CN109940908A - 一种碳纤维和酚醛树脂复合材料的成型工艺 - Google Patents
一种碳纤维和酚醛树脂复合材料的成型工艺 Download PDFInfo
- Publication number
- CN109940908A CN109940908A CN201711391396.7A CN201711391396A CN109940908A CN 109940908 A CN109940908 A CN 109940908A CN 201711391396 A CN201711391396 A CN 201711391396A CN 109940908 A CN109940908 A CN 109940908A
- Authority
- CN
- China
- Prior art keywords
- phenolic resin
- carbon fiber
- resin composite
- moulding
- type cavity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000002131 composite material Substances 0.000 title claims abstract description 34
- 239000005011 phenolic resin Substances 0.000 title claims abstract description 24
- 229920001568 phenolic resin Polymers 0.000 title claims abstract description 24
- 229920000049 Carbon (fiber) Polymers 0.000 title claims abstract description 21
- 239000004917 carbon fiber Substances 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 19
- 238000000465 moulding Methods 0.000 title claims abstract description 19
- 239000000835 fiber Substances 0.000 claims abstract description 25
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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[C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 22
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 238000001816 cooling Methods 0.000 claims abstract description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Chemical compound 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- 239000002184 metal Substances 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N phosphorus Chemical compound 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Abstract
一种碳纤维和酚醛树脂复合材料的成型工艺，该工艺包括下述步骤：1）配制预浸料；2）涂覆；3）制作产品型腔模具，在模具表面涂抹脱模计；4）碳纤维复合材料经过传送带进入加热引导机构，加热后放入型腔模具；5）将型腔模具合模后预热，同时对模具进行抽真空；6）在真空环境下进行热压成型，待冷却后脱模，得到碳纤维和酚醛树脂复合材料的成型产品。本发明能有效降低孔隙率，且操作简单、成本低廉。
Description
技术领域
本发明涉及复合材料技术领域，尤其是指一种碳纤维和酚醛树脂复合材料的成型工艺。
背景技术
碳纤维是由有机纤维经过一系列热处理转化而成，含碳量高于90%的无机高性能纤维，是一种力学性能优异的新材料，具有碳材料的固有本性特征，又兼备纺织纤维的柔软可加工型，是新一代增强纤维。传统使用碳纤维除用作绝热保温材料外，一般不单独使用，多作为增强材料加入到树脂、金属、陶瓷、混凝土等材料中，构成复合材料，已经广泛地被应用于航天、纺织、化工机械、体育器材、汽车制造等领域。
目前，碳纤维复合材料在生产过程中，由于各种因素，如环境中的杂质、工艺实施不完善等易造成多种缺陷，不同的缺陷对复合材料性能都有着或多或少的影响，孔隙是复合材料的主要缺陷之一，过多的孔隙可降低复合材料30%的层间剪切强度，拉伸强度下降约26%，当应用于制备产品时，无法发挥其最佳的使用性能。
发明内容
为了克服上述现有技术中存在的不足，本发明提供了一种碳纤维和酚醛树脂复合材料的成型工艺，该工艺能有效降低孔隙率，且操作简单、成本低廉。
为实现上述目的，本发明采用如下技术方案：
一种碳纤维和酚醛树脂复合材料的成型工艺，包括下述步骤：
1）配制预浸料：取酚醛树脂和稀释剂按质量比5:1的比例混合均匀，控制其粘度为2.0-2.5Pa·S，所述稀释剂为丙酮或工业酒精。
2）涂覆：在碳纤维材料或碳纤维织物表面均匀涂覆预浸料，形成碳纤维复合材料。
3）制作产品型腔模具，在模具表面涂抹脱模计。
4）碳纤维复合材料经过传送带进入加热引导机构，加热后放入型腔模具。
5）将型腔模具合模后预热，同时对模具进行抽真空。
6）在真空环境下进行热压成型，待冷却后脱模，得到碳纤维和酚醛树脂复合材料的成型产品。
优选的，所述步骤5）中，预热温度为60-70℃，预热时间为3-5min。
优选的，所述步骤5）中，真空度为-0.1MPa。
优选的，所述步骤6）中，热压成型的温度为150-200℃，热压成型的时间为12-14小时。
本发明的有益效果是：本发明含胶量大、二次成型界面粘结强度高、固化工艺合理，加压点控制精准，能有效降低孔隙率，且操作简单、成本低廉。
具体实施方式
下面结合具体实施例对本发明进行详细说明
实施例1
一种碳纤维和酚醛树脂复合材料的成型工艺，包括下述步骤：
1）配制预浸料：取酚醛树脂和稀释剂按质量比5:1的比例混合均匀，控制其粘度为2.0Pa·S，所述稀释剂为丙酮或工业酒精。
2）涂覆：在碳纤维材料或碳纤维织物表面均匀涂覆预浸料，形成碳纤维复合材料。
3）制作产品型腔模具，在模具表面涂抹脱模计。
4）碳纤维复合材料经过传送带进入加热引导机构，加热后放入型腔模具。
5）将型腔模具合模后预热，同时对模具进行抽真空，预热温度为℃，预热时间为3min，真空度为-0.1MPa。
6）在真空环境下进行热压成型，温度为150℃，时间为12小时，待冷却后脱模，得到碳纤维和酚醛树脂复合材料。
实施例2
一种碳纤维和酚醛树脂复合材料的成型工艺，包括下述步骤：
1）配制预浸料：取酚醛树脂和稀释剂按质量比5:1的比例混合均匀，控制其粘度为2.3Pa·S，所述稀释剂为丙酮或工业酒精。
2）涂覆：在碳纤维材料或碳纤维织物表面均匀涂覆预浸料，形成碳纤维复合材料。
3）制作产品型腔模具，在模具表面涂抹脱模计。
4）碳纤维复合材料经过传送带进入加热引导机构，加热后放入型腔模具。
5）将型腔模具合模后预热，同时对模具进行抽真空，预热温度为67℃，预热时间为4min。真空度为-0.1MPa。
6）在真空环境下进行热压成型，温度为168℃，时间为13小时，待冷却后脱模，得到碳纤维和酚醛树脂复合材料的成型产品。
实施例3
一种碳纤维和酚醛树脂复合材料的成型工艺，包括下述步骤：
1）配制预浸料：取酚醛树脂和稀释剂按质量比5:1的比例混合均匀，控制其粘度为2.5Pa·S，所述稀释剂为丙酮或工业酒精。
2）涂覆：在碳纤维材料或碳纤维织物表面均匀涂覆预浸料，形成碳纤维复合材料。
3）制作产品型腔模具，在模具表面涂抹脱模计。
4）碳纤维复合材料经过传送带进入加热引导机构，加热后放入型腔模具。
5）将型腔模具合模后预热，同时对模具进行抽真空，预热温度为70℃，预热时间为5min。真空度为-0.1MPa。
6）在真空环境下进行热压成型，温度为200℃，时间为14小时，待冷却后脱模，得到碳纤维和酚醛树脂复合材料的成型产品。
Claims (4)
1.一种碳纤维和酚醛树脂复合材料的成型工艺，其特征在于：包括下述步骤：
1）配制预浸料：取酚醛树脂和稀释剂按质量比5:1的比例混合均匀，控制其粘度为2.0-2.5Pa·S，所述稀释剂为丙酮或工业酒精；
2）涂覆：在碳纤维材料或碳纤维织物表面均匀涂覆预浸料，形成碳纤维复合材料；
3）制作产品型腔模具，在模具表面涂抹脱模计；
4）碳纤维复合材料经过传送带进入加热引导机构，加热后放入型腔模具；
5）将型腔模具合模后预热，同时对模具进行抽真空；
6）在真空环境下进行热压成型，待冷却后脱模，得到碳纤维和酚醛树脂复合材料的成型产品。
2.根据权利要求1所述的碳纤维和酚醛树脂复合材料的成型工艺，其特征在于：所述步骤5）中，预热温度为60-70℃，预热时间为3-5min。
3.根据权利要求1所述的碳纤维和酚醛树脂复合材料的成型工艺，其特征在于：所述步骤5）中，真空度为-0.1MPa。
4.根据权利要求1所述的碳纤维和酚醛树脂复合材料的成型工艺，其特征在于：所述步骤6）中，热压成型的温度为150-200℃，热压成型的时间为12-14小时。
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