CN109966208A - A kind of makeup removing facial mask and preparation method thereof - Google Patents
A kind of makeup removing facial mask and preparation method thereof Download PDFInfo
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- CN109966208A CN109966208A CN201910316075.3A CN201910316075A CN109966208A CN 109966208 A CN109966208 A CN 109966208A CN 201910316075 A CN201910316075 A CN 201910316075A CN 109966208 A CN109966208 A CN 109966208A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of makeup removing facial masks, it is characterized in that, it is made of the raw material of following parts by weight: 3-6 parts of glucosyl group amino betadex, 1-3 parts of green-tea extract, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino double -2, 1- second subunit polyethylene oxide-vinyl behenate-[N- (2- maleimidoethyl)] 3-7 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, 1-3 parts of triacetic acid red bayberry alcohol ester, 1-3 parts of myricetin 3-O- galactoside, 80-90 parts of water, 15-20 parts of grease, 3-5 parts of surfactant, 1-3 parts of emulsifier, 0.3-0.6 parts of the Chinese herbal medicine extract composition.The invention also discloses the production methods of the makeup removing facial mask.Makeup removing facial mask makeup removing effect disclosed by the invention is good, high-efficient, and small to skin irritation, skin remains to stay pale moist after makeup removing, using conveniently, safely, environmental protection.
Description
Technical field
The present invention relates to cosmetic technical fields more particularly to a kind of makeup removing facial mask and preparation method thereof.
Background technique
Like to be beautiful be the nature of people, especially female friend is even more to value oneself dressing.Exactly under these circumstances, it makes up
Industry development is rapid.Makeup has become essential a part in the modern life, and one can increase the beauty of women to make up
It is beautiful and self-confident, it is secondly also the respect to others on etiquette.But after face makeup, makeup removing becomes again has to face
Thing, if do not remove ornaments and formal dress thoroughly, remaining cosmetics can cause the pore of skin of face to block, and skin oil and fat water oil is caused to be secreted
The skin problem of puzzlement is made us in imbalance so as to cause acne, acne and blackhead etc..Therefore, a suitable makeup removal products have been
As important component indispensable in skin nursing.
Most commonly seen makeup removal products are that makeup remover, makeup removing breast and makeup removing condensation, these three types of products fill in the prior art
Loaded in container bottle, trouble is carried in out on tours or while going on business, and cannot carry when airplane.On the other hand, they go back
There is makeup removings not exclusively, easily causes dry skin, destroys the barrier function of skin, has certain irritation and allergy to skin
Property.In addition, makeup removal products are all in the strong fluid oil of mobility now, fallen off using Shi Yicong facial surface, causes to stain clothes
And it causes to be lost.
Chinese invention patent CN201410114416.6 discloses a kind of mild harmless makeup remover, and the makeup remover is by following
Ingredient is matched according to certain mass part: 10-15 parts of India's poponax resin, 7-10 parts of avocado oil, and 4-8 parts of horse cream is drawn
Fruit oil, 3-6 parts of aloe, 2-4 parts of glycerol, 8-13 parts of olive oil essence, 1-3 parts of pot marigold, 0.5-1.5 parts of wine
Essence.It is removed ornaments and formal dress using this makeup removal products, use is not easy enough, and the bad grasp of the dosage of toner easily causes various wastes;And
Step of removing ornaments and formal dress is more, not convenient enough.
Therefore, develop that a kind of makeup removal efficiency is high, effect is good, the makeup removal products using safety and environmental protection be related fields urgently
The technical issues of solution.
Summary of the invention
In order to overcome the defects of the prior art, the present invention is intended to provide a kind of makeup removing facial mask, makeup removing facial mask makeup removing effect
Fruit is good, high-efficient, small to skin irritation, and skin remains to stay pale moist after makeup removing, using conveniently, safely, environmental protection.Together
When, the invention also discloses the production methods of the makeup removing facial mask.
The present invention is realized by the following scheme:
A kind of makeup removing facial mask, is made of the raw material of following parts by weight: 3-6 parts of glucosyl group amino betadex, green
Double -2,1- second subunit polyethylene oxide-the second of 1-3 parts of tea extraction, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Alkenyl behenate-[N- (2- maleimidoethyl)] 3-7 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, triacetic acid
1-3 parts of red bayberry alcohol ester, 1-3 parts of myricetin 3-O- galactoside, 80-90 parts of water, 15-20 parts of grease, 3-5 parts of surfactant,
1-3 parts of emulsifier, 0.3-0.6 parts of the Chinese herbal medicine extract composition.
Further, the Chinese herbal medicine extract composition by following parts by weight component: almond powder extracts 10-15
Part, 15-20 parts of Herba Verbenae, 10-15 parts of Flos Osmanthi Fragrantis extract, 5-10 parts of black nightshade extract, Thunder God root extract 10-15
Part, 5-10 parts of Radix Gentianae extract.
Further, the emulsifier is in dimethyl silicone polymer, Polyoxyethylene Sorbitan Monooleate, polysorbate -20
It is one or more of;
Further, the grease is selected from pentaerythritol tetraoctyl stearate, myristyl alcohol acetic acid esters, niacin pentaerythrite
One or more of ester, tripalmitin.
Further, the surfactant is selected from surfactant peptides, 2-morpholine ethane sulfonic acid, dodecanamide propyl beet
One or more of alkali, surfactant 1727.
Further, the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino pair -2,1- second subunit polycyclic oxygen
The system of ethane-ethylene base behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer
Preparation Method includes the following steps: different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino pair -2,1- second subunit polycyclic
Oxidative ethane, vinyl behenate, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides, initiator add
Enter into high boiling solvent, stirring and dissolving is uniformly placed in micro-wave oven, under nitrogen or atmosphere of inert gases, in irradiation power
For Continuous irradiation 10-15 minutes under the microwave of 200-400W, after settle out in methyl alcohol, with ethanol washing product 3-5 times, after
It dries in vacuum oven at 75-85 DEG C to constant weight.
Preferably, the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino pair -2,1- second subunit polycyclic oxygen second
It is alkane, vinyl behenate, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides, initiator, high boiling
The mass ratio of point solvent is 1:2:0.5:(0.02-0.05): (10-18).
Preferably, the initiator is selected from peroxidized t-butyl perbenzoate, di-cyclohexylperoxy di-carbonate, the peroxidating moon
One or more of osmanthus acyl, azodiisobutyronitrile.
Preferably, the inert gas is selected from one of helium, neon, argon gas.
Preferably, the high boiling solvent is in dimethyl sulfoxide, n,N-dimethylacetamide, N-Methyl pyrrolidone
It is a kind of.
Further, the production method of the makeup removing facial mask, includes the following steps: by weight to mix each raw material, add
Enter into emulsion pot, stirred 3-5 hours at 50-60 DEG C, adjust PH to 6-8 with triethanolamine, samples inspection afterwards, go out after qualified
Material, sub-bottle packaging obtain finished product.
Preferably, when the sub-bottle packaging, every bottle of elder generation dispenses quantitative non-woven fabrics or carbon sponge on an equal basis.
The beneficial effects of adopting the technical scheme are that
1) production method of makeup removing facial mask provided by the invention, simple to operation, reaction condition is mild, and raw material is easy to get, nothing
Poison, small to skin irritation, cheap, Clinical practicability is strong.
2) makeup removing facial mask provided by the invention, makeup removing effect is good, high-efficient, small to skin irritation, and skin is still after makeup removing
Be able to maintain whitening moisten, using conveniently, safely, environmental protection;Addition is conducive to remove free radical by Chinese herbal medicine extract composition,
Assign the apparent skin-active of facial mask and Antiageing effect, at the same can also antimicrobial antiphlogistic, inhibit skin allergy;Add the different different Huang of trifoliate jewelvine chromene
Double -2,1- second subunit polyethylene oxide-vinyl behenate-[N- (the 2- maleimides of ketone-(Z) -9- octadecylene acylimino
Amido ethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer can not only play thickening power, moreover it is possible to play the work of beauty and skin care
With at the same time it can also increase the dissolubility of color make-up, raising makeup removing effect acts synergistically with other compositions, rear skin can be used
It is penetrating comfortable, pore also very clean feeling, and also it is not tight, the formation of melanin granule can be prevented, the new old of cell is accelerated
Metabolism promotes the activation of human senility cell, accelerates blood circulation, improves the intracorporal environment of people.
Specific embodiment
In order to make those skilled in the art more fully understand technical solution of the present invention, and make features described above of the invention,
Purpose and advantage are more clear understandable, and the present invention will be further explained with reference to the examples below.Embodiment is only used for
It is bright the present invention rather than limit the scope of the invention.
Raw material is commercially available in the following embodiments of the present invention.
Embodiment 1
A kind of makeup removing facial mask, is made of the raw material of following parts by weight: 3 parts of glucosyl group amino betadex, green tea
Double -2,1- second subunit polyethylene oxide-the vinyl of 1 part of extract, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Behenate-[N- (2- maleimidoethyl)] 3 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, triacetic acid myricanol
1 part of ester, 80 parts of water, 15 parts of pentaerythritol tetraoctyl stearate, 3 parts of surfactant peptides, gathers 1 part of myricetin 3-O- galactoside
1 part of dimethyl siloxane, 0.3 part of the Chinese herbal medicine extract composition.
The Chinese herbal medicine extract composition by following parts by weight component: 10 parts of almond powder extracts, Verbena officinalis extract
15 parts of object, 10 parts of Flos Osmanthi Fragrantis extract, 5 parts of black nightshade extract, 10 parts of Thunder God root extract, 5 parts of Radix Gentianae extract.
Double -2,1- second subunit polyethylene oxide-the ethylene of the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
The preparation method of base behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer, packet
Include following steps: by the double -2,1- second subunit polyethylene oxide of different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
100g, vinyl behenate 200g, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides 50g, mistake
Oxidation t-butyl perbenzoate 2g is added in dimethyl sulfoxide 1000g, and stirring and dissolving is uniformly placed in micro-wave oven, in nitrogen atmosphere
Under, irradiation power be 200W microwave under Continuous irradiation 10 minutes, after settle out in methyl alcohol, with ethanol washing product 3 times, after
It dries in the vacuum oven at 75 DEG C to constant weight.
The production method of the makeup removing facial mask, includes the following steps: by weight to mix each raw material, is added to emulsion pot
In, it is stirred 3 hours at 50 DEG C, adjusts PH to 6 with triethanolamine, sampled inspection afterwards, discharge after qualified, sub-bottle packaging is obtained into
Product.
When the sub-bottle packaging, every bottle of elder generation dispenses quantitative non-woven fabrics on an equal basis.
Embodiment 2
A kind of makeup removing facial mask, is made of the raw material of following parts by weight: 4 parts of glucosyl group amino betadex, green tea
Double -2,1- second subunit polyethylene oxide-the ethylene of 1.5 parts of extract, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Base behenate-[N- (2- maleimidoethyl)] 4.5 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, triacetic acid poplar
1.5 parts of plum alcohol ester, 1.5 parts of myricetin 3-O- galactoside, 83 parts of water, 16.5 parts of myristyl alcohol acetic acid esters, 2-morpholine ethane sulfonic acid
3.5 parts, 1.5 parts of Polyoxyethylene Sorbitan Monooleate, 0.4 part of the Chinese herbal medicine extract composition.
The Chinese herbal medicine extract composition by following parts by weight component: 12 parts of almond powder extracts, Verbena officinalis extract
17 parts of object, 12 parts of Flos Osmanthi Fragrantis extract, 7 parts of black nightshade extract, 12 parts of Thunder God root extract, 6.5 parts of Radix Gentianae extract.
Double -2,1- second subunit polyethylene oxide-the ethylene of the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
The preparation method of base behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer, packet
Include following steps: by the double -2,1- second subunit polyethylene oxide of different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
100g, vinyl behenate 200g, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides 50g, mistake
Two dicyclohexyl carbonate 3g are aoxidized to be added in n,N-dimethylacetamide 1200g, stirring and dissolving is uniformly placed in micro-wave oven,
Under helium atmosphere, irradiation power be 250W microwave under Continuous irradiation 12 minutes, after settle out in methyl alcohol, use ethanol washing
Product 4 times, after dry in the vacuum oven at 78 DEG C to constant weight.
The production method of the makeup removing facial mask, includes the following steps: by weight to mix each raw material, is added to emulsion pot
In, it is stirred 3.5 hours at 53 DEG C, adjusts PH to 6.5 with triethanolamine, sampled inspection afterwards, discharge after qualified, sub-bottle packaging obtains
To finished product.
When the sub-bottle packaging, every bottle of elder generation dispenses quantitative carbon sponge on an equal basis.
Embodiment 3
A kind of makeup removing facial mask, is made of the raw material of following parts by weight: 5 parts of glucosyl group amino betadex, green tea
Double -2,1- second subunit polyethylene oxide-the vinyl of 2 parts of extract, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Behenate-[N- (2- maleimidoethyl)] 5.5 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, triacetic acid red bayberry
2 parts of alcohol ester, 2 parts of myricetin 3-O- galactoside, 85 parts of water, 18 parts of pentaerythritol tetranicontinate, 4 parts of surfactant, sorbierite
- 202 parts of ester, 0.45 part of the Chinese herbal medicine extract composition.
The Chinese herbal medicine extract composition by following parts by weight component: 13 parts of almond powder extracts, Verbena officinalis extract
18 parts of object, 13 parts of Flos Osmanthi Fragrantis extract, 8 parts of black nightshade extract, 13 parts of Thunder God root extract, 8 parts of Radix Gentianae extract.
Double -2,1- second subunit polyethylene oxide-the ethylene of the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
The preparation method of base behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer, packet
Include following steps: by the double -2,1- second subunit polyethylene oxide of different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
100g, vinyl behenate 200g, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides 50g, mistake
Oxidation lauroyl 3.5g is added in N-Methyl pyrrolidone 1500g, and stirring and dissolving is uniformly placed in micro-wave oven, in neon atmosphere
Under enclosing, irradiation power be 300W microwave under Continuous irradiation 13 minutes, after settle out in methyl alcohol, with ethanol washing product 4 times,
It dries in the vacuum oven at 80 DEG C to constant weight afterwards.
The production method of the makeup removing facial mask, includes the following steps: by weight to mix each raw material, is added to emulsion pot
In, it is stirred 4 hours at 55 DEG C, adjusts PH to 7 with triethanolamine, sampled inspection afterwards, discharge after qualified, sub-bottle packaging is obtained into
Product.
When the sub-bottle packaging, every bottle of elder generation dispenses quantitative non-woven fabrics on an equal basis.
Embodiment 4
A kind of makeup removing facial mask, is made of the raw material of following parts by weight: 5.5 parts of glucosyl group amino betadex, green
Double -2,1- second subunit polyethylene oxide-the second of 2.5 parts of tea extraction, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Alkenyl behenate-[N- (2- maleimidoethyl)] 6 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, triacetic acid poplar
2.5 parts of plum alcohol ester, 2.5 parts of myricetin 3-O- galactoside, 88 parts of water, 19 parts of grease, 4.5 parts of surfactant, emulsifier 2.5
Part, 0.5 part of the Chinese herbal medicine extract composition;The emulsifier is dimethyl silicone polymer, Polyoxyethylene Sorbitan Monooleate, polysorbate
The 1:3:2 in mass ratio of ester -20 is mixed;The grease is pentaerythritol tetraoctyl stearate, myristyl alcohol acetic acid esters, niacin
Pentaerythritol ester, tripalmitin 3:5:2:3 in mass ratio are mixed;The surfactant be surfactant peptides,
2-morpholine ethane sulfonic acid, lauroylamidopropyl betaine, the 2:3:5:2 in mass ratio of surfactant 1727 are mixed;
The Chinese herbal medicine extract composition by following parts by weight component: 14 parts of almond powder extracts, Verbena officinalis extract
19 parts of object, 14 parts of Flos Osmanthi Fragrantis extract, 9 parts of black nightshade extract, 14 parts of Thunder God root extract, 9 parts of Radix Gentianae extract.
Double -2,1- second subunit polyethylene oxide-the ethylene of the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
The preparation method of base behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer, packet
Include following steps: by the double -2,1- second subunit polyethylene oxide of different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
100g, vinyl behenate 200g, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides 50g, draw
Hair agent 4g is added in high boiling solvent 1700g, and stirring and dissolving is uniformly placed in micro-wave oven, under argon atmosphere, is being irradiated
Power be 350W microwave under Continuous irradiation 14 minutes, after settle out in methyl alcohol, with ethanol washing product 5 times, after at 84 DEG C
Vacuum oven in dry to constant weight;The initiator be peroxidized t-butyl perbenzoate, di-cyclohexylperoxy di-carbonate,
Lauroyl peroxide, azodiisobutyronitrile 1:3:2:1 in mass ratio are mixed, and the high boiling solvent is dimethyl sulfoxide, N,
N- dimethyl acetamide, N-Methyl pyrrolidone 3:5:2 in mass ratio are mixed.
The production method of the makeup removing facial mask, includes the following steps: by weight to mix each raw material, is added to emulsion pot
In, it is stirred 4.5 hours at 57 DEG C, adjusts PH to 7.5 with triethanolamine, sampled inspection afterwards, discharge after qualified, sub-bottle packaging obtains
To finished product.
When the sub-bottle packaging, every bottle of elder generation dispenses quantitative carbon sponge on an equal basis.
Embodiment 5
A kind of makeup removing facial mask, is made of the raw material of following parts by weight: 6 parts of glucosyl group amino betadex, green tea
Double -2,1- second subunit polyethylene oxide-the vinyl of 3 parts of extract, different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Behenate-[N- (2- maleimidoethyl)] 7 parts of diethylene triamine pentacetic acid (DTPA) monoamides copolymer, triacetic acid myricanol
3 parts of ester, 3 parts of myricetin 3-O- galactoside, 90 parts of water, 20 parts of tripalmitin, 17275 parts of surfactant, poly- two
3 parts of methylsiloxane, 0.6 part of the Chinese herbal medicine extract composition.
The Chinese herbal medicine extract composition by following parts by weight component: 15 parts of almond powder extracts, Verbena officinalis extract
20 parts of object, 15 parts of Flos Osmanthi Fragrantis extract, 10 parts of black nightshade extract, 15 parts of Thunder God root extract, 10 parts of Radix Gentianae extract.
Double -2,1- second subunit polyethylene oxide-the ethylene of the different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
The preparation method of base behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer, packet
Include following steps: by the double -2,1- second subunit polyethylene oxide of different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
100g, vinyl behenate 200g, [N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides 50g, idol
Nitrogen bis-isobutyronitrile 5g is added in dimethyl sulfoxide 1800g, and stirring and dissolving is uniformly placed in micro-wave oven, under nitrogen atmosphere,
Irradiation power be 400W microwave under Continuous irradiation 15 minutes, after settle out in methyl alcohol, with ethanol washing product 5 times, after 85
It dries in vacuum oven at DEG C to constant weight.
The production method of the makeup removing facial mask, includes the following steps: by weight to mix each raw material, is added to emulsion pot
In, it is stirred 5 hours at 60 DEG C, adjusts PH to 8 with triethanolamine, sampled inspection afterwards, discharge after qualified, sub-bottle packaging is obtained into
Product.
When the sub-bottle packaging, every bottle of elder generation dispenses quantitative non-woven fabrics on an equal basis.
Comparative example 1
A kind of makeup removing facial mask, according to the formula and preparation method system of 201410836236.9 embodiment 1 of Chinese invention patent
At.
Comparative example 2
A kind of makeup removing facial mask, formula and preparation method are substantially the same manner as Example 1, the difference is that without addition glucose
Base amino betadex.
Comparative example 3
A kind of makeup removing facial mask, formula and preparation method are substantially the same manner as Example 1, the difference is that mentioning without addition green tea
Take object.
Comparative example 4
A kind of makeup removing facial mask, formula and preparation method are substantially the same manner as Example 1, the difference is that without adding different trifoliate jewelvine
Double -2,1- second subunit polyethylene oxide-vinyl behenate-[N- (the 2- of chromene isoflavones-(Z) -9- octadecylene acylimino
Maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer.
Comparative example 5
A kind of makeup removing facial mask, formula and preparation method are substantially the same manner as Example 1, the difference is that without addition triacetic acid
Red bayberry alcohol ester.
Comparative example 6
A kind of makeup removing facial mask, formula and preparation method are substantially the same manner as Example 1, the difference is that without addition Chinese herbal medicine
Extracting solution composition.
Meanwhile in order to assess the particular technique effect of makeup removing facial mask of the present invention, with the embodiment of the present invention and comparative example
In makeup removing facial mask carry out clinical trial, experimental result is shown in Table 1, and experimental method is as follows: making professional 100 status of judging panel by blind
Not Shi Yong three days each sample, answer questionnaire after use.Speed, the feel after cleaning are rinsed in evaluation, and makeup removing effect is classified as
A, B, C, D, it is good effect that rank, which is A, rank in B or C be it is effective, rank is invalid in D.
Table 1
As seen from Table 1, makeup removing facial mask disclosed by the embodiments of the present invention rinses speed more compared with comparative example existing product
Fastly, feeling is better after cleaning, and more preferably, this is the result of various raw material synergistic effects to makeup removing effect.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and what is described in the above embodiment and the description is only the present invention
Principle, various changes and improvements may be made to the invention without departing from the spirit and scope of the present invention, these variation and
Improvement is both fallen in the range of claimed invention.The present invention claims protection scope by appended claims and its
Equivalent defines.
Claims (10)
1. a kind of makeup removing facial mask, which is characterized in that be made of the raw material of following parts by weight: glucosyl group amino betadex
3-6 parts, 1-3 parts of green-tea extract, the double -2,1- second subunit polycyclics of different trifoliate jewelvine chromene isoflavones-(Z) -9- octadecylene acylimino
Oxidative ethane-vinyl behenate-[N- (2- maleimidoethyl)] diethylene triamine pentacetic acid (DTPA) monoamides copolymer 3-7
Part, 1-3 parts of triacetic acid red bayberry alcohol ester, 1-3 parts of myricetin 3-O- galactoside, 80-90 parts of water, 15-20 parts of grease, surface-active
3-5 parts of agent, 1-3 parts of emulsifier, 0.3-0.6 parts of the Chinese herbal medicine extract composition.
2. makeup removing facial mask according to claim 1, which is characterized in that the Chinese herbal medicine extract composition is by following weight
The component of part: 10-15 parts of almond powder extracts, 15-20 parts of Herba Verbenae, 10-15 parts of Flos Osmanthi Fragrantis extract, black nightshade extract
5-10 parts, 10-15 parts of Thunder God root extract, 5-10 parts of Radix Gentianae extract.
3. makeup removing facial mask according to claim 1, which is characterized in that the emulsifier is selected from dimethyl silicone polymer, gathers
One or more of sorbitol ester -80, polysorbate -20.
4. makeup removing facial mask according to claim 1, which is characterized in that the grease is selected from four isostearic acid of pentaerythrite
One or more of ester, myristyl alcohol acetic acid esters, pentaerythritol tetranicontinate, tripalmitin.
5. makeup removing facial mask according to claim 1, which is characterized in that the surfactant is selected from surfactant peptides, 2-
One or more of morpholino b acid, lauroylamidopropyl betaine, surfactant 1727.
6. makeup removing facial mask according to claim 1, which is characterized in that described different trifoliate jewelvine chromene isoflavones-(Z) -9- 18
Double -2,1- second subunit polyethylene oxide-vinyl behenate-[N- (2- the maleimidoethyl)] diethyls of alkene acylimino
The preparation method of alkene pentaacetic acid monoamides copolymer includes the following steps: different trifoliate jewelvine chromene isoflavones-(Z) -9- 18
Double -2,1- second subunit the polyethylene oxide of alkene acylimino, vinyl behenate, [N- (2- maleimidoethyl)] diethyl
Alkene pentaacetic acid monoamides, initiator are added in high boiling solvent, and stirring and dissolving is uniformly placed in micro-wave oven, in nitrogen
Or under atmosphere of inert gases, irradiation power be 200-400W microwave under Continuous irradiation 10-15 minutes, after sink in methyl alcohol
Out, with ethanol washing product 3-5 times, after dry in the vacuum oven at 75-85 DEG C to constant weight.
7. makeup removing facial mask according to claim 6, which is characterized in that described different trifoliate jewelvine chromene isoflavones-(Z) -9- 18
Double -2,1- second subunit the polyethylene oxide of alkene acylimino, vinyl behenate, [N- (2- maleimidoethyl)] diethyl
Alkene pentaacetic acid monoamides, initiator, high boiling solvent mass ratio be 1:2:0.5:(0.02-0.05): (10-18).
8. makeup removing facial mask according to claim 6, which is characterized in that the initiator is selected from the tertiary fourth of perbenzoic acid
One or more of ester, di-cyclohexylperoxy di-carbonate, lauroyl peroxide, azodiisobutyronitrile;The inert gas
Selected from one of helium, neon, argon gas;The high boiling solvent is selected from dimethyl sulfoxide, DMAC N,N' dimethyl acetamide, N- methyl
One of pyrrolidones.
9. makeup removing facial mask according to claim 1-8, which is characterized in that the production method of the makeup removing facial mask,
Include the following steps: by weight to mix each raw material, be added in emulsion pot, is stirred 3-5 hours at 50-60 DEG C, with three
Ethanol amine adjusts PH to 6-8, samples inspection afterwards, discharges after qualified, sub-bottle packaging obtains finished product.
10. makeup removing facial mask according to claim 9, which is characterized in that when the sub-bottle packaging, every bottle of elder generation dispenses fixed on an equal basis
Measure non-woven fabrics or carbon sponge.
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CN201910316075.3A CN109966208A (en) | 2019-04-19 | 2019-04-19 | A kind of makeup removing facial mask and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115135300A (en) * | 2020-02-25 | 2022-09-30 | 株式会社资生堂 | Cosmetic comprising high-molecular compound having siloxane bond and having host group and/or guest group |
-
2019
- 2019-04-19 CN CN201910316075.3A patent/CN109966208A/en not_active Withdrawn
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115135300A (en) * | 2020-02-25 | 2022-09-30 | 株式会社资生堂 | Cosmetic comprising high-molecular compound having siloxane bond and having host group and/or guest group |
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