CN110078368A - A kind of preparation method of sodium calcium white jade material glass tube - Google Patents
A kind of preparation method of sodium calcium white jade material glass tube Download PDFInfo
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- CN110078368A CN110078368A CN201910422558.1A CN201910422558A CN110078368A CN 110078368 A CN110078368 A CN 110078368A CN 201910422558 A CN201910422558 A CN 201910422558A CN 110078368 A CN110078368 A CN 110078368A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B25/00—Annealing glass products
- C03B25/02—Annealing glass products in a discontinuous way
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B9/00—Blowing glass; Production of hollow glass articles
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
- C03C3/064—Glass compositions containing silica with less than 40% silica by weight containing boron
- C03C3/068—Glass compositions containing silica with less than 40% silica by weight containing boron containing rare earths
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Abstract
A kind of preparation method of sodium calcium white jade material glass tube, belongs to glass making techniques field.Step are as follows: take 5-8 parts of SiO2, 15-17 parts of Na2O3, 0.5-0.8 parts of Na2B4O7·10H2O, 35-50 parts of Na2NO3, 15-25 parts of CaCO3, 0.3-1 parts of feldspar, 15-18 parts of fluorite, 14-17 parts of CeO2, it is mixed into A；Take 25-30 parts of CoO, 23-28 parts of Sb2O3, 15-19 parts of (NH4)2HPO4, 10-16 parts of Ca3(PO4)2, 27-30 parts ox bone crush, be mixed into B；A, B mixture are added in crucible, control to form stock by heating, cooling；It takes stock twice with steel pipe, blows out glass vacuole, form white jade emulsion opal glass product in a mold；7 hours are kept the temperature after annealing, 10-20 degree is cooled to and forms glass tube.
Description
Technical field
The invention belongs to glass making techniques fields, more particularly to a kind of preparation method of sodium calcium white jade material glass tube.
Background technique
Existing glass tube has transparent, blue or green products, and sodium calcium white jade glass product is chiefly used in pharmaceutical product packaging
And aviation, ship, high-speed rail, special dimension, currently without sodium calcium white jade material glass tubing products.
Summary of the invention
For the above technical problems, a kind of preparation method of sodium calcium white jade material glass tube is provided.
The purpose of the present invention is achieved through the following technical solutions:
A kind of preparation method of sodium calcium white jade material glass tube of the present invention, includes the following steps；
(1) 5-8 parts of SiO is taken by mass fraction2, 15-17 parts of Na2O3, 0.5-0.8 parts of Na2B4O7·10H2O, 35-
50 parts of Na2NO3, 15-25 parts of CaCO3, 0.3-1 parts of feldspar, 15-18 parts of fluorite, 14-17 parts of CeO2, it is mixed
At A mixture；
(2) by 25-30 parts of CoO, 23-28 parts of Sb of mass fraction2O3, 15-19 parts of (NH4)2HPO4, 10-16 parts of Ca3
(PO4)2, 27-30 parts ox bone crush, after stirring formed B mixture；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating, heat up 50-100 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 4-7 hours, then opens crucible and is cooled to
1200 degree are kept for one hour；
(5) steel pipe feeding is used for the first time, is cooled to 1200 degree, then secondary feeding, blows out glass vacuole, glass metal surface temperature
Degree is put into formation white jade emulsion opal glass product in mold at 1150 degree.
(6) glassware molding in step (5) is moved into 450-480 degree annealing furnace, keeps the temperature 7 hours, is cooled to 10-
20 degree form glass tube finished product.
Preferably, described (5) are replaced with the following method: being used steel pipe feeding for the first time, naturally cooled to glass metal table
After 1250 degree of face temperature, then secondary feeding, glass vacuole is blown out, glass metal surface temperature is put into mold at 1200 degree and is formed
White jade translucent glass product.
Preferably, described (5) are replaced with the following method: with glass metal bubble is blow molded into after steel pipe feeding, being cooled to
After 1150 degree, pattern steel mold is placed in by the secondary feeding of glass vacuole, keeps being cooled to 1100 degree in 1-2 minutes, be heated up to
1200 degree are presented white pattern by baking glass vacuole surface, finally enter the molding of glassware mold, obtain white jade and bake white glass
Glass product.
Preferably, described (NH4)2HPO4、Ca3(PO4)2And ox bone pulverized particles are less than 90 mesh.
Preferably, the SiO2Raw material is dry or aqueous.
The invention has the benefit that
1. the present invention adds ox bone raw material in the feed, the composition of ox bone is exactly calcium phosphate, white jade soda-lime glass of the present invention
Material side is studied successfully, and ox bone plays the role of pass and builds.In 1500 degree of glass meltings, the volatilization of carbide composition changes pure ox bone
Matter calcium phosphate makes glass become translucent, milkiness, appearance white pattern effect.It is that the current glass same industry is difficult the technology broken through
Bottleneck.It fills the domestic gaps, beautiful product appearance is the practical glassware of household, is the glass product of leading international high-quality.
It is white jade emulsion opal glass pipe, white jade respectively 2. three kinds of glass tubing products can be produced according to present invention process method
Translucent glass and white jade bake white glass, and glass tube obtained is used for common room temperature use environment, is unable to rapid heat cycle.Safety
Within the scope of 0-65 degree.Have class suitable for common tableware, water, is unsuitable for heating.
It is packaging product best in a kind of new material product and medicine 3. sodium calcium white jade glass product of the invention,
Sunlight can be covered outside the drop drug of part, help patient's rehabilitation as early as possible.
Specific embodiment
Below with reference to embodiment, the present invention will be described in detail.
Embodiment 1: a kind of preparation method of sodium calcium white jade material glass of the present invention includes the following steps:
(1) 5 parts of SiO is taken by mass fraction2, 17 parts of Na2O3, 0.8 part of Na2B4O7·10H2O, 45 parts of Na2NO3、
15 parts of CaCO3, 0.5 part feldspar, 16 parts of fluorite, 15 parts of CeO2, it is mixed into A mixture；
(2) by 25 parts of CoO of mass fraction, 26 parts of Sb2O3, 18 parts of (NH4)2HPO4, 12 parts of Ca3(PO4)2, 28 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 50 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 7 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) steel pipe feeding is used for the first time, is cooled to 1200 degree, then secondary feeding, blows out glass vacuole, glass metal surface temperature
Degree is put into formation white jade emulsion opal glass product in mold at 1150 degree；
(6) glassware molding in step (5) is moved into 450 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 20 degree of shapes
At glass finished-product.
(NH4)2HPO4、Ca3(PO4)2And ox bone pulverized particles are less than 90 mesh.The SiO2Raw material is dried feed.
Embodiment 2: this example unlike the first embodiment: (1) 8 parts of SiO is taken by mass fraction2, 17 parts of Na2O3、0.5
The Na of part2B4O7·10H2O, 50 parts of Na2NO3, 15 parts of CaCO3, 0.3 part feldspar, 15 parts of fluorite, 17 parts of CeO2, mix
Conjunction stirs into A mixture；
(2) by 28 parts of CoO of mass fraction, 23 parts of Sb2O3, 15 parts of (NH4)2HPO4, 16 parts of Ca3(PO4)2, 30 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 80 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 5 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) steel pipe feeding is used for the first time, is cooled to 1200 degree, then secondary feeding, blows out glass vacuole, glass metal surface temperature
Degree is put into formation white jade emulsion opal glass product in mold at 1150 degree；
(6) glassware molding in step (5) is moved into 480 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 20 degree of shapes
At glass finished-product.
The SiO2 raw material is aqueous material.
Embodiment 3: this example unlike the first embodiment: 5-8 parts of SiO is taken by mass fraction2, 15-17 parts of Na2O3、
0.5-0.8 parts of Na2B4O7·10H2O, 35-50 parts of Na2NO3, 15-25 parts of CaCO3, 0.3-1 parts feldspar, 15-18 parts
Fluorite, 14-17 parts of CeO2, it is mixed into A mixture；
(2) by 25-30 parts of CoO, 23-28 parts of Sb of mass fraction2O3, 15-19 parts of (NH4)2HPO4, 10-16 parts of Ca3
(PO4)2, 27-30 parts ox bone crush, after stirring formed B mixture；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating, heat up 50-100 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 4-7 hours, then opens crucible and is cooled to
1200 degree are kept for one hour；
(5) steel pipe feeding is used for the first time, is cooled to 1200 degree, then secondary feeding, blows out glass vacuole, glass metal surface temperature
Degree is put into formation white jade emulsion opal glass product in mold at 1150 degree.
(6) glassware molding in step (5) is moved into 450-480 degree annealing furnace, keeps the temperature 7 hours, is cooled to 10-
20 degree form glass finished-product.
The SiO2 raw material is aqueous material.
Embodiment 4: this example unlike the first embodiment: 5 parts of SiO is taken by mass fraction2, 15 parts of Na2O3, 0.5 part
Na2B4O7·10H2O, 35 parts of Na2NO3, 15 parts of CaCO3, 0.3 part feldspar, 15 parts of fluorite, 14 parts of CeO2, mixing
Stir into A mixture；
(2) by 30 parts of CoO of mass fraction, 28 parts of Sb2O3, 19 parts of (NH4)2HPO4, 16 parts of Ca3(PO4)2, 30 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 100 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 7 hours, then opens crucible and is cooled to 1200
Degree is kept for one hour；
(5) steel pipe feeding is used for the first time, after naturally cooling to 1250 degree of glass metal surface temperature, then secondary feeding, it blows out
Glass vacuole, glass metal surface temperature are put into formation white jade translucent glass product in mold at 1200 degree；
(6) glassware molding in step (5) is moved into 460 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 15 degree of shapes
At glass finished-product.
Embodiment 5: this example as different from Example 4: 8 parts of SiO is taken by mass fraction2, 17 parts of Na2O3, 0.8 part
Na2B4O7·10H2O, 50 parts of Na2NO3, 25 parts of CaCO3, 1 part feldspar, 18 parts of fluorite, 17 parts of CeO2, mixing stirs
Mix A mixture；
(2) by 25 parts of CoO of mass fraction, 23 parts of Sb2O3, 15 parts of (NH4)2HPO4, 10 parts of Ca3(PO4)2, 27 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 60 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 6 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) steel pipe feeding is used for the first time, after naturally cooling to 1250 degree of glass metal surface temperature, then secondary feeding, it blows out
Glass vacuole, glass metal surface temperature are put into formation white jade translucent glass product in mold at 1200 degree；
(6) glassware molding in step (5) is moved into 470 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 18 degree of shapes
At glass finished-product.
Embodiment 6: this example as different from Example 4: 6 parts of SiO is taken by mass fraction2, 16 parts of Na2O3, 0.7 part
Na2B4O7·10H2O, 45 parts of Na2NO3, 22 parts of CaCO3, 0.8 part feldspar, 16 parts of fluorite, 15 parts of CeO2, mixing
Stir into A mixture；
(2) by 27 parts of CoO of mass fraction, 25 parts of Sb2O3, 18 parts of (NH4)2HPO4, 14 parts of Ca3(PO4)2, 29 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 70 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 5 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) steel pipe feeding is used for the first time, after naturally cooling to 1250 degree of glass metal surface temperature, then secondary feeding, it blows out
Glass vacuole, glass metal surface temperature are put into formation white jade translucent glass product in mold at 1200 degree；
(6) glassware molding in step (5) is moved into 470 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 10-20 degree
Form glass finished-product.
Embodiment 7: this example unlike the first embodiment: 6 parts of SiO is taken by mass fraction2, 16 parts of Na2O3, 0.6 part
Na2B4O7·10H2O, 40 parts of Na2NO3, 17 parts of CaCO3, 0.9 part feldspar, 16 parts of fluorite, 15 parts of CeO2, mixing
Stir into A mixture；
(2) by 26 parts of CoO of mass fraction, 24 parts of Sb2O3, 16 parts of (NH4)2HPO4, 13 parts of Ca3(PO4)2, 29 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 60 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 7 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) it with glass metal bubble is blow molded into after steel pipe feeding, after being cooled to 1150 degree, is placed in by the secondary feeding of glass vacuole
Pattern steel mold, keeps being cooled to 1100 degree in 1-2 minutes, is heated up to 1200 degree and white print is presented by baking glass vacuole surface
Case finally enters the molding of glassware mold, obtains white jade and bakes white glass product；
(6) glassware molding in step (5) is moved into 480 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 10-20 degree
Form glass finished-product.
Embodiment 8: this example as different from Example 7: 5 parts of SiO is taken by mass fraction2, 17 parts of Na2O3, 0.5 part
Na2B4O7·10H2O, 35 parts of Na2NO3, 15 parts of CaCO3, 0.3 part feldspar, 18 parts of fluorite, 17 parts of CeO2, mixing
Stir into A mixture；
(2) by 25 parts of CoO of mass fraction, 23 parts of Sb2O3, 15 parts of (NH4)2HPO4, 16 parts of Ca3(PO4)2, 30 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 50 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 4 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) it with glass metal bubble is blow molded into after steel pipe feeding, after being cooled to 1150 degree, is placed in by the secondary feeding of glass vacuole
Pattern steel mold, keeps being cooled to 1100 degree in 1-2 minutes, is heated up to 1200 degree and white print is presented by baking glass vacuole surface
Case finally enters the molding of glassware mold, obtains white jade and bakes white glass product；
(6) glassware molding in step (5) is moved into 450 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 20 degree of shapes
At glass finished-product.
Embodiment 9: this example as different from Example 7: 8 parts of SiO is taken by mass fraction2, 17 parts of Na2O3, 0.5 part
Na2B4O7·10H2O, 50 parts of Na2NO3, 15 parts of CaCO3, 1 part feldspar, 15-18 parts of fluorite, 14 parts of CeO2, mix
Conjunction stirs into A mixture；
(2) by 30 parts of CoO of mass fraction, 23 parts of Sb2O3, 19 parts of (NH4)2HPO4, 10 parts of Ca3(PO4)2, 27 parts of ox
Bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, in charging
Heating heats up 90 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 4 hours, then opens crucible and is cooled to 1200 degree
It is kept for one hour；
(5) it with glass metal bubble is blow molded into after steel pipe feeding, after being cooled to 1150 degree, is placed in by the secondary feeding of glass vacuole
Pattern steel mold, keeps being cooled to 1100 degree in 1-2 minutes, is heated up to 1200 degree and white print is presented by baking glass vacuole surface
Case finally enters the molding of glassware mold, obtains white jade and bakes white glass product；
(6) glassware molding in step (5) is moved into 480 degree of annealing furnaces, keeps the temperature 7 hours, is cooled to 20 degree of shapes
At glass finished-product.
Claims (5)
1. a kind of preparation method of sodium calcium white jade material glass tube, it is characterised in that: include the following steps；
(1) 5-8 parts of SiO is taken by mass fraction2, 15-17 parts of Na2O3, 0.5-0.8 parts of Na2B4O7·10H2O, 35-50 parts
Na2NO3, 15-25 parts of CaCO3, 0.3-1 parts of feldspar, 15-18 parts of fluorite, 14-17 parts of CeO2, it is mixed into A
Mixture；
(2) by 25-30 parts of CoO, 23-28 parts of Sb of mass fraction2O3, 15-19 parts of (NH4)2HPO4, 10-16 parts of Ca3(PO4)2、
27-30 parts of ox bone crushes, and B mixture is formed after stirring；
(3) that A, B mixture are uniformly mixed into C mixture is spare；
(4) by 7 chargings of C mixture point into crucible, second is carried out after material dissolves after the last time and is fed, the liter in charging
Temperature, heat up 50-100 degree per hour, until temperature reaches 1380 degree in crucible, keeps the temperature 4-7 hours, then opens crucible and is cooled to
1200 degree are kept for one hour；
(5) steel pipe feeding is used for the first time, is cooled to 1200 degree, then secondary feeding, blows out glass vacuole, and glass metal surface temperature exists
Formation white jade emulsion opal glass product in mold is put at 1150 degree.
(6) glassware molding in step (5) is moved into 450-480 degree annealing furnace, keeps the temperature 7 hours, is cooled to 10-20 degree
Form glass tube finished product.
2. the preparation method of sodium calcium white jade material glass tube according to claim 1, it is characterised in that: described (5) are using such as
Lower method replacement: using steel pipe feeding for the first time, after naturally cooling to 1250 degree of glass metal surface temperature, then secondary feeding, it blows out
Glass vacuole, glass metal surface temperature are put into formation white jade translucent glass product in mold at 1200 degree.
3. the preparation method of sodium calcium white jade material glass tube according to claim 1, it is characterised in that: described (5) are using such as
Lower method replacement: it with glass metal bubble is blow molded into after steel pipe feeding, after being cooled to 1150 degree, is placed in by the secondary feeding of glass vacuole
Pattern steel mold, keeps being cooled to 1100 degree in 1-2 minutes, is heated up to 1200 degree and white print is presented by baking glass vacuole surface
Case finally enters the molding of glassware mold, obtains white jade and bakes white glass product.
4. the preparation method of sodium calcium white jade material glass tube according to claim 1, it is characterised in that: (NH4)2HPO4、
Ca3(PO4)2And ox bone pulverized particles are less than 90 mesh.
5. the preparation method of sodium calcium white jade material glass tube according to claim 1, it is characterised in that: the SiO2Raw material is dry
It is dry or aqueous.
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