CN105586445A - Real leather manufacturing method - Google Patents

Real leather manufacturing method Download PDF

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Publication number
CN105586445A
CN105586445A CN201510981909.4A CN201510981909A CN105586445A CN 105586445 A CN105586445 A CN 105586445A CN 201510981909 A CN201510981909 A CN 201510981909A CN 105586445 A CN105586445 A CN 105586445A
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CN
China
Prior art keywords
wormwood
corium
essential oil
preparation
distilled water
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Application number
CN201510981909.4A
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Chinese (zh)
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CN105586445B (en
Inventor
刘科江
段娜
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Guangzhou Panyu Polytechnic
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Guangzhou Panyu Polytechnic
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Priority to CN201510981909.4A priority Critical patent/CN105586445B/en
Publication of CN105586445A publication Critical patent/CN105586445A/en
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Publication of CN105586445B publication Critical patent/CN105586445B/en
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    • CCHEMISTRY; METALLURGY
    • C14SKINS; HIDES; PELTS; LEATHER
    • C14CCHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
    • C14C9/00Impregnating leather for preserving, waterproofing, making resistant to heat or similar purposes
    • AHUMAN NECESSITIES
    • A43FOOTWEAR
    • A43BCHARACTERISTIC FEATURES OF FOOTWEAR; PARTS OF FOOTWEAR
    • A43B1/00Footwear characterised by the material
    • CCHEMISTRY; METALLURGY
    • C14SKINS; HIDES; PELTS; LEATHER
    • C14CCHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
    • C14C11/00Surface finishing of leather
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Fats And Perfumes (AREA)
  • Footwear And Its Accessory, Manufacturing Method And Apparatuses (AREA)

Abstract

The invention discloses a real leather manufacturing method. The real leather manufacturing method comprises the steps of 1, distilling, wherein fresh wormwood is selected and chopped, mixed with added distilled water and then distilled for obtaining wormwood distillate; 2, skimming, wherein sodium chloride is added into the wormwood distillate obtained in the step 1 and then skimming is carried out for obtaining coarse wormwood essential oil; 3, oil manufacturing, wherein anhydrous sodium sulfate is added into the coarse wormwood essential oil obtained in the step 2 for obtaining wormwood essential oil for standby application; 4, boiling, wherein the fresh wormwood is selected and chopped and mixed with the distilled water for being heated and boiled, and then wormwood decoction is obtained; 5, soaking, wherein real leather is spread flatly, then soaked into the wormwood decoction obtained in the step 4 overnight and dried in the air; 6, oil applying, wherein the real leather dried in the air in the step 5 is wiped by the wormwood essential oil and then dried in the air and finally the real leather dispelling dampness and relieving itching is manufactured. The real leather manufactured through the method has the functions of resisting odors, relieving itching and dispelling dampness, has the natural fragrance, does not pollute the environment and is excellent in application performance.

Description

A kind of corium preparation method
Technical field
The invention belongs to leather processing technical field, relate to a kind of corium preparation method, also relate toA kind of leather shoe-pad and a kind of corium footwear boots.
Background technology
Corium is the very large product of use amount in current life, and corium can clothing, trousers, footwear, capEtc. every clothing accessories, but corium is airtight, difficult water suction, therefore wears the made clothing of corium,Especially when the article such as shoe-pad, footwear boots, the sweat that corium can not produce sole in time carry out, easily there is the illness that pin is smelly, pin is itched in gas and absorption.
And at present, a lot of corium adds chemical substance smelly antipruritic to stop, and the interpolation of chemical substanceBe unfavorable for health, and chemical substance all can be directly refining, in process of manufacture orContaminated environment indirectly.
Summary of the invention
Known wormwood is perennial herb or slightly becomes suffruticose, and plant has strong fragrance. HerbBe used as medicine, have Wen Jing, clearing damp, loose cold, hemostasis, anti-inflammatory, relieving asthma, cough-relieving, antiabortive, anti-mistakeEffect such as quick grade, is China's traditional Chinese medicine, and tarragon is dried and smashs to obtain " moxa " to pieces, and moxa stick processed is for moxa-moxibustionWith, go back edible, can make again the raw material of " ink paste ", therefore, utilize the functional components of wormwoodDevelop there is deodorization, the corium of antipruritic, clearing damp, to improving industrial value and the dimension of wormwoodProtect human body health significant.
Therefore, the object of the present invention is to provide a kind of preparation method of corium, the method utilizationWormwood incorporates in corium, and the corium deodorization, antipruritic, the clearing damp that adopt the method to make have certainlySo fragrance, free from environmental pollution, application performance is good.
Realizing object of the present invention can be by taking following technical scheme to reach:
1) distillation: select the chopping of fresh wormwood, mix after adding distilled water, then steamHeat up in a steamer, obtain wormwood distillate;
2) separatory: in step 1) add sodium chloride in the wormwood distillate that obtains, then useSeparatory funnel carries out separatory after vibrating, shaking up and leave standstill, and obtains oil reservoir and water layer; By oil reservoirIsolate, obtain the thick essential oil of wormwood;
3) liquefaction: in step 2) add anhydrous sodium sulfate, warp in the thick essential oil of wormwood that obtainsFiltration obtains wormwood essential oil, for subsequent use;
4) stew soup: select fresh wormwood chopping, after mixing with distilled water, heat and boil,First heat for the first time, after boiling, heat for the second time again, boil altogether 1-2 hour,Obtain wormwood decoction;
5) soak: corium is divided, be then immersed in step 4) in the wormwood decoction that obtains,Soaked overnight, dries; Soak again, dry, so repeat 9-12 time;
6) polish: by step 5) corium wormwood essential oil wiping after drying, dry; AgainCarry out wiping, dry, so repeat 9-12 time, make the corium of removing dampness to stop itchin.
Preferably, described corium is dermatine or animal corium.
Preferably, step 1) in, fresh wormwood and distilled water weight ratio are 1:(3-5).
Preferably, step 1) in, distillation time is 1-2 hour.
Preferably, step 4) in, fresh wormwood and distilled water weight ratio are 1:(2-4).
Preferably, step 4) in, heating-up temperature is 100-120 DEG C for the first time, adds for the second timeHot temperature degree is 40-60 DEG C.
Preferably, step 6) after also comprise the step of disinfecting mouldproof processing.
The present invention also provides a kind of leather shoe-pad, and the corium of described leather shoe-pad is according to above-mentioned trueThe corium that skin preparation method makes obtains through cutting.
The present invention also provides a kind of corium footwear boots, and the corium of described corium footwear boots is according to above-mentioned trueThe corium that skin preparation method makes is prepared from through shoemaking or boots technique processed.
As preferably, in step 1) in, the proportion control of fresh wormwood and distilled water weight existsBe 1:(3-5) for wormwood is dissolved in distilled water better, avoid distilled water not steam lessHeat up in a steamer completely, distilled water too much dilutes wormwood. Controlling distillation time 1-2 hour, is in order to makeWormwood essential oil fully discharges.
As preferably, in step 4) in, heating-up temperature is 100-120 DEG C for the first time, reachesThe object of disinfection, adjusts heating-up temperature for the second time and is the little fire of 40-60 DEG C slowly after boilingBoil, be not only beneficial to the enzyme differentiation activity in wormwood, make wormwood become soft rotten, make in wormwoodFunctional components is dissolved out to greatest extent, and little fire is endured the fiber that can also keep wormwood slowlyOrganize and do not suffer a loss, if big fire is boiled suddenly always, can cause the enzyme denaturation in wormwood, make wormwoodIn functional components be insoluble to distilled water, volatile flavor compounds also can be along with high temperature evaporationFall, go back water consumption fast. Fresh wormwood and distilled water weight ratio are 1:(2-4), boil 1-2 littleTime, the taste of wormwood is just dense, and the composition in wormwood all incorporates in soup, and the time can cause steaming too for a long timeHeat up in a steamer water consumption fast, reduce effect of wormwood.
Beneficial effect of the present invention is:
1, wormwood deodorization, functional components antipruritic, clearing damp are penetrated into corium by the present inventionIn, make corium also there is the function of deodorization, antipruritic, clearing damp;
The step twice of 2, stewing soup is adjusted heating-up temperature, has ensured the functional components in wormwoodFarthest incorporate in distilled water;
The step of 3, corium being soaked and being polished, twice functional components by wormwood incorporates veryPi Zhong, dually ensures that corium has the function of deodorization, antipruritic, clearing damp;
4, the leather shoe-pad, corium footwear boots or other corium article that utilize the method to make, allPossess effect of deodorization, antipruritic, clearing damp, delicate fragrance nature, is beneficial to health, does not pollute ringBorder, application performance is good.
Detailed description of the invention
Below, in conjunction with detailed description of the invention, the present invention is described further:
Embodiment 1:
A kind of leather shoe-pad, makes the preparation method of the corium of described leather shoe-pad, by following stepSuddenly carry out:
1) distillation: select the chopping of fresh wormwood, mix after adding distilled water, fresh wormwood withDistilled water weight ratio is 1:3, then distills, and obtains wormwood distillate;
2) separatory: in step 1) add sodium chloride in the wormwood distillate that obtains, then useSeparatory funnel carries out separatory after vibrating, shaking up and leave standstill, and obtains oil reservoir and water layer; By oil reservoirIsolate, obtain the thick essential oil of wormwood;
3) liquefaction: in step 2) add anhydrous sodium sulfate, warp in the thick essential oil of wormwood that obtainsFiltration obtains wormwood essential oil, for subsequent use;
4) stew soup: select fresh wormwood chopping, mix to heat boiling with distilled water, newFresh wormwood and distilled water weight ratio are 1:2, and heating-up temperature is 100 DEG C for the first time, after boiling, adjustWhole heating-up temperature is for the second time 40 DEG C, amounts to heating and boils 1 hour, obtains wormwood decoction;
5) soak: corium is divided, be then immersed in step 4) in the wormwood decoction that obtains,Soaked overnight, dries; Soak again, dry, so repeat 9 times;
6) polish: by step 5) corium wormwood essential oil wiping after drying, dry; AgainCarry out wiping, dry, so repeat 9 times, make the corium of removing dampness to stop itchin;
7) make: corium process cutting and disinfecting mouldproof processing that above-mentioned preparation method is made,Make the leather shoe-pad of removing dampness to stop itchin.
Embodiment 2:
The cotton boots of a kind of corium, make the preparation method of the corium of the cotton boots of described corium, by following stepSuddenly carry out:
1) distillation: select the chopping of fresh wormwood, mix after adding distilled water, fresh wormwood withThe weight ratio of distilled water is 1:5, then distills 2 hours, obtains wormwood distillate;
2) separatory: in step 1) add sodium chloride in the wormwood distillate that obtains, then useSeparatory funnel carries out separatory after vibrating, shaking up and leave standstill, and obtains oil reservoir and water layer; By oil reservoirIsolate, obtain the thick essential oil of wormwood;
3) liquefaction: in step 2) add anhydrous sodium sulfate, warp in the thick essential oil of wormwood that obtainsFiltration obtains wormwood essential oil, for subsequent use;
4) stew soup: select fresh wormwood chopping, after mixing with distilled water, heat and boil,Fresh wormwood and distilled water weight ratio are 1:4, and heating-up temperature is 120 DEG C for the first time, after boilingAdjusting heating-up temperature is for the second time 60 DEG C, and heating boils 2 hours, obtains wormwood decoction;
5) soak: dermatine is divided, be then immersed in step 4) the wormwood soup that obtainsIn agent, soaked overnight, dries; Soak again, dry, so repeat 12 times;
6) polish: by step 5) dermatine wormwood essential oil wiping after drying, dry;Carry out again wiping, dry, so repeat 12 times, make the dermatine of removing dampness to stop itchin;
7) make: the dermatine that above-mentioned preparation method is made through disinfecting mouldproof process after,Make again the cotton boots of dermatine of removing dampness to stop itchin through boots technique processed.
Embodiment 3:
A kind of ox-hide leather shoes, the ox-hide that makes described ox-hide leather shoes carries out according to the following steps:
1) distillation: select the chopping of fresh wormwood, mix after adding distilled water, fresh wormwood withThe weight ratio of distilled water is 1:4, then distills 1.5 hours, obtains wormwood distillate;
2) separatory: in step 1) add sodium chloride in the wormwood distillate that obtains, then useSeparatory funnel carries out separatory after vibrating, shaking up and leave standstill, and obtains oil reservoir and water layer; By oil reservoirIsolate, obtain the thick essential oil of wormwood;
3) liquefaction: in step 2) add anhydrous sodium sulfate, warp in the thick essential oil of wormwood that obtainsFiltration obtains wormwood essential oil, for subsequent use;
4) stew soup: select fresh wormwood chopping, after mixing with distilled water, heat and boil,Fresh wormwood and distilled water weight ratio are 1:3, and heating-up temperature is 110 DEG C for the first time, after boilingAdjusting heating-up temperature is for the second time 50 DEG C, boils altogether 1.5 hours, obtains wormwood decoction;
5) soak: ox-hide is divided, be then immersed in step 4) in the wormwood decoction that obtains,Soaked overnight, dries; Soak again, dry, so repeat 10 times;
6) polish: by step 5) ox-hide wormwood essential oil wiping after drying, dry; AgainCarry out wiping, dry, so repeat 10 times, make the ox-hide of removing dampness to stop itchin;
7) make: the ox-hide that above-mentioned preparation method is made through disinfecting mouldproof process after, thenMake the ox-hide leather shoes of removing dampness to stop itchin through shoe-making process.
The measure of merit of clearing damp prepared by the present invention, antipruritic, deodorizing shoe-pad:
With commercially available General Proper pad for leather shoes as a comparison case, choose the smelly and pin of 50 pin aspiration of itchingPerson, uses respectively commercially available one of the leather shoe-pad of the removing dampness to stop itchin described in embodiment 1 and comparative exampleAs leather shoe-pad, all results (using method: use embodiment's 1 in footwear on probationShoe-pad, uses the shoe-pad of comparative example in footwear), to index effects such as clearing damp, antipruritic, deodorizationsFruit is tested, and test result is as table 1:
Table 1 embodiment 1 and comparative example shoe-pad comparison of test results table
Reach a conclusion from above application test result: the clearing damp to sole in the use of this product,Antipruritic, odor-resistant result is better, has higher use value as a kind of removing dampness to stop itchin shoe-pad,We also further know, the corium being made by the present invention has preferably clearing damp, antipruritic, anti-Smelly effect.
For a person skilled in the art, can be according to technical scheme described above and structureThink, make other various corresponding changes and distortion, and all these changes and distortionWithin all should belonging to the protection domain of the claims in the present invention.

Claims (9)

1. a corium preparation method, is characterized in that, carries out according to the following steps:
1) distillation: select the chopping of fresh wormwood, mix after adding distilled water, then steamHeat up in a steamer, obtain wormwood distillate;
2) separatory: in step 1) add sodium chloride in the wormwood distillate that obtains, then useSeparatory funnel carries out separatory after vibrating, shaking up and leave standstill, and obtains oil reservoir and water layer; By oil reservoirIsolate, obtain the thick essential oil of wormwood;
3) liquefaction: in step 2) add anhydrous sodium sulfate, warp in the thick essential oil of wormwood that obtainsFiltration obtains wormwood essential oil, for subsequent use;
4) stew soup: select fresh wormwood chopping, after mixing with distilled water, heat and boil,First heat for the first time, after boiling, heat for the second time again, boil altogether 1-2 hour,Obtain wormwood decoction;
5) soak: corium is divided, be then immersed in step 4) in the wormwood decoction that obtains,Soaked overnight, dries; Soak again, dry, so repeat 9-12 time;
6) polish: by step 5) corium wormwood essential oil wiping after drying, dry; AgainCarry out wiping, dry, so repeat 9-12 time, make the corium of removing dampness to stop itchin.
2. corium preparation method according to claim 1, is characterized in that: described coriumFor dermatine or animal corium.
3. corium preparation method according to claim 1, is characterized in that: step 1)In, fresh wormwood and distilled water weight ratio are 1:(3-5).
4. corium preparation method according to claim 1, is characterized in that step 1)In, the time of distillation is 1-2 hour.
5. corium preparation method according to claim 1, is characterized in that step 4)In, fresh wormwood and distilled water weight ratio are 1:(2-4).
6. corium preparation method according to claim 1, is characterized in that step 4)In, heating-up temperature is 100-120 DEG C for the first time, heating-up temperature is 40-60 DEG C for the second time.
7. according to the corium preparation method described in claim 1-6 any one, it is characterized in that,Step 6) after also comprise the step of disinfecting mouldproof processing.
8. a leather shoe-pad, is characterized in that, the corium of described leather shoe-pad is by rightThe corium that corium preparation method described in requirement 1-7 any one makes obtains through cutting.
9. corium footwear boots, is characterized in that, the corium of described corium footwear boots is by rightThe corium that corium preparation method described in requirement 1-7 any one makes is through shoemaking or boots technique processedBe prepared from.
CN201510981909.4A 2015-12-22 2015-12-22 A kind of corium preparation method Expired - Fee Related CN105586445B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110117913A (en) * 2019-05-22 2019-08-13 佛山市欣比美纺织有限公司 A kind of dyeing liquid and preparation method thereof of natural herb drug

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4234679A1 (en) * 1992-10-14 1994-04-21 Philipp Schaefer Rendering leather hydrophobic without affecting its natural properties - by impregnating at least one side with soln. of silicone rubber which is crosslinked by moisture e.g. from atmosphere
CN103510382A (en) * 2012-09-26 2014-01-15 吴兴良 Odor-resistant and anti-microbial treatment method for shoe materials
CN104531919A (en) * 2014-12-17 2015-04-22 广东菲安妮皮具股份有限公司 Chinese herbal medicine leather product maintaining agent and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4234679A1 (en) * 1992-10-14 1994-04-21 Philipp Schaefer Rendering leather hydrophobic without affecting its natural properties - by impregnating at least one side with soln. of silicone rubber which is crosslinked by moisture e.g. from atmosphere
CN103510382A (en) * 2012-09-26 2014-01-15 吴兴良 Odor-resistant and anti-microbial treatment method for shoe materials
CN104531919A (en) * 2014-12-17 2015-04-22 广东菲安妮皮具股份有限公司 Chinese herbal medicine leather product maintaining agent and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王全杰等: "艾蒿精油的研究进展及其在皮革中的应用", 《皮革与化工》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110117913A (en) * 2019-05-22 2019-08-13 佛山市欣比美纺织有限公司 A kind of dyeing liquid and preparation method thereof of natural herb drug

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