CN109928721A - A kind of pug of high intensity health type Nixing pottery and the preparation process of vessel - Google Patents
A kind of pug of high intensity health type Nixing pottery and the preparation process of vessel Download PDFInfo
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- CN109928721A CN109928721A CN201910152032.6A CN201910152032A CN109928721A CN 109928721 A CN109928721 A CN 109928721A CN 201910152032 A CN201910152032 A CN 201910152032A CN 109928721 A CN109928721 A CN 109928721A
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- pug
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Abstract
The invention discloses the preparation processes of a kind of pug of high-intensitive health type Nixing pottery and vessel, the pug is in parts by weight, its component are as follows: 4~6 parts of auxiliary material of 20~40 parts of eastern mud, 60~80 parts of western mud, 0.01~0.04 part of tartaric acid, 0.1~0.4 part of molysite, 1~3 part of hydroxyapatite, 5~10 parts of conch meal, 1~2 part of titanium dioxide and firing, wherein the molysite is FeCl3、Fe(NO3)3Or Fe2(SO4)3, the firing auxiliary material is made of iron oxide, yttrium oxide and magnesia.Nixing pottery pug of the invention and vessel can greatly improve the flexibility of pug, pug avoided to hardening crack by adding tartaric acid and molysite in pug；And conch meal is added in pug, there is significant antibacterial bacteriostatic effect to bacteriums such as salmonella, yellow glucose fungus, conch meal can also absorb the harmful substances such as formaldehyde, benzene in air；Also, pug and vessel can efficiently inhibit long-term effectively and kill bacterium, press down mycostatic generation.
Description
Technical field
The invention belongs to the preparation technical fields of pottery, more particularly to the pug and device of a kind of high-intensitive health type Nixing pottery
The preparation process of ware.
Background technique
Nixing pottery admires the peculiar purplish red clay in the western two sides in the east of a river as raw material using Qinzhou, eastern mudding is closed storage, western mud
After fetching by four to six months or more sunshine, drenching with rain makes that its is granular, dissolution, oxidation, reach weathered state, using broken
Soil is mixed in the ratio of 4:6, pottery blank is made.Soft eastern mud is meat, and western mud is bone firmly, and bone and flesh is able to mutually support and pass through
Nixing pottery is fired after skill is fired and forms Nixing pottery.
Qiezhou Nixing pottery skill works were participated in 1915 and obtain gold in the international fair that Panama, U.S. San Francisco is held
Prize ranks the big name pottery of China four.It enjoys great prestige at home and abroad with Jiangsu's purple sand ceramics, Yunnan Jian Shui pottery, Sichuan Rong Chang pottery.In the last hundred years,
International and national exhibition is repeatedly participated in appraise through comparison and obtain that Grand Prix 40 is multinomial, and Nixing pottery product is exported to Southeast Asia, Eastern Europe, America
And more than 30 a countries and regions such as Chinese Hong Kong, Macao and Taiwan.Nixing pottery is liked by more and more users, more and more
People used Nixing pottery as daily necessities.
The production process of Nixing pottery, which generally comprises, at present takes soil, hack, prepares blank, molding, repaired biscuit, dry in the shade, examine hair
Base, firing, checks and accepts product, polishing at decoration.However the prior art, during execution, those skilled in the art at least have found
Following technical problem:
1) Nixing pottery montmorillonite in sintering procedure is largely dehydrated, and montmorillonite toughness is poor, is extremely easy to cause green body
Cracking；
2) the frit overwhelming majority used in current Nixing pottery raw material contains some toxic compounds, such as lead compound, cadmium
Compound etc., although these compounds be made toxin after frit obtain it is a degree of efficiently control, dangerous things
Precipitation but can hardly be avoided；
3) existing Nixing pottery porcelain tool has a single function, and with economic continuous development, requirement of the people to life is also more next
It is higher, while the demand also to " the antibacterial, antibacterial " of ceramic daily necessities is higher and higher；The Nixing pottery porcelain tool of the prior art does not have
This effect.
Therefore, it is necessary to a kind of pug of high-intensitive health type Nixing pottery and the preparation process of vessel are provided, it is existing to solve
There is defect present in technology.
Summary of the invention
In order to solve the above technical problems, the present invention provides the preparation of the pug and vessel of a kind of high-intensitive health type Nixing pottery
Technique.
The present invention provides a kind of pug of high-intensitive health type Nixing pottery, in parts by weight, component are as follows: eastern mud 20~40
Part, 60~80 parts of western mud, 0.01~0.04 part of tartaric acid, 0.1~0.4 part of molysite, 1~3 part of hydroxyapatite, conch meal 5~
4~6 parts of auxiliary material of 10 parts, 1~2 part of titanium dioxide and firing.Herein it should be noted that in pug add tartaric acid and
Molysite can greatly improve the flexibility of pug, while the broken base that can effectively absorb generation of the green body in sintering procedure is answered
Power avoids pug from hardening cracking；And conch meal is added in pug, the plasticity of blank not only can be improved, also to Salmonella
The bacteriums such as bacterium, yellow glucose fungus have significant antibacterial bacteriostatic effect, and conch meal can also absorb the nocuousness such as formaldehyde, benzene in air
Substance；Also, hydroxyapatite, titanium dioxide are added in pug, titanium dichloride load is made into mud on hydroxyapatite
Emerging fictile can efficiently inhibit long-term effectively and kill bacterium, press down mycostatic generation.
Preferably, the pug of a kind of high-intensitive health type Nixing pottery, component are as follows: 30~35 parts of eastern mud, western mud 70
~75 parts, 0.03~0.038 part of tartaric acid, 0.2~0.3 part of molysite, 1~2 part of hydroxyapatite, 6~8 parts of conch meal, dioxy
Change 4~6 parts of auxiliary material of 1~2 part of titanium and firing.
Further embodiment is that the molysite is FeCl3、Fe(NO3)3Or Fe2(SO4)3。
Further embodiment is that the firing auxiliary material is made of iron oxide, yttrium oxide and magnesia.
Preferably, the weight ratio for firing iron oxide, yttrium oxide and magnesia in auxiliary material is 1:(0.5~1): (2~
4)。
A kind of preparation process of high-intensitive health type Nixing pottery vessel of the invention uses a kind of above-mentioned high-intensitive health
Type Nixing pottery pug, when preparation the following steps are included:
S100: the processing mixing of raw material；
Each raw material is weighed according to above-mentioned weight fraction ratio, eastern mud, western mud, hydroxyapatite, shell, titanium dioxide are added
Pulverizer is crushed to 200~400 mesh, is uniformly mixed, obtains mixture；Mixture is mixed with tartaric acid part, molysite then and is mixed
It is even；
S200: mixed pulp；
Ball mill is added in mixture, abrading-ball and water, 2~4h of ball milling in the case where revolving speed is 200~400r/min, separation mill
Ball is to get slurry；
S300: enter mold forming；
Auxiliary material will be fired and be crushed to 300~600 mesh, be uniformly mixed with slurry, obtain mixed slurry, then mixed slurry is injected
Vessel die for molding obtains vessel green body after aging 2~4 days；
S400: the firing of green body；
Green body is placed in kiln and is fired, kiln discharge after cooling polishes to get vessel.
Preferably, in s 200, the weight ratio of the abrading-ball and water is 1:(0.3~0.6): (0.3~0.8).
Preferably, in S300, slurry is injected in mold using slip casing by pressure or vacuum injection mode.
It is preferably, described that green body is placed in the specific steps fired in kiln in S400 are as follows:
S401: vessel green body is put into kiln, first will be warm in kiln with the heating rate for increasing 50~80 DEG C per hour
Degree rises to 400~480 DEG C, then is warming up to 1000~1300 DEG C to increase 100~150 DEG C of heating rate per hour；
S402: keeping 1000~1300 DEG C of high temperature, fires 1~2h；
S403: then cooling, the specific steps of the cooling are as follows: will with the cooling rate for reducing by 80~100 DEG C per hour
Kiln in-furnace temperature is down to 700~800 DEG C, then is down to 300~400 DEG C to reduce by 50~75 DEG C of cooling rate per hour, finally
Room temperature is down to the cooling rate for reducing by 150~200 DEG C per hour.
Compared with the relevant technologies, the invention has the following beneficial effects:
Nixing pottery pug of the invention and vessel can greatly improve mud by adding tartaric acid and molysite in pug
The flexibility of material, while the broken base stress of generation of the green body in sintering procedure can be effectively absorbed, avoid pug from hardening cracking；And
Conch meal is added in pug, the plasticity of blank not only can be improved, also to bacteriums such as salmonella, yellow glucose fungus
With significant antibacterial bacteriostatic effect, conch meal can also absorb the harmful substances such as formaldehyde, benzene in air；Also, add in pug
Enter hydroxyapatite, titanium dioxide, titanium dichloride load is enabled on hydroxyapatite Nixing pottery product long-term effectively
Efficiently inhibit and kill bacterium, presses down mycostatic generation.
Specific embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
In the present embodiment, the present invention provides a kind of pug of high-intensitive health type Nixing pottery, in parts by weight, component
Are as follows: 30 parts of eastern mud, 70 parts of western mud, 0.03 part of tartaric acid, 0.2 part of molysite, 1 part of hydroxyapatite, 6 parts of conch meal, titanium dioxide 1
4 parts of auxiliary material of part and firing.Herein it should be noted that adding tartaric acid and molysite in pug, pug can be greatly improved
Flexibility, while can effectively absorb the broken base stress of generation of the green body in sintering procedure, pug is avoided to hardening crack；And
Conch meal is added in pug, the plasticity of blank not only can be improved, also has to bacteriums such as salmonella, yellow glucose fungus
There is significant antibacterial bacteriostatic effect, conch meal can also absorb the harmful substances such as formaldehyde, benzene in air；Also, it is added in pug
Titanium dichloride load is enabled Nixing pottery product high long-term effectively by hydroxyapatite, titanium dioxide on hydroxyapatite
Effect inhibits and kills bacterium, presses down mycostatic generation.
The molysite is FeCl3、Fe(NO3)3Or Fe2(SO4)3。
The firing auxiliary material is made of iron oxide, yttrium oxide and magnesia.
The weight ratio of iron oxide, yttrium oxide and magnesia is 1:0.5:2 in the firing auxiliary material.
A kind of preparation process of high-intensitive health type Nixing pottery vessel of the invention uses a kind of above-mentioned high-intensitive health
Type Nixing pottery pug, when preparation the following steps are included:
S100: the processing mixing of raw material；
Each raw material is weighed according to above-mentioned weight fraction ratio, eastern mud, western mud, hydroxyapatite, shell, titanium dioxide are added
Pulverizer is crushed to 200 mesh, is uniformly mixed, obtains mixture；Mixture is mixed with tartaric acid part, molysite then and is mixed thoroughly；
S200: mixed pulp；
Ball mill is added in mixture, abrading-ball and water, the ball milling 2h in the case where revolving speed is 200r/min separates abrading-ball to get slurry
Material；
S300: enter mold forming；
Auxiliary material will be fired and be crushed to 300 mesh, be uniformly mixed with slurry, obtain mixed slurry, then mixed slurry is injected into vessel
Die for molding obtains vessel green body after aging 2 days；
S400: the firing of green body；
Green body is placed in kiln and is fired, kiln discharge after cooling polishes to get vessel.
Preferably, in s 200, the weight ratio of the abrading-ball and water is 1:0.3:0.4.
In S300, slurry is injected in mold using slip casing by pressure or vacuum injection mode.
It is described that green body is placed in the specific steps fired in kiln in S400 are as follows:
S401: vessel green body is put into kiln, first to increase 50 DEG C of heating rate per hour for kiln in-furnace temperature liter
1000 DEG C are warming up to 400 DEG C, then to increase 100 DEG C of heating rate per hour；
S402: keeping 1000 DEG C of high temperature, fires 1h；
S403: then cooling, the specific steps of the cooling are as follows: will be in kiln with the cooling rate for reducing by 80 DEG C per hour
Temperature is down to 700 DEG C, then is down to 300 DEG C to reduce by 50 DEG C of cooling rate per hour, finally to reduce by 150 DEG C of drop per hour
Warm speed is down to room temperature.
Embodiment 2
In the present embodiment, the present invention provides a kind of pug of high-intensitive health type Nixing pottery, in parts by weight, component
Are as follows: 35 parts of eastern mud, 75 parts of western mud, 0.038 part of tartaric acid, 0.3 part of molysite, 2 parts of hydroxyapatite, 8 parts of conch meal, titanium dioxide
2 parts and 6 parts of auxiliary material of firing.Herein it should be noted that adding tartaric acid and molysite in pug, mud can be greatly improved
The flexibility of material, while the broken base stress of generation of the green body in sintering procedure can be effectively absorbed, avoid pug from hardening cracking；And
Conch meal is added in pug, the plasticity of blank not only can be improved, also to bacteriums such as salmonella, yellow glucose fungus
With significant antibacterial bacteriostatic effect, conch meal can also absorb the harmful substances such as formaldehyde, benzene in air；Also, add in pug
Enter hydroxyapatite, titanium dioxide, titanium dichloride load is enabled on hydroxyapatite Nixing pottery product long-term effectively
Efficiently inhibit and kill bacterium, presses down mycostatic generation.
The molysite is FeCl3、Fe(NO3)3Or Fe2(SO4)3。
The firing auxiliary material is made of iron oxide, yttrium oxide and magnesia.
The weight ratio of iron oxide, yttrium oxide and magnesia is 1:1:4 in the firing auxiliary material.
A kind of preparation process of high-intensitive health type Nixing pottery vessel of the invention uses a kind of above-mentioned high-intensitive health
Type Nixing pottery pug, when preparation the following steps are included:
S100: the processing mixing of raw material；
Each raw material is weighed according to above-mentioned weight fraction ratio, eastern mud, western mud, hydroxyapatite, shell, titanium dioxide are added
Pulverizer is crushed to 400 mesh, is uniformly mixed, obtains mixture；Mixture is mixed with tartaric acid part, molysite then and is mixed thoroughly；
S200: mixed pulp；
Ball mill is added in mixture, abrading-ball and water, the ball milling 4h in the case where revolving speed is 400r/min separates abrading-ball to get slurry
Material；
S300: enter mold forming；
Auxiliary material will be fired and be crushed to 600 mesh, be uniformly mixed with slurry, obtain mixed slurry, then mixed slurry is injected into vessel
Die for molding obtains vessel green body after aging 4 days；
S400: the firing of green body；
Green body is placed in kiln and is fired, kiln discharge after cooling polishes to get vessel.
In s 200, the weight ratio of the abrading-ball and water is 1:0.6:0.8.
In S300, slurry is injected in mold using slip casing by pressure or vacuum injection mode.
It is described that green body is placed in the specific steps fired in kiln in S400 are as follows:
S401: vessel green body is put into kiln, first to increase 80 DEG C of heating rate per hour for kiln in-furnace temperature liter
1300 DEG C are warming up to 480 DEG C, then to increase 150 DEG C of heating rate per hour；
S402: keeping 1300 DEG C of high temperature, fires 2h；
S403: then cooling, the specific steps of the cooling are as follows: to reduce by 100 DEG C of cooling rate per hour for kiln
Interior temperature is down to 800 DEG C, then is down to 400 DEG C to reduce by 75 DEG C of cooling rate per hour, finally to reduce by 200 DEG C per hour
Cooling rate is down to room temperature.
Embodiment 3
In the present embodiment, the present invention provides a kind of pug of high-intensitive health type Nixing pottery, in parts by weight, component
Are as follows: 33 parts of eastern mud, 73 parts of western mud, 0.036 part of tartaric acid, 0.25 part of molysite, 1.5 parts of hydroxyapatite, 7 parts of conch meal, dioxy
Change 5 parts of auxiliary material of 1.5 parts of titanium and firing.Herein it should be noted that adding tartaric acid and molysite in pug, can mention significantly
The flexibility of high pug, while the broken base stress of generation of the green body in sintering procedure can be effectively absorbed, avoid pug from hardening cracking；
And conch meal is added in pug, the plasticity of blank not only can be improved, also to salmonella, yellow glucose fungus etc.
Bacterium has significant antibacterial bacteriostatic effect, and conch meal can also absorb the harmful substances such as formaldehyde, benzene in air；Also, in pug
Middle addition hydroxyapatite, titanium dioxide, enable Nixing pottery product to have for a long time titanium dichloride load on hydroxyapatite
Effect ground efficiently inhibits and kills bacterium, presses down mycostatic generation.
The molysite is FeCl3、Fe(NO3)3Or Fe2(SO4)3。
The firing auxiliary material is made of iron oxide, yttrium oxide and magnesia.
Preferably, the weight ratio for firing iron oxide, yttrium oxide and magnesia in auxiliary material is 1:0.8:3.
A kind of preparation process of high-intensitive health type Nixing pottery vessel of the invention uses a kind of above-mentioned high-intensitive health
Type Nixing pottery pug, when preparation the following steps are included:
S100: the processing mixing of raw material；
Each raw material is weighed according to above-mentioned weight fraction ratio, eastern mud, western mud, hydroxyapatite, shell, titanium dioxide are added
Pulverizer is crushed to 300 mesh, is uniformly mixed, obtains mixture；Mixture is mixed with tartaric acid part, molysite then and is mixed thoroughly；
S200: mixed pulp；
Ball mill is added in mixture, abrading-ball and water, the ball milling 3h in the case where revolving speed is 300r/min separates abrading-ball to get slurry
Material；
S300: enter mold forming；
Auxiliary material will be fired and be crushed to 450 mesh, be uniformly mixed with slurry, obtain mixed slurry, then mixed slurry is injected into vessel
Die for molding obtains vessel green body after aging 3 days；
S400: the firing of green body；
Green body is placed in kiln and is fired, kiln discharge after cooling polishes to get vessel.
Preferably, in s 200, the weight ratio of the abrading-ball and water is 1:0.45:0.5.
Preferably, in S300, slurry is injected in mold using slip casing by pressure or vacuum injection mode.
It is preferably, described that green body is placed in the specific steps fired in kiln in S400 are as follows:
S401: vessel green body is put into kiln, first to increase 65 DEG C of heating rate per hour for kiln in-furnace temperature liter
1150 DEG C are warming up to 440 DEG C, then to increase 125 DEG C of heating rate per hour；
S402: keeping 1150 DEG C of high temperature, fires 1.5h；
S403: then cooling, the specific steps of the cooling are as follows: will be in kiln with the cooling rate for reducing by 90 DEG C per hour
Temperature is down to 750 DEG C, then is down to 350 DEG C to reduce by 63 DEG C of cooling rate per hour, finally to reduce by 175 DEG C of drop per hour
Warm speed is down to room temperature.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (9)
1. a kind of pug of high intensity health type Nixing pottery, which is characterized in that in parts by weight, component are as follows: eastern mud 20~40
Part, 60~80 parts of western mud, 0.01~0.04 part of tartaric acid, 0.1~0.4 part of molysite, 1~3 part of hydroxyapatite, conch meal 5~
4~6 parts of auxiliary material of 10 parts, 1~2 part of titanium dioxide and firing.
2. a kind of high-intensitive health type Nixing pottery pug as described in claim 1, which is characterized in that in parts by weight, group
It is divided into: 30~35 parts of eastern mud, 70~75 parts of western mud, 0.03~0.038 part of tartaric acid, 0.2~0.3 part of molysite, hydroxyapatite 1
4~6 parts of auxiliary material of~2 parts, 6~8 parts of conch meal, 1~2 part of titanium dioxide and firing.
3. a kind of high-intensitive health type Nixing pottery pug as claimed in claim 1 or 2, which is characterized in that the molysite is
FeCl3、Fe(NO3)3Or Fe2(SO4)3。
4. a kind of high-intensitive health type Nixing pottery pug as claimed in claim 1 or 2, which is characterized in that the firing auxiliary material
It is made of iron oxide, yttrium oxide and magnesia.
5. a kind of high-intensitive health type Nixing pottery pug as claimed in claim 4, which is characterized in that oxygen in the firing auxiliary material
The weight ratio for changing iron, yttrium oxide and magnesia is 1:(0.5~1): (2~4).
6. a kind of preparation process of high intensity health type Nixing pottery vessel, which is characterized in that any using such as Claims 1 to 5
A kind of described high-intensitive health type Nixing pottery pug, when preparation the following steps are included:
S100: the processing mixing of raw material；
Each raw material is weighed according to above-mentioned weight fraction ratio, eastern mud, western mud, hydroxyapatite, shell, titanium dioxide are added and crushed
Machine is crushed to 200~400 mesh, is uniformly mixed, obtains mixture；Mixture is mixed with tartaric acid part, molysite then and is mixed thoroughly；
S200: mixed pulp；
Ball mill is added in mixture, abrading-ball and water, 2~4h of ball milling in the case where revolving speed is 200~400r/min separates abrading-ball, i.e.,
Obtain slurry；
S300: enter mold forming；
Auxiliary material will be fired and be crushed to 300~600 mesh, be uniformly mixed with slurry, obtain mixed slurry, then mixed slurry is injected into vessel
Die for molding obtains vessel green body after aging 2~4 days；
S400: the firing of green body；
Green body is placed in kiln and is fired, kiln discharge after cooling polishes to get vessel.
7. a kind of preparation process of high-intensitive health type Nixing pottery vessel as claimed in claim 6, which is characterized in that in S200
In, the weight ratio of the abrading-ball and water is 1:(0.3~0.6): (0.3~0.8).
8. a kind of preparation process of high-intensitive health type Nixing pottery vessel as claimed in claim 6, which is characterized in that in S300
In, slurry is injected in mold using slip casing by pressure or vacuum injection mode.
9. a kind of preparation process of high-intensitive health type Nixing pottery vessel as claimed in claim 6, which is characterized in that in S400
In, it is described that green body is placed in the specific steps fired in kiln are as follows:
S401: vessel green body is put into kiln, first to increase 50~80 DEG C of heating rate per hour for kiln in-furnace temperature liter
1000~1300 DEG C are warming up to 400~480 DEG C, then to increase 100~150 DEG C of heating rate per hour；
S402: keeping 1000~1300 DEG C of high temperature, fires 1~2h；
S403: then cooling, the specific steps of the cooling are as follows: to reduce by 80~100 DEG C of cooling rate per hour for kiln
Interior temperature is down to 700~800 DEG C, then is down to 300~400 DEG C to reduce by 50~75 DEG C of cooling rate per hour, finally with every
The cooling rate that hour reduces by 150~200 DEG C is down to room temperature.
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| JPH11116956A (en) * | 1997-10-17 | 1999-04-27 | Taki Chem Co Ltd | Hardening of water glass for grout |
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| CN104150870A (en) * | 2014-07-31 | 2014-11-19 | 钦州市登峰陶艺有限公司 | Clay of nixing pottery |
| CN108530026A (en) * | 2018-06-30 | 2018-09-14 | 鹿寨知航科技信息服务有限公司 | A kind of heat-insulated Nixing pottery product of health and its preparation process |
| CN108658577A (en) * | 2018-05-28 | 2018-10-16 | 钦州学院 | The manufacture craft of high intensity Nixing pottery |
| CN108751946A (en) * | 2018-06-30 | 2018-11-06 | 鹿寨知航科技信息服务有限公司 | A kind of antibacterial heat preservation Nixing pottery teacup and its processing method |
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2019
- 2019-02-28 CN CN201910152032.6A patent/CN109928721A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11116956A (en) * | 1997-10-17 | 1999-04-27 | Taki Chem Co Ltd | Hardening of water glass for grout |
| WO2006027593A2 (en) * | 2004-09-10 | 2006-03-16 | Dytech Corporation Limited | Gelcasting of a ceramic catalyst carrier |
| CN104150870A (en) * | 2014-07-31 | 2014-11-19 | 钦州市登峰陶艺有限公司 | Clay of nixing pottery |
| CN108658577A (en) * | 2018-05-28 | 2018-10-16 | 钦州学院 | The manufacture craft of high intensity Nixing pottery |
| CN108530026A (en) * | 2018-06-30 | 2018-09-14 | 鹿寨知航科技信息服务有限公司 | A kind of heat-insulated Nixing pottery product of health and its preparation process |
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Application publication date: 20190625 |