in water, and dissolves completely and regulates pH value to be 4-6, cross 200 eye mesh screens, obtain pigment solution, for subsequent use; The pigment solution obtained is joined in the beverage raw material liquid prepared, the weight ratio of beverage raw material liquid and pigment solution is 30-80:1, pH value is regulated to be 4-5.5 after mixing and stirring, then ageing 36-48h, ageing terminates rear mistake 200 eye mesh screen, carry out filling after homogeneous twice, namely complete the preparation of beverage.
The root of case red peony headed by described tree peony root.
The acid of pH value is regulated to be acetic acid or citric acid in described step 2.
Beneficial effect of the present invention
The process of one, whole extraction pigment provided by the invention and use does not destroy the chemical composition of moutan root bark.Modern study finds, paeonol contained by moutan root bark and glucosides constituents in addition thereof all have antiinflammatory action; The ethanol extract of moutan bark has suppression Platelet; Paeonol has the effects such as central inhibitory action and antiatherosclerosis, diuresis, antiulcer such as calmness, cooling, antipyretic, analgesia, spasmolysis, and therefore, the pigment obtained has certain health-care efficacy, and has light Paeonol fragrance.
Two, the present invention prepares the raw material of tree peony pigment is tree peony root, the output of tree peony root will be far longer than the output of peony, and from tree peony root, extract the recovery rate of pigment higher than the efficiency extracted from peony, containing several functions composition in the pigment prepared, can as the field of food of function food additive application, tree peony root pigment is joined in beverage, the beverage of gained is bright in colour, non-commercial synthesis product, have no side effect, security is good, and has certain health care to human body; In the present invention, the preparation process of tree peony root pigment is simple, and easy to use, preparation process is full ecological technique, has energy-conservation, environmental protection, the advantages such as health care.
Detailed description of the invention
Apply the method that tree peony root pigment prepares beverage, comprise the following steps:
Step one, prepare tree peony root pigment
A. take fresh tree peony root, clean up with water, the laggard row airing of removing impurity, airing is not more than 10% to moisture content, namely obtains dry tree peony root, is pulverized by the tree peony root of drying, crosses 20 mesh sieves, obtains tree peony root powder, for subsequent use;
B. the ethanolic solution adding its weight 5 times in the tree peony root powder obtained to step a soaks, and the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, for subsequent use; Add the ethanolic solution of its weight 5 times in the filter residue obtained after filtration, the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, then merges twice filtrate, for subsequent use;
C. the filtrate after the merging obtained by step b is placed in rotary evaporation devices, concentrates and obtains medicinal extract, medicinal extract is placed in freeze drier, under-60 DEG C of conditions, carries out freeze drying, and the dry pressed powder terminating to obtain is tree peony root pigment, for subsequent use;
Step 2, application tree peony root pigment prepare beverage
Get the tree peony root pigment prepared, the ratio being 1:10 according to solid-liquid ratio is dissolved in water, and dissolves completely and regulates pH value to be 4-6, cross 200 eye mesh screens, obtain pigment solution, for subsequent use; The pigment solution obtained is joined in the beverage raw material liquid prepared, the weight ratio of beverage raw material liquid and pigment solution is 30-80:1, pH value is regulated to be 4-5.5 after mixing and stirring, then ageing 36-48h, ageing terminates rear mistake 200 eye mesh screen, carry out filling after homogeneous twice, namely complete the preparation of beverage.
The root of case red peony headed by described tree peony root.
The acid of pH value is regulated to be acetic acid or citric acid in described step 2.
below in conjunction with specific embodiment, the present invention will be further described:
embodiment 1:
Apply the method that tree peony root pigment prepares beverage, comprise the following steps:
Step one, prepare tree peony root pigment
A. take fresh SHOUANHONG tree peony root, clean up with water, the laggard row airing of removing impurity, airing is not more than 10% to moisture content, namely obtains dry tree peony root, is pulverized by the tree peony root of drying, crosses 20 mesh sieves, obtains tree peony root powder, for subsequent use;
B. the ethanolic solution adding its weight 5 times in the tree peony root powder obtained to step a soaks, and the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, for subsequent use; Add the ethanolic solution of its weight 5 times in the filter residue obtained after filtration, the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, then merges twice filtrate, for subsequent use;
C. the filtrate after the merging obtained by step b is placed in rotary evaporation devices, concentrates and obtains medicinal extract, medicinal extract is placed in freeze drier, under-60 DEG C of conditions, carries out freeze drying, and the dry pressed powder terminating to obtain is tree peony root pigment, for subsequent use;
Step 2, application tree peony root pigment prepare beverage
Get the tree peony root pigment prepared, the ratio being 1:10 according to solid-liquid ratio is dissolved in water, and dissolves completely and regulates pH value to be 4 with acetic acid, cross 200 eye mesh screens, obtain pigment solution, for subsequent use; Joined by the pigment solution obtained in the beverage raw material liquid prepared, the weight ratio of beverage raw material liquid and pigment solution is 30:1, regulates pH value to be 4 after mixing and stirring, then ageing 36h, ageing terminates rear mistake 200 eye mesh screen, carries out filling, namely complete the preparation of beverage after homogeneous twice.
embodiment 2:
Apply the method that tree peony root pigment prepares beverage, comprise the following steps:
Step one, prepare tree peony root pigment, preparation method is with embodiment 1;
Step 2, application tree peony root pigment prepare beverage
Get the tree peony root pigment prepared, the ratio being 1:10 according to solid-liquid ratio is dissolved in water, and dissolves completely and regulates pH value to be 6 with citric acid, cross 200 eye mesh screens, obtain pigment solution, for subsequent use; The pigment solution obtained is joined in the beverage raw material liquid prepared, the weight ratio of beverage raw material liquid and pigment solution is 80:1, pH value is regulated to be 5.5 with citric acid after mixing and stirring, then ageing 48h, ageing terminates rear mistake 200 eye mesh screen, carry out filling after homogeneous twice, namely complete the preparation of beverage.
embodiment 3:
Apply the method that tree peony root pigment prepares beverage, comprise the following steps:
Step one, prepare tree peony root pigment, preparation method is with embodiment 1;
Step 2, application tree peony root pigment prepare beverage
Get the tree peony root pigment prepared, the ratio being 1:10 according to solid-liquid ratio is dissolved in water, and dissolves completely and regulates pH value to be 5 with citric acid, cross 200 eye mesh screens, obtain pigment solution, for subsequent use; The pigment solution obtained is joined in the beverage raw material liquid prepared, the weight ratio of beverage raw material liquid and pigment solution is 50:1, pH value is regulated to be 5 with citric acid after mixing and stirring, then ageing 42h, ageing terminates rear mistake 200 eye mesh screen, carry out filling after homogeneous twice, namely complete the preparation of beverage.
Claims (1)
1. apply the method that tree peony root pigment prepares beverage, it is characterized in that: comprise the following steps:
Step one, prepare tree peony root pigment
A. take the root of fresh SHOUANHONG tree peony, clean up with water, the laggard row airing of removing impurity, airing is not more than 10% to moisture content, namely obtains dry tree peony root, is pulverized by the tree peony root of drying, crosses 20 mesh sieves, obtains tree peony root powder, for subsequent use;
B. the ethanolic solution adding its weight 5 times in the tree peony root powder obtained to step a soaks, and the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, for subsequent use; Add the ethanolic solution of its weight 5 times in the filter residue obtained after filtration, the mass concentration of ethanolic solution is 70%, filters after soaking 2d, collects filtrate, then merges twice filtrate, for subsequent use;
C. the filtrate after the merging obtained by step b is placed in rotary evaporation devices, concentrates and obtains medicinal extract, medicinal extract is placed in freeze drier, under-60 DEG C of conditions, carries out freeze drying, and the dry pressed powder terminating to obtain is tree peony root pigment, for subsequent use;
Step 2, application tree peony root pigment prepare beverage
Get the tree peony root pigment that step one prepares, the ratio being 1:10 according to solid-liquid ratio is dissolved in water, and dissolving completely rear is 4-6 by acetic acid adjust ph, crosses 200 eye mesh screens, obtains pigment solution, for subsequent use; The pigment solution obtained is joined in the beverage raw material liquid prepared, the weight ratio of beverage raw material liquid and pigment solution is 30-80:1, after mixing and stirring, adjust ph is 4-5.5, then ageing 36-48h, ageing terminates rear mistake 200 eye mesh screen, carry out filling after homogeneous twice, namely complete the preparation of beverage.
Priority Applications (1)
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CN201410019505.2A CN103767026B (en) | 2014-01-16 | 2014-01-16 | Method for preparing beverage by using peony root pigment |
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CN201410019505.2A CN103767026B (en) | 2014-01-16 | 2014-01-16 | Method for preparing beverage by using peony root pigment |
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CN103767026B true CN103767026B (en) | 2015-06-03 |
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102038261A (en) * | 2010-12-30 | 2011-05-04 | 河南科技大学 | Method for preparing tree peony beverage |
CN102754887A (en) * | 2012-08-01 | 2012-10-31 | 河南华美生物工程有限公司 | Peony air-free soda water and preparation method thereof |
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2014
- 2014-01-16 CN CN201410019505.2A patent/CN103767026B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102038261A (en) * | 2010-12-30 | 2011-05-04 | 河南科技大学 | Method for preparing tree peony beverage |
CN102754887A (en) * | 2012-08-01 | 2012-10-31 | 河南华美生物工程有限公司 | Peony air-free soda water and preparation method thereof |
Non-Patent Citations (2)
Title |
---|
牡丹皮中丹皮酚的提取工艺研究;张云升等;《河北省科学院学报》;20050930;第22卷(第03期);第49-51页 * |
王留兴.牡丹皮乙醇提取工艺研究.《长春中医药大学学报》.2008,第24卷(第01期),第35-36页. * |
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