CN110106699A - A kind of submissive fragrant garment piece of solid - Google Patents
A kind of submissive fragrant garment piece of solid Download PDFInfo
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- CN110106699A CN110106699A CN201910394573.XA CN201910394573A CN110106699A CN 110106699 A CN110106699 A CN 110106699A CN 201910394573 A CN201910394573 A CN 201910394573A CN 110106699 A CN110106699 A CN 110106699A
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- submissive
- fragrant
- garment piece
- solid
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to detergent technical fields, and for the problem of the lasting aroma retaining effect difference on clothing, provide a kind of submissive fragrant garment piece of solid, the component including following mass fraction: 1-85 parts of softener, the softener is cationic surfactant；Fatty acid or 1-65 parts of fatty alcohol；1-35 parts of polyethylene glycol；Essence microcapsule or 0.5-20 parts of capsule perfume.The preparation method of the submissive fragrant garment piece of a kind of solid, comprising the following steps: the preparation of S1, impregnating agent；S2, dipping；S3, hot rolling；S4, drying molding.By dryer, fricting movement is heated and rotated back and forth to the continuous of fragrant garment piece submissive to solid during the work time, so that the impregnating agent on the submissive fragrant garment piece of solid is detached from fabric, and is transferred on clothing, is conducive to the lasting aroma retaining effect for improving clothing.
Description
Technical field
The present invention relates to detergent technical fields, more specifically, it relates to a kind of submissive fragrant garment piece of solid.
Background technique
With the increasing living standards of the people, requirement of the people to clothes not only rests in clothes quality itself,
But the requirement to the fragrance being adapted with clothes also improves, and is especially eating up the tastes such as chafing dish, barbecue than heavier food
After object or after being moved through, people are intended to have the function of lasting on clothing.
Currently, most people can select the mode of perfumes for clothing add fragrance, still, perfume it is expensive,
Importantly, perfume can not continue lasting；Groups of people can also select the detergent washing clothing with lasting function, still,
Lasting ingredient in detergent is also dissolved in the water simultaneously in washing process, is discharged together with sewage so that clothing without
Method continues lasting, therefore, still there is improved space.
Summary of the invention
In view of the deficienciess of the prior art, the first object of the present invention is to provide a kind of solid submissive fragrant garment piece, tool
Have so that the advantages of continuing lasting using the clothing after the submissive fragrant garment piece of solid.
To achieve the above object, the present invention provides the following technical scheme that
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
1-85 parts of softener, the softener is cationic surfactant；
Fatty acid or 1-65 parts of fatty alcohol；
1-35 parts of polyethylene glycol；
Essence microcapsule or 0.5-20 parts of capsule perfume.
The present invention is further arranged to: the component including following mass fraction:
1-35 parts of softener；
Fatty acid or 5-45 parts of fatty alcohol；
1-10 parts of polyethylene glycol；
Essence microcapsule or 0.5-10 parts of capsule perfume.
By adopting the above technical scheme, polyethylene glycol has very strong wrapped, is conducive to wrap up essence microcapsule or capsule
Perfume, so that the stability of essence microcapsule or capsule perfume improves, so that essence microcapsule or capsule perfume are in solid
It is not easy to distribute during the storage of submissive perfume garment piece, is conducive to essence microcapsule or capsule perfume remains good lasting
Property, and then be conducive to improve the lasting aroma retaining effect using the clothing after the submissive fragrant garment piece of solid；Meanwhile polyethylene glycol belong to it is non-
Ionic surface active agent, it is not easy to be influenced by anion or cation, stability is high, so that being wrapped in poly- second
The stability of essence microcapsule or capsule perfume in glycol is high, and then is conducive to improve using after the submissive fragrant garment piece of solid
The lasting aroma retaining effect of clothing；In addition, the submissive fragrant garment piece of solid in the present invention is generally used in dryer, due to fatty acid or
The fusing point of fatty alcohol and polyethylene glycol is lower, is easy to melt after the heat treatment by dryer, so that by wrapping
The essence microcapsule or capsule perfume wrapped up in are released to be adhered on clothing, simultaneously as detergent is generally anion table
Face activating agent generally has anion, by using cationic surfactant as soft after clothing is using detergent washing
Along agent, be conducive to make while enhancing the flexibility of clothing the anion on clothing more easily and on the submissive fragrant garment piece of solid
Cation is attracted each other, to be conducive to enhance the adsorption capacity of solid submissive fragrant garment piece and clothing, so that clothing and perfume
The combination of precise and tiny capsule or capsule perfume is more stable, is conducive to the lasting lasting of clothing；By using essence microcapsule or glue
Capsule perfume is in conjunction with clothing so that clothing band is aromatic, since essence microcapsule or capsule perfume can be discharged by friction
Fragrance, be conducive to clothing sustained release fragrance, to be conducive to improve the lasting aroma retaining effect of clothing；Since polyethylene glycol has
There are good antistatic property, flexibility and moisture retention, by the cooperation of polyethylene glycol and softener, is conducive to improve holding for clothing
Be conducive to improve the flexibility and antistatic property of clothing while the effect of continuous lasting.
The present invention is further arranged to: further include the component of following mass fraction:
1-10 parts of vaseline.
By adopting the above technical scheme, by the way that vaseline is added, vaseline has fabulous film forming and ductility, is conducive to
Solid perfume (or spice) garment piece is preferably uniformly spread on clothing after melting, so that solid perfume (or spice) garment piece is easier to be attached on clothing after melting
On object, while being conducive to essence microcapsule and capsule perfume is evenly distributed on clothing, and then is conducive to improve and uses solid
The lasting aroma retaining effect of clothing after submissive perfume garment piece；Meanwhile vaseline also has splendid soothing effect, is conducive to improve clothing
The skin-friendly of object, so that clothing has the function of lubrication protection to skin, so that the wearing comfort of clothing improves.
The present invention is further arranged to: the vaseline is medical grade vaseline.
By adopting the above technical scheme, by using medical grade vaseline, be conducive to the use for improving the submissive fragrant garment piece of solid
Safety, so that being not easy in the submissive fragrant garment piece of solid containing to environment or to the disagreeableness substance of human body, so that making
It is not easy to affect human health with the clothing after the submissive fragrant garment piece of solid.
The present invention is further arranged to: the fatty acid is the long alkyl chain saturation higher aliphatic that carbon atom number is 8-18
Acid, the fatty alcohol are the fatty alcohol that carbon atom number is 8-22.
By adopting the above technical scheme, it for the long alkyl chain saturated higher fatty acid of 8-18 and is adopted by using carbon atom number
The fatty alcohol for being 8-22 with carbon atom number is conducive to the other components of fatty acid or fatty alcohol and the submissive fragrant garment piece of solid preferably
Cooperate and preferably dissolve each other, to be conducive to improve the stability of the submissive fragrant garment piece of solid, so that using the submissive fragrant clothing of solid
The lasting aroma retaining effect of clothing after piece is more preferable.
The present invention is further arranged to: the softener is Biester quarternary ammoniumsalt, dioctadecyl dimethyl ammonium chloride, soft
Piece or consistent lubricant essence in any one.
By adopting the above technical scheme, by using Biester quarternary ammoniumsalt, dioctadecyl dimethyl ammonium chloride, film or soft
For any one in olein as softener, the above substance all has extremely strong biological degradability, it is not easy to cause shadow to environment
It rings, is conducive to the feature of environmental protection for improving solid softening laundry piece.
The present invention is further arranged to: the softener is Biester quarternary ammoniumsalt.
By adopting the above technical scheme, by using Biester quarternary ammoniumsalt as softener, Biester quarternary ammoniumsalt has excellent
Softness and antistatic property, and dosage is few, effect is good, overall cost is low, has high cost performance；Meanwhile di-ester-base season
Ammonium salt has good heat resistance, not easily yellow after high temperature is dried with the processed clothing of Biester quarternary ammoniumsalt.
The present invention is further arranged to: the molecular weight of the polyethylene glycol is 1500-10000.
By adopting the above technical scheme, the polyethylene glycol for being 1500-10000 by using molecular weight, is conducive to poly- second two
The moisture retention and viscosity of alcohol are controlled, so that it is more preferable during the storage of the submissive fragrant garment piece of solid to be conducive to polyethylene glycol
Ground wraps up essence and essence microcapsule, while being conducive to polyethylene glycol in the use process of the submissive fragrant garment piece of solid preferably
Essence and essence microcapsule are discharged, and then is conducive to essence and essence microcapsule preferably sticks with clothing, so that clothing
Lasting aroma retaining effect enhancing.
In view of the deficienciess of the prior art, the second object of the present invention is to provide a kind of system of the submissive fragrant garment piece of solid
Preparation Method has the advantages that preparing the submissive fragrant garment piece of resulting solid has so that continuing lasting using the clothing after fragrant garment piece.
To achieve the above object, the present invention provides the following technical scheme that
A kind of preparation method of the submissive fragrant garment piece of solid, comprising the following steps:
The preparation of S1, impregnating agent: add by mass parts ratio mixing softener, fatty acid or fatty alcohol, polyethylene glycol, stirring
Heat to each component is completely dissolved to liquid condition, adds essence microcapsule or capsule perfume, and stir evenly, and forms dipping
Agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C -35 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
By adopting the above technical scheme, by first heating softener, fatty acid or fatty alcohol, polyethylene glycol and vaseline
Dissolution, adds essence microcapsule or capsule perfume, is conducive to polyethylene glycol and preferably wraps up essence microcapsule or capsule perfume,
So that essence microcapsule is more not easy to distribute during the storage of the submissive fragrant garment piece of solid, it is micro- to be conducive to raising essence
The stability of capsule or capsule perfume, so that more preferable using the lasting aroma retaining effect of the clothing after the submissive fragrant garment piece of solid；
Due to generally having containing anion by attracting each other between the cation in the anion and impregnating agent on fabric in fabric
Preferably and the combination of fabric conducive to impregnating agent, be conducive to improve stability of the impregnating agent in conjunction with fabric；By will sufficiently
Fabric in conjunction with impregnating agent is by hot-rolling hot rolling, so that impregnating agent extra on fabric is rolled, to be conducive to impregnating agent
Be distributed on the fabric it is more uniform, meanwhile, the temperature by controlling hot rolling is 30 DEG C -35 DEG C and is stained with using cold air drying
The fabric of impregnating agent is conducive to the rate of drying for accelerating impregnating agent, is conducive to the abundant drying of impregnating agent, is conducive to improve poly- second
The stability of glycol and essence microcapsule or capsule perfume, so that using the lasting lasting of the clothing after the submissive fragrant garment piece of solid
Effect is more preferable；When the submissive fragrant garment piece use of solid is in dryer, constantly heated by dryer fragrant garment piece submissive to solid
And fricting movement is rotated back and forth, the impregnating agent be conducive on fabric is separated from fabric, while being conducive to the micro- glue of essence
Capsule or capsule perfume release, and are sticked by the softener with cation with clothing, so that in the submissive fragrant garment piece of solid
The impregnating agent separated from fabric is preferably in conjunction with clothing, to be conducive to essence microcapsule or capsule perfume preferably
In conjunction with clothing, so that more preferable using the lasting aroma retaining effect of the clothing after the submissive fragrant garment piece of solid；In addition, the submissive fragrant clothing of solid
Piece uses anhydrous formulations, can not add preservative ingredient, is conducive to the safety in utilization for improving the submissive fragrant garment piece of solid, so that solid
The submissive fragrant garment piece of body is not easy to impact environment while being not easy to affect human health.
The present invention is further arranged to: in the step S1, the temperature control of agitating and heating is 45 DEG C -65 DEG C.
By adopting the above technical scheme, it is 45 DEG C -65 DEG C by controlling the temperature of agitating and heating, is conducive to the submissive fragrant clothing of solid
The each component of piece, which is easier to dissolve, forms liquid condition, so that each component of the submissive fragrant garment piece of solid more easily mutually mixes
It is even, to be conducive to improve the stability of the submissive fragrant garment piece of solid, so that continuing using the clothing after the submissive fragrant garment piece of solid
Aroma retaining effect is more preferable.
In conclusion the invention has the following advantages:
1. polyethylene glycol has very strong wrapped and stability, it is not easy to it is influenced by anion or cation,
Be conducive to wrap up essence microcapsule or capsule perfume, so that the storage of essence microcapsule or capsule perfume in the submissive fragrant garment piece of solid
It is not easy to distribute in the process, is conducive to improve the lasting aroma retaining effect using the clothing after the submissive fragrant garment piece of solid；
2. by dryer, friction fortune is heated and rotated back and forth to the continuous of fragrant garment piece submissive to solid during the work time
It is dynamic, so that the impregnating agent on the submissive fragrant garment piece of solid is detached from fabric, and it is transferred on clothing, is conducive to improve clothing
Lasting aroma retaining effect；
3. polyethylene glycol has good antistatic property, flexibility and moisture retention, pass through matching for polyethylene glycol and softener
Close, be conducive to be conducive to improve while improving the effect of the lasting lasting of clothing the softness of clothing, submissive performance and
Antistatic property；
4. the submissive fragrant garment piece of solid uses anhydrous formulations, preservative ingredient can not be added, so that the submissive fragrant garment piece of solid is not
It is not easy to impact environment while being easy to affect human health.
Specific embodiment
With reference to embodiments, invention is further described in detail.
In the examples below, fatty alcohol uses the brand of Ming Hua sugar alcohol Co., Ltd, Suzhou City for the 16 of Thailand's Corning
Octadecyl alcolol.
Embodiment 1
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 36kg, fatty acid 35kg, polyethylene glycol 11kg, capsule perfume 20kg.
In the present embodiment, softener is consistent lubricant essence.
In the present embodiment, fatty acid is polite hard using the Indonesia of the model 1801 of Guangzhou Xie Guang commerce and trade Co., Ltd
Resin acid, in other embodiments, fatty acid can also be lauric acid, myristic acid or palmitinic acid.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-8000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 7200-8800.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: being added softener 36kg, fatty acid 35kg, polyethylene glycol 11kg in heating emulsification pot,
It is heated with stirring to each component to be completely dissolved to liquid condition, adds capsule perfume 20kg, stir evenly, form impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 2
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 85kg, fatty acid 1kg, polyethylene glycol 35kg, capsule perfume 11kg.
In the present embodiment, softener is Biester quarternary ammoniumsalt, and softener is the type purchased from Si Taipan Co., Ltd, the U.S.
Number be SP90 double ethyl palmitate base hydroxyethyl methyl ammonium sulfate.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: being added softener 85kg, fatty acid 1kg, polyethylene glycol 35kg in heating emulsification pot,
It is heated with stirring to each component to be completely dissolved to liquid condition, adds capsule perfume 11kg, stir evenly, form impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 35 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 3
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 1kg, fatty alcohol 30kg, polyethylene glycol 5kg, essence microcapsule 8kg.
In the present embodiment, softener is Biester quarternary ammoniumsalt, and softener is the type purchased from Si Taipan Co., Ltd, the U.S.
Number be SP90 double ethyl palmitate base hydroxyethyl methyl ammonium sulfate.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-8000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 7200-8800.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: softener 1kg, fatty alcohol 30kg, polyethylene glycol 5kg are added in heating emulsification pot, stirs
It mixes and is heated to each component and is completely dissolved to liquid condition, and controlling heating temperature is 45 DEG C, adds essence microcapsule 8kg, stirs
It mixes uniformly, forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 4
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 1kg, fatty alcohol 30kg, polyethylene glycol 5kg, essence microcapsule 8kg.
In the present embodiment, softener is Biester quarternary ammoniumsalt, and softener is the type purchased from Si Taipan Co., Ltd, the U.S.
Number be SP90 double ethyl palmitate base hydroxyethyl methyl ammonium sulfate.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: softener 1kg, fatty alcohol 30kg, polyethylene glycol 5kg are added in heating emulsification pot, stirs
It mixes and is heated to each component and is completely dissolved to liquid condition, and controlling heating temperature is 45 DEG C, adds essence microcapsule 8kg, stirs
It mixes uniformly, forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 5
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 35kg, fatty alcohol 5kg, polyethylene glycol 8kg, essence microcapsule 10kg.
In the present embodiment, softener is dioctadecyl dimethyl ammonium chloride (D1821).
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: softener 35kg, fatty alcohol 5kg, polyethylene glycol 8kg are added in heating emulsification pot, stirs
It mixes and is heated to each component and is completely dissolved to liquid condition, and controlling heating temperature is 55 DEG C, adds essence microcapsule 10kg, stirs
It mixes uniformly, forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 33 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 6
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 18kg, fatty alcohol 25kg, polyethylene glycol 10kg, essence microcapsule 0.5kg.
In the present embodiment, softener is film.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: being added softener 18kg, fatty alcohol 25kg, polyethylene glycol 10kg in heating emulsification pot,
It is heated with stirring to each component to be completely dissolved to liquid condition, and controlling heating temperature is 65 DEG C, adds essence microcapsule
0.5kg is stirred evenly, and forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 35 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 7
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 17kg, fatty alcohol 45kg, polyethylene glycol 1kg, essence microcapsule 6kg.
In the present embodiment, softener is consistent lubricant essence.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: being added softener 17kg, fatty alcohol 45kg, polyethylene glycol 1kg in heating emulsification pot,
It is heated with stirring to each component to be completely dissolved to liquid condition, and controlling heating temperature is 60 DEG C, adds essence microcapsule 6kg,
It stirs evenly, forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 32 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 8
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 1kg, fatty acid 30kg, polyethylene glycol 5kg, capsule perfume 8kg, medical grade vaseline 1kg.
In the present embodiment, softener is Biester quarternary ammoniumsalt, and softener is the type purchased from Si Taipan Co., Ltd, the U.S.
Number be SP90 double ethyl palmitate base hydroxyethyl methyl ammonium sulfate.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-8000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 7200-8800.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: softener 1kg, fatty acid 30kg, polyethylene glycol 5kg, doctor are added in heating emulsification pot
It with grade vaseline 1kg, is heated with stirring to each component and is completely dissolved to liquid condition, and controlling heating temperature is 45 DEG C, is added
Capsule perfume 8kg, stirs evenly, and forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 9
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 1kg, fatty acid 30kg, polyethylene glycol 5kg, capsule perfume 8kg, medical grade vaseline 5kg.
In the present embodiment, softener is Biester quarternary ammoniumsalt, and softener is the type purchased from Si Taipan Co., Ltd, the U.S.
Number be SP90 double ethyl palmitate base hydroxyethyl methyl ammonium sulfate.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: softener 1kg, fatty acid 30kg, polyethylene glycol 5kg, doctor are added in heating emulsification pot
It with grade vaseline 5kg, is heated with stirring to each component and is completely dissolved to liquid condition, and controlling heating temperature is 45 DEG C, is added
Capsule perfume 8kg, stirs evenly, and forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Embodiment 10
A kind of submissive fragrant garment piece of solid, the component including following mass fraction:
Softener 1kg, fatty alcohol 30kg, polyethylene glycol 5kg, essence microcapsule 8kg, medical grade vaseline 10kg.
In the present embodiment, softener is Biester quarternary ammoniumsalt, and softener is the type purchased from Si Taipan Co., Ltd, the U.S.
Number be SP90 double ethyl palmitate base hydroxyethyl methyl ammonium sulfate.
In the present embodiment, polyethylene glycol uses the molecular weight of the model PEG-6000 of Jiangsu Hai'an Petrochemical Plant
For the polyethylene glycol of 5500-7000.
The preparation method of the submissive fragrant garment piece of solid the following steps are included:
The preparation of S1, impregnating agent: softener 1kg, fatty alcohol 30kg, polyethylene glycol 5kg, doctor are added in heating emulsification pot
It with grade vaseline 10kg, is heated with stirring to each component and is completely dissolved to liquid condition, and controlling heating temperature is 45 DEG C, is added
Essence microcapsule 8kg, stirs evenly, and forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
Comparative example 1
Using the system in a kind of Chinese patent application file " environmental protection clothing fumet " of Publication No. CN105297430A
Preparation Method prepares clothing fumet.
A kind of clothing fumet, the component including following mass fraction:
Cinnamomum camphora wood powder 4kg, Polyoxyalkylene ethers class compound 1kg, polyvinyl acetate 2kg, modified polyorganosiloxane compound
1kg, camphor 0.5kg.
In the present embodiment, Polyoxyalkylene ethers class compound uses the alkane of the model NP40 of Nantong Jin Lai Chemical Co., Ltd.
Base phenol polyethenoxy ether.
In the present embodiment, modified polyorganosiloxane compound uses the model TS-701 of Guangzhou Tian Ling silica gel Co., Ltd
Amino modified polysiloxane textile softener.
The preparation method of clothing fumet, comprising the following steps:
S1, Polyoxyalkylene ethers class compound 1kg is dissolved in 10kg water；
S2, polyvinyl acetate 2kg is dissolved in 13kg water；
S3, successively by cinnamomum camphora wood powder 4kg, modified polyorganosiloxane compound 1kg be put into the resulting aqueous solution of S2 sufficiently it is molten
Solution；
S4, Polyoxyalkylene ethers class compound water solution is poured into the resulting aqueous solution of S3；
S5, camphor is poured into the resulting aqueous solution of S4, is mixed.The above operation is normal-temperature operation.
Experiment 1
Same clothes is placed in dryer respectively, and into clothes be added 100g above embodiments prepare it is resulting solid
The submissive fragrant garment piece of body, opens dryer, and the temperature for controlling dryer is 70 DEG C, after drying 1h, takes out clothes, is placed in room temperature
It places, the clothes 10s of timing friction daily, record clothes no longer distributes the time (day) of fragrance in friction；It simultaneously will be same
Clothes prepares resulting clothing fumet immersion 2h using comparative example 1 and dries, and is placed in room temperature and places, record clothes is no longer
Distribute the time (day) of fragrance.
Experiment 2
Same clothes: being placed in dryer by clothes pretreatment respectively, and 100g above embodiments are added into clothes
The submissive fragrant garment piece of resulting solid is prepared, dryer is opened, the temperature for controlling dryer is 70 DEG C, after drying 1h, takes out clothes；
Same clothes is prepared into resulting clothing fumet immersion 2h using comparative example 1 simultaneously and is dried.
The above clothes is detected before pretreatment according to GB/T16801-2013 " measurement of fabric conditioner antistatic property "
And pretreated garment surface specific resistance decreasing value (Ω).
Experiment 3
Same clothes: being placed in dryer by clothes pretreatment respectively, and 100g above embodiments are added into clothes
The submissive fragrant garment piece of resulting solid is prepared, dryer is opened, the temperature for controlling dryer is 70 DEG C, after drying 1h, takes out clothes；
Same clothes is prepared into resulting clothing fumet immersion 2h using comparative example 1 simultaneously and is dried.
With feel by the comfort level of the above clothing after pretreatment, is scored, commented according to the soft comfortable degree of clothing
Minute mark standard is that the soft comfortable degree of clothing is higher, is scored higher, and score is 0-10 points.
The above detection data is shown in Table 1.
Table 1
It can be obtained according to the data comparison of embodiment 1-10 in table 1 and comparative example 1, embodiment 1-10 is all made of group of the invention
Distribution ratio and method prepare the submissive fragrant garment piece of solid, and comparative example 1 prepares clothing fumet using traditional preparation method, and real
The fragrance for applying a 1-10 completely disappears time, garment surface specific resistance decreasing value and soft comfortable degree and is much higher than comparative example 1
, illustrate to prepare the submissive fragrant garment piece of solid by using component proportion and preparation method of the invention, is conducive to improve use
The lasting aroma retaining effect of clothing after the submissive fragrant garment piece of solid, while also advantageously improving the antistatic property of clothing and submissive
Property, so that the wearing comfort of clothing improves.
It can be obtained according to the data comparison of embodiment 1-2 in table 1 and embodiment 3-10, the softener in embodiment 1-2 is in 1-
In the range of 85 parts and not in the range of 1-35 parts, fatty acid or fatty alcohol be not in the range of 1-65 parts and at 5-45 parts
In range, in the range of 1-35 parts and not in the range of 1-10 parts, essence microcapsule or capsule perfume exist polyethylene glycol
In the range of 0.5-20 parts and not in the range of 0.5-10 parts, the softener in embodiment 3-10 in the range of 1-35 parts,
In the range of 5-45 parts, polyethylene glycol is in the range of 1-10 parts, essence microcapsule or capsule perfume for fatty acid or fatty alcohol
In the range of 0.5-10 parts, and time and garment surface specific resistance decreasing value that the fragrance of embodiment 3-10 completely disappears are equal
Higher than embodiment 1-2, illustrate the usage ratio by control each component, is conducive to improve using after the submissive fragrant garment piece of solid
The lasting aroma retaining effect of clothing, while being conducive to improve the antistatic property of clothing.
Can be obtained according to the data comparison of embodiment 1 in table 1 and embodiment 2, embodiment 4 and embodiment 5-7, embodiment 2 with
And it is all made of Biester quarternary ammoniumsalt in embodiment 4 as softener, embodiment 1 and embodiment 5-7 and is all made of consistent lubricant essence or double
Octadecyldimethyl ammonium chloride or film are as softener, and the fragrance of embodiment 2 completely disappears time and garment surface
Specific resistance decreasing value is above embodiment 1, and the fragrance of embodiment 4 completely disappears time and garment surface specific resistance decreasing value
It is above embodiment 5-7, simultaneously as the softener in embodiment 4 is in the range of 1-35 parts, fatty acid or fatty alcohol exist
In the range of 5-45 parts, polyethylene glycol is in the range of 1-10 parts, the range of essence microcapsule or capsule perfume at 0.5-10 parts
Interior, the soft comfortable degree of embodiment 4 is above embodiment 1-3 and embodiment 5-7, illustrates by using Biester quarternary ammoniumsalt
As softener, be conducive to improve the lasting aroma retaining effect using the clothing after the submissive fragrant garment piece of solid, meanwhile, by using double
Ester group ammonium salt cooperates as the proportion of softener and control each component, also advantageously improves the antistatic property and softness of clothing
Comfort level.
It can be obtained according to embodiment 4 in table 1 and the data comparison of embodiment 8-10, when the fragrance of embodiment 8-10 completely disappears
Between, garment surface specific resistance decreasing value and soft comfortable degree be above embodiment 4, illustrate by the way that all scholars of medical grade are added
Woods is conducive to the impregnating agent to fall off from fabric more uniformly since vaseline has fabulous film forming and ductility
The surface of clothing is spread over, to be conducive to essence microcapsule or capsule perfume is evenly distributed on clothing, and then is conducive to mention
Height uses the lasting aroma retaining effect of the clothing after the submissive fragrant garment piece of solid, so that the time that fragrance completely disappears extends, meanwhile, it is all
Intellectual circle also has splendid soothing effect, is conducive to the skin-friendly for improving clothing, so that clothing has lubrication protection to skin
Effect, to be conducive to improve the antistatic property and soft comfortable degree of clothing.
The embodiment of present embodiment is presently preferred embodiments of the present invention, not limits protection of the invention according to this
Range, therefore: the equivalence changes that all structures under this invention, shape, principle are done, should all be covered by protection scope of the present invention it
It is interior.
Claims (10)
1. a kind of submissive fragrant garment piece of solid, it is characterized in that: including the component of following mass fraction:
1-85 parts of softener, the softener is cationic surfactant；
Fatty acid or 1-65 parts of fatty alcohol；
1-35 parts of polyethylene glycol；
Essence microcapsule or 0.5-20 parts of capsule perfume.
2. the submissive fragrant garment piece of solid according to claim 1, it is characterized in that: including the component of following mass fraction:
1-35 parts of softener；
Fatty acid or 5-45 parts of fatty alcohol；
1-10 parts of polyethylene glycol；
Essence microcapsule or 0.5-10 parts of capsule perfume.
3. the submissive fragrant garment piece of solid according to claim 1 to 2, it is characterized in that: further including the group of following mass fraction
Point:
1-10 parts of vaseline.
4. the submissive fragrant garment piece of solid according to claim 3, it is characterized in that: the vaseline is medical grade vaseline.
5. the submissive fragrant garment piece of solid according to claim 1 to 2, it is characterized in that: it is 8-18 that the fatty acid, which is carbon atom number,
Long alkyl chain saturated higher fatty acid, the fatty alcohol is the fatty alcohol that carbon atom number is 8-22.
6. the submissive fragrant garment piece of solid according to claim 1 to 2, it is characterized in that: the softener is di-ester-base quaternary ammonium
Salt, dioctadecyl dimethyl ammonium chloride, film or consistent lubricant essence in any one.
7. the submissive fragrant garment piece of solid according to claim 6, it is characterized in that: the softener is Biester quarternary ammoniumsalt.
8. the submissive fragrant garment piece of solid according to claim 1 to 2, it is characterized in that: the molecular weight of the polyethylene glycol is
1500-10000。
9. the preparation method of the submissive fragrant garment piece of a kind of solid a method as claimed in any one of claims 1-8, it is characterized in that: including following step
It is rapid:
The preparation of S1, impregnating agent: it by mass parts ratio mixing softener, fatty acid or fatty alcohol, polyethylene glycol, is heated with stirring to
Each component is completely dissolved to liquid condition, adds essence microcapsule or capsule perfume, and stir evenly, and forms impregnating agent；
S2, dipping: fabric is immersed in impregnating agent, so that the fully penetrated fabric of impregnating agent；
S3, hot rolling: by the fully penetrated fabric for having impregnating agent by hot-rolling, and the temperature for controlling hot-rolling is 30 DEG C -35 DEG C；
S4, drying molding: it forms drying under cold wind is placed in by the fabric of hot-rolling to get the submissive fragrant garment piece of solid.
10. the preparation method of the submissive fragrant garment piece of solid according to claim 9, it is characterized in that: in the step S1, stirring
The temperature control of heating is 45 DEG C -65 DEG C.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114960201A (en) * | 2022-06-08 | 2022-08-30 | 广州蓝海新材料有限公司 | Functional water-saving washing accompanying sheet for washing jeans wear |
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