CN109998943B - Essence with visual stable suspended colored oil bead particles - Google Patents
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- CN109998943B CN109998943B CN201910244520.XA CN201910244520A CN109998943B CN 109998943 B CN109998943 B CN 109998943B CN 201910244520 A CN201910244520 A CN 201910244520A CN 109998943 B CN109998943 B CN 109998943B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention discloses an essence with visual stable suspended colored oil bead particles, which is prepared from the following raw materials in percentage by mass: 88.5 to 95 percent of basic raw material, 4.5 to 11 percent of oily component, 0.2 to 0.6 percent of suspending agent, 0.01 to 0.1 percent of neutralizing agent and 0.0001 to 0.0004 percent of oil-soluble coloring agent, wherein the oily component is a mixture of diphenyl polydimethylsiloxane and perfluorooctyl triethoxysilane, and the suspending agent is a mixture of EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, xanthan gum and carbomer. The essence is transparent, and the colored oil droplets are uniformly and stably suspended in a particle shape, so that stable coexistence of oil and water is realized, no stimulation is caused, and the skin-care essence has moisturizing, moistening, smooth and compact skin feeling and is suitable for any skin.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an essence with visual stable suspended colored oil bead particles.
Background
The essence in the current market is mainly transparent water-based essence and micro-emulsion essence. Transparent water-based essence generally achieves the moisturizing effect by adding high-concentration water-soluble moisturizing ingredients into the formula, is fresh and cool in use and achieves the lasting moisturizing effect. The micro-emulsion type essence generally comprises two types of water-soluble raw materials and oil-soluble raw materials, and is mixed with the water-soluble raw materials and the oil-soluble raw materials by adding a surfactant, and the essence generally has the functions of moisturizing, moisturizing and moistening skin, but is generally slightly milky. However, with the development of the cosmetic industry and the improvement of the requirements of people on cosmetics, consumers have higher requirements on the visual appearance of the cosmetics while requiring the efficacy and the skin feel of the products.
It is known that when water and oil are mixed, the water and oil are not mixed, and most of the oil generally floats on the water surface with a small specific gravity. Thus, when water and oil are brought together, an aqueous phase and an oil phase appear, and the two phases separate. The water phase is mainly characterized by moisturizing and moisturizing, and the oil phase is mainly characterized by lubricating and moisturizing. In order to integrate the advantages of the two, the skin care product can keep moisture, moisten and smooth after being used, meanwhile, the grease can form a layer of oil film on the surface of the skin to firmly lock water, and can be used as a superfatting agent to supplement necessary fat of the skin while endowing the skin with softness, smoothness and glossiness, thereby playing a role in protecting the skin. The emulsifier is not added, and the water and the oil are combined to prepare a product with special appearance, so that the problem of instability of the water and the oil is solved, and the emulsifier is not generally applied to the cosmetic industry.
Disclosure of Invention
The invention aims to solve the problem of unbalanced water and oil and provide the essence with visual and stable suspended oil bead particles, which is high in transparency, good in stability and good in skin feel.
Aiming at the purposes, the essence adopted by the invention is prepared from the following raw materials in percentage by mass:
preferably, the essence is prepared from the following raw materials in percentage by mass:
in order to prepare good use skin feeling, the base raw materials comprise the following substances in parts by mass: 70-85 parts of water, 1-10 parts of glycerol, 1-10 parts of 1, 3-butanediol, 200.1-1 parts of methyl glucitol polyether, 1-10 parts of glycerol polymethacrylate, 0.01-0.1 part of allantoin, 0.1-2 parts of betaine, 0.1-5 parts of panthenol, 320.1-2 parts of polyethylene glycol-320.1, 0.01-1 part of nicotinamide, 0.1-0.2 part of methyl hydroxybenzoate and 0.15-0.25 part of phenoxyethanol.
Preferably, the base material comprises the following substances in parts by mass: 70-85 parts of water, 3-5 parts of glycerol, 2-4 parts of 1, 3-butanediol, 200.4-0.6 part of methyl glucitol polyether, 4-6 parts of glycerol polymethacrylate, 0.04-0.06 part of allantoin, 0.7-1 part of betaine, 1-3 parts of panthenol, 1-1.5 parts of polyethylene glycol-320.5, 0.4-0.6 part of nicotinamide, 0.12-0.18 part of methyl hydroxybenzoate and 0.17-0.23 part of phenoxyethanol.
In order to achieve good suspension stability and good skin feel, the oily component is selected from diphenyl polydimethylsiloxane and perfluorooctyl triethoxysilane in a mass ratio of 10: 5.5-6.5.
Preferably, the oily component is a mixture of diphenylpolydimethylsiloxane and perfluorooctyltriethoxysilane at a mass ratio of 5: 3.
For the stability, transparency, rheological property and the like of the base material, the suspending agent is a mixture of EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, xanthan gum and carbomer in a mass ratio of (0.08-0.12) to (0.2-0.3) to (0.1-0.2).
Preferably, the suspending agent is a mixture of EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, xanthan gum and carbomer in a mass ratio of 0.1:0.25: 0.18.
The neutralizing agent is one or more of potassium hydroxide, sodium hydroxide, triethanolamine and arginine, preferably potassium hydroxide, and the mass ratio of the potassium hydroxide to the carbomer is 1: 3-4.
The preparation method of the essence with the visual stable suspended colored oil bead particles comprises the following steps: sequentially adding a suspending agent and components needing to be heated and dissolved in the basic raw materials into an emulsifying pot, adding water, heating to 80-85 ℃ under the stirring condition until the components are completely dissolved, then cooling to 60 ℃, adding a neutralizing agent, uniformly stirring, cooling to below 45 ℃, adding the components needing to be added at low temperature in the basic raw materials, and fully and uniformly stirring; adding oily component and oil soluble colorant, stirring for dispersing, stopping stirring, and ultraviolet sterilizing for 60min to obtain the final product.
The invention has the following beneficial effects:
according to the invention, stable, safe and good skin feeling diphenyl polydimethylsiloxane and perfluorooctyl triethoxysilane are selected as oily components, EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, xanthan gum and carbomer are selected as suspending agents, a good skin feeling base material is selected as a water base, and an oil-soluble coloring agent is added to achieve a visual effect, so that oil globules are stably suspended and dispersed in the water base for a long time like a color particle, and finally, the essence with visual stable suspended oil globule particles, which is high in transparency, good in moisturizing effect and good in skin feeling, is obtained. The essence disclosed by the invention has no unstable phenomena such as layering and precipitation, has no stimulation, is moist and smooth in skin feel, is suitable for any skin type, has visual colored suspended oil droplets, and is novel in appearance.
Drawings
Fig. 1 is a photograph of a serum with visually stabilized suspended oil globule particles prepared in example 1.
Detailed Description
The invention will be further described in detail with reference to the following figures and examples, but the scope of the invention is not limited to these examples.
Example 1
Adding 0.1g carbomer, 0.3g xanthan gum, 0.1g Euglena GRACILIS (EUGLENA GRACILIS) polysaccharide, 4g glycerol, 3g 1, 3-butanediol, 0.5g methyl gluceth-20, 5g glycerol polymethacrylate, 0.05g allantoin, 0.8g betaine, 1g panthenol, 0.5g polyethylene glycol-32, 0.5g nicotinamide, 0.15g methyl hydroxybenzoate into 75.77475g water, heating to 80-85 ℃ under the stirring condition, stirring at constant temperature until the mixture is completely dissolved, then cooling to 60 ℃, adding 0.03g of potassium hydroxide, continuously cooling to 45 ℃ after uniformly stirring, adding 0.2g of phenoxyethanol, fully stirring uniformly, finally adding 0.00025g of CI61565 pigment, 5g of diphenyl polydimethylsiloxane and 3g of perfluoro octyl triethoxysilane, and uniformly stirring and dispersing to obtain the essence with the visual stable suspended oil bead particles (see figure 1).
Example 2
0.14g of carbomer, 0.28g of xanthan gum, 0.1g of EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, 4g of glycerol, 3g of 1, 3-butanediol, 0.5g of methyl gluceth-20, 5g of glycerol polymethacrylate, 0.05g of allantoin, 0.8g of betaine, 2g of panthenol, 1g of polyethylene glycol-32, 0.5g of nicotinamide and 0.15g of methylparaben are added into 74.24475g of water, the mixture is heated to 80-85 ℃ under the stirring condition and stirred at constant temperature until the mixture is completely dissolved, then the mixture is cooled to 60 ℃, 0.047g of potassium hydroxide is added, the mixture is stirred uniformly and then is continuously cooled to 45 ℃, 0.2g of phenoxyethanol is added, the mixture is stirred uniformly, finally 0.00025g of CI61565 pigment, 5g of diphenyl polydimethylsiloxane and 3g of perfluorooctyltriethoxysilane are added, and stirred and dispersed uniformly, and the essence liquid with the visual stable suspended oil bead particles is obtained.
Example 3
0.18g of carbomer, 0.25g of xanthan gum, 0.1g of EUGLENA GRACILIS polysaccharide, 4g of glycerol, 3g of 1, 3-butanediol, 1g of methyl glucitol polyether-20, 5g of glycerol polymethacrylate, 0.05g of allantoin, 0.8g of betaine, 2g of panthenol, 1g of polyethylene glycol-32, 0.5g of nicotinamide and 0.15g of methylparaben are added into 73.73175g of water, the mixture is heated to 80-85 ℃ under the stirring condition, the mixture is stirred at constant temperature until the mixture is completely dissolved, then the mixture is cooled to 60 ℃, 0.045g of potassium hydroxide is added, the mixture is continuously cooled to 45 ℃ after being uniformly stirred, 0.2g of phenoxyethanol is added, the mixture is fully stirred, finally 0.00025g of CI61565 pigment, 5g of diphenyl polydimethylsiloxane and 3g of perfluorooctyl triethoxysilane are added, the mixture is stirred and dispersed uniformly, and the essence with the visual stable suspended oil bead particles is obtained.
Example 4
0.2g of carbomer, 0.2g of xanthan gum, 0.08g of euglena gracilis (euglena gracilis) polysaccharide, 4g of glycerol, 3g of 1, 3-butanediol, 1g of methyl gluceth-20, 5g of glycerol polymethacrylate, 0.05g of allantoin, 0.8g of betaine, 2g of panthenol, 1g of polyethylene glycol-32, 0.5g of nicotinamide and 0.15g of methylparaben are added into 73.76975g of water, the mixture is heated to 80-85 ℃ under the stirring condition, the mixture is stirred at constant temperature until the mixture is completely dissolved, then the mixture is cooled to 60 ℃, 0.045g of potassium hydroxide is added, the mixture is continuously cooled to 45 ℃ after being uniformly stirred, 0.2g of phenoxyethanol is added, the mixture is fully stirred, finally 0.00025g of CI61565 pigment, 5g of diphenyl polydimethylsiloxane and 3g of perfluorooctyl triethoxysilane are added, and the mixture is stirred and dispersed uniformly, so that the essence liquid with the visual stable suspended oil globules is obtained.
In order to determine the raw material composition of the essence of the invention, the inventor carries out a large number of laboratory research tests, and the specific test conditions are as follows:
1. selection of oily component
5g of caprylic/capric triglyceride, polydimethylsiloxane, benzyltrimethicone, diphenylpolydimethylsiloxane, phenylpolytrimethicone and perfluorooctyltriethoxysilane were added to 45g of water, and gently stirred uniformly, followed by standing, and the dispersion of the oily raw material in water was observed, and the results are shown in Table 1.
TABLE 1
According to the test results in table 1, the oily component of the present invention was selected from diphenyl dimethicone compounded with perfluorooctyl triethoxysilane.
2. Selection of suspending agents
100g samples are prepared according to the mass percentage composition of the raw materials in the table 2, and the visual suspension phenomenon of the obtained samples is observed, and the result is shown in the table 3.
TABLE 2
TABLE 3
According to the test results in Table 3, the suspending agent of the present invention was formulated with carbomer, xanthan gum and Euglena GRACILIS (EUGLENA GRACILIS) polysaccharide.
In order to prove the beneficial effects of the invention, the inventor evaluates the skin feel of the essence prepared in the embodiments 1 to 4, and the evaluation method comprises the following steps: the appearance, skin feeling during smearing, sticky feeling, skin feeling after use, moisturizing effect, moistening effect and irritation of the product were comprehensively evaluated by using a questionnaire mode by 20 volunteers, and the average score was the highest at the end of 1-5 points of like and dislike. The results are shown in Table 4.
TABLE 4
As can be seen from Table 4, the essence of the invention has the advantages of good skin feel assessment, stable formula, mild action, convenient use, integration of water-based skin feel and oil skin feel, good suspension property, obvious visual color oil bead phenomenon, no stimulation and suitability for any skin type.
Claims (8)
1. The essence with the visual stable suspended colored oil bead particles is characterized by being prepared from the following raw materials in percentage by mass:
the oily component is diphenyl polydimethylsiloxane and perfluorooctyl triethoxysilane with the mass ratio of 10: 5.5-6.5;
the suspending agent is a mixture of EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, xanthan gum and carbomer in a mass ratio of (0.08-0.12) to (0.2-0.3) to (0.1-0.2).
2. The essence with visual stabilization of suspended colored oil globule particles of claim 1, wherein: the essence is prepared from the following raw materials in percentage by mass:
3. the essence with visual stabilization of suspended colored oil globule particles of claim 2, wherein: the oily component is a mixture of diphenyl polydimethylsiloxane and perfluorooctyl triethoxysilane in a mass ratio of 5: 3.
4. The essence with visual stabilization of suspended colored oil globule particles of claim 2, wherein: the suspending agent is a mixture of EUGLENA GRACILIS (EUGLENA GRACILIS) polysaccharide, xanthan gum and carbomer in a mass ratio of 0.1:0.25: 0.18.
5. The essence with visual stabilization of suspended colored oil globule particles of claim 1, wherein: the base raw material comprises the following substances in parts by mass:
70-85 parts of water, 1-10 parts of glycerol, 1-10 parts of 1, 3-butanediol, 200.1-1 parts of methyl glucitol polyether, 1-10 parts of glycerol polymethacrylate, 0.01-0.1 part of allantoin, 0.1-2 parts of betaine, 0.1-5 parts of panthenol, 320.1-2 parts of polyethylene glycol-320.1, 0.01-1 part of nicotinamide, 0.1-0.2 part of methyl hydroxybenzoate and 0.15-0.25 part of phenoxyethanol.
6. The essence with visual stabilization of suspended colored oil globule particles of claim 5, wherein: the base raw material comprises the following substances in parts by mass:
70-85 parts of water, 3-5 parts of glycerol, 2-4 parts of 1, 3-butanediol, 200.4-0.6 part of methyl glucitol polyether, 4-6 parts of glycerol polymethacrylate, 0.04-0.06 part of allantoin, 0.7-1 part of betaine, 1-3 parts of panthenol, 1-1.5 parts of polyethylene glycol-320.5, 0.4-0.6 part of nicotinamide, 0.12-0.18 part of methyl hydroxybenzoate and 0.17-0.23 part of phenoxyethanol.
7. The essence with visual stabilization of suspended colored oil globule particles of claim 1, wherein: the neutralizer is any one or more of potassium hydroxide, sodium hydroxide, triethanolamine and arginine.
8. The essence with visual stabilization of suspended colored oil globule particles of claim 7, wherein: the neutralizing agent is potassium hydroxide, and the mass ratio of the potassium hydroxide to the carbomer is 1: 3-4.
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111616990A (en) * | 2020-07-14 | 2020-09-04 | 广州美兮生物科技有限公司 | Solid spray, preparation method thereof and cosmetic |
| CN115813776A (en) * | 2022-12-30 | 2023-03-21 | 杭州菲丝凯化妆品有限公司 | Essence with suspended particles and preparation method thereof |
| CN117243832A (en) * | 2023-10-24 | 2023-12-19 | 铂臻(广州)生物科技有限公司 | Essence with anti-wrinkle effect and preparation method thereof |
| CN117562835B (en) * | 2024-01-17 | 2024-03-22 | 广州悦瑞化妆品有限公司 | Oil-containing bead essence and preparation method thereof |
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| CN1494417A (en) * | 2001-02-28 | 2004-05-05 | Mild moisturing liquids with soap-like rinse feel | |
| CN1509163A (en) * | 2001-02-28 | 2004-06-30 | Personal wash compositions containing particle-in-oil dispersion | |
| JP2008189642A (en) * | 2007-02-08 | 2008-08-21 | Shiseido Co Ltd | Production method of powder cosmetic and powder cosmetic |
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