CN105287737A - Preparation method of multi-efficacy water-soluble composite plant essential oil spray - Google Patents
Preparation method of multi-efficacy water-soluble composite plant essential oil spray Download PDFInfo
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- CN105287737A CN105287737A CN201410309912.7A CN201410309912A CN105287737A CN 105287737 A CN105287737 A CN 105287737A CN 201410309912 A CN201410309912 A CN 201410309912A CN 105287737 A CN105287737 A CN 105287737A
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Abstract
The invention relates to a preparation method of a multi-efficacy water-soluble composite plant essential oil spray. The essential oil spray is prepared from, by mass percentage, 0.2-0.3% of Korean pine essential oil, 0.05-0.1% of clove essential oil, 0.05-0.1 of Ledum palustre L. essential oil, 0.05-0.1% of rosemary essential oil, 0.1-0.2% of tea tree essential oil, 0.1-0.2% of lavender essential oil, 0.05-0.1% Korean pine bark polyphenol, 2.8-5.0% of hydrogenated castor oil, 0.5-1.0% of glycerin, 0.3-0.5% of propylene glycol and 92.4-95.8% of purified water. No artificial pigment, hormone, essence, heavy metal substance and preservative are added into the essential oil spray, so that the essential oil spray is high in safety; the essential oil spray is advanced and simple in production process and quick and complete in absorption, has efficacy of resisting bacteria and diminishing inflammation, repelling mosquitoes and preventing pests, relieving cold symptoms, purifying air, refreshing, relieving tension and resisting oxidation and radiation and is suitable for being directly used in environment and on skin.
Description
Technical field
The present invention relates to the method for production of a kind of many effects Water Soluble Compound plants essential oil spraying.
Background technology
Plants essential oil is the carrier of plant soul, can regulate the hormone of human body, has endocrine regulation and prophylactic function, can promote the balance of human physiology and psychology.Plants essential oil is at room temperature volatilizable forms unique fragrance atmosphere to air.Plants essential oil contains multiple bioactive ingredients, is of wide application, and as tranquillizing and allaying excitement, anti-inflammation, dispel the wind stomach invigorating, repelling mosquitoes and preventing insects etc.The olfactory of natural essential oil and derivant thereof, organoleptic feature and biological activity are that synthetic perfume is difficult to substitute, and have significant physiology and assist effect.But quintessence oil is mainly used in the fields such as specialty massage and maintenance at present, in most cases instruct use by virtue treatment teacher or cosmetologist, need specific environment and special tool(s), maneuver etc., and due to pure plants essential oil be oil-soluble, the problem such as effumability, not directly use causes the scope of application of plants essential oil to compare limitation, a lot of consumer is not due to professional or feel complicated and to contact quintessence oil less, a lot of occasion also directly cannot use essential oil product, causes the market application of quintessence oil to compare limitation.
Not yet there is being widely used in daily life in the market, possesses multi-efficiency and can the water miscible quintessence oil spray product that uses of many occasions, composite plant quintessence oil is prepared into the water solublity spray-like product of stable homogeneous by this product, there is multi-efficiency, and carry and use all very simple and convenient, family, office, the multiple occasions such as open air can use at any time, can be used to meet anti-inflammation, repelling mosquitoes and preventing insects, alleviate cold symptoms, purify air, refreshment, many-sided effect demand such as to releive nervous, this product form makes the plants essential oil of high-quality be applied in daily life, in this soluble fine spray product, without how, essence and preservative ingredient add, fragrant atmosphere is pure natural plant breath, wherein derived essential oil and polyphenol component self have efficient Antimicrobial preservative effect, product quality can be ensured, there is natural green, easy to use, effect is remarkable, the advantage such as of many uses.
Summary of the invention
The object of the invention is to for these problems above-mentioned, provide a kind of and present uniform and stable water soluble state containing various plants quintessence oil and Pinus koraiensis skin polyphenol isoreactivity composition, there is the method for production of the plants essential oil spraying of natural plant incense atmosphere.The quintessence oil spraying made by the inventive method is containing Pinus koraiensis quintessence oil, Ledum Palustre L.var.dilatatum Wahl. quintessence oil, clove oil, tea tree ethereal oil, Pinus koraiensis skin polyphenol etc., present uniform and stable aqueous phase quality, there is anti-inflammation, repelling mosquitoes and preventing insects, alleviation cold symptoms, purify air, refreshment, many-sided effect such as nervous of releiving, be a kind of product of pure natural.Manufacture method of the present invention, carry out successively according to the following steps:
(1) according to extract part needed for each plants essential oil, Pinus koraiensis extraction of essential oil extracts extract and take from blade, Herba Lysimachiae foenum-graeci quintessence oil extraction from flower from blade, rosemary ethereal oil from blade, tea tree ethereal oil from petal, Ledum Palustre L.var.dilatatum Wahl. extraction of essential oil from Pinus koraiensis tower, clove oil, collect appropriate plant material, vapor distillation is utilized to carry device, technique is water proof distillation, obtain faint yellow to yellow, the pure plants essential oil of clear;
(2) get Pinus koraiensis bark, dry, pulverize, prepare 60% ethanol as Extraction solvent by purified water, Extraction solvent and Pinus koraiensis bark volume are than being 10:1-12:1, and water need not have Pinus koraiensis bark, under 60 DEG C of conditions, in ultrasonic unit, ultrasonic power 300w extracts 0.5h-1h, extract the centrifugal 5min-10min of rear 3000 turns/min, get supernatant, concentrated, cross D-101 macroporous resin column, the water elution removal of impurity, merge collection 60% ethanol elution, concentrated, vacuum lyophilization obtains Pinus koraiensis skin polyphenol powder;
(3) certain mass quintessence oil is taken according to following mass percentage: Pinus koraiensis quintessence oil 0.2-0.3, clove oil 0.05-0.1, Ledum Palustre L.var.dilatatum Wahl. quintessence oil 0.05-0.1, rosemary ethereal oil 0.05-0.1, tea tree ethereal oil 0.1-0.2, Herba Lysimachiae foenum-graeci quintessence oil 0.1-0.2, mix homogeneously, should be noted when quintessence oil is volatile substances weighing and reduces the loss as far as possible and improve its accuracy (quintessence oil must store under lucifuge condition);
(4) take castor oil hydrogenated mass percentage 2.8-5.0, added in mixed quintessence oil, fully stir and form in stable condition A phase;
(5) take by the obtained Pinus koraiensis skin polyphenol powder 0.05-0.1 of method in (2) by mass percentage, add in purified water 92.4-95.8, ultrasonic dissolution assisting 5min-10min after magnetic stirrer, to be mixed uniform and stable after, add glycerol 0.5-1.0, propylene glycol 0.3-0.5 again, abundant stirring, with filter paper filtering after each material dissolves completely, obtaining filtrate is B phase;
(6) A phase is slowly added in B phase, add while stirring, stir more than 10min until product stable homogeneous, then through standing, canned (the professional brown lucifuge vial cooperation ultra micro atomisation pump head of packaging employing, packaging material need through professional cleaning sterilizing-drying), said process need operate under clean environment, and canned good product adds outer package and plastic packaging, make a kind of water-soluble quality, there is many effects composite plant quintessence oil spraying of natural plant incense atmosphere.
advantage of the present invention
1, be made up of various plants quintessence oil compounds such as Pinus koraiensis quintessence oils, have multi-efficiency, wherein pinecone of Pinus Koraiensis quintessence oil belongs to new resources exploitation;
2, dispersant is utilized plants essential oil to be made water solublity spraying, easy to use, applied range, family, office, open air all can use at any time, and effect is remarkable;
3, extract and add Pinus koraiensis skin polyphenol, there is the effect of radioprotective, oxidation, natural anticorrosion;
4, the present invention utilizes the antibacterial action of Pinus koraiensis quintessence oil etc. itself, in conjunction with the effect of Pinus koraiensis polyphenol Antimicrobial preservative, does not add antiseptic, safe green;
5, utilize the natural breath of quintessence oil, this product does not add essence.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment one
(1) pinecone of Pinus Koraiensis, Flos Caryophylli petal, Ledum Palustre L.var.dilatatum Wahl. blade, Herba Rosmarini Officinalis blade, tea leaf, each 5kg of lavandula angustifolia flower is got, put into vapor distillation extraction element (adding water proof baffle plate) respectively, purified water 20L is added in steam generator, power 3000W water proof distillation 2h, collect distillate, standing separation oil reservoir (upper strata) in oil water separator, obtains faint yellow to yellow, the pure plants essential oil of clear;
(2) get Pinus koraiensis bark 500g, air dry oven dry, pulverize, 60% ethanol 5L is prepared, under 60 DEG C of conditions, in ultrasonic unit with purified water and dehydrated alcohol, ultrasonic power 300w extracts 0.8h, extracts the centrifugal 10min of rear 3000 turns/min, gets supernatant, Rotary Evaporators concentrates, cross D-101 macroporous resin column, the water elution removal of impurity discards eluent, afterwards 60% ethanol elution collect eluent, Rotary Evaporators concentrates, and vacuum lyophilization obtains Pinus koraiensis skin polyphenol powder;
(3) take: Pinus koraiensis quintessence oil 10g, clove oil 2.5g, Ledum Palustre L.var.dilatatum Wahl. quintessence oil 2.5g, rosemary ethereal oil 2.5g, tea tree ethereal oil 5g, Herba Lysimachiae foenum-graeci quintessence oil 10g, mix homogeneously, should be noted when quintessence oil is volatile substances weighing and reduces the loss as far as possible and improve its accuracy (quintessence oil must store under lucifuge, air-proof condition);
(4) take castor oil hydrogenated 140g, added in mixed quintessence oil, fully stir and form in stable condition A phase;
(5) take by the obtained Pinus koraiensis skin polyphenol powder 5g of method in (2), add in purified water 4.77kg, ultrasonic dissolution assisting 5min after magnetic stirrer, to be mixed uniform and stable after, add glycerol 25g, propylene glycol 25g again, abundant stirring, with filter paper filtering after each material dissolves completely, obtaining filtrate is B phase;
(6) A phase is slowly added in B phase, add while stirring, stir 20min, product stable homogeneous, then after standing observation is stable, make a kind of water-soluble quality, there is many effects composite plant quintessence oil spraying of natural plant incense atmosphere.Said process need operate under clean environment, and packaging adopts professional brown lucifuge vial to coordinate ultra micro atomisation pump head, and packaging material need through professional cleaning sterilizing-drying.
embodiment two:
(1) pinecone of Pinus Koraiensis, Flos Caryophylli petal, Ledum Palustre L.var.dilatatum Wahl. blade, Herba Rosmarini Officinalis blade, tea leaf, each 3kg of lavandula angustifolia flower is got, put into vapor distillation extraction element (adding water proof baffle plate) respectively, purified water 15L is added in steam generator, power 3000W water proof distillation 1.5h, collect distillate, standing separation oil reservoir (upper strata) in oil water separator, obtains faint yellow to yellow, the pure plants essential oil of clear;
(2) get Pinus koraiensis bark 1kg, air dry oven dry, pulverize, 60% ethanol 12L is prepared, under 60 DEG C of conditions, in ultrasonic unit with purified water and dehydrated alcohol, ultrasonic power 300w extracts 1.0h, extracts the centrifugal 5min of rear 3000 turns/min, gets supernatant, Rotary Evaporators concentrates, cross D-101 macroporous resin column, the water elution removal of impurity discards eluent, afterwards 60% ethanol elution collect eluent, Rotary Evaporators concentrates, and vacuum lyophilization obtains Pinus koraiensis skin polyphenol powder;
(3) take: Pinus koraiensis quintessence oil 15g, clove oil 5g, Ledum Palustre L.var.dilatatum Wahl. quintessence oil 5g, rosemary ethereal oil 5g, tea tree ethereal oil 10g, Herba Lysimachiae foenum-graeci quintessence oil 10g, mix homogeneously, should be noted when quintessence oil is volatile substances weighing and reduces the loss as far as possible and improve its accuracy (quintessence oil must store under lucifuge, air-proof condition);
(4) take castor oil hydrogenated 250g, added in mixed quintessence oil, fully stir and form in stable condition A phase;
(5) take by the obtained Pinus koraiensis skin polyphenol powder 5g of method in (2), add in purified water 4.62kg, ultrasonic dissolution assisting 10min after magnetic stirrer, to be mixed uniform and stable after, add glycerol 50g, propylene glycol 25g again, abundant stirring, with filter paper filtering after each material dissolves completely, obtaining filtrate is B phase;
(6) A phase is slowly added in B phase, add while stirring, stir 30min, product stable homogeneous, then after standing observation is stable, make a kind of water-soluble quality, there is many effects composite plant quintessence oil spraying of natural plant incense atmosphere.Said process need operate under clean environment, and packaging adopts professional brown lucifuge vial to coordinate ultra micro atomisation pump head, and packaging material need through professional cleaning sterilizing-drying.
Claims (2)
1. the plants essential oil of effect Water Soluble Compound more than kind spraying, by Pinus koraiensis quintessence oil, clove oil, Ledum Palustre L.var.dilatatum Wahl. quintessence oil, rosemary ethereal oil, tea tree ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil, Pinus koraiensis skin polyphenol, castor oil hydrogenated, glycerol, propylene glycol, purified water forms, the raw material that its feature comprises content described in it calculates with the percentage composition of each component: Pinus koraiensis quintessence oil 0.2-0.3, clove oil 0.05-0.1, Ledum Palustre L.var.dilatatum Wahl. quintessence oil 0.05-0.1, rosemary ethereal oil 0.05-0.1, tea tree ethereal oil 0.1-0.2, Herba Lysimachiae foenum-graeci quintessence oil 0.1-0.2, Pinus koraiensis skin polyphenol 0.05-0.1, castor oil hydrogenated 2.8-5.0, glycerol 0.5-1.0, propylene glycol 0.3-0.5, purified water 92.4-95.8.
2. a concrete preparation method for the Water Soluble Compound of effect more than plants essential oil spraying, its feature comprises the steps:
(1) according to extract part needed for each plants essential oil, the Strobilus Pini, petal, blade, flower etc., collect appropriate plant material, utilize vapor distillation extraction element, and technique is water proof distillation, obtains faint yellow to yellow, the pure plants essential oil of clear;
(2) get Pinus koraiensis bark, dry, pulverize, prepare 60% ethanol as Extraction solvent by purified water, Extraction solvent and Pinus koraiensis bark volume are than being 10:1-12:1, and solvent need not have Pinus koraiensis bark, under 60 DEG C of conditions, supersound extraction 0.5-1.0h, centrifuging and taking supernatant, concentrated, cross D-101 macroporous resin column, the water elution removal of impurity, collect 60% ethanol elution, concentrated, vacuum lyophilization obtains Pinus koraiensis skin polyphenol powder;
(3) the Pinus koraiensis quintessence oil of certain mass is taken by formula proportion, clove oil, Ledum Palustre L.var.dilatatum Wahl. quintessence oil, rosemary ethereal oil, tea tree ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil, mix homogeneously, should be noted when quintessence oil is volatile substances weighing and reduces the loss as far as possible and improve its accuracy (lucifuge, sealed storage);
(4) take the castor oil hydrogenated of certain mass by formula proportion, added in mixed quintessence oil, fully stir and form in stable condition A phase;
(5) take Pinus koraiensis skin polyphenol obtained in (2) by formula proportion and add mixing in purified water and ultrasonic dissolution assisting, then add glycerol, propylene glycol, fully stir, with filter paper filtering after each material dissolves completely, obtaining micro-terra-cotta filtrate is B phase;
(6) A phase is slowly added in B phase, add while stirring, stir more than 10min until product stable homogeneous, then through standing, canned (the professional brown lucifuge vial cooperation ultra micro atomisation pump head of packaging employing, packaging material need through professional cleaning sterilizing-drying), said process need operate under clean environment, and canned good product adds outer package and plastic packaging, make a kind of water-soluble quality, there is many effects composite plant quintessence oil spraying of natural plant incense atmosphere.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107232187A (en) * | 2017-06-23 | 2017-10-10 | 骆琦 | Careless plant mosquito-repellent spray liquid of one kind hundred and preparation method thereof |
| WO2019171390A1 (en) * | 2018-03-04 | 2019-09-12 | Surjyoti Sujalchandra Bagchi | A composition useful as a pest-controlling agent for agricultural and horticultural crops |
| CN110616114A (en) * | 2018-06-20 | 2019-12-27 | 湖北中烟工业有限责任公司 | Water-soluble coconut essence for reconstituted tobacco and preparation method thereof |
| CN111700848A (en) * | 2020-07-27 | 2020-09-25 | 广东一芙化妆品有限公司 | Plant bacteriostatic spray and preparation method thereof |
| CN114059379A (en) * | 2020-08-07 | 2022-02-18 | 山东德泰纸业有限公司 | Mixed-fragrance household paper and production process thereof |
| CN114533928A (en) * | 2021-12-30 | 2022-05-27 | 上海芬尚生物科技有限公司 | Formula of oily essence dissolved in water-based fragrance product and preparation method thereof |
| CN115054625A (en) * | 2022-05-23 | 2022-09-16 | 齐齐哈尔大学 | Itching relieving repair lotion and preparation method and application thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107232187A (en) * | 2017-06-23 | 2017-10-10 | 骆琦 | Careless plant mosquito-repellent spray liquid of one kind hundred and preparation method thereof |
| WO2019171390A1 (en) * | 2018-03-04 | 2019-09-12 | Surjyoti Sujalchandra Bagchi | A composition useful as a pest-controlling agent for agricultural and horticultural crops |
| CN110616114A (en) * | 2018-06-20 | 2019-12-27 | 湖北中烟工业有限责任公司 | Water-soluble coconut essence for reconstituted tobacco and preparation method thereof |
| CN111700848A (en) * | 2020-07-27 | 2020-09-25 | 广东一芙化妆品有限公司 | Plant bacteriostatic spray and preparation method thereof |
| CN114059379A (en) * | 2020-08-07 | 2022-02-18 | 山东德泰纸业有限公司 | Mixed-fragrance household paper and production process thereof |
| CN114533928A (en) * | 2021-12-30 | 2022-05-27 | 上海芬尚生物科技有限公司 | Formula of oily essence dissolved in water-based fragrance product and preparation method thereof |
| CN115054625A (en) * | 2022-05-23 | 2022-09-16 | 齐齐哈尔大学 | Itching relieving repair lotion and preparation method and application thereof |
| CN115054625B (en) * | 2022-05-23 | 2023-11-21 | 齐齐哈尔大学 | Itching relieving repair lotion and preparation method and application thereof |
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