CN110093092A - A kind of anti-corrosion waterproof material and preparation method - Google Patents
A kind of anti-corrosion waterproof material and preparation method Download PDFInfo
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- CN110093092A CN110093092A CN201910458977.0A CN201910458977A CN110093092A CN 110093092 A CN110093092 A CN 110093092A CN 201910458977 A CN201910458977 A CN 201910458977A CN 110093092 A CN110093092 A CN 110093092A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
- C08G59/5046—Amines heterocyclic
- C08G59/5053—Amines heterocyclic containing only nitrogen as a heteroatom
- C08G59/5073—Amines heterocyclic containing only nitrogen as a heteroatom having two nitrogen atoms in the ring
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
- C08G59/56—Amines together with other curing agents
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/62—Alcohols or phenols
- C08G59/64—Amino alcohols
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/327—Aluminium phosphate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/328—Phosphates of heavy metals
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- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
Abstract
The embodiment of the present invention provides a kind of anti-corrosion waterproof material and preparation method, with TO resin anticorrosive paint based on the vegetable oil such as tung oil raw material, polar rubber makees intrinsic toughening agent, copolymer compound using cis-butenedioic anhydride etc. containing unsaturated double-bond is modified, cold high-molecular compound of the spelling with epoxy group, several functions auxiliary agent and mixed type solidifying agent etc. is added to be formulated, to solve the disadvantage that water-repellent paint is that cohesive force is low in the prior art, poor corrosion resistance, resistance to low temperature is poor, and has the problem of waterproof and breathable.
Description
Technical field
The present embodiments relate to construction material technical field more particularly to a kind of anti-corrosion waterproof material and preparation sides
Method.
Background technique
Coatings industry belongs to the modern industry, but coating itself has long history.China is in the world using natural
Coating of the resin as film forming matter --- the earliest country of lacquer.Really understand using solvent, with solvent come dissolved solid
Natural resin, it is inchoate in the middle of the 19th century that the coating of quick-drying, which is made,.Simplest water paint is lime slurry, is about existed
Emulsification linseed oil was added thereto with regard to once someone plan before 100 years to improve, it is exactly earliest emulsion paint that this, which I'm afraid,.70-
Representative of the eighties as contemporary water paint --- emulsion paint has obtained certain development, but promote and apply enter it is low
Paddy.Emulsion paint wants and is in fashion the interior wall coating in the whole nation to carry out price competition, as a result, losing all standing and reputation, or even substantial portion of
Builder and adnornment industry are negated, while boffo ceramic tile has seized the market of exterior wall latex paint most again.
Water-repellent paint is not suitable for the occasion containing corrosive media most without anti-corrosion function at present.It is widely used at present
Be polymer cement waterproof paint in national standard GB-23445-2009 " polymer cement waterproof paint ", wherein polymer emulsion
For acrylate, ethane-acetic acid ethyenyl ester etc..The shortcomings that such polymer cement waterproof paint is that cohesive force is low, corrosion resistance
Can be poor, resistance to low temperature is poor, and has waterproof and breathable (hydrone does not pass through, and gas molecule can pass through, and it is non-moistureproof to be commonly called as waterproof)
Characteristic.
Summary of the invention
The embodiment of the present invention provides a kind of anti-corrosion waterproof material and preparation method, to solve water-repellent paint in the prior art
The shortcomings that be that cohesive force is low, poor corrosion resistance, resistance to low temperature is poor, and has the problem of waterproof and breathable.
In a first aspect, the embodiment of the present invention provides a kind of anti-corrosion waterproof material, including tung oil acid anhydride, epoxy resin, iron oxide red
Powder, talcum powder, trbasic zinc phosphate, organobentonite, aluminium triphosphate, rutile type titanium white, carbon black, barium sulfate, defoaming agent, levelling
Agent, preservative, plasticizer, filler, portland cement;Wherein, tung oil acid anhydride, epoxy resin 1:1 in mass ratio are prepared into TO tree
Rouge;Portland cement, filler, preservative are that 1-2:1:0.2-0.5 is prepared by mixing into powder according to weight ratio.
Further, TO resin, iron oxide red, talcum powder, trbasic zinc phosphate, aluminium triphosphate, organobentonite in mass ratio 35:
15:15:14:5:0.5 being prepared into anti-decaying paint bottom;TO resin, carbon black, barium sulfate, organobentonite, disappears at rutile type titanium white
Infusion, levelling agent, filler, powder 50:22:1:10:0.5:0.3:0.3:10:10 in mass ratio are prepared into anti-corrosion lacquer painting.
Further, the filler be one or more of quartz sand, silica flour, calcium carbonate, talcum powder, titanium dioxide with
Arbitrary proportion mixing;The preservative is the mixture that one or both of trbasic zinc phosphate or aluminum phosphate are mixed with arbitrary proportion.
Second aspect, the embodiment of the present invention provide a kind of anti-corrosion waterproof material preparation method, comprising:
Tung oil pours into the four-hole boiling flask equipped with high speed agitator and heating device, is passed through nitrogen, is warming up to 120 DEG C, takes off
0.5~1h of water is cooled to 60 DEG C, and cis-butenedioic anhydride is slowly added into while stirring, automatic heating to 170 DEG C, maintain reaction 0.5~
1h obtains tung oil acid anhydride;
Tung oil acid anhydride obtained is mixed with toluene in mass ratio 1: 1, the transparent clarification of acquired solution;
Tung oil acid anhydride and epoxy resin 6101 in mass ratio 1: 1 are mixed at 80 DEG C, stirs evenly, is rapidly decreased to room
Temperature obtains TO resin;
By TO resin, iron oxide red, talcum powder, trbasic zinc phosphate, aluminium triphosphate, organobentonite 35:15:15 in mass ratio:
14:5:0.5 is prepared into anti-decaying paint bottom;By TO resin, rutile type titanium white, carbon black, barium sulfate, organobentonite, defoaming agent,
Levelling agent, filler, powder 50:22:1:10:0.5:0.3:0.3:10:10 in mass ratio are prepared into anti-corrosion lacquer painting.
Further, further includes:
The mixture of triethanolamine and methylimidazole is curing agent, curing agent and anti-corrosion lacquer painting or anti-decaying paint bottom mass ratio
For 1:20.
A kind of anti-corrosion waterproof material provided in an embodiment of the present invention and preparation method, with TO resin anticorrosive paint with tung oil
Raw material based on equal vegetable oil, polar rubber make intrinsic toughening agent, and the copolymer compound using cis-butenedioic anhydride etc. containing unsaturated double-bond is modified,
Cold high-molecular compound of the spelling with epoxy group, adds several functions auxiliary agent and mixed type solidifying agent etc. and is formulated, to
Solve the disadvantage that water-repellent paint is that cohesive force is low in the prior art, poor corrosion resistance, resistance to low temperature is poor, and has waterproof and breathable
The problem of.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making
Every other embodiment obtained, shall fall within the protection scope of the present invention under the premise of creative work.
In a first aspect, the embodiment of the present invention provides a kind of anti-corrosion waterproof material, including tung oil acid anhydride, epoxy resin, iron oxide red
Powder, talcum powder, trbasic zinc phosphate, organobentonite, aluminium triphosphate, rutile type titanium white, carbon black, barium sulfate, defoaming agent, levelling
Agent, preservative, plasticizer, filler, portland cement;Wherein, tung oil acid anhydride, epoxy resin 1:1 in mass ratio are prepared into TO tree
Rouge;Portland cement, filler, preservative are that 1-2:1:0.2-0.5 is prepared by mixing into powder according to weight ratio.
Further, TO resin, iron oxide red, talcum powder, trbasic zinc phosphate, aluminium triphosphate, organobentonite in mass ratio 35:
15:15:14:5:0.5 being prepared into anti-decaying paint bottom;TO resin, carbon black, barium sulfate, organobentonite, disappears at rutile type titanium white
Infusion, levelling agent, filler, powder 50:22:1:10:0.5:0.3:0.3:10:10 in mass ratio are prepared into anti-corrosion lacquer painting.
Further, the filler be one or more of quartz sand, silica flour, calcium carbonate, talcum powder, titanium dioxide with
Arbitrary proportion mixing;The preservative is the mixture that one or both of trbasic zinc phosphate or aluminum phosphate are mixed with arbitrary proportion.
Second aspect, the embodiment of the present invention provide a kind of anti-corrosion waterproof material preparation method, comprising:
Tung oil pours into the four-hole boiling flask equipped with high speed agitator and heating device, is passed through nitrogen, is warming up to 120 DEG C, takes off
0.5~1h of water is cooled to 60 DEG C, and cis-butenedioic anhydride is slowly added into while stirring, automatic heating to 170 DEG C, maintain reaction 0.5~
1h obtains tung oil acid anhydride;
Tung oil acid anhydride obtained is mixed with toluene in mass ratio 1: 1, the transparent clarification of acquired solution;
Tung oil acid anhydride and epoxy resin 6101 in mass ratio 1: 1 are mixed at 80 DEG C, stirs evenly, is rapidly decreased to room
Temperature obtains TO resin;
By TO resin, iron oxide red, talcum powder, trbasic zinc phosphate, aluminium triphosphate, organobentonite 35:15:15 in mass ratio:
14:5:0.5 is prepared into anti-decaying paint bottom;By TO resin, rutile type titanium white, carbon black, barium sulfate, organobentonite, defoaming agent,
Levelling agent, filler, powder 50:22:1:10:0.5:0.3:0.3:10:10 in mass ratio are prepared into anti-corrosion lacquer painting.
Further, further includes:
The mixture of triethanolamine and methylimidazole is curing agent, curing agent and anti-corrosion lacquer painting or anti-decaying paint bottom mass ratio
For 1:20.
A kind of anti-corrosion waterproof material provided in an embodiment of the present invention and preparation method, with TO resin anticorrosive paint with tung oil
Raw material based on equal vegetable oil, polar rubber make intrinsic toughening agent, and the copolymer compound using cis-butenedioic anhydride etc. containing unsaturated double-bond is modified,
Cold high-molecular compound of the spelling with epoxy group, adds several functions auxiliary agent and mixed type solidifying agent etc. and is formulated, to
Solve the disadvantage that water-repellent paint is that cohesive force is low in the prior art, poor corrosion resistance, resistance to low temperature is poor, and has waterproof and breathable
The problem of.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although
Present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: it still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features;
And these are modified or replaceed, technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution spirit and
Range.
Claims (5)
1. a kind of anti-corrosion waterproof material, which is characterized in that including tung oil acid anhydride, epoxy resin, iron oxide red, talcum powder, trbasic zinc phosphate,
Organobentonite, aluminium triphosphate, rutile type titanium white, carbon black, barium sulfate, defoaming agent, levelling agent, preservative, plasticizer,
Filler, portland cement;Wherein, tung oil acid anhydride, epoxy resin 1:1 in mass ratio are prepared into TO resin;Portland cement is filled out
Material, preservative are that 1-2:1:0.2-0.5 is prepared by mixing into powder according to weight ratio.
2. anti-corrosion waterproof material according to claim 1, which is characterized in that TO resin, iron oxide red, talcum powder, trbasic zinc phosphate,
Aluminium triphosphate, organobentonite 35:15:15:14:5:0.5 in mass ratio are prepared into anti-decaying paint bottom;TO resin, rutile-type
Titanium dioxide, carbon black, barium sulfate, organobentonite, defoaming agent, levelling agent, filler, powder 50:22:1:10:0.5 in mass ratio:
0.3:0.3:10:10 is prepared into anti-corrosion lacquer painting.
3. anti-corrosion waterproof material according to claim 1, which is characterized in that the filler is quartz sand, silica flour, carbonic acid
One or more of calcium, talcum powder, titanium dioxide are mixed with arbitrary proportion;The preservative is one in trbasic zinc phosphate or aluminum phosphate
Kind or two kinds of mixtures mixed with arbitrary proportion.
4. a kind of anti-corrosion waterproof material preparation method characterized by comprising
Tung oil pours into the four-hole boiling flask equipped with high speed agitator and heating device, is passed through nitrogen, is warming up to 120 DEG C, dehydration 0.5
~1h is cooled to 60 DEG C, and cis-butenedioic anhydride is slowly added into while stirring, and automatic heating maintains 0.5~1h of reaction, obtain to 170 DEG C
Tung oil acid anhydride;
Tung oil acid anhydride obtained is mixed with toluene in mass ratio 1: 1, the transparent clarification of acquired solution;
Tung oil acid anhydride and epoxy resin 6101 in mass ratio 1: 1 are mixed at 80 DEG C, stirs evenly, is rapidly decreased to room temperature, obtain
To TO resin;
By TO resin, iron oxide red, talcum powder, trbasic zinc phosphate, aluminium triphosphate, organobentonite 35:15:15:14:5 in mass ratio:
0.5 is prepared into anti-decaying paint bottom;By TO resin, rutile type titanium white, carbon black, barium sulfate, organobentonite, defoaming agent, levelling
Agent, filler, powder 50:22:1:10:0.5:0.3:0.3:10:10 in mass ratio are prepared into anti-corrosion lacquer painting.
5. anti-corrosion waterproof material preparation method according to claim 4, which is characterized in that further include:
The mixture of triethanolamine and methylimidazole is curing agent, curing agent and anti-corrosion lacquer painting or anti-decaying paint bottom mass ratio is 1:
20。
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101007921A (en) * | 2006-01-24 | 2007-08-01 | 中国科学院过程工程研究所 | Anticorrosion paint for chimney of electric plant and its uses |
CN101671515A (en) * | 2009-09-01 | 2010-03-17 | 中国人民解放军海军后勤技术装备研究所 | Anticorrosive coating for concrete structure reinforcing bars and preparation method thereof |
CN104231863A (en) * | 2014-09-26 | 2014-12-24 | 水利部交通运输部国家能源局南京水利科学研究院 | Solvent-free anticorrosive paint composition capable of being solidified in seawater |
CN108250936A (en) * | 2018-01-29 | 2018-07-06 | 山西聚脲防护材料有限公司 | Resin cement waterproof anticorrosive paint |
-
2019
- 2019-05-29 CN CN201910458977.0A patent/CN110093092A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101007921A (en) * | 2006-01-24 | 2007-08-01 | 中国科学院过程工程研究所 | Anticorrosion paint for chimney of electric plant and its uses |
CN101671515A (en) * | 2009-09-01 | 2010-03-17 | 中国人民解放军海军后勤技术装备研究所 | Anticorrosive coating for concrete structure reinforcing bars and preparation method thereof |
CN104231863A (en) * | 2014-09-26 | 2014-12-24 | 水利部交通运输部国家能源局南京水利科学研究院 | Solvent-free anticorrosive paint composition capable of being solidified in seawater |
CN108250936A (en) * | 2018-01-29 | 2018-07-06 | 山西聚脲防护材料有限公司 | Resin cement waterproof anticorrosive paint |
Non-Patent Citations (1)
Title |
---|
魏向阳等: "TO树脂重防腐涂料的研制", 《上海涂料》 * |
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Application publication date: 20190806 |