CN1099014A - Light silencing and refractory mineral decoration board and working method thereof - Google Patents

Light silencing and refractory mineral decoration board and working method thereof Download PDF

Info

Publication number
CN1099014A
CN1099014A CN 93109717 CN93109717A CN1099014A CN 1099014 A CN1099014 A CN 1099014A CN 93109717 CN93109717 CN 93109717 CN 93109717 A CN93109717 A CN 93109717A CN 1099014 A CN1099014 A CN 1099014A
Authority
CN
China
Prior art keywords
parts
decoration board
working method
water
refractory mineral
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 93109717
Other languages
Chinese (zh)
Other versions
CN1034728C (en
Inventor
李苏璋
郭冬发
高必娥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Research Institute of Uranium Geology
Original Assignee
Beijing Research Institute of Uranium Geology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing Research Institute of Uranium Geology filed Critical Beijing Research Institute of Uranium Geology
Priority to CN93109717A priority Critical patent/CN1034728C/en
Publication of CN1099014A publication Critical patent/CN1099014A/en
Application granted granted Critical
Publication of CN1034728C publication Critical patent/CN1034728C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/24Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
    • C04B28/26Silicates of the alkali metals
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/52Sound-insulating materials

Abstract

The invention discloses a kind of lightweight, silencing and refractory mineral decoration board and working method of making by expanded vermiculite, tackiness agent, additive and water-resisting agent thereof.The normal temperature pressurization is adopted in this invention, and the dry maintaining process of gradient increased temperature makes the product percent of pass height, has the advantages that technology is simple, cost is low.

Description

Light silencing and refractory mineral decoration board and working method thereof
The invention belongs to architectural decoration material field, be specifically related to a kind of light silencing and refractory mineral decoration board and working method thereof.
Generally adopt plasterboard and stone(mine)cotton plate as indoor furred ceiling or adherent decoration at present both at home and abroad.But plasterboard unit weight is big, sound absorbing coefficient is little, the moisture-sensitive distortion, and contain the shortcomings such as fiber that are unfavorable for HUMAN HEALTH; Stone(mine)cotton plate generally all adopts organic binder bond to process, and needs top coat, and fire resistance period is short, and poisonous in the course of processing, flavor, contaminate environment are arranged, harmful HUMAN HEALTH is unfavorable for that the workman operates.U.S. Pat 3778281 discloses a kind ofly makes light-weight refractory sheet material and working method thereof by materials such as vermiculite, clay and borates.The weak point of this sheet material is a processed complex, must roasting under 1300 temperature condition, and hot pressing under 400 temperature condition.
The object of the invention provides a kind of fibrous magnesium silicate that do not contain, and fire resistance period is long, and sound absorbing coefficient is big, and unit weight is little, without the decorative sheet and the working method thereof of high-temperature molding.
Technical scheme of the present invention is: the raw material of this decorative sheet consists of (weight percent): 100~300 parts of expanded vermiculites, 100~200 parts of inorganic adhesives, 5~20 parts of additives, 5~15 parts of water-resisting agents.The consisting of of inorganic adhesive (parts by weight): 1~20 part of potassium silicate solution, 1~6 part of silicon sol, 0~0.5 part of superpolymer, 0.1~0.5 part in water.The consisting of of additive (weight percent): 1~5 part of potassium primary phosphate, 0~10 part of Calcium Chloride Powder Anhydrous, 2~50 parts of semi-hydrated gypsums, 0.5~2 part of potassium silicofluoride (or sodium).The consisting of of water-resisting agent (weight percent): 0.1~2 part of hydrogeneous methyl-silicone oil emulsion, 0.1~2 part of hydroxymethyl silicone oil emulsion.
The working method of this decorative sheet is: with 100~300 parts of granularities is 80~100 purpose expanded vermiculites, and 100~200 portions of inorganic adhesives stir after 5~20 parts of additives and 5~15 parts of water-resisting agents mix; With the mixture mould of packing into; Use the oil press extrusion forming down at normal temperature (room temperature); The demoulding; The moulding product are carried out getting product after the gradient increased temperature segmentation maintenance drying.
The preparation method of inorganic adhesive is: with 1~20 part of potassium silicate solution, 1~6 part of silicon sol, 0~0.5 part of superpolymer and 0.1~0.5 part of water mixing post-heating stir to specific viscosity be 40~60 seconds.The preparation method of additive is: with 1~5 part of potassium primary phosphate, and 0~10 part of Calcium Chloride Powder Anhydrous, 2~50 parts of semi-hydrated gypsums, 0.5~2 part of potassium silicofluoride (or sodium) mixes, and grinds evenly on ball mill.The preparation method of water-resisting agent is: with 0.1~2 part of hydrogeneous methyl-silicone oil emulsion, stir after 0.1~2 part of hydroxymethyl silicone oil emulsion mixes.Gradient increased temperature segmentation maintenance drying is that advanced trip temperature is 40~60 ℃ of maintenance dryings under the condition, and carrying out temperature again is 80~100 ℃ of maintenance dryings under the condition.
Advantage of the present invention is: product has lightweight, sound-absorbing and fireproof characteristics; Simple and convenient processing method, nontoxic in the production process, harmless, pollution-free; Adopt normal temperature pressurization, gradient increased temperature segmentation maintenance drying process, improved product qualified rate and production efficiency greatly, reduced production cost.
Embodiment 1:
Get expanded vermiculite 2000g, additive 70g, water-resisting agent 45ml, tackiness agent 1600ml stirs in agitator, takes out material, with its mould (600 * 600 * 45mm) of packing into, extrusion forming on oil press after the demoulding, is delivered to the moulding product in the curing means and to be warmed up to 80 ℃ after 2 hours in 50 ℃ of following maintenances, continue maintenance 2 hours, promptly get the light silencing and refractory mineral decoration board of 600 * 600 * 10mm.Decorative sheet has following physical property after tested:
Specification: 600 * 600 * 10mm; Unit weight 631g/cm 2; Folding strength 0.83MPa; Bending strength 0.78MPa; Thermal conductivity 0.11w/mk; Sound absorbing coefficient 0.3~0.48; 1000 ℃ of constant temperature of fire resistance period did not burn in 1 hour, did not subside weight loss 16.12%; Water ratio 5%; Rate of moisture absorption (24 hours) 3.1%; Water-intake rate (24 hours) 28~30%; Surface pH value 7~8.
Wherein the preparation method of tackiness agent is: get potassium silicate solution 2000g, silicon sol 1000g, superpolymer 10g, water 100g is in the enamel reaction cylinder, 80 ℃ of following heated and stirred 2 hours, promptly get required tackiness agent, its specific viscosity is 50 seconds ± 5 seconds under 25 ℃ ± 5 ℃.
The preparation method of additive is: get potassium primary phosphate 100g, and semi-hydrated gypsum 500g, potassium silicofluoride 50g ground 1 hour on small grinder, promptly got desired additives.Or get potassium primary phosphate 50g, and Calcium Chloride Powder Anhydrous 50g, semi-hydrated gypsum 400g, Sodium Silicofluoride 100g ground 1 hour on little ball mill, promptly got desired additives.Or get potassium primary phosphate 10g, and semi-hydrated gypsum 100g, potassium silicofluoride 100g, Calcium Chloride Powder Anhydrous 100g ground 1 hour on small grinder, promptly got desired additives.
The preparation method of water-resisting agent is: with hydrogeneous methyl-silicone oil emulsion 50ml, hydroxymethyl silicone oil emulsion 50ml mixes and promptly gets required water-resisting agent.
Embodiment 2:
Get expanded vermiculite 2000g, additive 50g, water-resisting agent 40ml, tackiness agent 2000ml stirs in agitator, take out material, with its mould of packing into (600 * 600 * 45mm), extrusion forming on oil press, after the demoulding finished product delivered to and be warmed up to 85 ℃ after 2 hours in 45 ℃ of thermostatic curings in the curing means and continued thermostatic curings 2 hours, promptly get the light silencing and refractory mineral decoration board of 600 * 600 * 10mm.

Claims (10)

1, a kind of is the light silencing and refractory mineral decoration board that main raw material processes by expanded vermiculite, the raw material that it is characterized in that this sheet material consists of (parts by weight): 100~300 parts of expanded vermiculites, 100~200 parts of inorganic adhesives, 5~20 parts of additives, 5~15 parts of water-resisting agents.
2, light silencing and refractory mineral decoration board as claimed in claim 1 is characterized in that consist of (parts by weight) of described inorganic adhesive: 1~20 part of potassium silicate solution, 1~5 part of silicon sol, 0~0.5 part of superpolymer, 0.1~0.5 part in water.
3, light silencing and refractory mineral decoration board as claimed in claim 1 is characterized in that consist of (parts by weight) of described additive: 1~5 part of potassium primary phosphate, 0~10 part of Calcium Chloride Powder Anhydrous, 2~50 parts of semi-hydrated gypsums, 0.5~2 part of potassium silicofluoride.
4, light silencing and refractory mineral decoration board as claimed in claim 1 is characterized in that consist of (parts by weight) of described additive: 1~5 part of potassium primary phosphate, 0~10 part of Calcium Chloride Powder Anhydrous, 2~50 parts of semi-hydrated gypsums, 0.5~2 part of Sodium Silicofluoride.
5, light silencing and refractory mineral decoration board as claimed in claim 1 is characterized in that consist of (parts by weight) of described water-resisting agent: 0.1~2 part of hydrogeneous methyl-silicone oil emulsion, 0.1~2 part of hydroxymethyl silicone oil emulsion.
6, a kind of working method of decorative sheet as claimed in claim 1 is characterized in that with 100~300 parts of granularities be 80~100 purpose expanded vermiculites, and 100~200 portions of inorganic adhesives stir after 5~20 parts of additives and 5~15 parts of water-resisting agents mix; With the mixture mould of packing into; Use the oil press extrusion forming down at normal temperature (room temperature); The demoulding; The moulding product are carried out getting product after the gradient increased temperature segmentation maintenance drying.
7, the working method of decorative sheet as claimed in claim 6, the preparation method who it is characterized in that described inorganic adhesive is: with 1~20 part of potassium silicate solution, it is to get final product in 40~60 seconds that 1~6 part of silicon sol, 0~0.5 part of superpolymer and 0.1~0.5 part of water mixing post-heating stir to specific viscosity.
8, the working method of decorative sheet as claimed in claim 6, the preparation method who it is characterized in that described additive is: 1~5 part of potassium primary phosphate, 0~10 part of Calcium Chloride Powder Anhydrous, 2~50 parts of semi-hydrated gypsums, 0.5~2 part of potassium silicofluoride (or sodium) are mixed, grind on small grinder and evenly get final product.
9, the working method of decorative sheet as claimed in claim 6 is characterized in that the preparation method of described water-resisting agent is: with 0.1~2 part of hydrogeneous methyl-silicone oil emulsion, stirring after 0.1~2 part of hydroxymethyl silicone oil emulsion mixes gets final product.
10, the working method of decorative sheet as claimed in claim 6 is characterized in that described gradient increased temperature segmentation maintenance drying is meant that advanced trip temperature is 40~60 ℃ of maintenance dryings under the condition, and carrying out temperature again is 80~100 ℃ of maintenance dryings under the condition.
CN93109717A 1993-08-14 1993-08-14 Light silencing and refractory mineral decoration board and its processing method Expired - Fee Related CN1034728C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN93109717A CN1034728C (en) 1993-08-14 1993-08-14 Light silencing and refractory mineral decoration board and its processing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN93109717A CN1034728C (en) 1993-08-14 1993-08-14 Light silencing and refractory mineral decoration board and its processing method

Publications (2)

Publication Number Publication Date
CN1099014A true CN1099014A (en) 1995-02-22
CN1034728C CN1034728C (en) 1997-04-30

Family

ID=4987756

Family Applications (1)

Application Number Title Priority Date Filing Date
CN93109717A Expired - Fee Related CN1034728C (en) 1993-08-14 1993-08-14 Light silencing and refractory mineral decoration board and its processing method

Country Status (1)

Country Link
CN (1) CN1034728C (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101767973B (en) * 2009-12-30 2012-02-29 范金凤 Production process of pearlstone decoration acoustic panel
CN103435283A (en) * 2013-08-16 2013-12-11 北京理工大学 Inorganic adhesive used for shaping of swelling silicate material, and preparation method of same
CN104891944A (en) * 2015-05-21 2015-09-09 安徽鑫润新型材料有限公司 Double-layer composite glass magnesium board with high fireproof grade and preparation method of double-layer composite glass magnesium board
CN108026725A (en) * 2015-09-23 2018-05-11 韩国维尔美株式会社 Ultrathin architectural decoration vermiculite board
CN110015860A (en) * 2018-01-08 2019-07-16 北新集团建材股份有限公司 A kind of water-fast lightweight Thistle board and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3778281A (en) * 1971-12-16 1973-12-11 Grace W R & Co Fusion bonded vermiculite molding material

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101767973B (en) * 2009-12-30 2012-02-29 范金凤 Production process of pearlstone decoration acoustic panel
CN103435283A (en) * 2013-08-16 2013-12-11 北京理工大学 Inorganic adhesive used for shaping of swelling silicate material, and preparation method of same
CN103435283B (en) * 2013-08-16 2016-02-17 北京理工大学 Shaping inorganic adhesive of a kind of expanded silicate material and preparation method thereof
CN104891944A (en) * 2015-05-21 2015-09-09 安徽鑫润新型材料有限公司 Double-layer composite glass magnesium board with high fireproof grade and preparation method of double-layer composite glass magnesium board
CN108026725A (en) * 2015-09-23 2018-05-11 韩国维尔美株式会社 Ultrathin architectural decoration vermiculite board
US10450229B2 (en) 2015-09-23 2019-10-22 Vermikorea Co., Ltd. Slim vermiculite board for construction finishing
CN110015860A (en) * 2018-01-08 2019-07-16 北新集团建材股份有限公司 A kind of water-fast lightweight Thistle board and preparation method thereof

Also Published As

Publication number Publication date
CN1034728C (en) 1997-04-30

Similar Documents

Publication Publication Date Title
AU780369B2 (en) Composition for building material and building material
CN100358829C (en) Silicon magnesium fibre energy saving high strengthening composite building board of decoration and preparation process thereof
CN105236853B (en) A kind of composite stone material and preparation method thereof
CN102863189A (en) Preparation technique of waste residue composite light-weight thermal-insulation wallboard
CN103787642A (en) Efficient thermal insulation energy-saving material
CN101792290A (en) Composite silicate multifunctional paint and preparation method thereof
CN110698168A (en) Inorganic gelled biomass functional decorative plate and preparation method thereof
CN111571769A (en) Anion functional inorganic artificial marble block and microwave curing preparation process thereof
CN102910932A (en) Novel heat-insulation board for outer wall
KR101137176B1 (en) Eco-friendly volcanic stone using structural board and manufacturing method of that
CN1034728C (en) Light silencing and refractory mineral decoration board and its processing method
CN106242448A (en) A kind of aeroge is combined wood particle board and preparation method thereof
CN103723953A (en) Efficient thermal insulating energy-saving decorative plate
CN109020426A (en) Magnesial cementitious material and its preparation method on magnesium gelatinous material floor
CN103058598B (en) Production method of self-insulation block for building wall body
KR100548963B1 (en) Method of producing a porous building materials by using pearlite
CN109160797A (en) A kind of high-intensity anti-cracking plasterboard and preparation method thereof
CN102826789A (en) Fly-ash fiber heat-insulation acoustic board and preparation method thereof
CN108821695A (en) The formula and its production technology of ash wall body plate
CN107572947A (en) A kind of core for composite plate and preparation method thereof
CN107298572A (en) A kind of biomass gelling composite floor board and preparation method thereof
CN107021720A (en) A kind of high-strength insulation fire-fighting foam concrete and preparation method thereof
CN114315298A (en) Ardealite fireproof door core board and preparation method thereof
CN1927754A (en) Environment-friendly type energy-saving house heat-insulating material
CN1180921C (en) Process of making block using plaster as main raw material

Legal Events

Date Code Title Description
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C06 Publication
PB01 Publication
C14 Grant of patent or utility model
GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee