CN110051592A - A kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle - Google Patents
A kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle Download PDFInfo
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- CN110051592A CN110051592A CN201910442764.9A CN201910442764A CN110051592A CN 110051592 A CN110051592 A CN 110051592A CN 201910442764 A CN201910442764 A CN 201910442764A CN 110051592 A CN110051592 A CN 110051592A
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- artemisiae argyi
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- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D34/00—Containers or accessories specially adapted for handling liquid toiletry or cosmetic substances, e.g. perfumes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/49—Solubiliser, Solubilising system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The present invention relates to spraying technical field, it is related to that a kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle, the raw material including following mass percent: Folium Artemisiae Argyi extract 1-5%；Glycerol 1-5%；Dipropylene glycol 0.5-1.3%；Glycine betaine 0.5-1.2%；Natural antiseptic agent 0.1-0.7%；Bisabolol 0.1-0.6%；Pungent glycol 0.1-0.5%；Water 87-95%.What the present invention was added is Folium Artemisiae Argyi extract, and Folium Artemisiae Argyi extract complete extraction and can save effective component in folium artemisiae argyi, to play the role of anti-oxidant and sterilize；And production cost is low, it is easy to popularize.
Description
Technical field
The present invention relates to spraying technical field, more particularly, to a kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle.
Background technique
It is by spraying exactly Artificial Fog, principle is exactly to be ejected liquid with imperceptible water particle using high-pressure system.
Wormwood is that have Chinese medicine also known as argy wormwood, doctor's grass of long history etc. simply, there is extensive medical value.In Chinese medicine
In, wormwood has effects that anti-inflammatory, analgesic, activating microcirculation and removing stasis medicinal, mainly to the treatment to rheumatism patient；In terms of beauty, utilize
Folium artemisiae argyi, which fumigates face with vapor, so that dry skin is improved, and wormwood then can achieve anti-inflammatory, toxin expelling, active function
Effect.
Notification number are as follows: CN105326691A, patent name are as follows: a kind of spray of the hydrosol containing wormwood and preparation method thereof,
It discloses the sprays of the hydrosol containing wormwood, mainly by wormwood hydrosol, rose, camomile extract, trehalose, allantois
Element, dipotassium glycyrrhizinate, hyaluronic acid, glycerol, preservative and water composition.The spray of its hydrosol containing wormwood provided has wide spectrum
Bactericidal properties, antianaphylaxis and anti-inflammatory anti-itch effect, while also have slow down skin aging, promote skin blood circulation, mend
Water, moisturizing, the effect to refresh the mind.And this contains the spray of wormwood hydrosol to no skin irritation, and long-time service will not go out
The phenomenon that existing dermal toxicity.
However, hydrosol major function or moisturizing, even the hydrosol extracted from wormwood and rose, total Huang of acquisition
Ketone and Determination of Polyphenols are simultaneously few, can not reach the sterilization and other effects.Simultaneously because hydrosol its obtain general flavone and
Determination of Polyphenols is simultaneously few, it is therefore desirable to which the content for increasing hydrosol in spraying is unfavorable for substantially increase generation cost
It popularizes.
Summary of the invention
The object of the present invention is to provide a kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle, what is be added is folium artemisiae argyi extraction
Object, Folium Artemisiae Argyi extract can complete extraction and save folium artemisiae argyi in effective component, thus play the role of it is anti-oxidant and sterilize；And
Production cost is low, easy to popularize.
Above-mentioned technical purpose of the invention has the technical scheme that a kind of folium artemisiae argyi essence moisturizing spray
Mist, the raw material including following mass percent:
By using above-mentioned technical proposal, Folium Artemisiae Argyi extract by half bionical extraction steam distillation extract filtering technique into
Row extract, can complete extraction and save folium artemisiae argyi in effective component, pass through the suppression to Escherichia coli, staphylococcus aureus
Bacterium test determines that Folium Artemisiae Argyi extract has bacteriostasis.
Glycerol and dipropylene glycol exist in aerosol as solvent, it is miscible with water after for Folium Artemisiae Argyi extract and other
Dissolving each other with synergistic effect between component, and glycerol and dipropylene glycol have the function of moisturizing, and moisture can be improved in gas
Retention time in mist, makes aerosol when being sprayed on skin surface, can persistently be effectively improved dry skin state.
Pungent glycol i.e. Isosorbide-5-Nitrae-ethohexadiol, belong to alkane diol class, and alkane diol class is in addition to the function with moisturizing
Effect is outer, also has certain antibacterial activity.And pungent glycol and preservative have association for preservative when being used in compounding
The antibacterial anti-corrosion ability of preservative can be improved in same-action.
Glycine betaine can form stronger hydrogen bond in aqueous solution, and carboxyl attracts the hydrogen atom in hydrone, the water of absorption
Molecule is distributed in around glycine betaine under two kinds of opposite power effects by stereo directional.After glycine betaine is in conjunction with a molecular water, this
One molecular water is also easy to be replaced by another molecular water, so glycine betaine is easy to discharge hydrone when physical condition changes
Into the environment on periphery, to be more conducive to the balance of skin surface hydrone.
Bisabolol is nature there are one of more sesquiterpenoid, has the function of antiphlogistic and bactericidal, for
Aerosol plays certain antisepsis.Other than antiphlogistic and bactericidal, bisabolol is also a kind of preferable fixastive of stability, red
The light happiness of the fragrance of bisabol can play the role of deodorization so that aerosol has certain fragrance.
The further setting of the present invention are as follows: the moisturizing of folium artemisiae argyi essence includes the raw material of following mass percent by spraying:
By using above-mentioned technical proposal, mulberry-leaf extract extracts filtering technique also by half bionical extraction steam distillation
Extract, can complete extraction and save mulberry leaf in effective component, raising inhibit tyrosinase by spraying, to play beauty
White effect.
Camomile extract is extracted filtering technique also by half bionical extraction steam distillation and is extracted, can be complete
The effective component in chamomile is extracted and saves, improving by spraying has anti-oxidant, antiangiogenic, anti-inflammatory, anti-allergy and resist
Effect of virus.
The further setting of the present invention are as follows: the natural antiseptic agent includes following components in percentage by weight:
By using above-mentioned technical proposal, parahydroxyacet-ophenone is a kind of natural plant extracts, is had for fungi
Stronger killing ability, and it is all more stable in wide pH and temperature range.
Ginkgo lactones is also natural plants anticorrosive additive, also has stronger killing ability for microorganisms such as bacteriums.
Nucleoprotamine is a kind of basic protein, shows better bacteriostasis in neutral and alkaline medium,
The sterilization sterilization capability of the environment meta-alkalescence of aerosol, nucleoprotamine is preferable.
2,6- dimethyl-Isosorbide-5-Nitrae -1,4-benzoquinone is a kind of preservative of broad spectrum activity, is mentioned by raw materials such as henon bamboo, rigid bamboos
It obtains, for the ability to function that inhibits and kills of bacterium, and it is also fine in its thermal stability, under the higher situation of temperature,
Aerosol can be made still to keep all right antibacterial bacteriostatic ability.
The further setting of the present invention are as follows: the Folium Artemisiae Argyi extract extracts filtering by half bionical extraction steam distillation
Technology extracts, the extraction process the following steps are included:
Step (1): it by 65-75g folium artemisiae argyi powders, is added in four-hole boiling flask, is fixed in electric jacket；
Step (2): being added with folium artemisiae argyi powder weight ratio is (8-12): 1 distilled water, then adjusts PH=with acetic acid
It slowly heats up after 1.8-2.2, flow back 2.5-3h, cools down, and filtering obtains that water phase a is spare, and solid is refunded in flask；
Step (3): continuously adding with folium artemisiae argyi powder weight ratio is (5-7): 1 distilled water, adjusts PH=with acetic acid
It slowly heats up after 1.8-2.2, flow back 1.2-1.6h, cools down, and filtering obtains that water phase b is spare, and solid is refunded in flask；
Step (4): adding with folium artemisiae argyi powder weight ratio is (5-7): 1 distilled water, adjusts PH=8-9 with plant ash
Slowly heating afterwards, flow back 0.55-0.75h, cools down, and filtering, it is spare to obtain water phase c, and solid abandons；
Step (5): purification obtains Folium Artemisiae Argyi extract.
By using above-mentioned technical proposal, folium artemisiae argyi extracts filtering technique by half bionical extraction steam distillation and is mentioned
It takes, most of effective component in folium artemisiae argyi can be saved.The dissolution recovery rate of effective component in acid condition in folium artemisiae argyi is more
Height, so folium artemisiae argyi is extracted by acid solution twice during the extraction process, so that effective component is adequately extracted.Then alkali is used again
By the better constituents extraction of dissolution recovery rate partially under alkaline condition, and alkali can will be during the remaining acid in part carries out
With so that the soda acid of the mixed liquor obtained after the mixing of last three's extracting solution is moderate.Finally purified by Folium Artemisiae Argyi extract,
Obtain the less extract of impurity content.
The further setting of the present invention are as follows: the step (5) purification the following steps are included:
S1: gained three parts of water phases a, b, c being mixed, then distills, regathers distillate, evaporated when collecting 400ml -550ml
Out after liquid, stop distillation；
S2: the distillates obtained with points of 3 times extraction S1 of 280-320ml ethyl acetate, after organic phase merges, then with anhydrous
Sodium sulphate is dry, removes ethyl acetate using revolving, obtains Folium Artemisiae Argyi extract；
Or purification the following steps are included:
M1: gained three parts of water phases a, b, c are mixed, are then evaporated under reduced pressure, and collect 60~70 DEG C of distillates；
M2: the distillate in step s1 stands 20~28h, and then the oil reservoir on liquid upper layer is separated, takes subnatant；
M3: subnatant is placed 5~7 days at 3~5 DEG C, then takes upper layer absolute extract liquid, obtains Folium Artemisiae Argyi extract.
By using above-mentioned technical proposal, purification is basic by the pigment in the obtained clear liquid after distillation standing for long periods
It removes, so that extract is purer, and opposite operation is simpler.
The further setting of the present invention are as follows: the spraying spray bottle of folium artemisiae argyi essence moisturizing, including bottle body are installed on the bottle body
There is bottle cap, the storage bag of storage spray liquid is installed in the bottle body, delivery pipe, the delivery pipe are installed in the storage bag
One end is connected with the connecting tube being arranged on the outside of storage bag, and one end of the connecting tube is connected with delivery pipe, the connecting tube
The other end is connected with bottle cap；Pressurization flow-guiding mouth is offered on the bottle cap, in the connecting tube of pressurization flow-guiding mouth one end
Unidirectional blocking mechanism is installed.
By using above-mentioned technical proposal, it is stored with folium artemisiae argyi essence moisturizing in storage bag and is sprayed, when storage bag outside and bottle
When intracorporal pressure increases, it is defeated to make the folium artemisiae argyi essence moisturizing in storage bag pass through by spraying that the pressure of increase can squeeze storage bag
It is sprayed after sending pipe, connecting tube from pressurization flow-guiding mouth.Since storage bag keeps folium artemisiae argyi essence moisturizing spraying and gas-insulated, to avoid
Bacterium in gas makes folium artemisiae argyi essence moisturizing go bad by spraying, while also avoiding that synthesis anti-corrosion is added in folium artemisiae argyi essence moisturizing is spraying
Agent generates irritation or potential security risk to human body.
The further setting of the present invention are as follows: the unidirectional blocking mechanism includes blocking supporting baffle, the blocking support block
Plate passes through first connecting rod, the second connecting rod, third connecting rod and the 4th connecting rod respectively and is connected with the inner sidewall of delivery pipe, institute
It states and forms the first spray liquid transfer passage between first connecting rod and the second connecting rod, second connecting rod and third connecting rod
Between form the second spray liquid transfer passage, it is logical that the conveying of third spray liquid is formed between the third connecting rod and the 4th connecting rod
Road forms the 4th spray liquid transfer passage between the 4th connecting rod and first connecting rod；Pacify in the blocking supporting baffle
Equipped with buffer spring, far from the sealing block phase for blocking the buffer spring of supporting baffle one end with capable of separating pressurization flow-guiding mouth
Even, the sealing block is abutted with the inner sidewall of bottle cap, and it is recessed that pressurization is offered on the sealing block of pressurization flow-guiding mouth one end
Slot.
Add by using above-mentioned technical proposal when the pressure that the external world applies pressurizes to sealing block by pressurization flow-guiding mouth
Pressure gas stream directly generates impact force to pressurization groove；Sealing block make buffer spring after being under pressure deformation occurs simultaneously sealing block with
There are gaps between pressurization flow-guiding mouth；Forced air is entered in bottle body by the gap between sealing block and pressurization flow-guiding mouth, from
And increase the intracorporal pressure of bottle；The pressure of increase can squeeze storage bag to make the folium artemisiae argyi essence moisturizing in storage bag lead to by spraying
After crossing delivery pipe, then pass through the first spray liquid transfer passage, the second spray liquid transfer passage, third spray liquid transfer passage or the
Gap of the four spray liquid transfer passages finally between sealing block and pressurization flow-guiding mouth sprays storage bag.
First spray liquid transfer passage, the second spray liquid transfer passage, third spray liquid transfer passage and the 4th spray liquid
The setting of transfer passage effectively improves the flow velocity that the moisturizing of folium artemisiae argyi essence sprays storage bag by spraying.
The further setting of the present invention are as follows: the sealing block is cylindric sealing block, close to blocking supporting baffle one end
The area of the sealing block cross section is less than the area of the sealing block cross section close to pressurization flow-guiding mouth one end；Close to buffering
Positive stop lug boss is mounted in the first connecting rod of spring one end, the second connecting rod, third connecting rod and the 4th connecting rod；
Limit fin is installed, there are gaps between limit fin and the inner sidewall of connecting tube, and limit on the lateral wall of the sealing block
The sum of height and the height of positive stop lug boss of position fin are greater than the spacing between sealing block and connecting tube inner sidewall.
By using above-mentioned technical proposal, if the extraneous pressure applied is excessive, sealing block makes buffer spring after being under pressure
Deformation occurs be more than buffer spring itself deformability, it will cause buffer spring damage to can not active homing, from
And cause sealing block that cannot effectively be sealed to pressurization flow-guiding mouth.The setting of positive stop lug boss can limit the deformation of buffer spring
Highly, so that avoiding buffer spring deformation is more than the deformability of buffer spring itself, guarantee that buffer spring being capable of active homing.
There are gaps between limit fin and the inner sidewall of connecting tube, therefore the setting for limiting fin will not influence folium artemisiae argyi
Essence moisturizing is spraying from the first spray liquid transfer passage, the second spray liquid transfer passage, third spray liquid transfer passage or the 4th
Spray liquid transfer passage passes through；Simultaneously because the height of limit fin and the sum of the height of positive stop lug boss be greater than sealing block with connect
Spacing between pipe inner sidewall, therefore when sealing block is inserted into connecting tube, sealing block can't be protected by air-flow or folium artemisiae argyi essence
The ejection impact force of wet spray and rotated in connecting tube, influence that folium artemisiae argyi essence moisturizing is spraying to be sprayed from spray liquid transfer passage
Flow velocity.
The further setting of the present invention are as follows: it is recessed that buffering is offered in the blocking supporting baffle of delivery pipe one end
Slot offers buffer channel in the blocking supporting baffle, and one end of the buffer channel is connected to setting with buffer groove, described
The other end of buffer channel and the first spray liquid transfer passage, the second spray liquid transfer passage, third spray liquid transfer passage or
4th spray liquid transfer passage is connected setting.
By using above-mentioned technical proposal, it is spraying to blocking support that the setting of buffer groove can buffer folium artemisiae argyi essence moisturizing
The impact force of baffle；Folium artemisiae argyi essence moisturizing in buffer groove can be drained to by spraying the first spray liquid by the setting of buffer channel
Transfer passage, the second spray liquid transfer passage, third spray liquid transfer passage or the 4th spray liquid transfer passage, to guarantee to end
The flow velocity that the moisturizing of folic acid China sprays by spraying.
The further setting of the present invention are as follows: oxygen barrier sterilizing layer is coated on the inner sidewall of the storage bag, it is described oxygen barrier to disappear
Malicious layer includes the raw material of following mass fraction ratio:
By using above-mentioned technical proposal, aqueous polyurethane emulsion is connect under the action of wetting agent with storage bag inner sidewall
More abundant, then to generate again by crosslinking agent to aqueous polyurethane emulsion crosslinking curing effect is touched, so that aqueous polyurethane
Nucleoprotamine and octagonal alcohol extracting thing are coated the inner sidewall one layer of antimicrobial sealing film of formation for being solidificated in storage bag, fish by lotion together
Protamine is a kind of basic protein, shows better bacteriostasis, the ring of aerosol in neutral and alkaline medium
The sterilization sterilization capability of border meta-alkalescence, nucleoprotamine is preferable.In octagonal alcohol extracting thing containing illiciumverum in effective component, illiciumverum in
Extract there is certain antibacterial activity, and it belongs to natural antimicrobial, minimum for the irritation of human body, is not easy in bottle
Be sprayed and impact.
In conclusion advantageous effects of the invention are as follows:
(1) Folium Artemisiae Argyi extract extracts filtering technique by half bionical extraction steam distillation and extracts, can be complete
The effective component extracted and saved in folium artemisiae argyi determines that folium artemisiae argyi mentions by the bacteriostatic test to Escherichia coli, staphylococcus aureus
Take object that there is bacteriostasis；
(2) folium artemisiae argyi extracts filtering technique by half bionical extraction steam distillation and extracts, and can save in folium artemisiae argyi
Most of effective component；The dissolution recovery rate of effective component in acid condition in folium artemisiae argyi is higher, so folium artemisiae argyi was being extracted
It is extracted in journey by acid solution twice, so that effective component is adequately extracted；It then again will partially under alkaline condition with alkali
The better constituents extraction of dissolution recovery rate, and alkali can neutralize the remaining acid in part, so that last three extracts
The soda acid of the mixed liquor obtained after liquid mixing is moderate；
(3) it is spraying that it is stored with folium artemisiae argyi essence moisturizing in storage bag, on the outside of storage bag and when the intracorporal pressure of bottle increases, increases
Big pressure can squeeze storage bag thus from pressurization after making the folium artemisiae argyi essence moisturizing in storage bag pass through delivery pipe, connecting tube by spraying
Flow-guiding mouth sprays；Since storage bag keeps folium artemisiae argyi essence moisturizing spraying and gas-insulated, so that the bacterium in gas be avoided to make folium artemisiae argyi
Essence moisturizing is gone bad by spraying, while also avoiding that synthetic preservative is added in folium artemisiae argyi essence moisturizing is spraying, generates stimulation to human body
Property or potential security risk.
Detailed description of the invention
Fig. 1 is overall structure diagram of the invention；
Fig. 2 is the structural schematic diagram of storage bag；
Fig. 3 is the unidirectional structural schematic diagram for blocking mechanism；
Fig. 4 is the mounting structure schematic diagram for blocking supporting baffle；
Fig. 5 is the cross-sectional view for blocking supporting baffle.
Appended drawing reference: 1, bottle body；2, bottle cap；3, storage bag；4, delivery pipe；5, connecting tube；6, pressurize flow-guiding mouth；11, it hinders
Disconnected supporting baffle；12, first connecting rod；13, the second connecting rod；14, third connecting rod；15, the 4th connecting rod；16, the first spray
Spray film transfer passage；17, the second spray liquid transfer passage；18, third spray liquid transfer passage；19, the conveying of the 4th spray liquid is logical
Road；20, buffer spring；21, sealing block；22, pressurize groove；23, positive stop lug boss；24, fin is limited；25, buffer groove；26,
Buffer channel.
Specific embodiment
Below in conjunction with attached drawing, invention is further described in detail.
Embodiment 1:
A kind of folium artemisiae argyi essence moisturizing is spraying, the raw material including following mass percent:
The natural antiseptic agent includes following components in percentage by weight:
The Folium Artemisiae Argyi extract is extracted by half bionical extraction steam distillation extraction filtering technique, the extraction
Process the following steps are included:
Step (1): it by 70g folium artemisiae argyi powder, is added in four-hole boiling flask, is fixed in electric jacket；
Step (2): being added the distilled water for being 10: 1 with folium artemisiae argyi powder weight ratio, then with slow after acetic acid adjusting PH=2
Heating, flow back 2.7h, cools down, and filtering obtains that water phase a is spare, and solid is refunded in flask；
Step (3): the distilled water for being 6: 1 with folium artemisiae argyi powder weight ratio is continuously added, is slowly risen after adjusting PH=2 with acetic acid
Temperature, flow back 1.4h, cools down, and filtering obtains that water phase b is spare, and solid is refunded in flask；
Step (4): the distilled water for being 6: 1 with folium artemisiae argyi powder weight ratio is added, is slowly risen after adjusting PH=8 with plant ash
Temperature, flow back 0.65h, cools down, and filtering, it is spare to obtain water phase c, and solid abandons；
Step (5): purification obtains Folium Artemisiae Argyi extract.
The step (5) purification the following steps are included:
S1: gained three parts of water phases a, b, c being mixed, then distills, regathers distillate, evaporated when collecting 400ml -550ml
Out after liquid, stop distillation；
S2: the distillates obtained with points of 3 times extraction S1 of 280-320ml ethyl acetate, after organic phase merges, then with anhydrous
Sodium sulphate is dry, removes ethyl acetate using revolving, obtains Folium Artemisiae Argyi extract.
As shown in Figure 1, a kind of spray bottle that the moisturizing of folium artemisiae argyi essence is spraying, including cylindrical bottle body 1, it is equipped on bottle body 1
Bottle cap 2, bottle cap 2 are recessed connection convex block, connect and offer pressurization flow-guiding mouth 6 on convex block.
As shown in Figures 2 and 3, the storage bag 3 of storage spray liquid is installed in bottle body 1, delivery pipe 4 is installed in storage bag 3,
4 one end of delivery pipe is connected with the connecting tube 5 that 3 outside of storage bag is arranged in, and delivery pipe 4 and 3 touching position glue of storage bag seal, from
And guarantee the leakproofness of storage bag.One end of connecting tube 5 is connected with delivery pipe 4, and the other end of connecting tube 5 is connected with bottle cap 2；It leans on
Unidirectional blocking mechanism is installed in the connecting tube 5 of nearly pressurization 6 one end of flow-guiding mouth.
As shown in figure 4, unidirectionally blocking mechanism includes blocking supporting baffle 11, supporting baffle 11 is blocked to connect respectively by first
Extension bar 12, the second connecting rod 13, third connecting rod 14 and the 4th connecting rod 15 are connected with the inner sidewall of delivery pipe 4, the first connection
The first spray liquid transfer passage 16 is formed between bar 12 and the second connecting rod 13, between the second connecting rod 13 and third connecting rod 14
The second spray liquid transfer passage 17 is formed, forms third spray liquid transfer passage between third connecting rod 14 and the 4th connecting rod 15
18, the 4th spray liquid transfer passage 19 is formed between the 4th connecting rod 15 and first connecting rod 12.Block the week of supporting baffle 11
First connecting rod 12, the second connecting rod 13, third connecting rod 14 and the 4th connecting rod 15 are equidistantly provided on side wall, to make
One spray liquid transfer passage 16, the second spray liquid transfer passage 17, third spray liquid transfer passage 18 and the conveying of the 4th spray liquid
The aisle spare that channel 19 is formed is all the same.
Buffer spring 20 is installed in supporting baffle 11 as shown in figure 3, blocking, far from the slow of blocking 11 one end of supporting baffle
It rushes spring 20 and is connected with the sealing block 21 that can separate pressurization flow-guiding mouth 6, sealing block 21 is abutted with the inner sidewall of bottle cap 2, close
Pressurization groove 22 is offered on the sealing block 21 of pressurization 6 one end of flow-guiding mouth.The groove diameter of pressurization groove 22 is less than pressurization water conservancy diversion
The diameter of mouth 6.
As shown in Figure 3 and Figure 4, sealing block 21 is cylindric sealing block, close to the sealing block for blocking 11 one end of supporting baffle
The area of 21 cross sections is less than the area of 21 cross section of sealing block close to pressurization 6 one end of flow-guiding mouth；Close to buffer spring 20 1
Positive stop lug boss 23 is mounted in the first connecting rod 12 at end, the second connecting rod 13, third connecting rod 14 and the 4th connecting rod 15；
Limit fin 24 is installed on the lateral wall of sealing block 21, there are gaps between limit fin 24 and the inner sidewall of connecting tube 5, and
Limit the spacing that the sum of the height of fin 24 and the height of positive stop lug boss 23 are greater than between 5 inner sidewall of sealing block 21 and connecting tube.
As shown in figure 5, offering buffer groove 25 in the blocking supporting baffle 11 of 4 one end of delivery pipe, support is blocked
Offer buffer channel 26 on baffle 11, one end of buffer channel 26 is connected to setting with buffer groove 25, buffer channel 26 it is another
One end and the first spray liquid transfer passage 16, the second spray liquid transfer passage 17, third spray liquid transfer passage 18 or the 4th spray
Spray film transfer passage 19 is connected setting.
The spraying spray bottle of folium artemisiae argyi essence moisturizing described in the present embodiment when in use, is passed through by the pressure that the external world applies
When the flow-guiding mouth 6 that pressurizes pressurizes to sealing block 21, forced air directly generates impact force to pressurization groove 22；Sealing block 21 is pressed
Making buffer spring 20 after power, deformation occurs while there are gaps between sealing block 21 and pressurization flow-guiding mouth 6；Forced air passes through close
Gap between envelope block 21 and the flow-guiding mouth 6 that pressurizes enters in bottle body, so that the pressure in bottle body 1 be made to increase；The pressure meeting of increase
After storage bag 3 is squeezed to make the folium artemisiae argyi essence moisturizing in storage bag 3 pass through delivery pipe 4 by spraying, then it is defeated by the first spray liquid
Send channel 16, the second spray liquid transfer passage 17, third spray liquid transfer passage 18 or the 4th spray liquid transfer passage 19 last
Gap between sealing block 21 and pressurization flow-guiding mouth 6 sprays storage bag 3.
Oxygen barrier sterilizing layer is coated on the inner sidewall of storage bag 3, oxygen barrier sterilizing layer includes the former material of following mass fraction ratio
Material:
Embodiment 2~10 the difference from embodiment 1 is that: each component is following table by weight percentage in spraying.
Embodiment 11~14 the difference from embodiment 1 is that: under each component is by weight percentage in natural antiseptic agent
Table.
Embodiment 15~18 the difference from embodiment 1 is that: under each component is by weight percentage in natural antiseptic agent
Table.
Embodiment 19 the difference from embodiment 1 is that: method of purification, purification the following steps are included:
M1: gained three parts of water phases a, b, c are mixed, are then evaporated under reduced pressure, and collect 60~70 DEG C of distillates；
M2: the distillate in step s1 stands 20~28h, and then the oil reservoir on liquid upper layer is separated, takes subnatant；
M3: subnatant is placed 5~7 days at 3~5 DEG C, then takes upper layer absolute extract liquid, obtains Folium Artemisiae Argyi extract.
Comparative example
Comparative example 1 the difference from embodiment 1 is that: be not added with Folium Artemisiae Argyi extract in the component of aerosol；
Comparative example 2 the difference from embodiment 1 is that: be not added with natural antiseptic agent in the component of aerosol；
Comparative example 3 the difference from embodiment 1 is that: in the component of aerosol addition and Folium Artemisiae Argyi extract phase homogenous quantities percentage
Than folium artemisiae argyi hydrosol.
Detection method
Antibacterial detection
Conventional method is tested according to antibacterial activity, selects water as solvent carrier, difference testing example 1 and comparative example 1
The inhibitory effect of~3 pairs of Gram-negative bacterias, gram-positive bacteria.
100 (mg/ml) sample solutions are configured according to antibacterial activity test method, and select Gram-negative bacteria, gram
Positive bacteria representativeness mushroom: Escherichia coli, staphylococcus aureus, pseudomonas aeruginosa, bacillus subtilis and saccharomyces cerevisiae,
The antibacterial activity test experiments of carry out system.
Test result is as follows:
In upper table, "+", which represents, has obvious antibacterial activity, and "+" is more, and activity is stronger；It is unknown that "-" represents antibacterial activity
Aobvious, the number in table represents the diameter of inhibition zone in sterilization experiment, and numerical value is bigger, and bacteriostatic activity is stronger..
Conclusion: You Shangbiao it can be concluded that, the aerosol ratio in the embodiment 1 added with wormwood extract is not added with wormwood and mentions
Take the aerosol of object stronger compared to antibacterial activity, it can be concluded that, the addition of natural antiseptic agent mentions wormwood with the comparison of comparative example 2
Take object that there is preferable synergistic antisepsis, it can be concluded that, the aerosol of wormwood extract is pure compared to wormwood with comparative example 3
The antibacterial activity of dew is stronger.
The embodiment of present embodiment is presently preferred embodiments of the present invention, not limits protection of the invention according to this
Range, therefore: the equivalence changes that all structures under this invention, shape, principle are done, should all be covered by protection scope of the present invention it
It is interior.
Claims (10)
1. a kind of folium artemisiae argyi essence moisturizing is spraying, it is characterised in that the raw material including following mass percent:
2. a kind of folium artemisiae argyi essence moisturizing according to claim 1 is spraying, it is characterised in that: including following mass percent
Raw material:
3. a kind of folium artemisiae argyi essence moisturizing according to any one of claim 1 to 2 is spraying, it is characterised in that: described natural
Preservative includes following components in percentage by weight:
4. a kind of folium artemisiae argyi essence moisturizing according to any one of claim 1 to 2 is spraying, it is characterised in that: the folium artemisiae argyi
Extract is extracted by half bionical extraction steam distillation extraction filtering technique, and the extraction process includes following step
It is rapid:
Step (1): it by 65-75g folium artemisiae argyi powders, is added in four-hole boiling flask, is fixed in electric jacket；
Step (2): being added with folium artemisiae argyi powder weight ratio is (8-12): 1 distilled water, then adjusts PH=1.8-with acetic acid
It slowly heats up after 2.2, flow back 2.5-3h, cools down, and filtering obtains that water phase a is spare, and solid is refunded in flask；
Step (3): continuously adding with folium artemisiae argyi powder weight ratio is (5-7): 1 distilled water, adjusts PH=1.8-2.2 with acetic acid
Slowly heating afterwards, flow back 1.2-1.6h, cools down, and filtering obtains that water phase b is spare, and solid is refunded in flask；
Step (4): adding with folium artemisiae argyi powder weight ratio is (5-7): 1 distilled water, is delayed after adjusting PH=8-9 with plant ash
Slow heating, flow back 0.55-0.75h, cools down, filtering, obtains that water phase c is spare, and solid abandons；
Step (5): purification obtains Folium Artemisiae Argyi extract.
5. a kind of folium artemisiae argyi essence moisturizing according to claim 4 is spraying, it is characterised in that: the step (5), which purifies, includes
Following steps:
S1: gained three parts of water phases a, b, c being mixed, then distills, regathers distillate, when collection 400ml -550ml distillate
Afterwards, stop distillation；
S2: the distillate obtained with 280-320ml ethyl acetate point, 3 extraction S1 after organic phase merges, then uses anhydrous slufuric acid
Sodium is dry, removes ethyl acetate using revolving, obtains Folium Artemisiae Argyi extract；
Or purification the following steps are included:
M1: gained three parts of water phases a, b, c are mixed, are then evaporated under reduced pressure, and collect 60~70 DEG C of distillates；
M2: the distillate in step s1 stands 20~28h, and then the oil reservoir on liquid upper layer is separated, takes subnatant；
M3: subnatant is placed 5~7 days at 3~5 DEG C, then takes upper layer absolute extract liquid, obtains Folium Artemisiae Argyi extract.
6. a kind of spraying spray bottle of folium artemisiae argyi essence moisturizing according to claim 1, it is characterised in that: including bottle body (1),
It is equipped with bottle cap (2) on the bottle body (1), the storage bag (3) of storage spray liquid, the storage is installed in the bottle body (1)
It being equipped with delivery pipe (4) in bag (3), described delivery pipe (4) one end is connected with the connecting tube (5) being arranged on the outside of storage bag (3),
One end of the connecting tube (5) is connected with delivery pipe (4), and the other end of the connecting tube (5) is connected with bottle cap (2)；The bottle
Pressurization flow-guiding mouth (6) is offered on lid (2), and unidirectional resistance is installed in the connecting tube (5) of pressurization flow-guiding mouth (6) one end
Breaking mechanism.
7. a kind of spraying spray bottle of folium artemisiae argyi essence moisturizing according to claim 6, it is characterised in that: the unidirectional blocking
Mechanism includes blocking supporting baffle (11), and the blocking supporting baffle (11) passes through first connecting rod (12), the second connection respectively
Bar (13), third connecting rod (14) and the 4th connecting rod (15) are connected with the inner sidewall of delivery pipe (4), the first connecting rod
(12) the first spray liquid transfer passage (16) is formed between the second connecting rod (13), second connecting rod (13) and third connect
The second spray liquid transfer passage (17) is formed between extension bar (14), between the third connecting rod (14) and the 4th connecting rod (15)
It is formed third spray liquid transfer passage (18), it is spraying to form the 4th between the 4th connecting rod (15) and first connecting rod (12)
Liquid transfer passage (19)；Buffer spring (20) are installed on the blocking supporting baffle (11), far from blocking supporting baffle (11)
The buffer spring (20) of one end is connected with the sealing block (21) that can separate pressurization flow-guiding mouth (6), the sealing block (21)
It is abutted with the inner sidewall of bottle cap (2), offers pressurization groove on the sealing block (21) of pressurization flow-guiding mouth (6) one end
(22)。
8. a kind of spraying spray bottle of folium artemisiae argyi essence moisturizing according to claim 7, it is characterised in that: the sealing block
It (21) is cylindric sealing block, the area close to the sealing block (21) cross section for blocking supporting baffle (11) one end, which is less than, to be leaned on
The area of the sealing block (21) cross section of nearly pressurization flow-guiding mouth (6) one end；Close to described the of buffer spring (20) one end
Positive stop lug boss is mounted in one connecting rod (12), the second connecting rod (13), third connecting rod (14) and the 4th connecting rod (15)
(23)；Limit fin (24) is installed on the lateral wall of the sealing block (21), limits the inside of fin (24) and connecting tube (5)
There are gaps between wall, and limit the sum of the height of fin (24) and the height of positive stop lug boss (23) and be greater than sealing block (21) and connect
Take over the spacing between (5) inner sidewall.
9. a kind of spraying spray bottle of folium artemisiae argyi essence moisturizing according to claim 7, it is characterised in that: close to delivery pipe
(4) it offers buffer groove (25) on the blocking supporting baffle (11) of one end, is opened up on the blocking supporting baffle (11)
Have buffer channel (26), one end of the buffer channel (26) is connected to setting, the buffer channel (26) with buffer groove (25)
The other end and the first spray liquid transfer passage (16), the second spray liquid transfer passage (17), third spray liquid transfer passage
(18) or the 4th spray liquid transfer passage (19) is connected setting.
10. a kind of spraying spray bottle of folium artemisiae argyi essence moisturizing according to claim 6, it is characterised in that: the storage bag
(3) oxygen barrier sterilizing layer is coated on inner sidewall, the oxygen barrier sterilizing layer includes the raw material of following mass fraction ratio:
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910442764.9A CN110051592A (en) | 2019-05-25 | 2019-05-25 | A kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle |
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| CN201910442764.9A CN110051592A (en) | 2019-05-25 | 2019-05-25 | A kind of folium artemisiae argyi essence moisturizing is spraying and its spray bottle |
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