CN110117904A - A kind of soft finishing agent and its technique for applying - Google Patents

A kind of soft finishing agent and its technique for applying Download PDF

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Publication number
CN110117904A
CN110117904A CN201910436345.4A CN201910436345A CN110117904A CN 110117904 A CN110117904 A CN 110117904A CN 201910436345 A CN201910436345 A CN 201910436345A CN 110117904 A CN110117904 A CN 110117904A
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Prior art keywords
parts
finishing agent
soft finishing
soft
cloth
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栗国文
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Shaoxing Yiyang Chemical Additives Co Ltd
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Shaoxing Yiyang Chemical Additives Co Ltd
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Priority to CN201910436345.4A priority Critical patent/CN110117904A/en
Publication of CN110117904A publication Critical patent/CN110117904A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/46Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • D06M13/148Polyalcohols, e.g. glycerol or glucose
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53Polyethers
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M23/00Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/16General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673Inorganic compounds
    • D06P1/67333Salts or hydroxides
    • D06P1/6735Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/34Material containing ester groups
    • D06P3/52Polyesters
    • D06P3/54Polyesters using dispersed dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/25Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The present invention relates to the technical fields of textile auxiliary agent, disclose a kind of soft finishing agent, it is characterised in that: the chemical composition of the soft finishing agent includes: 250-300 parts of amido silicon oil in parts by weight;10-20 parts of emulsifier;50-80 parts of nano diatomite;70-100 parts of lauric alcohol;1-3 parts of pH adjusting agent;600-800 parts of water.It is able to maintain the dry and comfortable of polyester fabric surface, reduces the sweat sticking effect between human body and fabric, adjusts the humid tropical condition of human body microenvironment, human body is kept to wear pleasant sense.

Description

A kind of soft finishing agent and its technique for applying
Technical field
The present invention relates to the technical field of textile auxiliary agent, more specifically, it relates to a kind of soft finishing agent and its answer Use technique.
Background technique
Softening agent is a kind of quiet, dynamic friction coefficient chemical substance that can change fiber.When changing frictional coefficient of fiber, Feel, which touches fabric, smooth sense, is easy to move on fiber or fabric;When changing dynamic friction coefficient, between fiber and fiber Fine structure be easy to be mutually shifted, that is, fiber or fabric it is easily deformable.The comprehensive of the two feels to be exactly soft.It is soft Agent is divided as ionic cationic, non-ionic, anionic and four kinds of both sexes quaternary.
With the development of organosilicon chemistry after the 1970s, silicone softening agent is as a kind of novel high score Sub- softening agent develops rapidly.Compared with traditional non-silicon class softening agent, since Si-O key has rotation more lower than C-O key Free energy, silicone softening agent show more excellent softness, thus short since silicone softening agent occurs In tens years, promptly woven enterprise is used, and gradually becomes leading instead of traditional non-silicon class softening agent Softening agent kind.Common silicone softening agent includes hydroxy silicon oil, polyether silicone oil, amido silicon oil.Hydroxy silicon oil and polyethers Silicone oil hydrophilicity is preferable, and finish fabric wears good permeability, but the fabric that there is processing is not soft enough, washability is poor and feel The drawback of difference.Due to the polarity of amino in amido silicon oil, can and fiber surface hydroxyl, carboxyl etc. by the combination of chemical bond, Make siloxane main chain oriented attachment in fiber surface, to reduce the coefficient of friction between fiber, can be made with the power of very little It obtains and generates sliding between fiber, show soft, smooth characteristic.
Terylene is in textile using the synthetic fibers that relatively broad, comprehensive performance is more excellent.Terylene filament fabric is knitted Starching must be carried out before making, and so that strand surface is coated one layer of smooth, flexible and firm serous coat, to enhance the obvolvent of polyester filament Power and wearability enable to bear various frictional force and tension in weaving process, weaving production in good quality and high output It asks down and goes on smoothly.The fabric of usual terylene material has well-pressed characteristic, so it is often used production shirt, but its softness Property it is very poor, so in order to enable dress comfort, it will usually polyester fabric is handled using softening agent, so that washing Synthetic fibre cloth becomes flexible relative.
But the polyester fabric after being arranged using amido silicon oil has that hydrophobic, hygroscopicity is poor, summer is unfavorable for people Dress influences the comfort of dress.
Summary of the invention
One of the objects of the present invention is to provide a kind of soft finishing agents, are able to maintain the dry and comfortable of polyester fabric surface, subtract Sweat sticking effect between small human body and fabric adjusts the humid tropical condition of human body microenvironment, and human body is kept to wear pleasant sense.
Another object of the present invention is to provide a kind of technique for applying of soft finishing agent, enable to soft finishing agent Performance performs to maximum, so that the polyester fiber after processed is more soft, while washability is also improved.
Above-mentioned technical purpose of the invention has the technical scheme that
A kind of soft finishing agent, it is characterised in that: the chemical composition of the soft finishing agent includes: in parts by weight
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
10-30 parts of pH adjusting agent;
600-800 parts of water.
The very strong amino containing polarized on the strand of amido silicon oil, so amido silicon oil has good adsorptivity, ammonia Base silicone oil forms the lotion of O/W with water, so that the dosage of soft finishing agent entirety is subtracted in the presence of emulsifier It is few, and enable to having for terylene cloth soft, smooth with plentiful feel.Porosity of diatomite itself is big, absorbability Some advantages such as energy is strong, chemical property is stable, wearability and heat resistance are strong.Diatomite is added in soft finishing agent, due to washing Hole between synthetic fibre fiber molecule is smaller, so that the biggish substance of some molecular entities can not be dispersed to polyester fiber molecule It is interior.Nano diatomite is selected in the present invention, and diatomite is all diffused in polyester fiber molecule.With diatomite Grain diameter is gradually reduced, so that is be distributed in polyester fiber molecule is more uniform, so as to by the sweat of skin surface Liquid and moisture sponge.Woven dacron when human skin is perspired, after using in the present invention handled by soft finishing agent The sweat of human body surface and moisture can be absorbed rapidly, spread and evaporated by material, keep the dry and comfortable of polyester fabric surface, be reduced Sweat sticking effect between human body and fabric adjusts the humid tropical condition of human body microenvironment, and human body is kept to wear pleasant sense.
On the other hand, diatomite belongs to a kind of inorganic matter, and uses nanoscale diatomite, and diatomite enables to terylene The crystallinity of fiber molecule reduces, and amorphous area increases, so that Structure of PET Fiber is loose, the gap of polyester fiber molecule increases Greatly, so that amido silicon oil molecule can more enter polyester fiber intramolecular, so that the flexibility of polyester fabric enhances. Meanwhile diatomite can form small holes on the surface of terylene molecule, some sweat and moisture can be received into, to increase The hygroscopicity of terylene molecule is added.
There are many alcoholic extract hydroxyl group on the strand of lauric alcohol, belong to hydrophilic radical, and can in amido silicon oil strand Amino combine, to enhance the hydrophily of amido silicon oil, while containing the alcohol not in conjunction with amino in lauric alcohol strand Hydroxyl, so that the hydrophily for being attached with the polyester fiber molecule of amido silicon oil is stronger.As the hydrophily of terylene molecule increases By force, the sweat and moisture for enabling human body to distribute are combined in the form of hydrogen bond with alcoholic extract hydroxyl group, and that finally improves enhances The hygroscopicity of polyester fiber, so that human body is more comfortable when wearing next to the skin.
As a further improvement of the present invention, the chemical composition of the soft finishing agent includes: in parts by weight
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
60-80 parts of titanium dioxide;
10-30 parts of pH adjusting agent;
600-800 parts of water.
The shortcomings that amino generally existing easy flavescence, arrange light color or white fabrics will appear not when by high temperature drying With the yellowing of degree.Titanium dioxide is a kind of white inorganic filler, has best opacity, best whiteness and light Degree.Titanium dioxide is inorganic constituents, has good dispersion performance, and have the function of deodorization and sterilization, and chemical property is stablized, right Skin can be avoided light color or white by adding titanium dioxide in soft finishing agent without any irritation and toxicity Polyester fabric the phenomenon that turning yellow.
As a further improvement of the present invention, the chemical composition of the soft finishing agent includes: in parts by weight
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
20-40 parts of titanium dioxide;
5-7 parts of disperse blue;
10-30 parts of pH adjusting agent;
600-800 parts of water.
By using above-mentioned technical proposal, enable to the whiter of polyester fabric by adding titanium dioxide, prevent by In amido silicon oil processing and there is the phenomenon that flavescence.When handling white facestock, by being added in soft finishing agent Disperse blue, since the diatomite in aforementioned increases the gap of polyester fiber molecule, so that disperse blue be facilitated to be dispersed in terylene In molecule.By adding a small amount of disperse blue, after disperse blue is attached on dacron, the work for adjusting coloured light can be played With so that fabric shows blue violet light, the white sense of vision is stronger.
As a further improvement of the present invention, the chemical composition of the soft finishing agent includes: in parts by weight
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
20-40 parts of titanium dioxide;
5-7 parts of disperse blue;
20-30 parts of anhydrous sodium sulphate;
10-30 parts of pH adjusting agent;
600-800 parts of water.
The intermolecular gap of polyester fiber is smaller, and anhydrous sodium sulphate enables to the colourability of disperse blue as a kind of inorganic salts It is stronger.While promoting to contaminate in disperse blue, diluent can be made, reduce the intensity in polyester fiber molecule, eliminate woven dacron The internal stress of material, so that disperse blue is more easily entered into polyester fiber molecule, so that the washability of cloth is stronger.
As a further improvement of the present invention, the emulsifier is that isomerous tridecanol, alkyl phenol polyoxyethylene ether are therein One kind, and usage amount is 15 parts.
By using above-mentioned technical proposal, isomerous tridecanol and alkyl phenol polyoxyethylene ether are easily dispersed or dissolved in water, tool There are excellent wetability, permeability and emulsibility.Amido silicon oil and water is enabled to form stable emulsifier, so as to right Fabric plays excellent soft effect.
A kind of a kind of technique for applying of soft finishing agent according to claim 4, it is characterised in that: including walking as follows It is rapid:
S1: drain heating;
S2: cloth pads;
S3: wet cloth rubbing;
S4: secondary to pad;The temperature of the soft finishing agent rises to 70-80 DEG C when padding, and makes cloth after padding again Material impregnates 40-60min in the soft finishing agent;
S5: clear water rinses.
By using above-mentioned technique for applying, the performance of soft finishing agent is enabled to perform to maximum, so that processed Later polyester fiber is more soft, while washability is also improved.
As a further improvement of the present invention, the step S1, the soft finishing agent is emitted into slurry tank, and Soft finishing agent is warming up to 40-50 DEG C, cloth is then subjected to S2 processing.
By using above-mentioned technical proposal, first makes terylene cloth padding by soft finishing agent, then directly carry out Rubbing, so that soft finishing agent can be dispersed in as far as possible in polyester fiber molecule, then again pads cloth in temperature It spends in higher soft finishing agent, the soft finishing agent adhered to before in terylene cloth and the higher soft finishing agent of temperature at this time Formation temperature is poor, and the soft finishing agent under two kinds of different temperatures merges into each other, and the temperature of last soft finishing agent reaches more Suitable temperature enables to the molecule of soft finishing agent to obtain energy, has stronger reactivity worth, finally to process Cloth afterwards is more soft.Soft finishing agent when obtaining more energy, wash by can be stronger be attached to simultaneously In synthetic fibre fiber molecule, washability is enhanced.
As a further improvement of the present invention, the step S2, cloth pads at least 5 times repeatedly, then carries out at step S3 Reason.
By using above-mentioned technical proposal, step S2 enables to soft finishing agent dispersion more by multiple padding Uniformly, to enhance the effect of soft finishing agent.
In conclusion the advantages of the present invention are:
1, by using soft finishing agent, it is able to maintain the dry and comfortable of polyester fabric surface, reduces the sweat between human body and fabric Liquid sticking effect adjusts the humid tropical condition of human body microenvironment, and human body is kept to wear pleasant sense;
2, by adding titanium dioxide in soft finishing agent, the polyester fabric that can be avoided light color or white becomes Yellow phenomenon;
3, anhydrous sodium sulphate enables to the colourability of disperse blue stronger as a kind of inorganic salts.Promote to contaminate in disperse blue same When, diluent can be made, reduce the intensity in polyester fiber molecule, eliminate the internal stress of terylene cloth, so that dispersion Indigo plant is more easily entered into polyester fiber molecule, so that the washability of cloth is stronger;
4, it by using technique for applying disclosed by the invention, enables to the molecule of soft finishing agent to obtain energy, has Stronger reactivity worth finally makes the cloth after processing more soft.Soft finishing agent is obtaining more energy simultaneously When, can be stronger be attached in polyester fiber molecule enhances washability.
Detailed description of the invention
Fig. 1 is a kind of process flow chart of the technique for applying of soft finishing agent of the present invention.
Specific embodiment
With reference to the accompanying drawings and examples, present invention is further described in detail.
Embodiment 1:
A kind of soft finishing agent, each chemical composition are 275 parts of amido silicon oil in parts by weight;15 parts of isomerous tridecanol;It receives 65 parts of diatomite of rice;85 parts of lauric alcohol;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, using acetic acid, by system PH is adjusted to 6.When preparation, first water is added in reaction kettle, then amido silicon oil is added again, then by nano diatomite, Lauric alcohol, isomerous tridecanol are added, and stirring while adding, after stirring 60min, add acetic acid, and make the pH of system It is 6, then persistently stirs 40min.
As shown in Figure 1, a kind of technique for applying of soft finishing agent, comprising the following steps:
S1: drain heating.It is CN205856830U public that above-mentioned configured soft finishing agent, which is first drained into Authorization Notice No., In the rinsing bowl in a kind of two-layer fabric washing combination machine opened, and the temperature for the soft finishing agent being discharged into is made to rise to 45 ℃。
S2: cloth pads.Cloth is input to the rinsing bowl that step S1 is mentioned, then makes the one end of cloth from rinsing bowl Output, then the liquid above cloth is shut out by mop padding machine, 7 times repeatedly;And the softness for guaranteeing that cloth touches is whole The temperature for managing agent is always 45 DEG C.
S3: wet cloth rubbing.By the cloth output after S2 is processed, 50min is crumpled using hairbrush by staff, so It carries out again afterwards in next step.
S4: secondary to pad.The soft finishing agent temperature in rinsing bowl is first increased to 75 DEG C, then will be handled again by S3 Later cloth is input in rinsing bowl, and is impregnated and shut out by side, then makes cloth in the softness of rinsing bowl again 45min is impregnated in finishing agent.
S5: clear water rinses.Design on fabric surface is rinsed using clear water, 40min is rinsed, finally carries out conventional drying again Work.
Embodiment 2: the difference from embodiment 1 is that, a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;65 parts of nano diatomite;85 parts of lauric alcohol;70 parts of titanium dioxide;20 parts of pH adjusting agent; 700 parts of water, pH adjusting agent is acetic acid, and using acetic acid, the pH of system is adjusted to 6.When preparation, water is first added to reaction kettle It is interior, then amido silicon oil is added again, then nano diatomite, lauric alcohol, titanium dioxide, isomerous tridecanol are added, and It is stirring while adding, after stirring 60min, acetic acid is added, and the pH of system is made to be 6, then persistently stirs 40min.
Embodiment 3: the difference from example 2 is that, a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;65 parts of nano diatomite;85 parts of lauric alcohol;70 parts of titanium dioxide;6 parts of disperse blue;pH 20 parts of regulator;700 parts of water, pH adjusting agent is acetic acid, and using acetic acid, the pH of system is adjusted to 6.Disperse blue is fluffy using Shandong Lai Jia believes that the HA-RL of dye chemical industry Co., Ltd production is blue.When preparation, first water is added in reaction kettle, then again by amino Silicone oil is added, and then nano diatomite, lauric alcohol, titanium dioxide, disperse blue, isomerous tridecanol is added, and side edged stirs It mixes, after stirring 60min, adds acetic acid, and the pH of system is made to be 6, then persistently stir 40min.
Embodiment 4: the difference with embodiment 3 is that a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;65 parts of nano diatomite;85 parts of lauric alcohol;70 parts of titanium dioxide;6 parts of disperse blue;Member 25 parts of bright powder;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, and using acetic acid, the pH of system is adjusted to 6.Dispersion Indigo plant is blue using the HA-RL that Penglai, shandong Province Jia Xin dye chemical industry Co., Ltd produces.When preparation, first water is added in reaction kettle, Then amido silicon oil is added again, then by nano diatomite, lauric alcohol, titanium dioxide, disperse blue, anhydrous sodium sulphate, isomery 13 Alcohol is added, and stirring while adding, after stirring 60min, adds acetic acid, and the pH of system is made to be 6, then persistently stirs 40min。
Embodiment 5: the difference with embodiment 4 is that a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of alkyl phenol polyoxyethylene ether;65 parts of nano diatomite;85 parts of lauric alcohol;70 parts of titanium dioxide;Disperse blue 6 Part;25 parts of anhydrous sodium sulphate;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, and using acetic acid, the pH of system is adjusted to 6. Disperse blue is blue using the HA-RL that Penglai, shandong Province Jia Xin dye chemical industry Co., Ltd produces.When preparation, water is first added to reaction kettle It is interior, then amido silicon oil is added again, then by nano diatomite, lauric alcohol, titanium dioxide, disperse blue, anhydrous sodium sulphate, alkyl phenol Polyoxyethylene ether is added, and stirring while adding, after stirring 60min, adds acetic acid, and the pH of system is made to be 6, then Persistently stir 40min.
Embodiment 6-9 and the difference of embodiment 5 are that each chemical composition of soft finishing agent is in parts by weight such as following table institute Show: unit: part
Embodiment 6 Embodiment 7 Embodiment 8 Embodiment 9
Amido silicon oil 250 300 265 285
Alkyl phenol polyoxyethylene ether 10 20 13 17
Nano diatomite 50 80 60 70
Lauric alcohol 70 100 80 90
Titanium dioxide 20 40 25 35
Disperse blue 5 7 5.5 6.5
Anhydrous sodium sulphate 20 30 23 27
PH adjusting agent 10 30 15 25
Water 600 800 650 750
Embodiment 10-13 and the difference of embodiment 5 be, the temperature for the soft finishing agent being discharged into step S1 such as following table institute Show: unit: DEG C
Embodiment Embodiment 10 Embodiment 11 Embodiment 12 Embodiment 13
Temperature 40 50 43 47
Embodiment 14-17 and the difference of embodiment 5 are, first by the soft finishing agent temperature liter in rinsing bowl in step S4 It is up to as shown in the table: unit: DEG C
Embodiment Embodiment 14 Embodiment 15 Embodiment 16 Embodiment 17
Temperature 70 80 73 77
Embodiment 18-21 and the difference of embodiment 5 be, in step S4 last cloth impregnated in soft finishing agent when Between it is as shown in the table: unit: min
Embodiment Embodiment 18 Embodiment 19 Embodiment 20 Embodiment 21
Time 40 60 45 55
Comparative example 1: the difference from embodiment 1 is that, a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, using acetic acid, by system PH be adjusted to 6.When preparation, first water is added in reaction kettle, then amido silicon oil is added again, then by nanometer diatom Soil, lauric alcohol, isomerous tridecanol are added, and stirring while adding, after stirring 60min, add acetic acid, and make system PH is 6, then persistently stirs 40min.
Comparative example 2: the difference from embodiment 1 is that, a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;65 parts of nano diatomite;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, Using acetic acid, the pH of system is adjusted to 6.When preparation, first water is added in reaction kettle, then amido silicon oil is added again, Then nano diatomite, lauric alcohol, isomerous tridecanol are added, and stirring while adding, after stirring 60min, add acetic acid, And making the pH of system is 6, then persistently stirs 40min.
Comparative example 3: the difference from embodiment 1 is that, a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;85 parts of lauric alcohol;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, is used The pH of system is adjusted to 6 by acetic acid.When preparation, first water is added in reaction kettle, then amido silicon oil is added again, then Nano diatomite, lauric alcohol, isomerous tridecanol are added, and stirring while adding, after stirring 60min, add acetic acid, and So that the pH of system is 6,40min is then persistently stirred.
Comparative example 4: the difference from example 2 is that, a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;70 parts of titanium dioxide;20 parts of pH adjusting agent;700 parts of water, pH adjusting agent is acetic acid, using acetic acid, by system PH is adjusted to 6.When preparation, first water is added in reaction kettle, then amido silicon oil is added again, then by nano diatomite, Lauric alcohol, titanium dioxide, isomerous tridecanol are added, and stirring while adding, after stirring 60min, add acetic acid, and make The pH of system is 6, then persistently stirs 40min.
Comparative example 5: the difference with embodiment 3 is that a kind of soft finishing agent, each chemical composition is amino in parts by weight 275 parts of silicone oil;15 parts of isomerous tridecanol;65 parts of nano diatomite;85 parts of lauric alcohol;6 parts of disperse blue;20 parts of pH adjusting agent;Water 700 parts, pH adjusting agent is acetic acid, and using acetic acid, the pH of system is adjusted to 6.Disperse blue uses the good letter dyestuff of Penglai, shandong Province The HA-RL of work Co., Ltd production is blue.When preparation, first water is added in reaction kettle, then amido silicon oil is added again, then Nano diatomite, lauric alcohol, titanium dioxide, disperse blue, isomerous tridecanol are added, and stirring while adding, stir 60min Afterwards, acetic acid is added, and the pH of system is made to be 6, then persistently stirs 40min.
Test one: hygroscopicity test.
The terylene cloth for first choosing same batch is remembered using the soft finishing agent recorded in embodiment 1-5, in embodiment 1 Cloth is handled under the technique of load, and numbering is 1-5.Then, in same a batch of terylene cloth mentioned above again, using pair The soft finishing agent recorded in ratio 1-5 handles cloth under the technique that embodiment 1 is recorded, and numbering is 6-10.
Use the test method mentioned in " National Standard of the People's Republic of China GB/T 21655.1-2008 " to number 1- 10 cloth carries out hygroscopicity test, and testing experiment result is as shown in the table.
Test two: cloth whiteness detection.
By above-mentioned number be 1-10 cloth and meanwhile use Datacolor 600 carry out whiteness measurement, measurement data is such as Shown in following table.
Test data record:
Number Water absorption rate/% Drip the expanding time/s Measure wicking height/mm Whiteness value/%
1 113 3 107 82
2 112 2 112 102
3 114 2 117 109
4 112 3 112 113
5 113 3 112 113
6 67.8 113 53 82
7 77.6 63 83 82
8 72.1 83 63 83
9 73.3 71 76 93
10 112 3 113 87
Data analysis:
As can be seen from the above table, the good hygroscopicity of the corresponding cloth of number 1-5, and the corresponding cloth moisture absorption of number 6-9 Property it is poor, this explanation using the present invention in documented soft finishing agent, can significantly improve the hygroscopicity of polyester fabric.
From upper table, can significantly it find out, the whiteness of the corresponding cloth of number 2-5 is greater than 100, and other number institutes are right The whiteness for the cloth answered is lower than 100, this explanation, and documented soft finishing agent can prevent cloth in 2-5 of the embodiment of the present invention There is the phenomenon that yellowing.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications It should be regarded as protection scope of the present invention.

Claims (8)

1. a kind of soft finishing agent, it is characterised in that: the chemical composition of the soft finishing agent includes: in parts by weight
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
10-30 parts of pH adjusting agent;
600-800 parts of water.
2. a kind of soft finishing agent according to claim 1, it is characterised in that: the chemical composition of the soft finishing agent with Parts by weight meter includes:
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
60-80 parts of titanium dioxide;
10-30 parts of pH adjusting agent;
600-800 parts of water.
3. a kind of soft finishing agent according to claim 2, it is characterised in that: the chemical composition of the soft finishing agent with Parts by weight meter includes:
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
20-40 parts of titanium dioxide;
5-7 parts of disperse blue;
10-30 parts of pH adjusting agent;
600-800 parts of water.
4. a kind of soft finishing agent according to claim 3, it is characterised in that: the chemical composition of the soft finishing agent with Parts by weight meter includes:
250-300 parts of amido silicon oil;
10-20 parts of emulsifier;
50-80 parts of nano diatomite;
70-100 parts of lauric alcohol;
20-40 parts of titanium dioxide;
5-7 parts of disperse blue;
20-30 parts of anhydrous sodium sulphate;
10-30 parts of pH adjusting agent;
600-800 parts of water.
5. a kind of soft finishing agent according to claim 1, it is characterised in that: the emulsifier is isomerous tridecanol, alkane Base phenol polyethenoxy ether is one such, and usage amount is 15 parts.
6. a kind of a kind of technique for applying of soft finishing agent according to claim 4, it is characterised in that: including walking as follows It is rapid:
S1: drain heating;
S2: cloth pads;
S3: wet cloth rubbing;
S4: secondary to pad;The temperature of the soft finishing agent rises to 70-80 DEG C when padding, and again cloth is existed after padding 40-60min is impregnated in the soft finishing agent;
S5: clear water rinses.
7. a kind of soft finishing agent according to claim 6, it is characterised in that: the step S1, by the soft finish Agent is emitted into slurry tank, and soft finishing agent is warming up to 40-50 DEG C, and cloth is then carried out S2 processing.
8. a kind of soft finishing agent according to claim 6, it is characterised in that: the step S2, cloth pad repeatedly to It is 5 times few, then carry out step S3 processing.
CN201910436345.4A 2019-05-23 2019-05-23 A kind of soft finishing agent and its technique for applying Pending CN110117904A (en)

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Application publication date: 20190813