CN110116291A - A kind of surface ultrasonic burnishing treatment process improving uranium material corrosion resisting property - Google Patents

A kind of surface ultrasonic burnishing treatment process improving uranium material corrosion resisting property Download PDF

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Publication number
CN110116291A
CN110116291A CN201910411882.3A CN201910411882A CN110116291A CN 110116291 A CN110116291 A CN 110116291A CN 201910411882 A CN201910411882 A CN 201910411882A CN 110116291 A CN110116291 A CN 110116291A
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uranium material
pressure head
uranium
ultrasonic burnishing
treatment process
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Chinese (zh)
Inventor
刘柯钊
刘泾源
陈德华
苏斌
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Institute of Materials of CAEP
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Institute of Materials of CAEP
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Priority to CN201910411882.3A priority Critical patent/CN110116291A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23PMETAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
    • B23P9/00Treating or finishing surfaces mechanically, with or without calibrating, primarily to resist wear or impact, e.g. smoothing or roughening turbine blades or bearings; Features of such surfaces not otherwise provided for, their treatment being unspecified
    • B23P9/02Treating or finishing by applying pressure, e.g. knurling

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)

Abstract

The invention discloses a kind of surface ultrasonic burnishing treatment process for improving uranium material corrosion resisting property, it is characterized in that, ultrasonic burnishing processing is carried out to its surface using rolling pressure head again after carrying out surface machining to uranium material, wherein, rotation is kept in every control uranium material in ultrasonic burnishing process, Proper Match rolling processing process parameter, control rolling pressure head are moved along the side axial and/or end face normal direction of uranium material and are remained and the contact of uranium material under pressure control.The present invention provides a kind of specific adaptation in the surface ultrasonic burnishing treatment process of uranium material, initial oxidation caused by the technique can weaken in rolling process, improve Part Surface Roughness, forms the metamorphic layer of a layer specific on the surface of the material and improve the corrosion resistance of uranium material.

Description

A kind of surface ultrasonic burnishing treatment process improving uranium material corrosion resisting property
Technical field
The invention belongs to the technical fields of metal material machining, and it is resistance to be more particularly related to a kind of raising uranium material The surface ultrasonic burnishing treatment process of corrosion energy.
Background technique
Uranium is a kind of metal that chemical property is extremely active, be subject to the chemistry of medium in environment, electrochemical action and send out Raw corrosion forms a variety of corrosion products, to influence its materialization and nuclearity energy.
Surface rolling handles the mantle micro structure of controllable uranium material, and then its corrosion behavior is made to change.But In uranium material rolling process, due to inputting very high energy when rolling, a degree of initial oxidation, and material after rolling will cause Grain size, texture, residual stress state, surface topography of material etc. all can great changes will take place, various factors coupling together, to uranium The influence of material corrosion is complicated, if the improper corrosion rate that can accelerate uranium material of regulation, causes even more serious economic damage It loses.
Summary of the invention
In order to solve the problems in the existing technology, the object of the present invention is to provide a kind of specific adaptations in uranium material Surface ultrasonic burnishing treatment process, initial oxidation caused by which can weaken in rolling process improve Part Surface Roughness, The metamorphic layer of a layer specific is formed on the surface of the material and improves the corrosion resistance of uranium material.
The present invention provides a kind of surface ultrasonic burnishing treatment process for improving uranium material corrosion resisting property, carry out to uranium material It is processed again using the ultrasonic burnishing that rolling pressure head carries out several times to uranium material surface after the machining of surface, wherein at every time Uranium material is controlled in ultrasonic burnishing process keeps rotation, side axial and/or end of the control rolling pressure head along uranium material Face normal direction is mobile and remains and the contact of uranium material.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property, the uranium are improved according to the present invention Material is metallic uranium or uranium alloy, and the uranium material surface roughness after the machining of surface is in Ra1.6 or less.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property, the rolling are improved according to the present invention Pressure pressure head is hardness not less than the spherical ball pressure head that 60HRC, diameter D are 10~20mm.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property is improved according to the present invention, it is described super The input supersonic frequency f of sound rolling processing is 20~40kHz and rolling pressure head output end amplitude A is 3~10 μm.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property is improved according to the present invention, it is described super Sound rolling processing specifically includes the following steps:
A, uranium material is loaded on lathe, controls the top for rolling pressure head and uranium material surface contact and guarantees rolling pressure The center of head and the axis of uranium material are in sustained height;
B, opening lathe rotates uranium material, and control knife rest displacement makes to roll pressure head indentation uranium material surface Δ X and control Knife rest and rolling pressure head are fed along the axial direction and/or normal direction of uranium material, keep depressing force F that rolling is pressed on rolling pressure head Head is remained to be contacted with the side of uranium material and/or end face;
C, follow rest makes rolling pressure head return to initial position and keep drafts Δ X after completing 1 time ultrasonic burnishing processing It is constant, the processing of surface ultrasonic burnishing is completed after repeating several processing all over ultrasonic burnishing.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property, the uranium are improved according to the present invention The rotation speed V of material1For 20~100r/min, the drafts Δ X for rolling pressure head is 0.01~0.1mm, and depressing force F is 200 ~1000N.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property is improved according to the present invention, it is described super The depressing force F acted on rolling pressure head during sound rolling and processing meets following formula:
F=(k1×D)×(k2× A),
Wherein k1=0.05~0.15, k2=0.6 × 102~1.5 × 102, D is rolling pressure head diameter, and A is rolling pressure head Output end amplitude.
One embodiment of the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property, the rolling are improved according to the present invention Press the feed speed V of pressure head2For 2~10mm/min, the processing pass of ultrasonic burnishing processing is 2~3 times.
One embodiment for improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to the present invention, on surface Oil lubrication and cooling are used in ultrasonic burnishing treatment process.
Compared with prior art, the beneficial effect comprise that
(1) greatly save uranium material antiseptic erosion processing cost: the corrosion resistance of Yao Tigao uranium material is usually required to uranium Material integral manufacturing method improves or carries out the surface treatment such as coating to part, and cost is high and technical process is complicated, passes through Rolling processing appropriate realizes uranium material surface reconstructed tissue to improve its corrosion resistance, and method is simple and exploitativeness is strong, Part manufacturing cost can greatly be saved.
(2) realize that uranium material property is set using processing technology organization of regulation control structure: the present invention utilizes ultrasonic burnishing method, For the special physico-chemical property of uranium material high activity, in conjunction with the evolution characteristics of rolling process materials microstructure, by special The promotion of uranium material corrosion resistance is realized in technique customization.
Detailed description of the invention
Fig. 1 is shown the metallic uranium material handled in embodiment 1 using surface ultrasonic burnishing of the present invention and only carries out surface The oxidation rate comparison diagram of the metallic uranium material of machining.
Fig. 2 a is shown in embodiment 1 using the surface state of surface ultrasonic burnishing of the present invention treated metallic uranium material Microcosmic schematic diagram, Fig. 2 b show original rolling technology treated the microcosmic schematic diagram of surface state of metallic uranium material.
Fig. 3 shows the micro- of the metamorphic layer in embodiment 2 using surface ultrasonic burnishing of the present invention treated u-ni alloy See sectional view.
Specific embodiment
All features disclosed in this specification or disclosed all processing methods or in the process the step of, in addition to mutual Other than the feature and/or step of repulsion, it can combine in any way.
Any feature disclosed in this specification unless specifically stated can be equivalent or with similar purpose by other Alternative features are replaced.That is, unless specifically stated, each feature is an example in a series of equivalent or similar characteristics ?.
The surface ultrasonic burnishing treatment process for improving uranium material corrosion resisting property to the present invention is described in detail below.
Uranium is a kind of metal that chemical property is extremely active, and the corrosion of uranium material can seriously affect the service life of product, The corrosion resistance of material can be improved by institutional framework regulation, rolling processing is exactly a kind of method easily and effectively.
But severe plastic deformation, which occurs, for surfacing in rolling process causes energy higher, high activity this for uranium Serious oxidative phenomena can occur during processing for material;In addition, rolling processing will affect the grain size of material, texture, residual These influence factors are only carried out Proper Match by many factors such as residue stress, can be only achieved the effect for improving corrosion resistance, If matching is improper, good metamorphic layer cannot be formed, can accelerate the corrosion rate during uranium material military service instead, therefore for The rolling processing of high active material needs to design special treatment process according to material structure evolution characteristics.
The present invention is according to the relationship between uranium materials microstructure structure and corrosion behavior, by becoming to during ultrasonic burnishing The control requirement of shape, has devised the ultrasonic burnishing technique specifically for uranium material, configuration state needed for obtaining on the surface of the material Metamorphic layer, can obviously improve the corrosion resistance of uranium material after the process.
An exemplary embodiment of the present invention, the surface ultrasonic burnishing treatment process for improving uranium material corrosion resisting property Specifically: it is rolled again using the ultrasound that rolling pressure head carries out several times to uranium material surface after carrying out surface machining to uranium material Pressure processing, wherein keep rotation in every control uranium material in ultrasonic burnishing process, control rolling pressure head is along uranium material Side axial and/or end face normal direction it is mobile and remain and the contact of uranium material.
The uranium material that is applicable in of the present invention can be metallic uranium or uranium alloy, can be common blank, bar, can also be with It is part.Wherein it is preferred to control the uranium material surface roughness after the machining of surface in Ra1.6 or less.Pass of the invention It is in place of key through suitable process parameter control, the accurate deformation process for adjusting material, so that skin-material acquisition is specific Institutional framework (couplings such as grain size, texture, residual stress state, surface smoothness), to make the anticorrosive of material Performance improves.
The purpose of machining is to remove the oxide skin of uranium material surface, and it is subsequent to adapt to obtain lower roughness Rolling and processing.It controls roughness and in Ra1.6 or less is in order to obtain better surface smoothness before rolling, if original processing material Expect roughness it is larger, then subsequent rolling and processing need to obtain biggish deflection could be by wave crest rolling, one side component ruler The very little accuracy of form and position it is difficult to ensure that, another aspect material deformation uniformity is poor, by deform it is uneven caused by surface potential difference It increases, it is easier to cause local corrosion behavior.
The rolling pressure head that the present invention uses is preferably that hardness is not less than 60HRC, diameter D for the spherical ball pressure of 10~20mm Head, surface have good finish to avoid the adverse effect to uranium material as far as possible.
Method of the invention can process end face and side, can individually process or process together.Wherein, side is Along the axis rolling and processing of uranium material bar, the metamorphic layer that side rolling obtains is entire side surface;End face be then pressure head with The end face of uranium material bar contacts and gradually moves so that entire end face is moulded along normal direction ecto-entad or from inside to outside Property deformation, end face rolling obtain metamorphic layer be a plane, sample is conveniently used for the analysis of institutional framework and corrosion resistance Test.
Specifically, the ultrasonic burnishing processing that the present invention carries out includes the following steps.
Step a:
Uranium material is loaded on lathe, the top for rolling pressure head and uranium material surface contact are controlled and guarantees to roll pressure head Center and uranium material axis in sustained height.
Wherein, uranium material is preferably bar.
Step b:
Opening lathe rotates uranium material, and control knife rest displacement makes to roll pressure head indentation uranium material surface Δ X and controls knife Frame and rolling pressure head are fed along the axial direction and/or normal direction of uranium material, and depressing force F is kept to roll pressure head on rolling pressure head It remains and is contacted with the side of uranium material and/or end face.
Preferably, the rotation speed V of uranium material is controlled1For 20~100r/min, the drafts Δ X for rolling pressure head is 0.01 ~0.1mm and depressing force F are 200~1000N, roll the feed speed V of pressure head2For 2~10mm/min.
Also, the input supersonic frequency f of ultrasonic burnishing processing be 20~40kHz and rolling pressure head output end amplitude A be 3~ 10 μm, A value depends on the plastic property of uranium material, and the poor uranium material of plasticity then chooses lesser A value.
Wherein, the depressing force F acted in ultrasonic burnishing process on rolling pressure head should meet following formula:
F=(k1×D)×(k2× A),
Wherein, k1=0.05~0.15, k2=0.6 × 102~1.5 × 102, D is rolling pressure head diameter, and A is rolling pressure head Output end amplitude, k1、k2Optimal value depend on processing uranium materials microstructure performance characteristics.
That is, depressing force F value is determined according to the diameter of rolling pressure head and the amplitude binding constant of uranium material property selection, Initial oxidation caused by so as to weaken in rolling process simultaneously improves Part Surface Roughness, forms one layer of spy on the surface of the material Fixed metamorphic layer improves the corrosion resistance of uranium material.
Step c:
Follow rest makes rolling pressure head return to initial position and keep drafts Δ X not after completing 1 time ultrasonic burnishing processing Become, completes the processing of surface ultrasonic burnishing after repeating several processing all over ultrasonic burnishing.
Wherein, the processing pass of ultrasonic burnishing processing is not easy excessively, and preferably 2~3 times.
It is needed in the ultrasonic burnishing treatment process of surface using oil lubrication and cooling to prevent part heating and oxidation, and subtracted Friction between small rolling pressure head and uranium material surface.
It should be understood that above embodiment and following embodiment that the present invention is described in detail are merely to illustrate the present invention rather than limit The scope of the present invention processed, some nonessential improvement and tune that those skilled in the art's above content according to the present invention is made It is whole to all belong to the scope of protection of the present invention.
The present invention is further explained in the light of specific embodiments.
Embodiment 1:
It realizes the surface ultrasonic burnishing processing that metallic uranium material corrosion resistance is promoted, sequentially includes the following steps:
(1) turning machining in side is carried out to the metallic uranium bar having a size of Ф 60mm × 150mm first, after turning Surface roughness is Ra1.6.
(2) ultrasonic burnishing processing is carried out to the side after turning, using hardness be 75HRC and diameter is the spherical shape of Ф 15mm The top of spherical ball pressure head is in contact with the side after turning, and guarantees pressure head center and metallic uranium bar by ball pressure head Axis in sustained height.
(3) it opens ultrasonic generator and controls that supersonic frequency is 28kHz, bulb output end amplitude A is 4 μm, open lathe It rotates metallic uranium bar with the speed of 30r/min, makes to roll pressure head indentation metallic uranium billet surface by control knife rest displacement 0.02mm, control knife rest move rolling pressure head with the speed of 5mm/min along the axial direction of metallic uranium bar, complete entire 1 time ultrasonic burnishing of side is processed.
(4) stop the rotation of metallic uranium bar, control knife rest returns to initial position, completes surface after step 3 is repeated 2 times Ultrasonic burnishing processing uses oil lubrication and cooling metallic uranium bar and rolling pressure head in above-mentioned process.
Fig. 1 is shown the metallic uranium material handled in embodiment 1 using surface ultrasonic burnishing of the present invention and only carries out surface The oxidation rate comparison diagram of the metallic uranium material of machining.As seen from Figure 1, it is rolled using institute of the invention to technique Processing can obviously reduce the oxidation rate of uranium material.
Fig. 2 a is shown in embodiment 1 using the surface state of surface ultrasonic burnishing of the present invention treated metallic uranium material Microcosmic schematic diagram, Fig. 2 b show original rolling technology treated the microcosmic schematic diagram of surface state of metallic uranium material.By scheming 2a and Fig. 2 b can be seen that since uranium material activity is very high, the initial oxidation that conventional rolling depression method can cause material surface strong, After being handled using present invention process, initial oxidation problem be improved significantly.
Embodiment 2:
It realizes the ultrasonic burnishing technique that U-Nb alloy material corrosion resistance is promoted, sequentially includes the following steps:
(1) processing of facing machinery is carried out to the U-Nb alloy bar having a size of Ф 40mm × 100mm first, after turning Surface roughness be Ra0.8.
(2) ultrasonic burnishing processing is carried out to the end face after turning, using hardness be 70HRC and diameter is the spherical shape of Ф 14mm The top of spherical ball pressure head is in contact with the end face after turning, and guarantees pressure head center and U-Nb alloy bar by ball pressure head The axis of material is in sustained height.
(3) it opens ultrasonic generator and controls that supersonic frequency is 28kHz, bulb output end amplitude A is 6 μm, open lathe Make U-Nb alloy bar with the rotation of 40r/min speed, makes to roll pressure head indentation U-Nb alloy bar table by control knife rest displacement Face 0.04mm, control knife rest make to roll pressure head along the normal orientation of U-Nb alloy bar with the speed ecto-entad of 6mm/min 1 time ultrasonic burnishing processing of entire end face is completed in movement.
(7) stop the rotation of U-Nb alloy bar, control knife rest returns to initial position, completion table after step 3 is repeated 2 times Ultrasonic burnishing processing in face uses oil lubrication and cooling metallic uranium bar and rolling pressure head in above-mentioned process.
Fig. 3 shows the micro- of the metamorphic layer in embodiment 2 using surface ultrasonic burnishing of the present invention treated u-ni alloy See sectional view.As seen from Figure 3, embodiment 2 using having of obtaining of present invention process treated U-Nb alloy surface compared with The metamorphic layer (left side white ribbon) of good corrosion resistance
In conclusion the present invention is according to uranium materials microstructure and corrosion behavior feature, by ultrasonic burnishing technology controlling and process, A layer specific metamorphic layer is processed in uranium material surface, realizes the promotion of uranium material corrosion resistance, simple process is flexible, anti-corruption It is obvious to lose effect.The technique can meet the surface treatment of uranium and variety classes uranium alloy, carry out appropriate adjustment according to material property It can also be used for the surface treatment of other high chemically active materials (such as magnesium metal and its alloy), there is the wider scope of application.
The invention is not limited to specific embodiments above-mentioned.The present invention, which expands to, any in the present specification to be disclosed New feature or any new combination, and disclose any new processing method or process the step of or any new combination.

Claims (9)

1. a kind of surface ultrasonic burnishing treatment process for improving uranium material corrosion resisting property, which is characterized in that carry out table to uranium material It is processed again using the ultrasonic burnishing that rolling pressure head carries out several times to uranium material surface after the machining of face, wherein every all over super Uranium material is controlled during sound rolling and processing keeps rotation, side axial and/or end face of the control rolling pressure head along uranium material Normal direction is mobile and remains and the contact of uranium material.
2. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 1, which is characterized in that institute Stating uranium material is metallic uranium or uranium alloy, and the uranium material surface roughness after the machining of surface is in Ra1.6 or less.
3. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 1, which is characterized in that institute Stating rolling pressure head is hardness not less than the spherical ball pressure head that 60HRC, diameter D are 10~20mm.
4. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 1, which is characterized in that institute The input supersonic frequency f for stating ultrasonic burnishing processing is 20~40kHz and rolling pressure head output end amplitude A is 3~10 μm.
5. according to claim 1 to described in any one of 4 improve uranium material corrosion resisting property surface ultrasonic burnishing treatment process, Be characterized in that, ultrasonic burnishing processing specifically includes the following steps:
A, uranium material is loaded on lathe, controls the top for rolling pressure head and uranium material surface contact and guarantees to roll pressure head The axis of center and uranium material is in sustained height;
B, opening lathe rotates uranium material, and control knife rest displacement makes to roll pressure head indentation uranium material surface Δ X and controls knife rest It is fed with rolling pressure head along the axial direction and/or normal direction of uranium material, keeps depressing force F that rolling pressure head is begun on rolling pressure head It keeps contacting with the side of uranium material and/or end face eventually;
C, follow rest makes rolling pressure head return to initial position and keep drafts Δ X constant after completing 1 time ultrasonic burnishing processing, The processing of surface ultrasonic burnishing is completed after repeating several processing all over ultrasonic burnishing.
6. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 5, which is characterized in that institute State the rotation speed V of uranium material1For 20~100r/min, the drafts Δ X for rolling pressure head is 0.01~0.1mm, and depressing force F is 200~1000N.
7. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 6, which is characterized in that institute It states the depressing force F acted on rolling pressure head in ultrasonic burnishing process and meets following formula:
F=(k1×D)×(k2× A),
Wherein k1=0.05~0.15, k2=0.6 × 102~1.5 × 102, D is rolling pressure head diameter, and A is rolling pressure head output end Amplitude.
8. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 5, which is characterized in that institute State the feed speed V of rolling pressure head2For 2~10mm/min, the processing pass of ultrasonic burnishing processing is 2~3 times.
9. improving the surface ultrasonic burnishing treatment process of uranium material corrosion resisting property according to claim 1, which is characterized in that Oil lubrication and cooling are used in the ultrasonic burnishing treatment process of surface.
CN201910411882.3A 2019-05-17 2019-05-17 A kind of surface ultrasonic burnishing treatment process improving uranium material corrosion resisting property Pending CN110116291A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114147236A (en) * 2021-11-30 2022-03-08 大连海事大学 Method for manufacturing stainless steel through ultrasonic rolling and strengthening laser additive
CN114799776A (en) * 2022-06-29 2022-07-29 中国空气动力研究与发展中心超高速空气动力研究所 Process method for improving surface roughness and hardness of inner surface of axisymmetric nozzle

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CN101220406A (en) * 2008-01-29 2008-07-16 天津大学 Executing agency and processing method for half wave length ultrasonic surface rolling process
CN101220405A (en) * 2007-10-10 2008-07-16 天津大学 Ultrasonic surface rolling process nanoparticlization method and apparatus
WO2010136010A1 (en) * 2009-05-28 2010-12-02 Mtu Aero Engines Gmbh Method and apparatus for surface hardening a component, which is made of an intermetallic compound at least in the region of the surface to be hardened
CN105127668A (en) * 2015-08-28 2015-12-09 华东交通大学 Multi-directional ultrasonic rolling and processing device
CN108098253A (en) * 2017-12-27 2018-06-01 中国工程物理研究院材料研究所 A kind of processing method for improving metal material cutting ability

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Publication number Priority date Publication date Assignee Title
CN101220405A (en) * 2007-10-10 2008-07-16 天津大学 Ultrasonic surface rolling process nanoparticlization method and apparatus
CN101220406A (en) * 2008-01-29 2008-07-16 天津大学 Executing agency and processing method for half wave length ultrasonic surface rolling process
WO2010136010A1 (en) * 2009-05-28 2010-12-02 Mtu Aero Engines Gmbh Method and apparatus for surface hardening a component, which is made of an intermetallic compound at least in the region of the surface to be hardened
CN105127668A (en) * 2015-08-28 2015-12-09 华东交通大学 Multi-directional ultrasonic rolling and processing device
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Publication number Priority date Publication date Assignee Title
CN114147236A (en) * 2021-11-30 2022-03-08 大连海事大学 Method for manufacturing stainless steel through ultrasonic rolling and strengthening laser additive
CN114799776A (en) * 2022-06-29 2022-07-29 中国空气动力研究与发展中心超高速空气动力研究所 Process method for improving surface roughness and hardness of inner surface of axisymmetric nozzle

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