CN110037220A - The production method of intelligence Qi particle - Google Patents
The production method of intelligence Qi particle Download PDFInfo
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- CN110037220A CN110037220A CN201910433528.0A CN201910433528A CN110037220A CN 110037220 A CN110037220 A CN 110037220A CN 201910433528 A CN201910433528 A CN 201910433528A CN 110037220 A CN110037220 A CN 110037220A
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- Prior art keywords
- particle
- intelligence
- production method
- concentrate
- supernatant
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- 239000002245 particle Substances 0.000 title claims abstract description 52
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 33
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims abstract description 31
- 230000008569 process Effects 0.000 claims abstract description 30
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 27
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000006228 supernatant Substances 0.000 claims abstract description 22
- 239000012141 concentrate Substances 0.000 claims abstract description 19
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 17
- 229960003080 taurine Drugs 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000005507 spraying Methods 0.000 claims abstract description 13
- 239000000341 volatile oil Substances 0.000 claims abstract description 13
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 11
- 229930006000 Sucrose Natural products 0.000 claims abstract description 11
- 239000004310 lactic acid Substances 0.000 claims abstract description 11
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 11
- 239000005720 sucrose Substances 0.000 claims abstract description 11
- 229920002472 Starch Polymers 0.000 claims abstract description 10
- 238000004821 distillation Methods 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 10
- 235000019698 starch Nutrition 0.000 claims abstract description 10
- 239000008107 starch Substances 0.000 claims abstract description 10
- 235000020985 whole grains Nutrition 0.000 claims abstract description 10
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims abstract description 9
- 229940013618 stevioside Drugs 0.000 claims abstract description 9
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000019202 steviosides Nutrition 0.000 claims abstract description 9
- 235000015165 citric acid Nutrition 0.000 claims abstract description 8
- 230000000694 effects Effects 0.000 claims abstract description 8
- 239000000047 product Substances 0.000 claims abstract description 8
- 238000001694 spray drying Methods 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 6
- 239000012528 membrane Substances 0.000 claims description 14
- 239000003814 drug Substances 0.000 claims description 9
- 238000005469 granulation Methods 0.000 claims description 9
- 230000003179 granulation Effects 0.000 claims description 9
- 238000004806 packaging method and process Methods 0.000 claims description 9
- 238000007789 sealing Methods 0.000 claims description 9
- 239000007921 spray Substances 0.000 claims description 9
- 238000012856 packing Methods 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 4
- 239000008187 granular material Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000012360 testing method Methods 0.000 claims description 3
- 239000002244 precipitate Substances 0.000 claims description 2
- 230000000717 retained effect Effects 0.000 claims description 2
- 238000004321 preservation Methods 0.000 abstract description 3
- 235000020636 oyster Nutrition 0.000 description 5
- 241000237502 Ostreidae Species 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000011068 loading method Methods 0.000 description 3
- LEVWYRKDKASIDU-QWWZWVQMSA-N D-cystine Chemical compound OC(=O)[C@H](N)CSSC[C@@H](N)C(O)=O LEVWYRKDKASIDU-QWWZWVQMSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 229960003067 cystine Drugs 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 210000003734 kidney Anatomy 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000018102 proteins Nutrition 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 208000004998 Abdominal Pain Diseases 0.000 description 1
- 206010004542 Bezoar Diseases 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 208000008967 Enuresis Diseases 0.000 description 1
- STECJAGHUSJQJN-GAUPFVANSA-N Hyoscine Natural products C1([C@H](CO)C(=O)OC2C[C@@H]3N([C@H](C2)[C@@H]2[C@H]3O2)C)=CC=CC=C1 STECJAGHUSJQJN-GAUPFVANSA-N 0.000 description 1
- 235000002710 Ilex cornuta Nutrition 0.000 description 1
- 241001310146 Ilex cornuta Species 0.000 description 1
- 244000241838 Lycium barbarum Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000237852 Mollusca Species 0.000 description 1
- STECJAGHUSJQJN-UHFFFAOYSA-N N-Methyl-scopolamin Natural products C1C(C2C3O2)N(C)C3CC1OC(=O)C(CO)C1=CC=CC=C1 STECJAGHUSJQJN-UHFFFAOYSA-N 0.000 description 1
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 description 1
- 241000208292 Solanaceae Species 0.000 description 1
- 244000228451 Stevia rebaudiana Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000004596 appetite loss Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 235000018417 cysteine Nutrition 0.000 description 1
- XUJNEKJLAYXESH-UHFFFAOYSA-N cysteine Natural products SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 description 1
- -1 cysteine sulfurous acid carboxylic acid Chemical class 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000004345 fruit ripening Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 235000021266 loss of appetite Nutrition 0.000 description 1
- 208000019017 loss of appetite Diseases 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000027939 micturition Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000001243 protein synthesis Methods 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 235000019600 saltiness Nutrition 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 235000015067 sauces Nutrition 0.000 description 1
- STECJAGHUSJQJN-FWXGHANASA-N scopolamine Chemical compound C1([C@@H](CO)C(=O)O[C@H]2C[C@@H]3N([C@H](C2)[C@@H]2[C@H]3O2)C)=CC=CC=C1 STECJAGHUSJQJN-FWXGHANASA-N 0.000 description 1
- 229960002646 scopolamine Drugs 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 230000014616 translation Effects 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
- A23L33/175—Amino acids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Molecular Biology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Botany (AREA)
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of production methods of intelligence Qi particle, comprising: processes fructus alpiniae oxyphyllae, fructus lycii and calcined oyster shell for net medicinal material；Fructus alpiniae oxyphyllae plus water are distilled and collect volatile oil；Filtering is after the dregs of a decoction after distillation are decocted with fructus lycii to retain supernatant, and supernatant is concentrated to the concentrate for being 1.08~1.12 for relative density；Calcined oyster shell, sucrose and taurine, soluble starch, citric acid, stevioside are crushed respectively, are sieved, as supplementary material；Supplementary material and lactic acid are added after concentrate is heated, particle is made using spray drying；Particle after whole grain carries out spraying into volatile oil, and closed mixing preset time in polynary movement mixed process.According to the technical solution of the present invention, the effect of can efficiently playing each component and particle is made in order to the preservation of product and reconstitutes.
Description
Technical field
The present invention relates to plant beverage technical field more particularly to a kind of production methods of intelligence Qi particle.
Background technique
Fructus lycii is the ripening fruits of matrimony vine of solanaceae plant, and when summer, autumn fruit maturation picks, and removes carpopodium, sets shady place
It dries in the air to pericarp after corrugating, then is exposed to the sun to crust is stiff, pulp is soft to obtain the final product, meeting wet weather can be dried with small fire, have a variety of guarantors
Strong effect, is the dual-purpose of drug and food food of Ministry of Public Health's approval, and proper amount of edible is good for health.Intelligence development has special fragrance, acrid flavour, slight bitter,
Fruit hyoscine, there is an Energy benefit taste, manages vigour, the function of the sliding drip of kidney tonifying void, control diarrhea caused by taste (or kidney) cold of insufficiency type, abdominal pain,
The diseases such as vomiting, loss of appetite, salivary secretion increase, the enuresis, frequent urination.Oyster software has shell, the animal of micropredation, the degree of saltiness
Water boundary produces especially fertile, is mollusk, there are two shell, one small and flat, another is swelled greatly, and the surface of shell is recessed
Convex injustice, meat is edible, and can obtain through refining oyster sauce, and meat, shell, oil can all be used as medicine, and also cries oyster or oyster.Taurine (Taurine)
Also known as β-aminoethanesulfonic acid earliest by separating in cow-bezoar, therefore is gained the name, and sterling is colourless or white ramp-like crystal, odorless, ox
Sulfonic acid chemical property is stablized, and is a kind of non-protein amino acid of sulfur-bearing insoluble in organic solvents such as ether, in vivo with the shape that dissociates
State exists, and is not involved in the biosynthesis of vivo protein.Although taurine is not involved in protein synthesis, but it and cystine, half
The metabolism of cystine is closely related, and the cysteine sulfurous acid carboxylic acid (CSAD) of human body synthesizing taurine activity is lower, mainly according to
Meet body needs by absorbing the taurine in food.
On existing market, it can rush not comprising the above-mentioned plant beverage to the specific health-care efficacy substance of human body or indirectly
The drink of tune, to realize the healthcare function to body during daily drinking.
Summary of the invention
Aiming at the shortcomings existing in the above problems, the present invention provides a kind of production method of intelligence Qi particle, pass through
Processing respectively to fructus alpiniae oxyphyllae, fructus lycii and calcined oyster shell, the effect of can efficiently playing each component and in supplementary material and lactic acid
Under the action of particle is made using spray dried form, convenient for product preservation and reconstitute.
To achieve the above object, the present invention provides a kind of production methods of intelligence Qi particle, comprising: by fructus alpiniae oxyphyllae, fructus lycii
It is net medicinal material that son and calcined oyster shell, which process,；The fructus alpiniae oxyphyllae is added water to distill and collects volatile oil；By after distillation the dregs of a decoction with it is described
Filtering is after fructus lycii decocts to retain supernatant, and the supernatant is concentrated to the concentration for being 1.08~1.12 for relative density
Liquid；The calcined oyster shell, sucrose and taurine, soluble starch, citric acid, stevioside are crushed respectively, are sieved, as former auxiliary
Material；The supplementary material and lactic acid will be added after concentrate heating, particle is made using spray drying；Particle after whole grain
It carries out spraying into the volatile oil in polynary movement mixed process, and closed mixing preset time.
In the above-mentioned technical solutions, it is preferable that the fructus alpiniae oxyphyllae is added 2 times of amount water and is distilled.
In the above-mentioned technical solutions, it is preferable that filtering is after the dregs of a decoction by after distillation are decocted with the fructus lycii to stay
Deposit supernatant detailed process are as follows: add water to cook the dregs of a decoction after distillation three times with the fructus lycii, every time plus the water of 8 times of amounts decoct
1.5 hour；It is filtered after the completion of decocting, filtrate is centrifuged to remove and precipitates and retains supernatant.
In the above-mentioned technical solutions, it is preferable that the described supernatant is concentrated as relative density is 1.08~1.12
Concentrate detailed process are as follows: the vacuum degree of two effect inspissator of control is -0.070Mpa~-0.080Mpa, steam pressure 0.05-
0.15Mpa, thickening temperature are 70-80 DEG C and the supernatant are concentrated that the relative density for obtaining 60 DEG C is 1.08~1.12
Concentrate.
In the above-mentioned technical solutions, it is preferable that described by the calcined oyster shell, sucrose and taurine, soluble starch, Chinese holly
The detailed process that rafter acid, stevioside are crushed respectively, are sieved are as follows: take calcined oyster shell, crushed between dressing sieve, cross 60 meshes, be packed into
In plastic barrel with clean inner membrane bag, materiel designation card is hung up, warehousing after passing please be test；It takes sucrose to crush between dressing sieve, crosses 60
Mesh is fitted into the plastic barrel with clean inner membrane bag, hangs up material mark card, spare；Take taurine, soluble starch, citric acid,
Stevioside crosses 60 meshes respectively, is fitted into the clean bucket with clean inner membrane bag, sealing hangs up materiel designation card, spare.
In the above-mentioned technical solutions, it is preferable that the supplementary material is added after the heating by the concentrate and lactic acid is adopted
Particle detailed process is made with spray drying are as follows: the concentrate is placed in spraying granulation material-compound tank, and it is heated to 80~
90 DEG C, the supplementary material and lactic acid is added；Particle is made in the drying of above-mentioned medicine liquid spray with preset spraying granulation parameter, and is sieved
Powder goes out fine powder and coarse granule；Particle will be sifted out to be fitted into the plastic barrel with clean inner membrane bag, retained spare.
In the above-mentioned technical solutions, it is preferable that the particle after whole grain spray into polynary movement mixed process
The detailed process of the volatile oil and closed mixing preset time are as follows: the particle after whole grain is placed in polynary movement mixer,
Uniformly spray into the volatile oil；Mixing 15 minutes, and released after closed 30 minutes, it is fitted into the plastic barrel with clean inner membrane bag,
It retains spare.
In the above-mentioned technical solutions, it is preferable that the production method of intelligence Qi particle further include: utilize the particle after total mix certainly
Dynamic particles packing machine is packed；Leakproofness after packaging is checked, sealing qualified products carry out outer packing.
In the above-mentioned technical solutions, it is preferable that the spraying granulation of supplementary material described in production process, the supernatant it is dense
Compression process is in the interior progress of clean area of 18~26 DEG C, 45~65%RH.
Compared with prior art, the invention has the benefit that passing through the place respectively to fructus alpiniae oxyphyllae, fructus lycii and calcined oyster shell
Reason, the effect of can efficiently playing each component and is made under the action of supplementary material and lactic acid using spray dried form
Grain, convenient for product preservation and reconstitute.
Detailed description of the invention
Fig. 1 is the flow diagram of the production method of intelligence Qi particle disclosed in an embodiment of the present invention.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention
In attached drawing, technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is
A part of the embodiments of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, ordinary skill people
Member's every other embodiment obtained without making creative work, shall fall within the protection scope of the present invention.
The present invention is described in further detail with reference to the accompanying drawing:
As shown in Figure 1, a kind of production method of the intelligence Qi particle provided according to the present invention, comprising: by fructus alpiniae oxyphyllae, fructus lycii
Process with calcined oyster shell is net medicinal material；Fructus alpiniae oxyphyllae plus water are distilled and collect volatile oil；The dregs of a decoction after distillation are decocted with fructus lycii
After filter to retain supernatant, and supernatant is concentrated to the concentrate for being 1.08~1.12 for relative density；By calcined oyster shell, sucrose
And taurine, soluble starch, citric acid, stevioside crush respectively, are sieved, as supplementary material；Add after concentrate is heated
Enter supplementary material and lactic acid, particle is made using spray drying；Particle after whole grain spray into polynary movement mixed process
Volatile oil, and closed mixing preset time.
In this embodiment, to the arrangement of crude drug and concocting process are as follows: fructus alpiniae oxyphyllae is gone out decontamination and shell, the used time smashes
It is broken, it also can purchase medicine materical crude slice；By fructus lycii hot-air seasoning, carpopodium is removed, or is dried after drying in the air to rhicnosis, carpopodium, or purchase drink are removed
Piece；Net oyster is taken, crisp, an or purchase medicine materical crude slice is calcined to according to method of direct calcination.
It is distilled in the above embodiment, it is preferable that 2 times of amount water are added in fructus alpiniae oxyphyllae.
In the above embodiment, it is preferable that filtering is after the dregs of a decoction after distillation are decocted with fructus lycii to retain supernatant tool
Body process are as follows: add water to cook the dregs of a decoction after distillation three times with fructus lycii, every time plus the water of 8 times of amounts decoct 1.5 hours；It has decocted
At rear filtering, filtrate is centrifuged removal precipitating and retains supernatant.
In the above embodiment, it is preferable that it is specific that the concentrate for being 1.08~1.12 for relative density is concentrated in supernatant
Process are as follows: the vacuum degree of two effect inspissators of control is -0.070Mpa~-0.080Mpa, steam pressure 0.05-0.15Mpa, dense
Contracting temperature is 70-80 DEG C and supernatant is concentrated, and obtains 60 DEG C of relative density as 1.08~1.12 concentrate, juxtaposition is cold
Library saves.
In the above embodiment, it is preferable that by calcined oyster shell, sucrose and taurine, soluble starch, citric acid, stevia rebaudianum
The detailed process that sugar Fen Sui, not be sieved are as follows: take calcined oyster shell, crushed between dressing sieve, cross 60 meshes, be packed into the clean inner membrance of band
In the plastic barrel of bag, materiel designation card is hung up, warehousing after passing please be test；It takes sucrose to crush between dressing sieve, crosses 60 meshes, be packed into band
In the plastic barrel of clean inner membrane bag, material mark card is hung up, it is spare；Take taurine, soluble starch, citric acid, stevioside difference
60 meshes are crossed, are fitted into the clean bucket with clean inner membrane bag, sealing hangs up materiel designation card, spare.
It is made in the above embodiment, it is preferable that supplementary material and lactic acid are added after concentrate is heated of spray drying
Particle detailed process are as follows: concentrate is placed in spraying granulation material-compound tank, and is heated to 80~90 DEG C, supplementary material and cream is added
Acid；Particle is made in the drying of above-mentioned medicine liquid spray with preset spraying granulation parameter, and sieves powder and goes out fine powder and coarse granule；It will sift out
Particle is fitted into the plastic barrel with clean inner membrane bag, is hung up materiel designation card, is kept in.
In the above embodiment, it is preferable that the particle after whole grain carries out spraying into volatile oil in polynary movement mixed process
And the detailed process of closed mixing preset time are as follows: the particle after whole grain is placed in polynary movement mixer, uniformly sprays into and waves
Hair oil；Mixing 15 minutes, and released after closed 30 minutes, it is fitted into the plastic barrel with clean inner membrane bag, hangs up materiel designation card,
It is temporary.
In the above embodiment, it is preferable that the production method of intelligence Qi particle further include: by the particle after total mix using automatically
Particles packing machine is packed；Leakproofness after packaging is checked, sealing qualified products carry out outer packing.
Specifically, particle is packed between granule packaging with automatic granular packaging machine, according to instruction adjust lot number,
Date of manufacture, validity period are simultaneously checked by QA, 2 grams of every bag of packing specification, suitable separate-loading packaging are controlled, according to medicinal compound
Film situation adjusts horizontal sealing temperature at 110~130 DEG C, and longitudinal sealing temperature is at 110~130 DEG C.Booting is first debugged, and checks sealing situation,
Content uniformity controls within the scope of 1.90~2.10 grams, confirms through live QA, and can formally produce after checking leakproofness qualification,
During packing, control separate-loading packaging is no more than 350 bags/minute, and operator is primary every censored sample in 30 minutes, when sampling
Continuously take 10 bags of progress content uniformity inspections every time, every 60 minutes of QA takes a sample to check loading amount with method.The another device storage of substandard product,
It can be repacked after QA checks approval.Qualified product identifies after counting and is passed to outer parlor.With * 12 bags of 2g/ bag/middle bag * 1
Middle bag/150 boxes of box */part specification by pouch drug be fitted into seal after bag, be packed into external packing box.
In the above embodiment, it is preferable that the spraying granulation of supplementary material, the concentration process of supernatant are in production process
18~26 DEG C, carry out in the clean area of 45~65%RH.
These are only the preferred embodiment of the present invention, is not intended to restrict the invention, for those skilled in the art
For member, the invention may be variously modified and varied.All within the spirits and principles of the present invention, it is made it is any modification,
Equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (9)
1. a kind of production method of intelligence Qi particle characterized by comprising
Fructus alpiniae oxyphyllae, fructus lycii and calcined oyster shell are processed as net medicinal material；
The fructus alpiniae oxyphyllae is added water to distill and collects volatile oil；
Filtering is after the dregs of a decoction after distillation are decocted with the fructus lycii to retain supernatant, and it is opposite that the supernatant, which is concentrated,
The concentrate that density is 1.08~1.12；
The calcined oyster shell, sucrose and taurine, soluble starch, citric acid, stevioside are crushed respectively, are sieved, as original
Auxiliary material；
The supplementary material and lactic acid will be added after concentrate heating, particle is made using spray drying；
Particle after whole grain carries out spraying into the volatile oil, and closed mixing preset time in polynary movement mixed process.
2. the production method of intelligence Qi particle according to claim 1, which is characterized in that 2 times of amount water are added in the fructus alpiniae oxyphyllae
It is distilled.
3. the production method of intelligence Qi particle according to claim 1, which is characterized in that the dregs of a decoction and institute by after distillation
It states after fructus lycii decocts and filters to retain supernatant detailed process are as follows:
The dregs of a decoction after distillation are added water to cook three times with the fructus lycii, every time plus the water of 8 times of amounts decoct 1.5 hours；
It is filtered after the completion of decocting, filtrate is centrifuged to remove and precipitates and retains supernatant.
4. the production method of intelligence Qi particle according to claim 1, which is characterized in that described to be by supernatant concentration
The concentrate detailed process that relative density is 1.08~1.12 are as follows:
The vacuum degree of two effect inspissator of control is -0.070Mpa~-0.080Mpa, steam pressure 0.05-0.15Mpa, is concentrated
Temperature is 70-80 DEG C and the supernatant is concentrated, and obtains 60 DEG C of relative density as 1.08~1.12 concentrate.
5. the production method of intelligence Qi particle according to claim 1, which is characterized in that described by the calcined oyster shell, sucrose
And the detailed process that taurine, soluble starch, citric acid, stevioside are crushed respectively, are sieved are as follows:
Calcined oyster shell is taken, is crushed between dressing sieve, 60 meshes are crossed, is fitted into the plastic barrel with clean inner membrane bag, hangs up material mark
Show card, warehousing after passing please be test；
It takes sucrose to crush between dressing sieve, crosses 60 meshes, be fitted into the plastic barrel with clean inner membrane bag, hang up material mark card, it is spare；
It takes taurine, soluble starch, citric acid, stevioside to cross 60 meshes respectively, is fitted into the clean bucket with clean inner membrane bag,
Sealing, hangs up materiel designation card, spare.
6. the production method of intelligence Qi particle according to claim 1, which is characterized in that after the heating by the concentrate
The supplementary material and lactic acid is added, particle detailed process is made using spray drying are as follows:
The concentrate is placed in spraying granulation material-compound tank, and is heated to 80~90 DEG C, the supplementary material and lactic acid is added；
Particle is made in the drying of above-mentioned medicine liquid spray with preset spraying granulation parameter, and sieves powder and goes out fine powder and coarse granule；
Particle will be sifted out to be fitted into the plastic barrel with clean inner membrane bag, retained spare.
7. the production method of intelligence Qi particle according to claim 1, which is characterized in that the particle after whole grain carries out
The detailed process of the volatile oil and closed mixing preset time is sprayed into polynary movement mixed process are as follows:
Particle after whole grain is placed in polynary movement mixer, the volatile oil is uniformly sprayed into；
Mixing 15 minutes, and released after closed 30 minutes, it is fitted into the plastic barrel with clean inner membrane bag, retains spare.
8. the production method of intelligence Qi particle according to claim 1, which is characterized in that further include:
Particle after total mix is packed using automatic granular packaging machine；
Leakproofness after packaging is checked, sealing qualified products carry out outer packing.
9. the production method of intelligence Qi particle according to claim 1, which is characterized in that calcined oyster shell described in production process
Concocting process, the spraying granulation of the supplementary material, the dressing sieve process of the sucrose, the packaging of the total mix process of particle and particle
Journey is in the interior progress of clean area of 18~26 DEG C, 45~65%RH.
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| CN201910433528.0A CN110037220A (en) | 2019-05-23 | 2019-05-23 | The production method of intelligence Qi particle |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1156031A (en) * | 1995-12-04 | 1997-08-06 | 南京臣功制药有限公司 | Oral medicine for dropping blood lead and its preparing method |
| CN101623496A (en) * | 2009-07-27 | 2010-01-13 | 广西博科药业有限公司 | Preparation method of Fuyankan particles treating chronic pelvic inflammation |
| AU2014352441A1 (en) * | 2013-11-22 | 2016-06-16 | Li Fu | Use of ginsenoside-Rg3 in preparing medicine for preventing or/and treating dementia and medicine |
-
2019
- 2019-05-23 CN CN201910433528.0A patent/CN110037220A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1156031A (en) * | 1995-12-04 | 1997-08-06 | 南京臣功制药有限公司 | Oral medicine for dropping blood lead and its preparing method |
| CN101623496A (en) * | 2009-07-27 | 2010-01-13 | 广西博科药业有限公司 | Preparation method of Fuyankan particles treating chronic pelvic inflammation |
| AU2014352441A1 (en) * | 2013-11-22 | 2016-06-16 | Li Fu | Use of ginsenoside-Rg3 in preparing medicine for preventing or/and treating dementia and medicine |
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