CN110016572A - A kind of device of aluminium alloy melt in-line purification - Google Patents

A kind of device of aluminium alloy melt in-line purification Download PDF

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Publication number
CN110016572A
CN110016572A CN201910260409.XA CN201910260409A CN110016572A CN 110016572 A CN110016572 A CN 110016572A CN 201910260409 A CN201910260409 A CN 201910260409A CN 110016572 A CN110016572 A CN 110016572A
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CN
China
Prior art keywords
melt
clean room
aluminium alloy
gas
purification
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Pending
Application number
CN201910260409.XA
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Chinese (zh)
Inventor
范超
彭迪
张炯
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Guangxi University of Science and Technology
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Guangxi University of Science and Technology
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Priority to CN201910260409.XA priority Critical patent/CN110016572A/en
Publication of CN110016572A publication Critical patent/CN110016572A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00Obtaining aluminium
    • C22B21/06Obtaining aluminium refining
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00Obtaining aluminium
    • C22B21/06Obtaining aluminium refining
    • C22B21/066Treatment of circulating aluminium, e.g. by filtration
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/05Refining by treating with gases, e.g. gas flushing also refining by means of a material generating gas in situ
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/10General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals with refining or fluxing agents; Use of materials therefor, e.g. slagging or scorifying agents
    • C22B9/103Methods of introduction of solid or liquid refining or fluxing agents
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Abstract

The invention belongs to non-ferrous metal purified treatment fields, are related to a kind of device of aluminium alloy melt in-line purification.It includes: the screwfeed firm gas powder mixed organization being made of variable-frequency motor (1), hopper (2), screw rod (3), gas powder mixing chamber (14), crucible (8) is separated into clean room (15) and filter chamber (16) by partition (13), clean room is connected to filter chamber by runner, ceramic foam filter plate (12) are arranged in the top of setting biasing rotating injecting powder device (6) and bottom blowing device in clean room, filter chamber (16).The present invention is able to achieve aluminum melt on-line continuous composite refining, greatly improves alloy refining quality and purification efficiency, while solving the problems such as refining agent and melt contacts are insufficient, liquid level is unstable, purification blind area, not high, the replacement inconvenience of filter service life.

Description

A kind of device of aluminium alloy melt in-line purification
Technical field
The invention belongs to non-ferrous metallurgy fields, more particularly to a kind of device of aluminium alloy melt in-line purification.
Background technique
Cleaning molten is to ensure that the key technology of aluminum alloy materials metallurgical quality.Purifying aluminium alloy melt main purpose is Except the hydrogen content and oxide inclusion in melt, to improve the quality of aluminium alloy.The method of aluminium melt purifying mainly has: solvent Method, air blast, rotating and puffing argon method etc..Common addition refining agent purifies aluminum melt, although certain refining can be played the role of, Since refining agent is easily clumped together, in order to reach effect, the amount of addition can be very big.Therefore, also there is gas+solvent Method of refining.It is found through retrieval, a kind of " material-spraying device " participation number of patent application: 20092014473.8, gas and solvent are mixed It is emitted directly toward in melt after conjunction, solvent is distributed in the surface of bubble in the melt, realizes the effect of dual refining.But this side The bubble of method, formation is not tiny enough, and the dosage of solvent is also bigger.Shanghai Communications University develops " purifying aluminium alloy melt method " Referring to number of patent application: purification gas is blown into aluminium using the method for rotary blowing by 0510026593.X, the purification device top In melt, while purification gas is blown into melt by the bottom installation air brick of device.Shanghai College of Mechanical Engineering develops a kind of " apex angle Multiple blowing type aluminum melt degassing method and device " is referring to number of patent application: 0910044935.9, the purification device by purification gas from Rotating device is blown into aluminum melt, while purification gas is also blown into aluminum melt from the peripheral inlet port of purification device.These methods It is larger to purify building volume, to be rectangular, in refining process the melt of the periphery of clean room and corner areas cannot with it is sufficient amount of Bubble is in contact, and purification blind area occurs;It is more tiny in order to obtain and more in addition, these methods belong to center rotary blowing Good bubble distribution situation, generally requires to realize using high speed rotation.But with the raising of revolving speed, melt liquid level will appear whirlpool The protective film of whirlpool and vibration, melt liquid level is destroyed, and the slag and air on surface can enter in melt, increases the miscellaneous of melt Matter;Air reacts with melt, i.e. scaling loss melt, and generates more hydrogen and be mingled with.In actual production, in order to prevent The generation of liquid level swirl, is usually arranged baffle near rotor.But when melt refines, melt temperature is very high, rotary speed of rotator Quickly, melt is very strong to the erosion corrosion effect of baffle, and the environment of baffle work is very severe, and service life is not high, higher cost, And the material to fall off, which invades, will cause pollution in melt, the final quality for influencing melt.Suzhou Bo Neng stove scientific & technical corporation " a kind of turbulence structure of depassing unit " is developed referring to number of patent application: 201210414279.9, the device is in deaeration One piece of raised flow-disturbing block is respectively arranged in lining four sides, for eliminating liquid level swirl.This method increase the complexities of deaeration, together When also shed into melt without solving the problems, such as that flow-disturbing block is easily washed.In addition, after existing technology purified treatment, often Melt is passed through ceramic filter plate to be filtered, this mode is used to capture fine folder especially with aperture is smaller When miscellaneous filter plate, it is easy to gap and is mingled with blocking and shortens the filter plate service life.
Summary of the invention
It is an object of the invention to overcome above-mentioned the deficiencies in the prior art, providing one kind can continuously in-line purification aluminium melt Body significantly increases the activated interface of refining agent purification, sphere of action, extends action time, and it is blind to eliminate purification for liquid level stabilizing Area is conveniently replaceable, the device of the aluminium melt purifying of high service life filter.
The present invention is achieved in the following ways:
A kind of device of aluminium alloy melt in-line purification, feature include by variable-frequency motor, hopper, screw rod, the mixing of gas powder The screwfeed firm gas powder mixed organization of room composition, crucible are separated into clean room and filter chamber, clean room and filtering by partition Room is connected to by runner, and setting biasing rotating injecting powder device and bottom blowing device in clean room, pottery is arranged in the top of filter chamber Porcelain foamed filter plate.Bottom blowing device is made of air brick and inflatable mouth.Melt inlet is located above clean room, and melt is from upper Flow through clean room under and, melt outlet is located above filter chamber, and purified melt passes through after filter plate from bottom to top from melt Outlet outflow.Inert gas gas powder mixing chamber and refining agent form gas powder and circulate in biasing rotating injecting powder device after being sufficiently mixed Form full and uniform tiny uniformly distributed cleaning by solvent bubble.
The device of above-mentioned aluminium alloy melt in-line purification, feature screw speed are controlled by variable-frequency motor, can be realized essence Refine agent weight feed.
The device of above-mentioned aluminium alloy melt in-line purification, the content of refining agent is melt inlet melt in feature gas powder stream The 0.1~0.5% of flow.
The device of above-mentioned aluminium alloy melt in-line purification, the rotary head of characteristic offset rotating injecting powder device to clean room bottom Distance be 50~300mm, the distance at rotary head distortion clean room center is the 1/5~1/3 of clean room's base diameter.
The device of above-mentioned aluminium alloy melt in-line purification, feature air brick geomery is consistent with clean room, hole Diameter is 10~100 μm.
The device of above-mentioned aluminium alloy melt in-line purification, characteristic filter plate are foamed ceramic filter plate, specification 40 ~50ppi.
The present invention in use, dry refining agent is put into hopper, give screw rod reasonable revolving speed, make refining agent by variable-frequency motor Feeding flow be melt flow 0.1~0.5% and inert gas after gas powder mixing chamber is sufficiently mixed, be blown into rotation spray It in powder device, is sheared by high-speed rotating blade, purification bubble surface of the meeting Dispersed precipitate in fine uniform.This surface dispersion The purification bubble of distribution solvent slowly rises in clean room, is sufficiently mixed, collides with the melt of downlink, the hydrogen diffusion in melt Nonmetal inclusion collision into the bubble of rising, while in the bubble and melt risen is adsorbed and carries them and floats.More The refining agent for dissipating distribution increases concentration gradient that hydrogen is spread into bubble and to field trash wetability, thus be easier to inhale hydrogen and Dross inclusion adsorption, melt are also also stirred, thus significantly increase refining agent and purify the activated interface of bubble, sphere of action, Time of contact is extended, while stirring also promotes the tiny aggregation being mingled with, is more advantageous to flotation removal.Agitating mode is biased, Slipstream, pressure field and the velocity field of peritrochanteric melt are in mal-distribution, it is not easy to centripetal acceleration and centrifugal force are generated, Liquid level is not in whirlpool when thus refining, and not increase baffle also can make liquid level steady.Purification gas is blown into and purifies simultaneously Bottom shape size consistent bottom air brick in room is capable of forming the bubble that a large amount of diameters are 5mm and is full of clean room, disappears completely Except purification dead angle.Behind clean room, large-sized nonmetal inclusion is efficiently removed melt, is then steeped by 40~50ppi After foam ceramic filter plate, 10 μm or more of nonmetal inclusion is completely removed, and obtains pure very high aluminium alloy melt, complete The full up industrial requirement of foot;Melt passes through filter plate from bottom to top, and impurity particle is blocked in filter lower end, when them Reunite to certain size, can be mentioned significantly from the filter sedimentation that falls off to realize self purifying for filter due to self weight The high service life of filter.
Detailed description of the invention
Fig. 1 is structural schematic diagram of the invention.
In figure, 1 is variable-frequency motor, and 2 be hopper, and 3 be screw rod, and 4 be inert gas, and 5 be gas powder stream, and 6 be biasing rotation spray Powder device, 7 be melt inlet, and 8 be crucible, and 9 be air brick, and 10 be purification gas, and 11 be melt outlet, and 12 be filter plate, 13 It is gas powder mixing chamber for partition, 14,15 be clean room, and 16 be filter chamber.
Specific embodiment
Aluminum melt flows into clean room 15 from melt inlet 7 with 400kg/h flow from top to bottom, and aluminum melt temperature is 750 DEG C; 15 base diameter of clean room is 400mm, liquid level 350mm;Dry refining agent is put into hopper 2, adjusts variable-frequency motor 1 The revolving speed for controlling screw rod 3 makes to refine agent flux 0.6kg/h, is 99.9% technical argon with air inflow 160ml/ by purity Min, gas pressure are that 0.1MPa is blown into gas powder mixing chamber 14, form gas powder stream 5 after being sufficiently mixed and are passed through biasing rotating injecting powder dress Set 6;Biasing 6 root diameter of rotating injecting powder device is 40mm, away from clean room bottom 60mm, in rotary head distortion clean room 15 The distance of the heart is 100mm, rotary speed of rotator 600rpm, the shear action of rotor, formation slowly rising Dispersed precipitate refining The minute bubbles of the fine uniform of agent collide with reverse melt, carry out degasification removal of impurities;Bottom air brick 9 is blown into gas and adopts It is 99.9% technical argon with purity, gas flow 0.18m3/h, gas pressure position 0.1MPa, 9 aperture of air brick is 20 μ M, diameter 400mm, it is the uniform of 5mm effect that diameter can be generated in clean room 15, completely eliminates the purification of purification blind area Bubble.The melt handled enters filter chamber 16, the foamed ceramic filter plate for being from bottom to top then 40ppi by specification 12, finally flowed out from melt outlet 11.In decontamination process, liquid level stabilizing absence of vortices, change efficiency and melt quality are mentioned Height, available hydrogen content 0.08ml/100g;10 μm or less non-metallic inclusions are lower than the aluminum melt of 0.02% high-quality.

Claims (6)

1. a kind of device of aluminium alloy melt in-line purification, feature includes by variable-frequency motor (1), hopper (2), screw rod (3), gas The screwfeed firm gas powder mixed organization of powder mixing chamber (14) composition, crucible (8) are separated into clean room (15) by partition (13) With filter chamber (16), clean room is connected to filter chamber by runner, setting biasing rotating injecting powder device (6) and bottom in clean room Ceramic foam filter plate (12) are arranged in the top of blowning installation, filter chamber (16).Bottom blowing device has air brick (9) and blows Mouth (10) composition.Melt inlet (7) is located above clean room (15), and melt flows through clean room (15), melt outlet from top to bottom (11) it is located above filter chamber (16), purified melt flows after passing through filter plate (12) from bottom to top from melt outlet (11) Out.Inert gas (4) is blown into after gas powder mixing chamber (14) is sufficiently mixed with refining agent and forms gas powder stream (5), then passes to biasing Full and uniform tiny uniformly distributed cleaning by solvent bubble is formed in rotating injecting powder device (6).
2. the device of aluminium alloy melt in-line purification according to claim 1, feature screw rod (3) revolving speed is by variable-frequency motor (1) it controls, can be realized refining agent weight feed.
3. the device of aluminium alloy melt in-line purification according to claim 1, the content of feature gas powder stream (5) refining agent It is the 0.1~0.5% of melt inlet (7) melt flow.
4. the device of aluminium alloy melt in-line purification according to claim 1, characteristic offset rotating injecting powder device (6) Rotary head to clean room's (15) distance from bottom is 50~300mm, and the distance at rotary head distortion clean room (15) center is purification The 1/5~1/3 of room bottom (15) diameter.
5. the device of aluminium alloy melt in-line purification according to claim 1, feature air brick (9) geomery and net It is consistent to change room (15) bottom, aperture is 10~100 μm.
6. the device of aluminium alloy melt in-line purification according to claim 1, characteristic filter plate (12) is foamed ceramics Filter plate, specification are 40~50ppi.
CN201910260409.XA 2019-03-19 2019-03-19 A kind of device of aluminium alloy melt in-line purification Pending CN110016572A (en)

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Application Number Priority Date Filing Date Title
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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110343917A (en) * 2019-08-20 2019-10-18 惠州市华顺祥实业有限公司 The technique and its equipment of interruption preparation liquid silumin or silumin semi solid slurry
CN110527861A (en) * 2019-10-16 2019-12-03 南通众福新材料科技有限公司 A kind of aluminium alloy molten aluminum purification system and technique
CN111020224A (en) * 2019-12-31 2020-04-17 徐州汉裕铝业有限公司 Degassing box for aluminum cast-rolling coil
CN111496242A (en) * 2020-05-09 2020-08-07 南通大学 Turbulent flow type aluminum alloy melt deslagging and filtering device and using method thereof
CN112349440A (en) * 2020-11-01 2021-02-09 百色学院 Liquid metal purification device and application method thereof
CN117587239A (en) * 2024-01-19 2024-02-23 北京航空航天大学 Alloy melt purification method by co-blowing refining agent and refining gas
CN117604311A (en) * 2024-01-24 2024-02-27 北京航空航天大学 Aluminum alloy rotary blowing refining method based on three-channel rotor
CN117587239B (en) * 2024-01-19 2024-04-19 北京航空航天大学 Alloy melt purification method by co-blowing refining agent and refining gas

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CN206887188U (en) * 2017-06-26 2018-01-16 广元市金易建材有限公司 A kind of duster and aluminum liquid purifying device
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CN108642297A (en) * 2018-07-06 2018-10-12 广西科技大学 A kind of method of the online compounding flux processing of light-alloy
CN210104043U (en) * 2019-03-19 2020-02-21 广西科技大学 Device for online purification of aluminum alloy melt

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CN202823690U (en) * 2012-09-13 2013-03-27 济宁矿业集团有限公司安居煤矿 Pneumatic spiral mixing injection machine
CN103964205A (en) * 2014-04-30 2014-08-06 程辉 Uninterrupted automatic batching and feeding pneumatic conveying injection pump
CN107779632A (en) * 2016-08-29 2018-03-09 上海交通大学 The method of aluminum matrix composite melt treatment
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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110343917A (en) * 2019-08-20 2019-10-18 惠州市华顺祥实业有限公司 The technique and its equipment of interruption preparation liquid silumin or silumin semi solid slurry
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CN111020224A (en) * 2019-12-31 2020-04-17 徐州汉裕铝业有限公司 Degassing box for aluminum cast-rolling coil
CN111496242A (en) * 2020-05-09 2020-08-07 南通大学 Turbulent flow type aluminum alloy melt deslagging and filtering device and using method thereof
CN112349440A (en) * 2020-11-01 2021-02-09 百色学院 Liquid metal purification device and application method thereof
CN112349440B (en) * 2020-11-01 2022-10-18 百色学院 Liquid metal purification device and application method thereof
CN117587239A (en) * 2024-01-19 2024-02-23 北京航空航天大学 Alloy melt purification method by co-blowing refining agent and refining gas
CN117587239B (en) * 2024-01-19 2024-04-19 北京航空航天大学 Alloy melt purification method by co-blowing refining agent and refining gas
CN117604311A (en) * 2024-01-24 2024-02-27 北京航空航天大学 Aluminum alloy rotary blowing refining method based on three-channel rotor
CN117604311B (en) * 2024-01-24 2024-04-19 北京航空航天大学 Aluminum alloy rotary blowing refining method based on three-channel rotor

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