CN110089530A - A kind of essential oil composition and preparation method thereof with insecticidal function - Google Patents
A kind of essential oil composition and preparation method thereof with insecticidal function Download PDFInfo
- Publication number
- CN110089530A CN110089530A CN201910544747.6A CN201910544747A CN110089530A CN 110089530 A CN110089530 A CN 110089530A CN 201910544747 A CN201910544747 A CN 201910544747A CN 110089530 A CN110089530 A CN 110089530A
- Authority
- CN
- China
- Prior art keywords
- parts
- essential oil
- oil
- tree
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 236
- 239000000203 mixture Substances 0.000 title claims abstract description 49
- 230000000749 insecticidal effect Effects 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 36
- 235000019441 ethanol Nutrition 0.000 claims abstract description 18
- 239000003921 oil Substances 0.000 claims abstract description 18
- 235000001405 Artemisia annua Nutrition 0.000 claims abstract description 16
- 240000000011 Artemisia annua Species 0.000 claims abstract description 16
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 15
- 244000050510 Cunninghamia lanceolata Species 0.000 claims abstract description 15
- 235000002566 Capsicum Nutrition 0.000 claims abstract description 14
- 240000000716 Durio zibethinus Species 0.000 claims abstract description 14
- 235000006025 Durio zibethinus Nutrition 0.000 claims abstract description 14
- 239000006002 Pepper Substances 0.000 claims abstract description 14
- 235000016761 Piper aduncum Nutrition 0.000 claims abstract description 14
- 235000017804 Piper guineense Nutrition 0.000 claims abstract description 14
- 235000008184 Piper nigrum Nutrition 0.000 claims abstract description 14
- 235000003351 Brassica cretica Nutrition 0.000 claims abstract description 13
- 235000003343 Brassica rupestris Nutrition 0.000 claims abstract description 13
- QKSKPIVNLNLAAV-UHFFFAOYSA-N bis(2-chloroethyl) sulfide Chemical compound ClCCSCCCl QKSKPIVNLNLAAV-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000010460 mustard Nutrition 0.000 claims abstract description 13
- 244000203593 Piper nigrum Species 0.000 claims abstract 4
- 244000056139 Brassica cretica Species 0.000 claims abstract 3
- 240000005819 Magnolia denudata Species 0.000 claims description 14
- 235000016094 Magnolia denudata Nutrition 0.000 claims description 14
- 244000246386 Mentha pulegium Species 0.000 claims description 14
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 14
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 14
- 244000294611 Punica granatum Species 0.000 claims description 14
- 235000014360 Punica granatum Nutrition 0.000 claims description 14
- 235000001050 hortel pimenta Nutrition 0.000 claims description 14
- DEDOPGXGGQYYMW-UHFFFAOYSA-N molinate Chemical compound CCSC(=O)N1CCCCCC1 DEDOPGXGGQYYMW-UHFFFAOYSA-N 0.000 claims description 14
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims description 13
- 240000003553 Leptospermum scoparium Species 0.000 claims description 13
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 13
- 238000012856 packing Methods 0.000 claims description 13
- 235000011449 Rosa Nutrition 0.000 claims description 12
- 239000003995 emulsifying agent Substances 0.000 claims description 12
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 7
- 235000010445 lecithin Nutrition 0.000 claims description 7
- 239000000787 lecithin Substances 0.000 claims description 7
- 229940067606 lecithin Drugs 0.000 claims description 7
- 239000012895 dilution Substances 0.000 claims description 4
- 238000010790 dilution Methods 0.000 claims description 4
- PUSKHXMZPOMNTQ-UHFFFAOYSA-N ethyl 2,1,3-benzoselenadiazole-5-carboxylate Chemical group CCOC(=O)C1=CC=C2N=[Se]=NC2=C1 PUSKHXMZPOMNTQ-UHFFFAOYSA-N 0.000 claims description 3
- 239000008236 heating water Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000012178 vegetable wax Substances 0.000 claims description 2
- ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 238000003860 storage Methods 0.000 abstract description 11
- 241000607479 Yersinia pestis Species 0.000 abstract description 7
- 102000002322 Egg Proteins Human genes 0.000 abstract description 5
- 108010000912 Egg Proteins Proteins 0.000 abstract description 5
- 210000004681 ovum Anatomy 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 3
- 244000144977 poultry Species 0.000 abstract description 2
- 238000004321 preservation Methods 0.000 abstract description 2
- 235000013339 cereals Nutrition 0.000 description 26
- 241000219198 Brassica Species 0.000 description 10
- 240000003889 Piper guineense Species 0.000 description 10
- 238000012360 testing method Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 241000238631 Hexapoda Species 0.000 description 4
- 241001465754 Metazoa Species 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 230000036541 health Effects 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 240000002234 Allium sativum Species 0.000 description 1
- 229920000858 Cyclodextrin Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000001116 FEMA 4028 Substances 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 240000003829 Sorghum propinquum Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 240000004922 Vigna radiata Species 0.000 description 1
- 235000010721 Vigna radiata var radiata Nutrition 0.000 description 1
- 235000011469 Vigna radiata var sublobata Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 1
- 229960004853 betadex Drugs 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000004611 garlic Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002541 mycostatic Substances 0.000 description 1
- 230000001557 mycostatic effect Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Agronomy & Crop Science (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of essential oil composition and preparation method thereof with insecticidal function, particularly belong to grain storage preservation field, with weight, which includes following component: 20~30 parts of artemisia annua essential oil, 15~25 parts of Fructus Perillae quintessence oil, 15~20 parts of European China fir essential oil, 10~15 parts of Ivy Tree Bark essential oil, 10~20 parts of camphor tree essential oil, 5~10 parts of durian essential oil, 5~12 parts of Japan pepper essential oil, 3~7 parts of mustard essential oil and 30~50 parts of ethyl alcohol.The present invention has the advantages that kill the pest on grain and worm's ovum and to person poultry harmless.
Description
Technical field
The invention belongs to grain storage preservation field, specially a kind of essential oil composition and its preparation with insecticidal function
Method.
Background technique
China's grain yield in 2011 realizes " eight even increase ", and grain supply and demand situation is obviously improved, but from now on
In quite a long time, problems faced is to reduce grain post-harvest loss.According to related data introduction, the annual grain storage in China
During depositing, grain is serious because losing caused by the harm of insect, mite class and mould during storage, especially because of insect pest caused by
Grain loss is up to 5~10%, the Quality Grade of the grain seriously affected, until making grain taste electrochromic variable, induces people and animals one after eating
The disease of series.
In order to kill the insect pest that grain is bred in storing process, grain farmers mostly using chemical agent to grain at
Reason.However, aforesaid operations, while generally using, problem is also following.Although grain carries out anti-corrosion using chemical reagent
Effect is good, but people and animals are easy to influence its health for a long time when eating such grain.Therefore, a kind of health environment-friendly and effect are found
The high insecticide of rate is technical staff's urgent problem to be solved.
Summary of the invention
The present invention provides a kind of essential oil composition with insecticidal function, which, which has, is killed on grain
Pest and worm's ovum and the advantages of to person poultry harmless.
To achieve the above object, the invention provides the following technical scheme:
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 20~30 parts of artemisia annua essential oil, 15~25 parts of Fructus Perillae quintessence oil, 15~20 parts of European China fir essential oil, 10~15 parts of Ivy Tree Bark essential oil, camphor tree
10~20 parts of essential oil of tree, 5~10 parts of durian essential oil, 5~12 parts of Japan pepper essential oil, 3~7 parts of mustard essential oil and ethyl alcohol 30~50
Part.
Preferably, the essential oil composition further includes in Peppermint essential oil, Essential Oil From Pine Needles, yulan essential oil and Rosa Damascana
The mixture of any one or they.
Preferably, the essential oil composition further includes at least one in pomegranate tree essential oil, tea tree ethereal oil and galic essential oil
Kind.
Preferably, the essential oil composition includes following component: artemisia annua essential oil 20~30 with weight
Part, 15~25 parts of Fructus Perillae quintessence oil, 15~20 parts of European China fir essential oil, 10~15 parts of Ivy Tree Bark essential oil, 10~20 parts of camphor tree essential oil, pomegranate
5~10 parts of lotus essential oil, 5~12 parts of Japan pepper essential oil, 3~7 parts of mustard essential oil, 10~15 parts of Peppermint essential oil, Essential Oil From Pine Needles 5~10
Part, 3~8 parts of yulan essential oil, 5~10 parts of Rosa Damascana, 10~15 parts of pomegranate tree essential oil, 5~10 parts of tea tree ethereal oil, galic essential oil
3~6 parts, 30~50 parts of ethyl alcohol and 8~13 parts of emulsifier.
Preferably, the essential oil composition includes following component with weight: 26 parts of artemisia annua essential oil,
18 parts of Fructus Perillae quintessence oil, 17 parts of European China fir essential oil, 12 parts of Ivy Tree Bark essential oil, 16 parts of camphor tree essential oil, 7 parts of durian essential oil, Japan pepper essential oil 8
Part, 6 parts of mustard essential oil, 13 parts of Peppermint essential oil, 8 parts of Essential Oil From Pine Needles, 6 parts of yulan essential oil, 6 parts of Rosa Damascana, pomegranate tree essential oil 12
Part, 7 parts of tea tree ethereal oil, 5 parts of galic essential oil, 40 parts of ethyl alcohol and 10 parts of emulsifier.
Preferably, the emulsifier is selected from lecithin, solidifying fragrant at least one of body and palm vegetable wax.
The present invention also provides a kind of preparation method of essential oil composition with insecticidal function, which includes such as
Lower step:
S01, the component of preset weight number is uniformly mixed, and heating water bath is to 20~30 DEG C, the duration 10~
15min obtains mixed liquor；
S02, emulsifier is added in obtained mixed liquor, persistently stirs 15~20 minutes, is cooled to room temperature to get institute
State essential oil composition；
S03, obtained essential oil composition is uniformly mixed with ethyl alcohol 1:10 in mass ratio, obtains essential oil composition dilution
Liquid；
S04, essential oil composition dilution is drawn with sponge, and sponge is placed in packing ball, that is, can be placed in silo
Middle use.
Preferably, the packing ball includes the first hollow hemisphere and the second hollow hemisphere in step S02
Body, first hemisphere and the second hollow hemisphere are detachably fixed, first hemisphere and the second hollow hemisphere
The through-hole to volatilize away for essential oil is equipped on body.
Preferably, the first hemisphere inner wall is equipped with internal screw thread, correspondingly, second hemisphere in step S02
Body is equipped with thread segment compatible with internal screw thread.
The invention has the benefit that
In the present invention, artemisia annua essential oil has effects that bactericidal and prevents the magical of worm's ovum growth.In grain storage
Mycostatic growth can not only be pressed down using artemisia annua essential oil, Fructus Perillae quintessence oil and European China fir essential oil, can also prevent the growth of ostomatid.
Ivy Tree Bark essential oil has effects that improve storage space inner air quality and desinsection, to prevent grain in storing process
Generate rear harmful toxin edible to people and animals.Camphor tree essential oil, durian essential oil, Japan pepper essential oil and mustard essential oil are natural plants
Pesticide can kill worm's ovum, prevent erosion of the grain by pest, to reduce the economic loss of grain farmer.Above-mentioned essential oil component tool
There is good compatibility, complement each other, use is more excellent than insecticidal effect possessed by single essential oil after matching.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of embodiment packing ball.
In figure: 1, the first hemisphere, the 2, second hemisphere, 21, thread segment, 3, through-hole.
Specific embodiment
Embodiment 1
The present embodiment provides a kind of technical solutions:
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 26 parts of artemisia annua essential oil, 18 parts of Fructus Perillae quintessence oil, 17 parts of European China fir essential oil, 12 parts of Ivy Tree Bark essential oil, 16 parts of camphor tree essential oil, durian
7 parts of essential oil, 8 parts of Japan pepper essential oil, 6 parts of mustard essential oil, 13 parts of Peppermint essential oil, 8 parts of Essential Oil From Pine Needles, 6 parts of yulan essential oil, Rosa Damascana
6 parts, 12 parts of pomegranate tree essential oil, 7 parts of tea tree ethereal oil, 5 parts of galic essential oil, 40 parts of ethyl alcohol and 10 parts of emulsifier.
Above-mentioned essential oil composition the preparation method is as follows:
S01, each component of above-mentioned preset weight number is uniformly mixed, and heating water bath is to 24 DEG C, the duration
13min obtains mixed liquor；
S02, the lecithin that preset weight number is added in obtained mixed liquor, solidifying fragrant body and beta-cyclodextrin, continue
Stirring 16 minutes, is cooled to room temperature to get the essential oil composition.
Embodiment 2
The present embodiment provides a kind of technical solutions:
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 20 parts of artemisia annua essential oil, 15 parts of Fructus Perillae quintessence oil, 15 parts of European China fir essential oil, 10 parts of Ivy Tree Bark essential oil, 10 parts of camphor tree essential oil, durian
5 parts of essential oil, 5 parts of Japan pepper essential oil, 3 parts of mustard essential oil, 10 parts of Peppermint essential oil, 5 parts of Essential Oil From Pine Needles, 3 parts of yulan essential oil, Rosa Damascana
5 parts, 10 parts of pomegranate tree essential oil, 5 parts of tea tree ethereal oil, 3 parts of galic essential oil, 30 parts of ethyl alcohol and 8 parts of emulsifier.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Embodiment 3
The present embodiment provides a kind of technical solutions:
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 26 parts of artemisia annua essential oil, 18 parts of Fructus Perillae quintessence oil, 16 parts of European China fir essential oil, 13 parts of Ivy Tree Bark essential oil, 16 parts of camphor tree essential oil, durian
7 parts of essential oil, 10 parts of Japan pepper essential oil, 6 parts of mustard essential oil, 12 parts of Peppermint essential oil, 8 parts of Essential Oil From Pine Needles, 6 parts of yulan essential oil, rhodamine toner
6 parts of oil, 12 parts of pomegranate tree essential oil, 8 parts of tea tree ethereal oil, 5 parts of galic essential oil, 40 parts of ethyl alcohol and 9 parts of emulsifier.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Embodiment 4
The present embodiment provides a kind of technical solutions:
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 30 parts of artemisia annua essential oil, 25 parts of Fructus Perillae quintessence oil, 20 parts of European China fir essential oil, 15 parts of Ivy Tree Bark essential oil, 20 parts of camphor tree essential oil, durian
10 parts of essential oil, 12 parts of Japan pepper essential oil, 7 parts of mustard essential oil, 15 parts of Peppermint essential oil, 10 parts of Essential Oil From Pine Needles, 8 parts of yulan essential oil, rose
10 parts of essential oil, 15 parts of pomegranate tree essential oil, 10 parts of tea tree ethereal oil, 6 parts of galic essential oil, 50 parts of ethyl alcohol and 13 parts of emulsifier.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Embodiment 5
As shown in Figure 1, the present embodiment provides a kind of packing ball (specification is of different sizes, the silo for different scales), it should
Packing ball includes the first hollow hemisphere 1 and the second hollow hemisphere 2, the first hemisphere 1 and the second hollow hemisphere 2
It is detachably fixed, is equipped with the through-hole 3 to volatilize away for essential oil on the first hemisphere 1 and the second hollow hemisphere 2.
As shown in Figure 1,1 inner wall of the first hemisphere is equipped with internal screw thread, and correspondingly, the second hemisphere 2 is set in step S02
There is thread segment 21 compatible with internal screw thread.
Grain farmer can be used essential oil composition provided by the Examples 1 to 4 after sponge absorption is diluted with ethyl alcohol, and by sponge
Be placed in packing ball provided by the present embodiment, and packing ball be placed in silo so that essential oil component can slowly from
It is released in through-hole 3, so that the pest bred on grain or worm's ovum are killed, to play the effect of desinsection.
Comparative example 1
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point:
12 parts of Ivy Tree Bark essential oil, 16 parts of camphor tree essential oil, 7 parts of durian essential oil, 8 parts of Japan pepper essential oil, 6 parts of mustard essential oil, peppermint
13 parts of essential oil, 8 parts of Essential Oil From Pine Needles, 6 parts of yulan essential oil, 6 parts of Rosa Damascana, 12 parts of pomegranate tree essential oil, 7 parts of tea tree ethereal oil, garlic
5 parts of essential oil, 40 parts of ethyl alcohol, 2 parts of lecithin and solidifying fragrant 4 parts of body.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Comparative example 2
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 26 parts of artemisia annua essential oil, 18 parts of Fructus Perillae quintessence oil, 17 parts of European China fir essential oil, 16 parts of camphor tree essential oil, 7 parts of durian essential oil, Japan pepper essential oil
8 parts, 6 parts of mustard essential oil, 13 parts of Peppermint essential oil, 8 parts of Essential Oil From Pine Needles, 6 parts of yulan essential oil, 6 parts of Rosa Damascana, pomegranate tree essential oil 12
Part, 7 parts of tea tree ethereal oil, 5 parts of galic essential oil, 40 parts of ethyl alcohol, 4 parts of lecithin and solidifying fragrant 4 parts of body.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Comparative example 3
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point: 26 parts of artemisia annua essential oil, 18 parts of Fructus Perillae quintessence oil, 17 parts of European China fir essential oil, 12 parts of Ivy Tree Bark essential oil, 13 parts of Peppermint essential oil, pine needle
8 parts of essential oil, 6 parts of yulan essential oil, 6 parts of Rosa Damascana, 12 parts of pomegranate tree essential oil, 7 parts of tea tree ethereal oil, 5 parts of galic essential oil, ethyl alcohol 40
Part, 3 parts of lecithin and solidifying fragrant 4 parts of body.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Comparative example 4
A kind of essential oil composition with insecticidal function, with weight, which includes such as the following group
Point:
26 parts of artemisia annua essential oil, 18 parts of Fructus Perillae quintessence oil, 17 parts of European China fir essential oil, 12 parts of Ivy Tree Bark essential oil, 16 parts of camphor tree essential oil,
7 parts of durian essential oil, 13 parts of Peppermint essential oil, 8 parts of Essential Oil From Pine Needles, 6 parts of yulan essential oil, 6 parts of Rosa Damascana, 40 parts of ethyl alcohol, lecithin 3
Part and solidifying fragrant 4 parts of body.
The preparation method is the same as that of Example 1 for above-mentioned essential oil composition.
Test case 1
This test case selects fresh paddy to implement body as specific, for probing into insecticide provided by the invention to storehouse
The influence of the holding time of grain storage food.Testing time selected by this test case is 4~October, because this period is harmful
Worm high-incidence season.
By 24 same specifications (cylindrical, diameter 3.8m, height 4.8m) and fill the paddy of the fresh paddy of same batch
Storage silo is divided into 8 groups, and number is A~H, and the combination of essential oil provided by Examples 1 to 4 is placed in A~D group paddy storage warehouse
Object.Essential oil composition provided by comparative example 1~4 is placed in E~H group grain storage silo.Above-mentioned essential oil composition is both placed in
In packing ball provided by embodiment 5 (diameter 10cm), and between the two neighboring packing ball placed between be divided into 2~3m,
Packing ball is placed in silo bottommost surrounding inner wall and the surrounding inner wall of height 2.4m height respectively (to stack grain and put in the process
Enter), packing ball is not put in the top layer of grain.After six months, paddy situation statistics such as table 1 in paddy storage silo:
1 paddy worm of table bites situation statistical form
Although this test case only has chosen paddy as test object, prevention and treatment reserves pest agent provided by the invention is same
Sample is suitable for corn, wheat, sorghum and soybean, and the insect prevention of the grains such as mung bean saves.
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art,
It is still possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is carried out etc.
With replacement, all within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in this
Within the protection scope of invention.
Claims (9)
1. a kind of essential oil composition with insecticidal function, which is characterized in that with weight, including following component:
20~30 parts of artemisia annua essential oil, 15~25 parts of Fructus Perillae quintessence oil, 15~20 parts of European China fir essential oil, 10~15 parts of Ivy Tree Bark essential oil, camphor tree
10~20 parts of essential oil, 5~10 parts of durian essential oil, 5~12 parts of Japan pepper essential oil, 3~7 parts of mustard essential oil and 30~50 parts of ethyl alcohol.
2. a kind of essential oil composition with insecticidal function according to claim 1, which is characterized in that further include peppermint essence
The mixture of any one or they in oil, Essential Oil From Pine Needles, yulan essential oil and Rosa Damascana.
3. a kind of essential oil composition with insecticidal function according to claim 1, which is characterized in that further include pomegranate tree
At least one of essential oil, tea tree ethereal oil and galic essential oil.
4. any a kind of essential oil composition with insecticidal function according to claim 1~3, which is characterized in that with weight
Amount percentage composition meter, including following component: 20~30 parts of artemisia annua essential oil, 15~25 parts of Fructus Perillae quintessence oil, European China fir essential oil 15~20
Part, 10~15 parts of Ivy Tree Bark essential oil, 10~20 parts of camphor tree essential oil, 5~10 parts of durian essential oil, 5~12 parts of Japan pepper essential oil, mustard essence
3~7 parts of oil, 10~15 parts of Peppermint essential oil, 5~10 parts of Essential Oil From Pine Needles, 3~8 parts of yulan essential oil, 5~10 parts of Rosa Damascana, pomegranate
10~15 parts of essential oil of tree, 5~10 parts of tea tree ethereal oil, 3~6 parts of galic essential oil, 30~50 parts of ethyl alcohol and 8~13 parts of emulsifier.
5. a kind of essential oil composition with insecticidal function according to claim 4, which is characterized in that contained with weight percent
Meter, including following component: 26 parts of artemisia annua essential oil, 18 parts of Fructus Perillae quintessence oil, 17 parts of European China fir essential oil, 12 parts of Ivy Tree Bark essential oil, camphor tree
16 parts of essential oil of tree, 7 parts of durian essential oil, 8 parts of Japan pepper essential oil, 6 parts of mustard essential oil, 13 parts of Peppermint essential oil, 8 parts of Essential Oil From Pine Needles, yulan
6 parts of essential oil, 6 parts of Rosa Damascana, 12 parts of pomegranate tree essential oil, 7 parts of tea tree ethereal oil, 5 parts of galic essential oil, 40 parts of ethyl alcohol and emulsifier
10 parts.
6. a kind of essential oil composition with insecticidal function according to claim 5, which is characterized in that the emulsifier choosing
From lecithin, solidifying fragrant at least one of body and palm vegetable wax.
7. a kind of preparation method of the essential oil composition with insecticidal function, which comprises the steps of:
S01, the component of preset weight number is uniformly mixed, and heating water bath is to 20~30 DEG C, 10~15min of duration,
Obtain mixed liquor；
S02, emulsifier is added in obtained mixed liquor, persistently stirs 15~20 minutes, is cooled to room temperature to get the essence
Fluid composition；
S03, obtained essential oil composition is uniformly mixed with ethyl alcohol 1:10 in mass ratio, obtains essential oil composition dilution；
S04, essential oil composition dilution is drawn with sponge, and sponge is placed in packing ball, that is, can be placed in silo makes
With.
8. preparation method according to claim 7, which is characterized in that in step S02, the packing ball includes hollow
First hemisphere (1) and hollow the second hemisphere (2), first hemisphere (1) and hollow the second hemisphere (2) are removable
Fixation is unloaded, is equipped with the through-hole (3) to volatilize away for essential oil on first hemisphere (1) and hollow the second hemisphere (2).
9. preparation method according to claim 8, which is characterized in that in step S02, in first hemisphere (1)
Wall is equipped with internal screw thread, and correspondingly, second hemisphere (2) is equipped with thread segment (21) compatible with internal screw thread.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810855781 | 2018-07-31 | ||
| CN2018108557810 | 2018-07-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110089530A true CN110089530A (en) | 2019-08-06 |
Family
ID=67451107
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910544747.6A Pending CN110089530A (en) | 2018-07-31 | 2019-06-21 | A kind of essential oil composition and preparation method thereof with insecticidal function |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110089530A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85204376U (en) * | 1985-10-14 | 1986-08-13 | 韦保江 | Hollow gymnastic ball with protuberances & small holes on the surface |
| CN2556234Y (en) * | 2002-05-31 | 2003-06-18 | 吕秀娟 | Clothes-washing ball |
| CN104886183A (en) * | 2015-05-27 | 2015-09-09 | 闭炳春 | Cinnamon oil contained insect repelling mildew preventive for grain storage |
| CN105996331A (en) * | 2016-07-23 | 2016-10-12 | 广西钱隆投资管理有限公司 | Anti-mosquito bracelet |
| CN106106582A (en) * | 2016-08-15 | 2016-11-16 | 青岛悦邦农种业有限公司 | A kind of plant pesticide |
| CN108208018A (en) * | 2017-12-25 | 2018-06-29 | 中国科学院沈阳应用生态研究所 | Application and agricultural chemical composition for disinsection of the Chinese pine needles essential oil in insecticide pesticide |
-
2019
- 2019-06-21 CN CN201910544747.6A patent/CN110089530A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85204376U (en) * | 1985-10-14 | 1986-08-13 | 韦保江 | Hollow gymnastic ball with protuberances & small holes on the surface |
| CN2556234Y (en) * | 2002-05-31 | 2003-06-18 | 吕秀娟 | Clothes-washing ball |
| CN104886183A (en) * | 2015-05-27 | 2015-09-09 | 闭炳春 | Cinnamon oil contained insect repelling mildew preventive for grain storage |
| CN105996331A (en) * | 2016-07-23 | 2016-10-12 | 广西钱隆投资管理有限公司 | Anti-mosquito bracelet |
| CN106106582A (en) * | 2016-08-15 | 2016-11-16 | 青岛悦邦农种业有限公司 | A kind of plant pesticide |
| CN108208018A (en) * | 2017-12-25 | 2018-06-29 | 中国科学院沈阳应用生态研究所 | Application and agricultural chemical composition for disinsection of the Chinese pine needles essential oil in insecticide pesticide |
Non-Patent Citations (4)
| Title |
|---|
| 杨群芳,周祖基,李庆: "植物精油对云南松纵坑切梢小蠹的驱避活性研究", 西南农业大学学报, no. 04, pages 357 - 359 * |
| 殷瑜霞 等: "植物源杀虫剂防制家蝇研究进展", 中国媒介生物学及控制杂志, vol. 27, no. 3, pages 205 - 206 * |
| 赵慧龙 等: "植物精油对土耳其扁谷盗的驱避和熏蒸活性研究", 环境昆虫学报, vol. 39, no. 5, pages 1 - 2 * |
| 黄素青;梁炳泉;苏兆雄;徐汉虹;: "植物精油的生物活性及其在有害生物控制上的应用", 农药, no. 06, pages 397 - 402 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Jackai et al. | Rearing the legume pod borer, Maruca testulalis Geyer (Lepidoptera: Pyralidae) on artificial diet | |
| JP2011519815A (en) | Fertilizer and pesticide throw-in pack | |
| CN106069732A (en) | A kind of method improving hybrid soybean production of hybrid seeds bee colony visit flower | |
| CN102283255B (en) | Nicotine-containing botanical synergist compound insecticide and preparation method thereof | |
| CN104770397A (en) | Beauveria bassiana pulvis and application thereof | |
| CN105379761A (en) | Cockroach attractant, preparation method of cockroach attractant and cockroach drug | |
| CN104872216A (en) | Plant-source synergist and insect aerosol prepared by same | |
| CN110089530A (en) | A kind of essential oil composition and preparation method thereof with insecticidal function | |
| CN106538586A (en) | A kind of Synergistic insecticidal compositions containing double third ring worm esters | |
| CN107821413A (en) | A kind of cockroach bait formulation and preparation method thereof | |
| CN112293419A (en) | Graphene oxide-containing pesticide composition | |
| CN109793014A (en) | A kind of high-efficient low toxicity insecticide and preparation method thereof | |
| CN105532656A (en) | Environment-friendly dinotefuran microemulsion and preparation method thereof | |
| CN110447498B (en) | Carnation seed cutting rooting process | |
| CN103314936B (en) | Conch bait and preparation method thereof | |
| CN106508944A (en) | Pesticidal composition containing 2-methylsulfonyl-5-(2,4-dichlorophenyl)-1,3,4-oxadiazole and prochloraz | |
| CN112514903A (en) | Pesticide composition containing fenpyroximate and application thereof | |
| CN106376598B (en) | Pesticidal combination containing Empedobacter brevis and Cupric sulfate | |
| Van Dinther et al. | Rearing of Diatraea saccharalis on diets in Surinam | |
| CN103828649A (en) | Method for preventing and treating eggplant diseases and insect pests | |
| CN114794118B (en) | Preparation and method for reducing harm of tea leafhoppers to tea trees | |
| CN108184886A (en) | A kind of sesame defoliation ripening agent and its method of administration | |
| CN108308206A (en) | A kind of fish pelargonium is aestivated special resistance reinforcing agent | |
| CN107047630A (en) | A kind of black melon seed seed treatment and preparation method thereof | |
| CN108902213A (en) | A kind of mould inhibitor and preparation method thereof in grain storage |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190806 |
|
| RJ01 | Rejection of invention patent application after publication |