CN110031486A - A kind of method of quick identification seawater and fresh water pearl powder - Google Patents
A kind of method of quick identification seawater and fresh water pearl powder Download PDFInfo
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- CN110031486A CN110031486A CN201910313398.7A CN201910313398A CN110031486A CN 110031486 A CN110031486 A CN 110031486A CN 201910313398 A CN201910313398 A CN 201910313398A CN 110031486 A CN110031486 A CN 110031486A
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- pearl powder
- fresh water
- seawater
- irradiation
- powder
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/02—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
Abstract
The invention discloses a kind of methods for quickly identifying seawater and fresh water pearl powder, its technical solution is: with the commercially available pearl powder sample of -60 radiated by gamma-ray of cobalt of doses, irradiated sample discoloration is fresh water pearl powder, and what irradiated sample did not change colour is sea water pearls powder.The beneficial effects of the present invention are: this method identifies, speed is fast, it is easy to operate to identify, it is low-cost to identify.
Description
Technical field
The present invention relates to a kind of methods for identifying seawater and fresh water pearl powder, and in particular to a kind of fast using nuclear radiation technology
The method that speed identifies seawater and fresh water pearl powder, belongs to radiation physics technical field.
Background technique
Pearl powder is exactly the good merchantable brand of skin maintenance and cosmetic benefits from ancient times, have calm the nerves arresting convulsion, improving eyesight disappear screen, solution taking poison and growing muscle due, moistening skin and eliminating spot
The effect of, the deep favor by people always.Pearl powder is divided into sea water pearls powder and fresh water pearl powder, and currently on the market, seawater is precious
Pearl powder is made by the nacre of the pteria martensii shell of seawater, and fresh water pearl powder is made by fresh water pipless pearl.Seawater and light
Water pearl powder is all white or canescence, it is difficult to the naked eye be distinguished.Because the raw material and seawater, the fresh water that produce pearl powder are precious
The price of the difference of pearl powder function, seawater and fresh water pearl powder has larger difference, and general sea water pearls powder is compared with fresh water pearl powder valence
The expensive 2 times or more of lattice.But market pearl powder product is more chaotic, and most of product does not indicate that the raw material of pearl powder is sea water pearls shell
Or fresh water pipless pearl, not necessarily true being labelled with, the serious infringement interests and rights of consumer.
Patent No. ZL200610155553.X national inventing patent and paper " pearl radiation coloring (not this letter one,
Huang Rongmin) ", " Pear Dyeing Techniques By Irradiation research (Zou Weimin) ", " Radiation-induced Colouring of pearl studies (Sha Renli) " report
Change the technology of fresh water pearl color using irradiation, which is that can convert tetravalence for bivalent manganese using high-energy ray
Manganese and the principle that color is presented change, deepen pearl color.In fresh water pearl divalent manganese content it is higher (mass fraction be greater than 100
×10-6), the radiation treatment through doses, wherein bivalent manganese is converted into tetravalent manganese, and color is substantially change, and seawater is precious
Extremely low (mass fraction is less than 100 × 10 for manganese element content in pearl layer-6), it is also difficult to reach the effect obviously changed colour even across irradiation
Fruit.
Fresh water pearl can be changed colour and the sea water pearls that cannot change colour using radiation treatment, can also equally make fresh water pearl powder
Change colour and sea water pearls powder cannot be made to change colour, but up to the present, there are no using irradiancebased method technology for identify seawater and
The report of fresh water pearl powder.
Summary of the invention
The purpose of the present invention is to provide a kind of the identification seawater and fresh water pearl powder simple and quick using irradiation technique
Method is used for operating unit and the selection of market surpervision department.
In order to reach the purpose of the present invention, the technical solution adopted by the present invention is that:
With the sample of the commercially available pearl powder of -60 radiated by gamma-ray of cobalt of doses, irradiated sample discoloration is fresh water
Pearl powder, what irradiated sample did not change colour is sea water pearls powder.
The irradiation dose of -60 gamma ray of cobalt must be greater than 10kGy.Irradiation dose pearl powder discoloration less than 10kGy is unknown
It is aobvious, identification effect is not achieved；When greater than 10kGy irradiation dose, the bigger discoloration of irradiation dose is more obvious.
The irradiation dose of above-mentioned -60 gamma ray of cobalt is 10kGy~13kGy.
The irradiation time of above-mentioned -60 gamma ray of cobalt is irradiation 6~12 hours.
Can observe its color change more clearly as degree, usual 0.5g or so can meet to be wanted the sample size of pearl powder
It asks.
The beneficial effects of the present invention are: 1. identifying quickly, accurate identification result can be obtained in 12 hours；2. method is simple
Single, sample is not required to special pre-treatment, and irradiation technique process is simple；3. low-cost, 200 yuan of left sides of per kilogram irradiated material charge
The right side identifies only 10 yuan or so of expense of each sample；4. irradiation technique is mature and there are irradiation processing in popularization and application, all parts of the country
Mechanism is available.
Detailed description of the invention
Fig. 1 is the fresh water pearl powder before and after radiation treatment；
Fig. 2 is the sea water pearls powder before and after radiation treatment.
1. predose is in canescence；2. being in grey black after irradiation；3. predose is in canescence；4. after irradiation, in greyish white
Color.
Specific embodiment
The present invention is described in further details below with reference to embodiment, these embodiments are merely to illustrate the present invention, and
It does not limit the scope of the invention.
Embodiment 1
A kind of method of quick identification seawater and fresh water pearl powder carries out as follows:
(1) the commercially available pearl powder sample of 0.5g or so is taken, loaded in white clear polybag；
(2) polybag equipped with pearl powder sample is sent into -60 gamma irradiation device of cobalt that loading of source amount is 1000k Curie
After irradiation 12 hours, irradiation dose is made to reach 10kGy；
(3) by pearl powder sample from taken out in polybag and from, the pearl powder of graying black is fresh water pearl powder, is not had
Discoloration is sea water pearls powder.
Embodiment 2
A kind of method of quick identification seawater and fresh water pearl powder carries out as follows:
(1) the commercially available pearl powder sample of 0.5g or so is taken, loaded in white clear polybag；
(2) polybag equipped with pearl powder sample is sent into -60 gamma irradiation device of cobalt that loading of source amount is 1500K Curie
After irradiation 8 hours, irradiation dose is made to reach 10kGy；
(3) by pearl powder sample from taken out in polybag and from, the pearl powder of graying black is fresh water pearl powder, is not had
Discoloration is sea water pearls powder.
Embodiment 3
A kind of method of quick identification seawater and fresh water pearl powder carries out as follows:
(1) the commercially available pearl powder sample of 0.5g or so is taken, loaded in white clear polybag；
(2) polybag equipped with pearl powder sample is sent into -60 gamma irradiation device of cobalt that loading of source amount is 2000k Curie
After irradiation 6 hours, irradiation dose is made to reach 10kGy；
(3) by pearl powder sample from taken out in polybag and from, the pearl powder of graying black is fresh water pearl powder, is not had
Discoloration is sea water pearls powder.
Embodiment 4
A kind of method of quick identification seawater and fresh water pearl powder carries out as follows:
(1) the commercially available pearl powder sample of 0.5g or so is taken, loaded in white clear polybag；
(2) polybag equipped with pearl powder sample is sent into -60 gamma irradiation device of cobalt that loading of source amount is 2000k Curie
After irradiation 8 hours, irradiation dose is made to reach 13kGy；
(3) by pearl powder sample from taken out in polybag and from, the pearl powder of graying black is fresh water pearl powder, is not had
Discoloration is sea water pearls powder.
Claims (4)
1. a kind of method for quickly identifying seawater and fresh water pearl powder, it is characterised in that: use the commercially available treasure of -60 radiated by gamma-ray of cobalt
The sample of pearl powder, irradiated sample discoloration is fresh water pearl powder, and what irradiated sample did not change colour is sea water pearls powder.
2. a kind of method for quickly identifying seawater and fresh water pearl powder according to claim 1, it is characterised in that: described
The irradiation dose of -60 gamma ray of cobalt is greater than 10kGy.
3. a kind of method for quickly identifying seawater and fresh water pearl powder according to claim 1, it is characterised in that: described
The irradiation dose of -60 gamma ray of cobalt is 10kGy~13kGy.
4. a kind of method for quickly identifying seawater and fresh water pearl powder according to claim 1, it is characterised in that: described
The irradiation time of -60 gamma ray of cobalt is irradiation 6~12 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910313398.7A CN110031486A (en) | 2019-04-18 | 2019-04-18 | A kind of method of quick identification seawater and fresh water pearl powder |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910313398.7A CN110031486A (en) | 2019-04-18 | 2019-04-18 | A kind of method of quick identification seawater and fresh water pearl powder |
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| CN110031486A true CN110031486A (en) | 2019-07-19 |
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| CN201910313398.7A Pending CN110031486A (en) | 2019-04-18 | 2019-04-18 | A kind of method of quick identification seawater and fresh water pearl powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110470681A (en) * | 2019-09-24 | 2019-11-19 | 海南海润珍珠股份有限公司 | A method of identifying seawater and the medicinal pearl of fresh water |
| CN111771784A (en) * | 2020-08-07 | 2020-10-16 | 广东荣辉珍珠养殖有限公司 | Method for producing blister pearl and regenerative cell bead by using pinctada martensii golden-lip pearl culturing shell |
| CN113693000A (en) * | 2021-09-23 | 2021-11-26 | 广东海洋大学 | Production method of steel gray pearls |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102323280A (en) * | 2011-05-11 | 2012-01-18 | 浙江长生鸟珍珠生物科技有限公司 | Quality detection methods of pearl powder and application thereof |
| CN108538423A (en) * | 2017-12-20 | 2018-09-14 | 南京喜悦科技股份有限公司 | A kind of irradiation devices using Co 60 radiated by gamma-ray |
| CN109444186A (en) * | 2018-12-25 | 2019-03-08 | 浙江大学 | A kind of pearl powder X-ray diffraction differential method |
-
2019
- 2019-04-18 CN CN201910313398.7A patent/CN110031486A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102323280A (en) * | 2011-05-11 | 2012-01-18 | 浙江长生鸟珍珠生物科技有限公司 | Quality detection methods of pearl powder and application thereof |
| CN108538423A (en) * | 2017-12-20 | 2018-09-14 | 南京喜悦科技股份有限公司 | A kind of irradiation devices using Co 60 radiated by gamma-ray |
| CN109444186A (en) * | 2018-12-25 | 2019-03-08 | 浙江大学 | A kind of pearl powder X-ray diffraction differential method |
Non-Patent Citations (3)
| Title |
|---|
| 李耿: "浙江诸暨淡水养殖珍珠的宝石学和优化处理研究", 《中国博士学位论文全文数据库 工程科技I辑》 * |
| 蒲月华 等: "差热分析方法在鉴别珍珠粉与珍珠层粉中的应用", 《广东科技》 * |
| 蒲月华 等: "珍珠粉与珍珠层粉微量元素的对比研究", 《食品研究与开发》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110470681A (en) * | 2019-09-24 | 2019-11-19 | 海南海润珍珠股份有限公司 | A method of identifying seawater and the medicinal pearl of fresh water |
| CN111771784A (en) * | 2020-08-07 | 2020-10-16 | 广东荣辉珍珠养殖有限公司 | Method for producing blister pearl and regenerative cell bead by using pinctada martensii golden-lip pearl culturing shell |
| CN113693000A (en) * | 2021-09-23 | 2021-11-26 | 广东海洋大学 | Production method of steel gray pearls |
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Application publication date: 20190719 |