CN110075051A - A kind of Wash-free mask adapting to the different times - Google Patents
A kind of Wash-free mask adapting to the different times Download PDFInfo
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- CN110075051A CN110075051A CN201910279803.8A CN201910279803A CN110075051A CN 110075051 A CN110075051 A CN 110075051A CN 201910279803 A CN201910279803 A CN 201910279803A CN 110075051 A CN110075051 A CN 110075051A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/671—Vitamin A; Derivatives thereof, e.g. ester of vitamin A acid, ester of retinol, retinol, retinal
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9722—Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The Wash-free mask that the different times use is adapted to the invention discloses a kind of, belongs to facial mask field.The facial mask is avoided commercially available facial mask and is only focused on skin itself and the defect not strong to external environment specific aim by basic ingredient and the material composition added according to the different times, the facial mask, and the facial mask for adapting to different times, different geographical is made, and achievees the effect that inside and outside and shield.
Description
Technical field
The present invention relates to facial mask fields, and in particular to one group of serial Wash-free mask designed according to four seasons climate difference,
Consumer can select suitable mask product according to the gentle candidate in region locating for me to carry out the skin of face and other positions
Maintenance.
Background technique
For facial mask as a kind of skin care tool, major function is extraneous environment, air and the pollution of isolation, improves skin temperature
Degree promotes sweat gland secretion and metabolism, increase the oxygen content of skin, is conducive to skin and excludes epidermal cell metabolism
The oil substances of product and accumulation make moisture penetrate into the cuticula of epidermis, and skin becomes soft, and skin nature light has bullet
Property, realize the maintenance functions such as its moisturizing, whitening, moist, anti-ageing, Sage Extract.
Skin is the maximum organ of human body and a big Microcosmic ecosystem, and the rear face of people from birth is sudden and violent always
It exposes outside, both being increased the internal metabolic alterations of appearance by the age is influenced, also by the long-term of the environment such as external warm, wet, wind, heat, light
It influences.Have research report to think: finely ground particles can cause skin oxidative in atmosphere, so that skin be caused prematurely to decline
Always, the generation for and promoting wrinkle or color spot etc..With regard to daylight for the damage of human body, other than UVA or UVB, it is seen that light or
Near infrared ray can also generate active oxygen, superoxide anion, hydroxyl radical free radical, hydrogen peroxide, singlet oxygen, nitric oxide, peroxide
Change lipid etc..These substances cause various genetic transfer factor activations, to promote the skins such as wrinkle or color spot old
The generation of change problem.In China, nearly 50 DEG C of four seasons maximum temperature difference, north and south maximal humidity difference nearly 70% and other varying environments
Factor, the influence to skin of face are even more that cannot ignore.However market majority skin care item have focused on the oiliness of skin, water at present
Property, the internal factors such as neutrality and mixed type, but ignore environmental factor greatest differences be it is cutaneous it is important be also unique
External cause.So Jiangnan application on human skin is fine and smooth, northwest application on human skin is coarse, and plateau application on human skin has glaze colours.Therefore protecting a face should be from
From the aspect of inside and outside two, a set of facial mask for adapting to different times, different geographical is designed, to achieve the effect that inside and outside and shield.
Summary of the invention
In view of the deficiencies of the prior art, the purpose of the present invention is to provide a kind of Wash-free mask for adapting to the different times and its
Preparation method, facial mask is by basic ingredient and the material composition added according to the different times.The facial mask avoids commercially available facial mask from only focusing on
Skin itself and the defect not strong to external environment specific aim.
Inventor passes through a large number of experiments, obtains a kind of Wash-free mask for adapting to the different times, the facial mask is by basic ingredient
With the material composition added according to the different times;The basic ingredient is by water, glycerol, butanediol, pyrrolidines ketone acid sodium, transparent
Matter acid, xanthan gum, glycerol polymethacrylates, beta glucan, glycine betaine, bletilla polysaccharide, panthenol, Vc and its derivative, Ve
And its derivative, saualane, ceramide, allantoin, PEG-60 rilanit special, allium extract, EDETATE SODIUM, lemon
Lemon acid composition;
The substance of the difference time addition is spring facial mask additive or summer facial mask additive or the addition of autumn facial mask
Object or winter facial mask additive;
The spring facial mask additive by caryophyllus oil, Pogostemon cablin essential, angelica essential oil, Flos Magnoliae oil, eucalyptus oil, tea oil,
Quercetin, Fructus Kochiae extract, Radix Sangusorbae extract, Radix Et Rhizoma Rhei extract, Baical Skullcap root P.E, tribulus fruit extract, Rhizoma Chuanxiong extract,
Shrubby sophora extract, phellodendron extract, tuckahoe extracts, Honegsukle flower P.E, flower of JINHUAKUI extract, forsythia suspense extraction, ocean are sweet
Chrysanthemum extract, dandelion extract, licoflavone, Schisandra chinens P.E, Cortex Dictamni extract, Herba Hedyotidis Diffusae extract, the sophora bud
Extract, calendula extract, red paeonia extract, Astragalus Root P.E, vitamin A, bisabolol, vitamin B6, arbutin, dimension
Raw element B3, biotin, azalaic acid and PEG-60 rilanit special composition;
The summer facial mask additive is by Baical Skullcap root P.E, coptis extract, Radix Sangusorbae extract, Folum Ilicis extract, gold
Honeysuckle flower extract, Sambucus Chinensis extract, hippophae rhamnoides, eucommia ulmoides extracts, angelica extract, Gnetum parvifolium extract, kuh-seng
Extract, Cortex Dictamni extract, mulberry bark extract, Acer palmatum extract, pterostilbene, bisabolol, menthanol lactic acid ester, cigarette
Amide, luteolin, galangal oil, caryophyllus oil, catnip oil, linolenic acid and PEG-60 rilanit special composition;
The autumn facial mask additive is by SIMMONDSIA CHINENSIS SEED OIL, fat of Oromaius norvaehollandeae, olibanum essential oil, licoflavone, Gotu Kola P.E, aobvious
Tooth porcelain ampelopsis extract, inula flower extractive, extractive of perilla, Rosmarinus officinalis extract, achyranthes bidentata extract, Arnica extract,
Hamamelis extract, calendula extract, flower of JINHUAKUI extract, Sorbus alnifloria extract, coltsfoot extract, gadol extract,
Turmeric P.E, chlorella extract, vitamin B3, isomery hexadecane, vitamin E, vitamin A, collagen, two palmityls
Hydroxyproline, sodium lactate, D- arbutin, PEG-60 rilanit special composition;
The winter facial mask additive by D- arbutin, phytosphingosine, Cyanotis arachnoides P.E, wolfberry fruit extract, it is climing more
Certain kind of berries extract, sad certain herbaceous plants with big flowers acid glycerol acid esters, dipalmitoyl hydroxyproline, bisabolol, stearic acid sucrose ester, Fructus Foeniculi quintessence oil,
Isononyl isononanoate, isomery hexadecane, male cicada moth extract, fat of Oromaius norvaehollandeae, palmityl tripeptides, polyquaternium -51, PEG-60 hydrogenation
Castor oil composition.
Preferably, a kind of Wash-free mask for adapting to the different times as described above, each group in the spring facial mask additive
The weight by volume ratio divided are as follows: caryophyllus oil 0.05-0.1, Pogostemon cablin essential 0.05-0.10, angelica essential oil 0.2-0.4, the flower bud of lily magnolia
Oily 0.2-0.4, eucalyptus oil 0.1-0.3, tea oil 0.1-0.3, Quercetin 0.04-0.06, licoflavone 0.02-0.04, summer cypress
Seed extract 0.1-0.03, Radix Sangusorbae extract 0.1-0.3, Radix Et Rhizoma Rhei extract 0.1-0.2, Baical Skullcap root P.E 0.1-0.3, puncture vine
Extract 0.05-0.07, Rhizoma Chuanxiong extract 0.1-0.3, shrubby sophora extract 0.05-0.08, tuckahoe extracts 0.2-0.5, shaggy-fruited dittany
Bark extract 0.2-0.4, phellodendron extract 0.1-0.2, Honegsukle flower P.E 0.1-0.3, flower of JINHUAKUI extract 0.1-0.3,
Chamomile extract 0.2-0.4, Fructus Forsythiae oil 0.05-0.1, Schisandra chinens P.E 0.05-0.1, Herba Hedyotidis Diffusae extract 0.1-0.3,
Calendula extract 0.1-0.3, Huai Goat 0.06-0.12, dandelion extract 0.3-0.4, red paeonia extract 0.05-
0.08, Astragalus Root P.E 0.1-0.3, vitamin A 0.1-0.3, bisabolol 0.2-0.5, vitamin B6 0.1-0.3, arbutin
0.01-0.06, vitamin B3 0.1-0.13, biotin 0.1-1, azalaic acid 0-0.05, PEG-60 rilanit special 0.1-
0.3;
The weight by volume ratio of each component in the summer facial mask additive are as follows: Baical Skullcap root P.E 0.5-1, the coptis are extracted
Object 0.1-0.3, Radix Sangusorbae extract 0.1-0.4, Folum Ilicis extract 0.1-0.5, Honegsukle flower P.E 0.1-0.3, Sambucus chinensis extract
Object 0.1-0.4, hippophae rhamnoides 0.2-0.5, eucommia ulmoides extracts 0.3-0.5, angelica extract 0.1-0.3, Gnetum parvifolium mention
Take object 0.1-0.2, Cortex Dictamni extract 0.1-0.3, shrubby sophora extract 0.1-0.2, mulberry bark extract 0.1-0.3, Acer palmatum
Extract 0.1-0.4, pterostilbene 0.03-0.1, bisabolol 0.03-0.06, menthanol lactic acid ester 0.04-0.08, niacinamide
0.1-0.4, luteolin 0.05-0.1, galangal oil 0.03-0.08, caryophyllus oil 0.05-0.1, catnip oil 0.1-0.3, flax
Oleic acid 0.1-0.5, PEG-60 rilanit special 0.1-3;
The weight by volume ratio of each component in the autumn facial mask additive are as follows: SIMMONDSIA CHINENSIS SEED OIL 0.1-0.3, fat of Oromaius norvaehollandeae
0.1-0.3, olibanum essential oil 0.1-0.4, licoflavone 0.03-0.05, Gotu Kola P.E 0.2-0.4, ampelopsis grossdentata extract
Object 0.1-0.3, inula flower extractive 0.1-0.3 extractive of perilla 0.1-0.3, Rosmarinus officinalis extract 0.05-0.1, radix achyranthis bidentatae extract
Object 0.1-0.3, Arnica extract 0.1-0.3, hamamelis extract 0.1-0.4, calendula extract 0.1-0.4, Golden flower
Flower extract 0.1-0.3, Sorbus alnifloria extract 0.2-0.4, coltsfoot extract 0.2-0.4, gadol extract 0.1-0.3, turmeric
Extract 0.1-0.3, chlorella extract 0.2-0.4, vitamin B3 0.1-0.3, isomery hexadecane 0.3-0.5, vitamin
E0.1-0.3, vitamin A 0.1-0.3, dipalmitoyl hydroxyproline 0.1-0.4, collagen 1-3, sodium lactate 0.1-0.3, D-
Arbutin 0.1-0.4, PEG-60 rilanit special 0.1-0.3;
The weight by volume ratio of the winter facial mask additive each component are as follows: D- arbutin 0.05-0.1, plant sheath ammonia
Alcohol 0.2-0.4, Cyanotis arachnoides P.E 0.1-0.3, wolfberry fruit extract 0.3-0.5, Cranberry extract 0.2-0.4, sad certain herbaceous plants with big flowers acid
Monoglyceride 0.4-0.6, dipalmitoyl hydroxyproline 0.4-0.6, bisabolol 0.05-0.1, stearic acid sucrose ester 0.1-0.3,
Fructus Foeniculi quintessence oil 0.08-0.12, isononyl isononanoate 0.1-0.3, isomery hexadecane 0.1-0.3, male cicada moth extract 0.1-
0.3, fat of Oromaius norvaehollandeae 0.1-0.3, palmityl tripeptides 1-3, polyquaternium -51 (1-3), PEG-60 rilanit special 0.1-0.3.
Preferably, a kind of Wash-free mask for adapting to the different times as described above, the body of each component in the basic ingredient
Product weight percent are as follows: water 70-80, glycerol 3-5, butanediol 3-5, pyrrolidines ketone acid sodium (NL-50) 3-5, hyaluronic acid (it is high,
Low molecular weight) 0.1-0.4, xanthan gum 0.2-0.4, glycerol polymethacrylates 0.8-1.5, beta glucan 0.1-0.3, beet
Alkali 0.2-0.5, bletilla polysaccharide 0.6-1.5, panthenol 0.1-0.3, Vc and its derivative 0.1-0.3, Ve and its derivative 0.06-
0.1, saualane 0.6-1.2, ceramide 0.2-0.4, allantoin 0.1-0.4, PEG-60 rilanit special 0.1-0.4, allium
Plant extracts 2-5, EDETATE SODIUM 0.02-0.04, citric acid 0.05-0.08.
Compared with prior art, advantages of the present invention are as follows: the facial mask is by basic ingredient and the plant added according to the different times
Object extract composition, the facial mask avoid commercially available facial mask and only focus on skin itself and the defect not strong to external environment specific aim,
The climatic environment in different times, different geographical is adapted to, inside and outside and shield effect can be played.
Embodiment
It is to be described further to technical solution of the present invention, but the contents of the present invention are not limited solely to embodiment below
The range, it is all to be included within protection scope of the present invention without departing substantially from the change of present inventive concept or equivalent substitute.
One, the index components in candidate crops original material are determined, see the table below:
Table 1, candidate crops and index components
Two, feedstock specifications component analyzing method is as follows:
Plant material or semi-finished product before treatment before, proportionately it is sub-category carry out respectively corresponding polysaccharide and glycoside, alkaloid,
The quantitative analysis of flavonoids, terpene, volatile oil, saponin(e, tannin.Each constituents are quantitative with corresponding reference substance, and analysis method is as follows:
1, alkaloid is quantitative: raw material 10g pulverizes and sieves 3O~6O mesh, and 70% ethyl alcohol of 15 times of volumes is added (containing 1% salt
Acid), it is heated to reflux 1 hour, is repeated 3 times, merge, constant volume, it is to be measured after 0.22 filter membrane excessively.High-efficient liquid phase chromatogram condition: chromatographic column
Chroma-trex C18 (200mm × 4.6mm, 5 μm), mobile phase: methanol-water-phosphoric acid (47: 53: 0.2), flow velocity 1.0mL/
Triethylamine is added in min, adjusts pH3.0, Detection wavelength 280nm, sample volume 5ul.
2, flavones is quantitative: raw material 10g pulverizes and sieves 3O~6O mesh, 80% methanol-water of 15 times of volumes is added, 80 DEG C are lauched
Bath heating 1h.It is repeated 3 times, merges, constant volume.It crosses to be measured after 0.22 filter membrane.Chromatographic condition mobile phase is acetonitrile and 0.1% formic acid.
Flow gradient elution program: 0~0.5min, 10% acetonitrile;0.5~10min, 10%~45% acetonitrile;10~12min, 45%
~100% acetonitrile, flow velocity: 0.3mL/min, column temperature: 45 DEG C, ultraviolet detection wavelength 260nm;Sample volume 1uL.
3, terpene volatile oil is quantitative: raw material 10g pulverizes and sieves 3O~6O mesh, and the n-hexane/acetic acid second of 15 times of volumes is added
Ester (8:2) soxhlet type 2 hours, cooling, constant volume, cross 0.22 filter membrane after it is to be measured.Capillary gas chromatography condition: chromatographic column DB-5
(30m×0.25mm i.d×0.25um);Shunting/Splitless injecting samples, temperature: 250 DEG C;Detector temperature: 270 DEG C;High Purity Nitrogen
Make carrier gas;Hydrogen flowing quantity 45mL/min;Air mass flow 400mL/min;Stigma pressure 58.6kPa;Column flow rate 1.0mL/min;It shunts
Than: 5:1;Sample volume 1uL;Temperature programming: 60 DEG C of initial temperature, after keeping 1min, 270 DEG C is risen to 6 DEG C/min, is kept
1min.
4, saponin(e is quantitative: 1 0g of raw material pulverizes and sieves 3O~6O mesh, sets in triangular flask, adds the positive fourths of 15 times of amounts 70%
Alcohol solution impregnates 2h, is ultrasonically treated 30min, and fast grade filter paper filters, and separates lower water layer in separatory funnel, 80 DEG C depressurize back
N-butanol is received to dry, methanol constant volume, is crossed to be measured after 0.22 filter membrane.High performance liquid chromatography chromatographic column be DiamonsilC (250mm ×
4.6mm, 5um), with one water of acetonitrile (25:75) for mobile phase, volume flow 1mL/min, Detection wavelength 210nm, sample volume
1uL。
5, tannin is quantitative: 1 0g of raw material pulverizes and sieves 3O~6O mesh, adds 15 times of 70% acetone room temperatures of amount to extract, extracting solution 40
DEG C be concentrated to dryness, be made into 50% methanol solution, high performance liquid chromatography chromatographic column be zorbax300SB-C18 (2.1mm × 150mm,
5 μm), acetonitrile: water (80:20), flow velocity: 0.2ml/min, Detection wavelength 270nm, sample volume 5uL.
Three, according to the above analysis acquired results, raw material mixed ratio is calculated.All kinds of constituents extraction purification process are as follows:
1, alkaloids extracts: raw material pulverizes and sieves 3O~6O mesh, and 70% ethyl alcohol of 15 times of volumes is added (containing 1% salt
Acid), it is heated to reflux 2 hours, is repeated 3 times, merging is concentrated into the 20% of total volume, and the active carbon decoloring of 60 DEG C of additions filters, filtrate
PH value is adjusted to 10 with ammonium hydroxide, by the addition abundant shaking of chloroform of 1:1 volume ratio, after stratification, extracts two again after separating water layer
It is secondary, merge chloroform solution, 50 DEG C of recycling chloroforms filter gained alkaloid, vacuum drying, through detecting nothing to doing, with a small amount of acetone washing
Residual solvent detection can be spare.
2, flavonoids extracts: raw material pulverizes and sieves 3O~6O mesh, 80% methanol-water of 15 times of volumes is added, 80 DEG C of water-baths add
Heat 2 hours.It is repeated 3 times, merging is condensed into flowing soaking paste, and the petroleum ether of 60-90 boiling range is added, and 40 DEG C of thermosols go out stone after cooling
Oily ether, is added a times amount ethyl acetate, 50 DEG C of thermosols, cooled and filtered, and recycling ethyl acetate is to dry.Again with being dried in vacuo, through examining
Surveying the detection of noresidue solvent can be spare.
It flows back 2 hours within ethyl ester (8:2) soxhlet type 2 hours or 60 DEG C, is repeated 3 times, merge concentration, 1 times of amount 90% is added
Ethyl alcohol, be sufficiently stirred, ethanol separated after standing.Or use supercritical carbon dioxide extracting, extracting parameter: separation temperature 80
DEG C, 4h, CO are extracted under the conditions of pressure 400MPa2Flow velocity 40Lh-1.
4, saponins extract: raw material pulverizes and sieves 3O~6O mesh, adds the n-butanol aqueous solutions of 15 times of amounts 70%, impregnates 2h,
90 DEG C are stirred at reflux 2 hours, are repeated 3 times, and merge concentrate, separate water layer, and 80 DEG C are recovered under reduced pressure n-butanol to dry, then use vacuum
It is dry, it can be spare through detection noresidue solvent detection.
5, tannin class is extracted: raw material pulverizes and sieves 3O~6O mesh, is extracted 2 hours, is repeated 3 times with 15 times of 60 DEG C of water measured,
The calcium hydroxide of saturation is added to PH10 in filtering, combined extract, and filtering, gained, which precipitates, is added 1 times of amount ethyl alcohol, stirs lower point
The secondary oxalic acid solution that 2mol/L is added filters, filtrate recycling ethanol is to doing, through detecting noresidue solvent detection side again to neutrality
It can be spare.
Embodiment 1
1, basic ingredient:
Number | Ingredient | Additional amount % (W/V) |
1. | Butanediol | 5 |
2. | Glycerol | 5 |
3. | Pyrrolidines ketone acid sodium (NL-50) | 5 |
4. | Hyaluronic acid (high low molecular weight 1:1) | 0.2 |
5. | Xanthan gum | 0.2 |
6. | Glycerol polymethacrylates | 1 |
7. | Beta glucan | 0.2 |
8. | Glycine betaine | 0.2 |
9. | Bletilla polysaccharide | 1 |
10. | Panthenol | 0.3 |
11. | Vc and its derivative | 0.2 |
12. | Ve and its derivative | 0.1 |
13. | Saualane | 1 |
14. | Ceramide | 0.2 |
15. | Allantoin | 0.4 |
16. | PEG-60 rilanit special | 0.1 |
17. | Allium extract | 3 |
18. | EDETATE SODIUM | 0.02 |
19. | Citric acid | 0.02 |
20. | Water | 70-80 |
2, basic ingredient preparation method
1) EDTA is added in water to be used with total amount percentage (similarly hereinafter), it is molten even spare.
2) it is dry-mixed uniformly that hyaluronic acid, glycine betaine, allantoin, xanthan gum, beta glucan are weighed, adds butanediol, sweet
Oil stirs pulp, and water, citric acid and the Vc of 1/2 volume of total amount is then added, and the speed of agitator of homogeneous emulsifying machine is 150-
180 revs/min, until all the components are uniformly dissolved distribution gelled, obtain material A.
3) it takes panthenol, saualane, the PEG-60 rilanit special in basic ingredient, is added the water of material 1:1,60 revs/min
It is mixed to lotion state with material A, 40 revs/min 5 minutes emulsified, obtains material B within clock emulsified 5 minutes.
4) pyrrolidines ketone acid sodium (NL-50), bletilla polysaccharide, garlic P.E are added the water of one times of amount, are sufficiently stirred, with
Material B mixing, 40 revs/min 5 minutes emulsified, obtains material C.
5) water of 3 times of amounts is added in glycerol polymethacrylates, stirs, and imports material C and stirs,
Obtain material D.
6) water of total amount 20% is left, remaining water is supplemented in material D, and 150-180 revs/min 15 minutes emulsified.
It 3, is suitable for the facial mask used in spring
Spring suitable compositions:
4, spring suitable compositions are prepared:
A, A phase substance is weighed in proportion, 7 times of amounts, 60 DEG C of hot water dissolvings are added, and is filtered, is obtained material E.
B, B phase substance is measured in proportion, PEG-60 rilanit special is added, 60 revs/min 15 minutes emulsified, at cream
Shape obtains material F.
C, with after 10 times of amounts, 50 DEG C of hot water dissolving's C phase substances, material G is obtained.
D, material E, F, G are merged, is added in basic ingredient material D, continues to homogenize 15 minutes under 180 revs/min.
G, product inspection, storage, filling, packaging, storage.
2 summer of embodiment is applicable in facial mask
1, basic ingredient and its preparation are same with spring facial mask, are A phase;
2, summer suitable compositions:
3, summer suitable compositions are prepared:
A, B phase extract is weighed in proportion, 7 times of amounts, 60 DEG C of hot water dissolvings of extract total amount are added, is filtered, and filtrate is standby
With.
B, C phase substance is weighed in proportion, and 7 times of amount water dissolution of extract total amount is added.
C, D phase substance is weighed in proportion, PEG-60 rilanit special is added, and 150-180 revs/min of emulsifying 10 divides
Clock.
D, by A, B, C, D phased soln object mix, be added in basic ingredient, 150-180 revs/min emulsifying 5 minutes,
Astaxanthin is added, continues 15 minutes of emulsifying
E, product inspection, storage, filling, packaging, storage.
3 autumn of embodiment is applicable in facial mask
1, basic ingredient and its preparation are the same, are A phase;
2, autumn suitable compositions:
3, autumn suitable compositions are prepared:
A, B phase extract is weighed in proportion, and 7 times of amounts, 60 DEG C of hot water dissolvings of extract total amount, filtering is added.
B, C phase substance is measured in proportion, PEG-60 rilanit special is added, and 150-180 revs/min of emulsifying 10 divides
Clock.
C, D phase substance is weighed in proportion, and 10 times of amounts, 50 DEG C of hot water dissolvings are added.
D, A, B, C, D phased soln object are mixed, is added in basic ingredient, 150-180 revs/min homogenizes 15 minutes.
E, product inspection, storage, filling, packaging, storage.
Embodiment 4, winter are applicable in facial mask
1, winter suitable compositions:
2, basic ingredient and its preparation are the same, are A phase;
3, winter suitable compositions are prepared:
A, B phase extract is weighed in proportion, and 7 times of amounts, 60 DEG C of hot water dissolvings of extract total amount, filtering is added.
B, C phase substance is measured in proportion, PEG-60 rilanit special is added, and 150-180 revs/min of emulsifying 10 divides
Clock.
C, D phase substance is weighed in proportion, and 10 times of amounts, 40 DEG C of hot water dissolvings are added.
D, A, B, C, D phased soln object are mixed, is added in basic ingredient, 150-180 revs/min homogenizes 15 minutes.
E, product inspection, storage, filling, packaging, storage.
Claims (3)
1. a kind of Wash-free mask for adapting to the different times, it is characterised in that: the facial mask adds by basic ingredient and according to the different times
The material composition added;The basic ingredient is by water, glycerol, butanediol, pyrrolidines ketone acid sodium, hyaluronic acid, xanthan gum, glycerol
Polymethacrylates, beta glucan, glycine betaine, bletilla polysaccharide, panthenol, Vc and its derivative, Ve and its derivative, spiny dogfish
Alkane, ceramide, allantoin, PEG-60 rilanit special, allium extract, EDETATE SODIUM, citric acid composition;
The substance of the difference time addition be spring facial mask additive or summer facial mask additive or autumn facial mask additive or
Winter facial mask additive;
The spring facial mask additive is by caryophyllus oil, Pogostemon cablin essential, angelica essential oil, Flos Magnoliae oil, eucalyptus oil, tea oil, quercitrin
Element, Fructus Kochiae extract, Radix Sangusorbae extract, Radix Et Rhizoma Rhei extract, Baical Skullcap root P.E, tribulus fruit extract, Rhizoma Chuanxiong extract, kuh-seng
Extract, phellodendron extract, tuckahoe extracts, Honegsukle flower P.E, flower of JINHUAKUI extract, forsythia suspense extraction, chamomile mention
Object, dandelion extract, licoflavone, Schisandra chinens P.E, Cortex Dictamni extract, Herba Hedyotidis Diffusae extract, the sophora bud is taken to extract
Object, calendula extract, red paeonia extract, Astragalus Root P.E, vitamin A, bisabolol, vitamin B6, arbutin, vitamin
B3, biotin, azalaic acid and PEG-60 rilanit special composition;
The summer facial mask additive is by Baical Skullcap root P.E, coptis extract, Radix Sangusorbae extract, Folum Ilicis extract, honeysuckle
Extract, Sambucus Chinensis extract, hippophae rhamnoides, eucommia ulmoides extracts, angelica extract, Gnetum parvifolium extract, kuh-seng mention
Take object, Cortex Dictamni extract, mulberry bark extract, Acer palmatum extract, pterostilbene, bisabolol, menthanol lactic acid ester, cigarette
Amide, luteolin, galangal oil, caryophyllus oil, catnip oil, linolenic acid and PEG-60 rilanit special composition;
The autumn facial mask additive is by SIMMONDSIA CHINENSIS SEED OIL, fat of Oromaius norvaehollandeae, olibanum essential oil, licoflavone, Gotu Kola P.E, aobvious tooth snake
Grape extract, inula flower extractive, extractive of perilla, Rosmarinus officinalis extract, achyranthes bidentata extract, Arnica extract, gold thread
Prunus mume extract, calendula extract, flower of JINHUAKUI extract, Sorbus alnifloria extract, coltsfoot extract, gadol extract, turmeric
Extract, chlorella extract, vitamin B3, isomery hexadecane, vitamin E, vitamin A, collagen, two palmityl hydroxyl dried meat
Propylhomoserin, sodium lactate, D- arbutin, PEG-60 rilanit special composition;
The winter facial mask additive by D- arbutin, phytosphingosine, Cyanotis arachnoides P.E, wolfberry fruit extract, it is climing more
Certain kind of berries extract, sad certain herbaceous plants with big flowers acid glycerol acid esters, dipalmitoyl hydroxyproline, bisabolol, stearic acid sucrose ester, Fructus Foeniculi quintessence oil,
Isononyl isononanoate, isomery hexadecane, male cicada moth extract, fat of Oromaius norvaehollandeae, palmityl tripeptides, polyquaternium -51, PEG-60 hydrogenation
Castor oil composition.
2. a kind of Wash-free mask for adapting to the different times as described in claim 1, it is characterised in that: the spring facial mask addition
The weight by volume ratio of each component in object are as follows: caryophyllus oil 0.05-0.1, Pogostemon cablin essential 0.05-0.10, angelica essential oil 0.2-
0.4, Flos Magnoliae oil 0.2-0.4, eucalyptus oil 0.1-0.3, tea oil 0.1-0.3, Quercetin 0.04-0.06, licoflavone 0.02-
0.04, Fructus Kochiae extract 0.1-0.03, Radix Sangusorbae extract 0.1-0.3, Radix Et Rhizoma Rhei extract 0.1-0.2, Baical Skullcap root P.E
0.1-0.3, tribulus fruit extract 0.05-0.07, Rhizoma Chuanxiong extract 0.1-0.3, shrubby sophora extract 0.05-0.08, tuckahoe extracts
0.2-0.5, Cortex Dictamni extract 0.2-0.4, phellodendron extract 0.1-0.2, Honegsukle flower P.E 0.1-0.3, flower of JINHUAKUI mention
Object 0.1-0.3, chamomile is taken to extract 0.2-0.4, Fructus Forsythiae oil 0.05-0.1, Schisandra chinens P.E 0.05-0.1, oldenlandia and mention
Take object 0.1-0.3, calendula extract 0.1-0.3, Huai Goat 0.06-0.12, dandelion extract 0.3-0.4, radix paeoniae rubra
Extract 0.05-0.08, Astragalus Root P.E 0.1-0.3, vitamin A 0.1-0.3, bisabolol 0.2-0.5, vitamin B6
0.1-0.3, arbutin 0.01-0.06, vitamin B3 0.1-0.13, biotin 0.1-1, azalaic acid 0-0.05, PEG-
60 rilanit special 0.1-0.3;
The weight by volume ratio of each component in the summer facial mask additive are as follows: Baical Skullcap root P.E 0.5-1, coptis extract
0.1-0.3, Radix Sangusorbae extract 0.1-0.4, Folum Ilicis extract 0.1-0.5, Honegsukle flower P.E 0.1-0.3, Sambucus Chinensis extract
0.1-0.4, hippophae rhamnoides 0.2-0.5, eucommia ulmoides extracts 0.3-0.5, angelica extract 0.1-0.3, Gnetum parvifolium mention
Take object 0.1-0.2, Cortex Dictamni extract 0.1-0.3, shrubby sophora extract 0.1-0.2, mulberry bark extract 0.1-0.3, chicken feet
Maple extract 0.1-0.4, pterostilbene 0.03-0.1, bisabolol 0.03-0.06, menthanol lactic acid ester 0.04-0.08, niacinamide
0.1-0.4, luteolin 0.05-0.1, galangal oil 0.03-0.08, caryophyllus oil 0.05-0.1, catnip oil 0.1-0.3, flax
Oleic acid 0.1-0.5, PEG-60 rilanit special 0.1-3;
The weight by volume ratio of each component in the autumn facial mask additive are as follows: SIMMONDSIA CHINENSIS SEED OIL 0.1-0.3, fat of Oromaius norvaehollandeae 0.1-
0.3, olibanum essential oil 0.1-0.4, licoflavone 0.03-0.05, Gotu Kola P.E 0.2-0.4, Ampelopsis grossdentata (Hand.-Mazz.) W.T.Wang extract
0.1-0.3, inula flower extractive 0.1-0.3 extractive of perilla 0.1-0.3, Rosmarinus officinalis extract 0.05-0.1, achyranthes bidentata extract
0.1-0.3, Arnica extract 0.1-0.3, hamamelis extract 0.1-0.4, calendula extract 0.1-0.4, flower of JINHUAKUI
Extract 0.1-0.3, Sorbus alnifloria extract 0.2-0.4, coltsfoot extract 0.2-0.4, gadol extract 0.1-0.3, turmeric mention
Take object 0.1-0.3, chlorella extract 0.2-0.4, vitamin B3 0.1-0.3, isomery hexadecane 0.3-0.5, vitamin
E0.1-0.3, vitamin A 0.1-0.3, dipalmitoyl hydroxyproline 0.1-0.4, collagen 1-3, sodium lactate 0.1-0.3, D-
Arbutin 0.1-0.4, PEG-60 rilanit special 0.1-0.3;
The weight by volume ratio of the winter facial mask additive each component are as follows: D- arbutin 0.05-0.1, phytosphingosine
0.2-0.4, Cyanotis arachnoides P.E 0.1-0.3, wolfberry fruit extract 0.3-0.5, Cranberry extract 0.2-0.4, sad certain herbaceous plants with big flowers acid are sweet
It is oleate 0.4-0.6, dipalmitoyl hydroxyproline 0.4-0.6, bisabolol 0.05-0.1, stearic acid sucrose ester 0.1-0.3, small
Fennel essential oil 0.08-0.12, isononyl isononanoate 0.1-0.3, isomery hexadecane 0.1-0.3, male cicada moth extract 0.1-0.3,
Fat of Oromaius norvaehollandeae 0.1-0.3, palmityl tripeptides 1-3, polyquaternium -51(1-3), PEG-60 rilanit special 0.1-0.3.
3. a kind of Wash-free mask for adapting to the different times as described in claim 1, it is characterised in that: each in the basic ingredient
The weight by volume ratio of component are as follows: water 70-80, glycerol 3-5, butanediol 3-5, pyrrolidines ketone acid sodium (NL-50) 3-5, transparent
Matter acid (high and low molecular weight) 0.1-0.4, xanthan gum 0.2-0.4, glycerol polymethacrylates 0.8-1.5, beta glucan 0.1-
0.3, glycine betaine 0.2-0.5, bletilla polysaccharide 0.6-1.5, panthenol 0.1-0.3, Vc and its derivative 0.1-0.3, Ve and its derivative
Object 0.06-0.1, saualane 0.6-1.2, ceramide 0.2-0.4, allantoin 0.1-0.4, PEG-60 rilanit special 0.1-
0.4, allium extract 2-5, EDETATE SODIUM 0.02-0.04, citric acid 0.05-0.08.
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