CN109944098A - A kind of microbial staining method of protein fiber - Google Patents
A kind of microbial staining method of protein fiber Download PDFInfo
- Publication number
- CN109944098A CN109944098A CN201910279474.7A CN201910279474A CN109944098A CN 109944098 A CN109944098 A CN 109944098A CN 201910279474 A CN201910279474 A CN 201910279474A CN 109944098 A CN109944098 A CN 109944098A
- Authority
- CN
- China
- Prior art keywords
- microbial staining
- protein fiber
- microbial
- bath
- staining method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Coloring (AREA)
Abstract
The present invention provides a kind of microbial staining methods of protein fiber.Specifically include following steps, it will ferment in the cleaning of required raw material and stripping and slicing merging water, microbial staining stoste is obtained by filtration, after adjusting pH value, prepare microbial staining bath, then the pretreated protein fiber sample of hydrogen peroxide is impregnated in dyeing in the microbial staining bath with certain bath raio to handle, is washed through warm water, cold water is washed, is baked, is soaped.A kind of microbial staining method of protein fiber of the present invention, environmentally protective, simple process, strong operability, application value are extensive, institute's dying product color uniqueness, biocompatibility and health-care medical effect with higher.
Description
Technical field
The present invention relates to textile dyeing technical fields, particularly relate to a kind of microbial staining side of protein fiber
Method.
Background technique
Textile is that mankind's daily life consumes one of biggish necessity, with the continuous improvement of living standards, ecology,
Green, environmentally friendly class textile become the focus of people's growing interest.Protein fiber product is mainly by hair class and sericterium point
Secrete fiber composition, derive from naturally, it is with higher ecology index, if during its dyeing process, using green contaminate
Material and environmental protection processing, product will have the higher ecological value.Currently, protein fiber product dyeing dyestuff used is main
Based on chemical dye, for chemical dye during making and using, there are more environmental issues.Therefore, a kind of to be applicable in
The it is proposed of the environmentally protective colouring method of protein fiber product has the higher ecological value.
Summary of the invention
The present invention proposes a kind of microbial staining method of protein fiber, solves existing applicable protein fiber
The environmentally protective colouring method of product.
The technical scheme of the present invention is realized as follows:
A kind of microbial staining method of protein fiber, steps are as follows:
(1) preparation of microbial staining stoste: will be enriched in fruits ferment raw material clean up mixed with water after apple vinegar is added
It ferments, is filtered to obtain microbial staining stoste after fermentation；
(2) configuration of microbial staining bath: it is 10%-100%, pH 4- that microbial staining stoste, which is configured to mass concentration with water,
The bath of 6 solution, as microbial staining；
(3) protein fiber sample pretreatment: protein fiber sample is immersed by certain bath raio by hydrogen peroxide and silicon
In the aqueous solution of sour sodium composition, 50-60 DEG C of processing 30-60min obtains pretreating specimen；
(4) microbial staining is handled: certain bath is pressed in the microbial staining bath of the pretreating specimen of step (3) and step (2)
Than carrying out impregnation, ethanol amine being then added, be warming up to 80-90 DEG C, keep the temperature 30-60min, washed and baked and to obtain dyeing
Sample；
(5) it soaps processing: by the dyeing sample of step (4) and 2-3g/L detergent by certain bath raio, being washed under the conditions of 95 DEG C
Wash, then eluted with cold water, dry microbial staining protein fiber.
It is one of fruit containing anthocyanidin or a variety of that fruits ferment raw material is rich in the step (1).
Mixing mass ratio in the step (1) rich in fruits ferment raw material, apple vinegar and water is (3-5): (1-3):
(300-900).
Fermentation time is 20-45 days in the step (1), and fermentation temperature is 15-32 DEG C, is filtered into room temperature filtering, filtering
Mesh number be 80-100.
Final concentration of 1.5g/L of the final concentration of 15g/L of hydrogen peroxide, sodium metasilicate in the step (3), bath raio 1:
(20-50).
Protein fibre sample is one or more of wool, cashmere, silk in the step (3).
Bath raio is 1:(20-50 in the step (4)), the time of impregnation is 15-30min, with protein fibre
Quality is that the mass fraction of benchmark ethanol amine is 1-2%.
Washing refers to that washing primary, cold water using 50 DEG C of warm water washes twice, bakes as in 120-140 DEG C of item in the step (4)
2-3min is baked under part.
Dyeing sample and the bath raio of 2-3g/L detergent processing are 1:(30-50 in the step (5)), wherein detergent is
Detergent suitable for the detergent of wool fabric, as being suitable for wool, real silk fabric in blue moon, gold spinning.
The beneficial effects of the present invention are:
1, a kind of microbial staining method of protein fiber of the present invention is rich in microorganism using microbial fermentation processes preparation
Stoste is dyed, protein fiber is dyed under weakly acidic condition.Protein fibre high-temperature dyeing under weak acid environment
Fibre damage is smaller, and the addition of ethanol amine can effectively reduce dyeing temperature, improves dye-uptake.
2, a kind of microbial staining method of protein fiber of the present invention prepares microbial staining using apple vinegar fermentation
Stoste effectively improves the concentration of pigment in microbial staining stoste conducive to the generation of microorganism in fermentation liquid, and raising contaminates system
The dye level of product.
3, a kind of microbial staining method of protein fiber of the present invention, on fiber is realized in microbial staining stoste
Dye, institute's dying product biocompatibility with higher and health-care medical effect.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical solution of the present invention is clearly and completely described, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
Those of ordinary skill in the art's every other embodiment obtained under that premise of not paying creative labor, belongs to this hair
The range of bright protection.
Embodiment 1
A kind of microbial staining method of protein fiber, specifically includes the following steps:
The preparation of microbial staining stoste, it is cleaned using apple, dragon fruit, mulberries, and (the fruit that ferments in stripping and slicing merging water
Fermentoid raw material and water mixed proportion are 1:200), in fermentation process and add apple vinegar (fruits ferment raw material and apple vinegar
Ratio is 3:1), fermentation time is 30 days, and temperature is 20 DEG C, crosses 80 mesh filter screens and obtains microbial staining stoste.
The configuration of microbial staining bath, by microorganism stoste configuration concentration is 30%, pH is 5 aqueous solution to get protein
Base fibre microorganism dye bath.
Wool fabric sample pretreatment is immersed by wool fabric with 1:20 bath raio by 15g/L hydrogen peroxide and 1.5g/L silicon
In the aqueous solution of sour sodium composition, 60 DEG C of processing 30min.
Microbial staining processing, by the pretreating specimen with bath raio 1:20, is placed in 50 DEG C of protein fiber microorganisms
15min is impregnated in dye bath, 1% ethanol amine is added, is warming up to 85 DEG C, keeps the temperature 30min, 50 DEG C of warm water are washed 1 time, and cold water is washed 2 times,
120 DEG C of baking 3min.
It soaps processing, bath raio 1:30, wool fabric washs 10min, cold water under the conditions of 95 DEG C in 2g/L detergent
After elution, naturally dry.
Embodiment 2
A kind of microbial staining method of protein fiber, specifically includes the following steps:
The preparation of microbial staining stoste, it is cleaned using apple, blueberry, mulberries, and (the fruits that ferment in stripping and slicing merging water
Ferment raw material and water mixed proportion are 1:200), in fermentation process and add apple vinegar (fruits ferment raw material and apple vinegar ratio
Example is 3:1), fermentation time is 20 days, and temperature is 30 DEG C, crosses 90 mesh filter screens and obtains microbial staining stoste.
The configuration of microbial staining bath, by microorganism stoste configuration concentration is 50%, pH is 6 aqueous solution to get protein
Base fibre microorganism dye bath.
Silk fabric pretreatment is immersed by silk fabric with 1:40 bath raio by 15g/L hydrogen peroxide and 1.5g/L sodium metasilicate
In the aqueous solution of composition, 50 DEG C of processing 50min.
Microbial staining processing, by the pretreating specimen with bath raio 1:20, is placed in 50 DEG C of protein fiber microorganisms
20min is impregnated in dye bath, 2% ethanol amine is added, is warming up to 80 DEG C, keeps the temperature 40min, 50 DEG C of warm water are washed 1 time, and cold water is washed 2 times,
130 DEG C of baking 2min.
It soaps processing, bath raio 1:30, silk fabric washs 10min, cold water under the conditions of 95 DEG C in 2g/L detergent
After elution, naturally dry.
Embodiment 3
A kind of microbial staining method of protein fiber, specifically includes the following steps:
The preparation of microbial staining stoste, blueberry is cleaned, and (fruits ferment raw material is mixed with water for fermentation in stripping and slicing merging water
Ratio is 1:300), in fermentation process and add apple vinegar (fruits ferment raw material and apple vinegar ratio be 5:1), fermentation time
It is 45 days, temperature is 15 DEG C, crosses 100 mesh filter screens and obtains microbial staining stoste.
Microorganism stoste, that is, protein fiber microbial staining that pH is 6 is bathed in the configuration of microbial staining bath.
Silk fabric pretreatment is immersed by silk fabric with 1:30 bath raio by 15g/L hydrogen peroxide and 1.5g/L sodium metasilicate
In the aqueous solution of composition, 55 DEG C of processing 40min.
Microbial staining processing, by the pretreating specimen with bath raio 1:20, is placed in 50 DEG C of protein fiber microorganisms
20min is impregnated in dye bath, the ethanol amine of silk fabric quality 2% is added, is warming up to 90 DEG C, keeps the temperature 60min, and 50 DEG C of warm water wash 1
Secondary, cold water is washed 2 times, 120 DEG C of baking 3min.
It soaps processing, bath raio 1:50, silk fabric washs 10min, cold water under the conditions of 95 DEG C in 3g/L detergent
After elution, naturally dry.
Embodiment 4
A kind of microbial staining method of protein fiber, specifically includes the following steps:
The preparation of microbial staining stoste, it is cleaned using apple, blueberry, mulberries, and (the fruits that ferment in stripping and slicing merging water
Ferment raw material and water mixed proportion are 1:100), in fermentation process and add apple vinegar (fruits ferment raw material and apple vinegar ratio
Example is 1:1), fermentation time is 30 days, and temperature is 15 DEG C, crosses 80 mesh filter screens and obtains microbial staining stoste.
The configuration of microbial staining bath, by microorganism stoste configuration concentration is 10%, pH is 5.5 aqueous solution to get albumen
Matter base fibre microorganism dye bath.
Wool fabric pretreatment immerses wool fabric by 15g/L hydrogen peroxide and 1.5g/L sodium metasilicate group with 1:50 bath raio
At aqueous solution in, 50 DEG C of processing 60min.
Microbial staining processing, by the pretreating specimen with bath raio 1:20, is placed in 50 DEG C of protein fiber microorganisms
15min is impregnated in dye bath, 1% ethanol amine is added, is warming up to 80 DEG C, keeps the temperature 30min, 50 DEG C of warm water are washed 1 time, and cold water is washed 2 times,
140 DEG C of baking 2.5min.
It soaps processing, bath raio 1:40, wool fabric washs 10min under the conditions of 95 DEG C in 2.5g/L detergent, cold
After water elution, naturally dry.
Embodiment 5
A kind of microbial staining method of protein fiber, specifically includes the following steps:
The preparation of microbial staining stoste, it is cleaned using apple, blueberry, mulberries, and (the fruits that ferment in stripping and slicing merging water
Ferment raw material and water mixed proportion are 5:900), in fermentation process and add apple vinegar (fruits ferment raw material and apple vinegar ratio
Example is 5:3), fermentation time is 20 days, and temperature is 30 DEG C, and microbial staining stoste is obtained by filtration.
The configuration of microbial staining bath, by microorganism stoste configuration concentration is 60%, pH is 6 aqueous solution to get protein
Base fibre microorganism dye bath.
Silk fabric pretreatment is immersed by silk fabric with 1:50 bath raio by 15g/L hydrogen peroxide and 1.5g/L sodium metasilicate
In the aqueous solution of composition, 60 DEG C of processing 40min.
Microbial staining processing, by the pretreating specimen with bath raio 1:20, is placed in 50 DEG C of protein fiber microorganisms
30min is impregnated in dye bath, 1.5% ethanol amine is added, is warming up to 80 DEG C, keeps the temperature 60min, and 50 DEG C of warm water are washed 1 time, and cold water washes 2
It is secondary, 130 DEG C of baking 2min.
It soaps processing, bath raio 1:30, silk fabric washs 10min, cold water under the conditions of 95 DEG C in 2g/L detergent
After elution, naturally dry.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (9)
1. a kind of microbial staining method of protein fiber, it is characterised in that steps are as follows:
(1) preparation of microbial staining stoste: will be enriched in fruits ferment raw material clean up mixed with water after apple vinegar is added
It ferments, is filtered to obtain microbial staining stoste after fermentation；
(2) configuration of microbial staining bath: it is 10%-100%, pH 4- that microbial staining stoste, which is configured to mass concentration with water,
The bath of 6 solution, as microbial staining；
(3) protein fiber sample pretreatment: protein fiber sample is immersed by certain bath raio by hydrogen peroxide and silicon
In the aqueous solution of sour sodium composition, 50-60 DEG C of processing 30-60min obtains pretreating specimen；
(4) microbial staining is handled: certain bath is pressed in the microbial staining bath of the pretreating specimen of step (3) and step (2)
Than carrying out impregnation, ethanol amine being then added, be warming up to 80-90 DEG C, keep the temperature 30-60min, washed and baked and to obtain dyeing
Sample；
(5) it soaps processing: by the dyeing sample of step (4) and 2-3g/L detergent by certain bath raio, being washed under the conditions of 95 DEG C
Wash, then eluted with cold water, dry microbial staining protein fiber.
2. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (1)
In rich in fruits ferment raw material be one of fruit containing anthocyanidin or a variety of.
3. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (1)
In rich in fruits ferment raw material, apple vinegar and water mixing mass ratio be (3-5): (1-3): (300-900).
4. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (1)
Middle fermentation time is 20-45 days, and fermentation temperature is 15-32 DEG C, is filtered into room temperature filtering, and the mesh number of filtering is 80-100.
5. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (3)
Final concentration of 1.5g/the L, bath raio 1:(20-50 of the final concentration of 15g/L of middle hydrogen peroxide, sodium metasilicate).
6. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (3)
Middle protein fibre sample is one or more of wool, cashmere, silk.
7. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (4)
Middle bath raio is 1:(20-50), the time of impregnation is 15-30min, using the quality of protein fibre as the matter of benchmark ethanol amine
Amount number is 1-2%.
8. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (4)
Middle washing refers to that washing primary, cold water using 50 DEG C of warm water washes twice, bakes to dry 2-3min under the conditions of 120-140 DEG C.
9. the microbial staining method of protein fiber according to claim 1, it is characterised in that: the step (5)
Middle dyeing sample and the bath raio of 2-3g/L detergent processing are 1:(30-50).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910279474.7A CN109944098A (en) | 2019-04-09 | 2019-04-09 | A kind of microbial staining method of protein fiber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910279474.7A CN109944098A (en) | 2019-04-09 | 2019-04-09 | A kind of microbial staining method of protein fiber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109944098A true CN109944098A (en) | 2019-06-28 |
Family
ID=67013958
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910279474.7A Pending CN109944098A (en) | 2019-04-09 | 2019-04-09 | A kind of microbial staining method of protein fiber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109944098A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111235916A (en) * | 2020-03-23 | 2020-06-05 | 江苏鑫缘丝绸科技有限公司 | Silk floss dyeing method based on bluish black purple bacillus spore powder |
| CN111286999A (en) * | 2020-03-23 | 2020-06-16 | 江苏鑫缘丝绸科技有限公司 | Silk floss dyeing method based on metarhizium anisopliae spore powder |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101476248A (en) * | 2009-01-20 | 2009-07-08 | 西安际华三五一一家纺有限公司 | Method for using natural grape seed dyeing extract in textile dyeing |
| CN101525326A (en) * | 2008-03-06 | 2009-09-09 | 陕西嘉禾植物化工有限责任公司 | Method for extracting anthocyanin |
| CN102628227A (en) * | 2012-03-29 | 2012-08-08 | 江南大学 | Grape-seed-based ecological preparation method for ultravioresistant woolen and silk textiles |
| CN103266508A (en) * | 2013-06-13 | 2013-08-28 | 太仓协大申泰羊毛衫有限公司 | Low-temperature cashmere dyeing method adopting ethanolamine for pretreatment |
| CN108532324A (en) * | 2018-03-09 | 2018-09-14 | 广州番禺职业技术学院 | A method of wool is dyed using mulberry juice |
-
2019
- 2019-04-09 CN CN201910279474.7A patent/CN109944098A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525326A (en) * | 2008-03-06 | 2009-09-09 | 陕西嘉禾植物化工有限责任公司 | Method for extracting anthocyanin |
| CN101476248A (en) * | 2009-01-20 | 2009-07-08 | 西安际华三五一一家纺有限公司 | Method for using natural grape seed dyeing extract in textile dyeing |
| CN102628227A (en) * | 2012-03-29 | 2012-08-08 | 江南大学 | Grape-seed-based ecological preparation method for ultravioresistant woolen and silk textiles |
| CN103266508A (en) * | 2013-06-13 | 2013-08-28 | 太仓协大申泰羊毛衫有限公司 | Low-temperature cashmere dyeing method adopting ethanolamine for pretreatment |
| CN108532324A (en) * | 2018-03-09 | 2018-09-14 | 广州番禺职业技术学院 | A method of wool is dyed using mulberry juice |
Non-Patent Citations (4)
| Title |
|---|
| 吴卫华: "《苹果综合加工新技术》", 31 May 1996, 中国轻工业出版社 * |
| 尹卫平: "《精细化工产品及工艺》", 31 August 2009, 华东理工大学出版社 * |
| 李光红 等: "青海红花用于藏毯羊毛染色的研究", 《广东化工》 * |
| 陈美云 等: "羊毛乙醇胺预处理及其染色性能", 《印染》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111235916A (en) * | 2020-03-23 | 2020-06-05 | 江苏鑫缘丝绸科技有限公司 | Silk floss dyeing method based on bluish black purple bacillus spore powder |
| CN111286999A (en) * | 2020-03-23 | 2020-06-16 | 江苏鑫缘丝绸科技有限公司 | Silk floss dyeing method based on metarhizium anisopliae spore powder |
| CN111286999B (en) * | 2020-03-23 | 2022-05-31 | 江苏鑫缘丝绸科技有限公司 | Silk floss dyeing method based on metarhizium anisopliae spore powder |
| CN111235916B (en) * | 2020-03-23 | 2022-06-24 | 江苏鑫缘丝绸科技有限公司 | Silk floss dyeing method based on bluish black purple bacillus spore powder |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102978980B (en) | Polyester cotton one bath process dye | |
| CN101270550B (en) | Method for dyeing of loose fibre with natural dye | |
| CN106368014B (en) | A kind of Modal/cotton blended fabric dyeing | |
| CN105970697B (en) | The color fixing process method of textile natural dyeing | |
| CN101046067A (en) | Process of dyeing silk with dye yam extract | |
| CN110172840A (en) | A kind of colouring method of nylon fabric | |
| CN102182078B (en) | Monascorubrin mordant dyeing method of silk textile | |
| CN102021846A (en) | Process method for dying flax fabric by vegetable dye | |
| CN104420365A (en) | Modal/cotton blended fabric dyeing process | |
| CN109944098A (en) | A kind of microbial staining method of protein fiber | |
| CN106498764A (en) | A kind of smooth power antimicrobial form acrylon dyed yarn and preparation method thereof | |
| CN1804206A (en) | One-bath dyeing method for soybean fiber/tencel blended fabric | |
| CN104278558A (en) | Active dye applied to wool and wool dyeing method | |
| CN113249983B (en) | Method for dyeing black cashmere fiber or fabric by using natural plant pigment | |
| CN109295757A (en) | A kind of natural dye dying method of regenerated fiber fabric | |
| CN103088678A (en) | Method used for textile dyeing and finishing after-treatment | |
| CN106120404B (en) | Dyestuff and fiber separation used additives and application in the dyeing of protein fibre original position mineralising | |
| CN102965978B (en) | Dyeing method for hybrid loose fibers | |
| CN103485206A (en) | Dyeing process of soybean fibers by active dye | |
| CN103255645B (en) | Goat cashmere/viscose blend fabric dyeing | |
| CN110438640A (en) | A kind of multicomponent is same to bathe dyeing at normal pressure fancy fabric and preparation method thereof | |
| CN109505157A (en) | Nylon-cotton fabric One Bath Dyeing Process | |
| CN109930395A (en) | A kind of microbial staining method of cellulose-based fiber | |
| CN114934395A (en) | Method for dyeing natural fiber fabric by using rosa roxburghii tratt extract | |
| CN104109691A (en) | Preparation method and dyeing method of red pigment secreted by ginkgo leaf endophyte |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190628 |
|
| RJ01 | Rejection of invention patent application after publication |