CN109875932A - A kind of toner and preparation method thereof - Google Patents

Abstract

The invention discloses a kind of toners and preparation method thereof, belong to cosmetic field.Include: to sequentially add water, moisturizer in stirring container, and heating the first scheduled duration makes temperature rise to the first preset temperature, and heats while stirring, and obtains the first mixed liquor, stops heating until being completely dissolved；Second preset temperature is cooled to the first mixed liquor, while being stirred after deodorant tune is added, and is cooled to third preset temperature, obtains toner.By toner prepared by the present invention is mild comfortably, fragrance harmony and natural, cost is relatively low.

Description

A kind of toner and preparation method thereof

Technical field

The present invention relates to cosmetic field more particularly to a kind of toners.

Background technique

Fragrance in cosmetics is mainly to pass through addition essence or essential oil obtains at present.Wherein add the cosmetics of essence Allergic reaction or phototoxic injury may be generated due to essence and to skin, and the fragrance that generates of essence not from So, it is difficult to the approval by customer.The price of essential oil is prohibitively expensive, can obviously increase cost, does not have good economy. And the fragrance of essential oil is excessively strong, and fragrance process is difficult to the harmony of fragrance.

Summary of the invention

The object of the invention is that overcome above-mentioned deficiency, a kind of toner and preparation method thereof is provided, by adding hydrosol, is kept away Exempt to use essence or essential oil in toner.Reaching keeps toner more mild comfortable non-stimulated and can reduce toner The production cost that middle blending uses.Using being used cooperatively for a variety of hydrosols, make the fragrance harmony and natural of toner.

To solve the above problems, one aspect of the present invention provides a kind of preparation method of toner, comprising:

S1: water, moisturizer are sequentially added in stirring container, and heat the first scheduled duration so that temperature is risen to first default Temperature, and heat while stirring, stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.

S2: the second preset temperature is cooled to the first mixed liquor, while being stirred after deodorant tune is added, and it is pre- to be cooled to third If temperature obtains toner.

Further, the deodorant tune includes rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon horse One of whip grass hydrosol, flores aurantii hydrosol, chamomile hydrosol are a variety of.Further, the moisturizer includes glycerol and/or third Glycol.

First scheduled duration is greater than or equal to 20 minutes.

First preset temperature is 80~85 DEG C.

Further, the step S1 specifically includes the following steps:

S11: taking parts by weight is that 20~50 parts of the water and 7~13 parts of the moisturizer sequentially add the stirring In container.

S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, increase fluid temperature To 80~85 DEG C.

S13: stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.

Further, the step S1 specifically includes the following steps:

S11 ': the water that parts by weight are 50~8020~50 parts is taken to be added in the stirring container.

S12 ': 3~5 parts of parts by weight of the glycerol is taken to be added in the stirring container.

S13 ': 4~8 parts of parts by weight of the propylene glycol is taken to be added in the stirring container.

S14 ': 0.01~0.05 part of xanthan gum of parts by weight, 0.01~0.05 part of sodium alginate, 0.05~0.15 are taken The gellan gum of part, 0.01~0.03 part of pectin are added in the stirring container；

S15 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, increase fluid temperature To 80~85 DEG C.

S16 ': stopping heating being completely dissolved up to the glycerol and the propylene glycol, obtains the first mixed liquor.

Further, the step S2 the following steps are included:

S21: to the cooling of the first mixed solution and when temperature is down to 45~55 DEG C, it is 2~50 parts that parts by weight, which are added, Rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, flores aurantii hydrosol, in chamomile hydrosol One or more deodorant tunes, stir evenly.

S22: continue to be cooled to 32~35 DEG C, discharging encapsulation obtains the toner.

Further, the deodorant tune further includes white pond lily hydrosol and/or lotus hydrosol.

Shown deodorant tune further includes Rhododendron fastigiatum extracting solution.

Further, the step S2 the following steps are included:

S21 ': cool down to the first mixed solution.

S22 ': when temperature is down to 45~55 DEG C, taking parts by weight is that stirring is added in 10~15 parts of Rhododendron fastigiatum extracting solutions In container, take parts by weight be 15~20 parts of rose, 5~10 parts of flores aurantii hydrosol, 3~8 parts of bodhi hydrosols, 3~ 10 parts of balm hydrosols, 3~8 parts of white pond lily hydrosols and/or 2~4 parts of lotus hydrosols are added in the stirring container and stir equal It is even.

S23 ': continue to be cooled to 32~35 DEG C, discharging encapsulation obtains the toner.

Further, the step S2 the following steps are included:

S21 ": cool down to the first mixed solution；

S22 ": when temperature is down to 45~55 DEG C, taking parts by weight is 12~18 parts of sweet osmanthus hydrosol, 8~12 parts of lemon Lemon Verbena officinalis hydrosol, 2~5 parts of bodhi hydrosols, 4.5~9 parts of balm hydrosols, 3~8 parts of white pond lily hydrosols and/or 2~4 parts Lotus hydrosol is added in the stirring container and stirs evenly；

S23 ": the safflower petal that parts by weight are 0.5~1.5 part is taken to be added in the stirring container and stir evenly.

S24 ": continue to be cooled to 32~35 DEG C, discharging encapsulation obtains the toner.

The another aspect of of the invention one provides a kind of toner, uses toner preparation method system described in any of the above-described It is standby to form.

The preparation method of toner provided by the invention, using the by-product hydrosol during extraction of essential oil replace essence and The use of essential oil, which can not only reduce cost, can also make fragrance more harmony and natural, stimulate toner mildly not.Hydrosol is essential oil A kind of byproduct, composition is naturally pure, and fragrance is light pleasant, and a variety of hydrosols keep the fragrance in toner rich Level, smell are novel, are liked by customer.

Specific embodiment

In order to make the objectives, technical solutions and advantages of the present invention clearer, With reference to embodiment, to this Invention is further described.It should be understood that these descriptions are merely illustrative, and it is not intended to limit the scope of the invention.This Outside, in the following description, descriptions of well-known structures and technologies are omitted, so as not to unnecessarily obscure the concept of the present invention.

According to the application embodiment, a kind of preparation method of toner, comprising the following steps:

S1: water, moisturizer are sequentially added in stirring container, and heat the first scheduled duration so that temperature is risen to first default Temperature, and heat while stirring, stopping heating being completely dissolved up to moisturizer, obtains the first mixed liquor.Wherein, water can be pure Water purification, deionized water or cosmetics dedicated water, but be not limited to it is above-mentioned enumerate, preferably deionized water.

S2: the second preset temperature is cooled to the first mixed liquor, while being stirred after deodorant tune is added, and it is pre- to be cooled to third If temperature obtains toner.Wherein cool-down method can be cold cooling water cycle water, fan for cooling and natural cooling, but unlimited It is enumerated in above-mentioned, preferably natural cooling.

In an alternative embodiment, deodorant tune includes rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon One of lemon Verbena officinalis hydrosol, flores aurantii hydrosol, chamomile hydrosol are a variety of.Hydrosol, refer to essential oil during distillation extraction, The distillation stoste that the one kind 100% separated when refining essential oil is saturated, is a kind of byproduct of essential oil, composition is naturally pure Only, fragrance is light pleasant.Use hydrosol that can prevent to generate the bad of allergy because essence is added well as deodorant tune Reaction.Also there is no essential oil blending because essential oil fragrance is excessively strong and it is discordant to lead to the problem of smell.Wherein, in the present invention Deodorant tune can also be other hydrosols for applying to cosmetic industry；Or the fragrance in plant is extracted using grease, such as use Absolute oil etc..

Wherein, rose is that the way of distillation is refined, and just has slightly sour taste by high temperature and pressure, what essence blended out Product does not have the taste of draft.Include inside rose is the volatile aromatic ingredient of a large amount of fresh rose flower, it is simultaneously Fragrance ingredient containing macromolecular.Have the effects that keep the skin wet, moisturizing, quick anti-inflammatory, antiallergy, it is antipruritic, delay senescence.

Bodhi hydrosol has the fresh breath with a small gangs of wheat beer again of some fragrance of a flower.Releive with moisturizing, desalinate it is black Spot, the effect repaired damage, resist aging, smoothing wrinkle, consolidation, anti-inflammatory.

Contain the substances such as sweet osmanthus alcohol, palmitinic acid, lauric acid, linalool and irisone in sweet osmanthus hydrosol.Content is high Irisone, so the violet keynote as typical fruity can be drifted after dilution.With exclusion toxin, Whitening, spot, moisturizing The effect of anti-ageing, consolidation skin.

Balm hydrosol smell is lighter, with bitter lemonene.Has effects that anti-oxidant and anti-inflammatory.

The smell of lemon verbena hydrosol is simple and elegant, mixes the salubrious of green grass tender shoots with a lemonene, is very easy to allow People receives.Have effects that restrain anti-inflammatory, disinfection and sterilization.

Flores aurantii hydrosol (flavouring agent, skin whitening, moisturizing ingredient) containing thatch alcohol, linalool, young tiger geraniol, nerol, stupid ethyl alcohol, Geraniol, rose oxide, rosefuran, with Quercetin, flavonoids, tannin, vitamin B and vitamin E, beta carotene and more Kind amino acid, several mineral materials.Smell has the lily flowery odour of a bitter taste, flavour of a drug.Have both the double action of whitening and moisturizing.

Chamomile hydrosol smell is strong, has the sense of moisturizing antiallergic, eliminates skin sensitivity, go black eye, restrains, anti-inflammatory, disappears The effect of swollen analgesic, elimination red capillary, tightening pore, calm skin.

Deodorant tune be preferably rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, Two or more composition in flores aurantii hydrosol, chamomile hydrosol, the compound fragrance of a flower that a variety of hydrosols generate can more make us Pleasure is further preferably rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, orange The deodorant tune of flower hydrosol, four kinds of hydrosols composition in chamomile hydrosol, be further preferably rose, bodhi hydrosol, Flores aurantii hydrosol, balm hydrosol, another is preferably that bodhi hydrosol, sweet osmanthus hydrosol, lemon verbena hydrosol, chamomile are pure Dew.The smell of preferred hydrosol collocation is more coordinated, and mixed flavor can make one to feel comfortable.

In an alternative embodiment,

Moisturizer includes glycerol and/or propylene glycol.

First scheduled duration is greater than or equal to 20 minutes.

First preset temperature is 80~85 DEG C.

The step S1 includes sequentially adding water, glycerol, propylene glycol, xanthan gum, sodium alginate, gellan gum, pectin to stir Mix in container, and heating the first scheduled duration makes temperature rise to the first preset temperature, and heats while stirring, stop heating until The moisturizer is completely dissolved, and obtains the first mixed liquor.

Xanthan gum, sodium alginate, gellan gum, pectin are polysaccharide natural polymers, can make toner viscosity improve and It is not easy drippage during smearing to cause to waste, keeps toner more stable, the petal that can make to add in toner is outstanding It is floating, it is improved toner appearance.Polysaccharide natural polymer is not easy the generation precipitating that reacts with metal ion.Make product Appearance long term storage is also able to maintain beauty.Xanthan gum, sodium alginate, gellan gum, pectin and carragheen and skin affinity are good, make With more comfortable on the skin, it is added in cosmetics and use feeling can be improved.

In the present embodiment, first scheduled duration can for 20 minutes, 21 minutes, 22 minutes, 23 minutes, 25 minutes, 28 minutes, 32 minutes, 37 minutes, 44 minutes, 48 minutes, 50 minutes, 55 minutes, 60 minutes etc. but be not limited to it is above-mentioned enumerate, can With according to the degree of the effect and dissolution that actually mix it is appropriate adjustment heating duration, preferably 20~60 minutes, into One step is preferably 25~35 minutes.First preset temperature can also be 81 DEG C, 82 DEG C, 83 DEG C, 84 DEG C but be not limited to above-mentioned column It lifts.It for example, can be increased or decreased according to environmental condition is appropriate to the first preset temperature, such as can be 80~100 DEG C, or Person is 70~85 DEG C.

In an alternative embodiment, step S1 specifically includes the following steps:

S11: taking parts by weight is that 20~50 parts of water and 7~13 parts of moisturizer sequentially add in stirring container.

In the present embodiment, the parts by weight of water can be 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 Part, 28 parts, 29 parts, 30 parts, 31 parts, 32 parts, 33 parts, 34 parts, 35 parts, 36 parts, 37 parts, 38 parts, 39 parts, 40 parts, 41 parts, 42 Part, 43 parts, 44 parts, 45 parts, 46 parts, 47 parts, 48 parts, 49 parts, 50 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixing Effect and other materials content adjustment water appropriate parts by weight, it is preferably 55~75 parts, further preferred It is 60~70 parts, such as can is 15~25 parts, 25~30 parts, 30~50 parts, or be 35~75 parts.The parts by weight of moisturizer Number can for 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts etc. but be not limited to it is above-mentioned enumerate, can be according to actually mixing The adjustment appropriate of the content of effect and other materials, such as can be 5~10 parts, 8~20 parts.

S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C.

S13: stopping heating being completely dissolved up to moisturizer, obtains the first mixed liquor.

In an alternative embodiment, step S1 specifically includes the following steps:

S11 ': the water that parts by weight are 20~50 parts is taken to be added in stirring container.

S12 ': 3~5 parts of parts by weight of glycerol is taken to be added in stirring container.The parts by weight of glycerol can be 3 parts, 4 Part, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 3~8 parts, 4 ~6 parts etc..

S13 ': 4~8 parts of parts by weight of propylene glycol is taken to be added in stirring container.The parts by weight of propylene glycol can be 4 Part, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can Think 2~6 parts, 5~10 parts etc..

S14 ': 0.01~0.05 part of xanthan gum of parts by weight, 0.01~0.05 part of sodium alginate, 0.05~0.15 are taken The gellan gum of part, 0.01~0.03 part of pectin are added in the stirring container.

Wherein xanthan gum can for 0.01 part, 0.02 part, 0.03 part, 0.04 part, 0.05 part etc. but be not limited to it is above-mentioned enumerate, Adjustment appropriate can be carried out according to the actual situation, and sodium alginate can be 0.01 part, 0.02 part, 0.03 part, 0.04 part, 0.05 It is part equal but be not limited to it is above-mentioned enumerate, adjustment appropriate can be carried out according to the actual situation, gellan gum can be 0.05 part, 0.06 Part, 0.07 part, 0.08 part, 0.09 part, 0.10 part, 0.11 part, 0.12 part, 0.13 part, 0.14 part, 0.15 part etc. but be not limited to It states and enumerates, adjustment appropriate can be carried out according to the actual situation, pectin can be for 0.01 part, 0.02 part, 0.03 part etc. but unlimited It is enumerated in above-mentioned, adjustment appropriate can be carried out according to the actual situation.

S15 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C.

S16 ': stopping heating being completely dissolved up to glycerol and propylene glycol, obtains the first mixed liquor.

It should be noted that S11 ', S12 ', S13 ', S14 ' and S15 ' are only the code name that step carries out, it is not offered as step The sequencing of execution also may be performed simultaneously for example, S11 '-S13 ' can be sequencing.

In an alternative embodiment, step S2 the following steps are included:

S21: to the cooling of the first mixed solution and when temperature is down to 45~55 DEG C, it is 2~20 parts that parts by weight, which are added, Rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, flores aurantii hydrosol, in chamomile hydrosol One or more deodorant tunes, stir evenly.

Being cooled to 45~55 DEG C can be 45 DEG C, 46 DEG C, 47 DEG C, 48 DEG C, 49 DEG C, 50 DEG C, 51 DEG C, 52 DEG C, 53 DEG C, 54 DEG C, 55 DEG C but be not limited to above-mentioned enumerate.For example, can be increased or decreased according to environmental condition is appropriate, for example, can for 35~ 50 DEG C, or be 52~62 DEG C.

S22: continue to be cooled to 32~35 DEG C, discharging encapsulation obtains toner.

Being cooled to 32~35 DEG C can be 32 DEG C, 33 DEG C, 34 DEG C, 35 DEG C but be not limited to above-mentioned enumerate.For example, can basis Environmental condition is appropriate to be increased or decreased, such as can be 20~32 DEG C, or be 33~40 DEG C.

The fragrance and effective component of hydrosol can not only be kept by adding plant hydrosol at 45~55 DEG C, moreover it is possible to keep toner mixed It closes uniformly, quality is more stable.

In an alternative embodiment, deodorant tune further includes white pond lily hydrosol and/or lotus hydrosol.

Deodorant tune further includes Rhododendron fastigiatum extracting solution.

Specifically can be with white pond lily hydrosol, can also be down to using lotus hydrosol, or can be slept simultaneously using white Lotus hydrosol and lotus hydrosol, are reconciled in proportion.

White pond lily hydrosol, lotus hydrosol used in the present embodiment, smell is simple and elegant pure and fresh, can make the gas between a variety of hydrosols Taste is more coordinated, and increases the fragrance of white pond lily, lotus in smell, both smells are more rare in toner, making The fragrance of adornment water is more novel.

Wherein Rhododendron fastigiatum (scientific name: Rhododendron fastigiatum), evergreen shrubs, 0.8-1 meters high, branch is thick It is close, often at cushion or prostrate.Sprout is short, band bronzing, by crineous scale.Leaf bud squama is caducous.Leaf collection is born in sprig top, leather Matter, oblong, ellipse or it is oval above dirty-green, below celadon.Inflorescence basidixed, the total shape of umbrella shape, there is colored 3-5；Corolla Wide funnel-form, 1-1.5 centimetres long, hyacinthine or fresh lilac red.Capsule oval.The month at florescence 5-6, the fruiting period 8-9 month.It is born in rock Slope, cliff, high mountain gravel meadow, tor shrubbery, rose bay shrublet or occasionally under pine forest, produce Qinghai, Sichuan, Yunnan.It should Species are because of flower beauty, bright-colored, artificial cultivation, horticultural importance with higher.

It is generally acknowledged that containing azalaic acid in azalea, also known as azelaic acid, azalaic acid have antibiotic property, and it is anti-to can be used as food Rotten agent.Just there is apparent antibacterial effect when azalaic acid concentration reaches 20%.

In an alternative embodiment, step S2 the following steps are included:

S21 ': cool down to the first mixed solution.

S22 ': taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in stirring containers, 45 are down to temperature~ At 55 DEG C, take parts by weight be 15~20 parts of rose, 5~10 parts of flores aurantii hydrosol, 3~8 parts of bodhi hydrosols, 3~ 10 parts of balm hydrosols, 3~8 parts of white pond lily hydrosols and/or 2~4 parts of lotus hydrosols are added in stirring container and stir evenly.It presses The fragrance for matching to obtain according to deodorant tune of the invention is more coordinated, and not in ratio range of the present invention, the harmony of fragrance becomes Difference.Being adjusted according to certain hydrosol proportion can make do not have the product quality of batch more stable, without by quality between hydrosol The influence of difference.

In the present embodiment, the parts by weight of Rhododendron fastigiatum extracting solution can for 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts it is equal but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 12~14 parts, 11 ~13 parts, or be 11.5~14.5 parts.The pleasantly surprised discovery Rhododendron fastigiatum extracting solution of inventor can not only reconcile various hydrosols Smell be allowed to more harmonious, there are also good bacteriostasis efficacy.When the parts by weight of addition are 10~15 parts, fungistatic effect reaches To best, good fungistatic effect can not be played when the parts by weight of addition are less than 10 parts, when the parts by weight of addition are greater than Fragrance can be made uncoordinated at 15 parts.

The parts by weight of rose can be 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts etc. but be not limited to above-mentioned column It lifts, can be according to the effect actually mixed adjustment appropriate, such as can be 10~15 parts, 18~25 parts, or be 5~25 Part.

The parts by weight of flores aurantii hydrosol can for 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to it is above-mentioned enumerate, can It with according to the effect actually mixed adjustment appropriate, such as can be 2~8 parts, 6~12 parts, or be 3~15 parts.

The parts by weight of bodhi hydrosol can for 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, Can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts, or be 6~15 parts.

The parts by weight of balm hydrosol can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to It is above-mentioned to enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~15 parts, or for 8~ 20 parts.

The parts by weight of white pond lily hydrosol can for 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, Can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts, or be 6~18 parts.

The parts by weight of lotus hydrosol can for 2 parts, 3 parts, 4 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixed The adjustment appropriate of the effect of conjunction, such as can be 1~6 part, 2~10 parts, or be 3~15 parts.S23 ': continue to be cooled to 32~ 35 DEG C, discharging encapsulation obtains toner.

In an alternative embodiment, step S2 the following steps are included:

S21 ": cool down to the first mixed solution.

S22 ": when temperature is down to 45~55 DEG C, the sweet osmanthus hydrosol, 8~12 parts that parts by weight are 12~18 parts are taken Lemon verbena hydrosol, 2~5 parts of bodhi hydrosols, 4.5~9 parts of balm hydrosols, 3~8 parts of white pond lily hydrosols and/or 2~ 4 parts of lotus hydrosols are added in stirring container and stir evenly.

The parts by weight of sweet osmanthus hydrosol can be 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts etc. but be not limited to It is above-mentioned to enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 5~15 parts, 15~20 parts, or be 16 ~25 parts.

The parts by weight of lemon verbena hydrosol can be 8 parts, 9 parts, 10 parts, 11 parts, 12 parts etc. but be not limited to above-mentioned column It lifts, can be according to the effect actually mixed adjustment appropriate, such as can be 4~8 parts, 10~15 parts, or be 6~18 parts.

S23 ": the safflower petal that parts by weight are 0.5~1.5 part is taken to be added in the stirring container and stir evenly.

Wherein safflower, (Classification system: Carthamus tinctorius L.), alias: red blue flower, thorn safflower, composite family, Safflower plant, dry tubular flower is orange red, and floral tube is narrow thin, and apex 5 is split, sliver narrow line shape, and anther yellow is unified into pipe, It is higher by except sliver, there is column cap exposing in center.Safflower petal is added again after need to first passing through heating decoloration.

S24 ": continue to be cooled to 32~35 DEG C, discharging encapsulation obtains toner.

According to the another embodiment of the application, a kind of toner, the toner as described in any of the above-described embodiment Preparation method is prepared.

Embodiment 1

The water that parts by weight are 44 parts is taken to be added in the stirring container；It is stirred described in the glycerol addition for taking 3 parts of parts by weight It mixes in container；4 parts of parts by weight of propylene glycol is taken to be added in the stirring container；Take 0.01 part of parts by weight xanthan gum, 0.01 part of sodium alginate, 0.05 part of gellan gum, 0.01 part of pectin are added in the stirring container；Stirring container is heated 20 minutes, and heat while stirring, so that fluid temperature is risen to 80 DEG C, stops heating until glycerol and propylene glycol are completely dissolved To the first mixed liquor.Cool down to the first mixed solution；When temperature is down to 45 DEG C, taking parts by weight is that 10 parts of Rhododendron fastigiatums extract Liquid is added in stirring container, and taking parts by weight is 15 parts of rose, 5 parts of flores aurantii hydrosol, 3 parts of bodhi hydrosols, 3 parts of perfume (or spice) Beeweed hydrosol, 3 parts of white pond lily hydrosols are added in the stirring container and stir evenly；Continuing to be cooled to 32 DEG C, discharging encapsulates, Obtain toner.

Embodiment 2

The water that parts by weight are 40 parts is taken to be added in the stirring container；It is stirred described in the glycerol addition for taking 4 parts of parts by weight It mixes in container；6 parts of parts by weight of propylene glycol is taken to be added in the stirring container；Take 0.03 part of parts by weight xanthan gum, 0.03 part of sodium alginate, 0.08 part of gellan gum, 0.02 part of pectin are added in the stirring container；To the stirring container Heating 25 minutes, and heat while stirring, so that fluid temperature is risen to 83 DEG C, stops heating until glycerol and propylene glycol are completely molten Solution, obtains the first mixed liquor.Cool down to the first mixed solution；When temperature is down to 50 DEG C, taking parts by weight is 12 parts of close branch Du Cuckoo extracting solution is added in stirring container, takes parts by weight pure for 10 parts of rose, 8 parts of flores aurantii hydrosol, 6 portions of bodhis Dew, 6 parts of balm hydrosols, 5 parts of white pond lily hydrosols and 3 parts of lotus hydrosols are added in the stirring container and stir evenly；After Continuous to be cooled to 33 DEG C, discharging encapsulation obtains toner.

Embodiment 3

The water that parts by weight are 24 parts is taken to be added in the stirring container；It is stirred described in the glycerol addition for taking 5 parts of parts by weight It mixes in container；8 parts of parts by weight of propylene glycol is taken to be added in the stirring container；Take 0.05 part of parts by weight xanthan gum, 0.05 part of sodium alginate, 0.15 part of gellan gum, 0.03 part of pectin are added in the stirring container；Stirring container is heated 30 minutes, and heat while stirring, so that fluid temperature is risen to 85 DEG C, stopping heating being completely dissolved up to glycerol and propylene glycol, Obtain the first mixed liquor.Cool down to the first mixed solution；When temperature is down to 55 DEG C, taking parts by weight is that 15 parts of Rhododendron fastigiatums mention Liquid is taken to be added in stirring container, taking parts by weight is 20 parts of rose, 10 parts of flores aurantii hydrosol, 8 parts of bodhi hydrosols, 10 Part balm hydrosol is added in the stirring container and stirs evenly；Continue to be cooled to 35 DEG C, discharging encapsulation obtains toner.

Embodiment 4

The water that parts by weight are 20 parts is taken to be added in the stirring container；It is stirred described in the glycerol addition for taking 5 parts of parts by weight It mixes in container；8 parts of parts by weight of propylene glycol is taken to be added in the stirring container；Take 0.04 part of parts by weight xanthan gum, 0.04 part of sodium alginate, 0.1 part of gellan gum, 0.02 part of pectin are added in the stirring container；Stirring container is heated 30 minutes, and heat while stirring, so that fluid temperature is risen to 85 DEG C, stopping heating being completely dissolved up to glycerol and propylene glycol, Obtain the first mixed liquor.Cool down to the first mixed solution；When temperature is down to 48 DEG C, taking parts by weight is that 13 parts of Rhododendron fastigiatums mention Liquid is taken to be added in stirring container, taking parts by weight is 16 parts of sweet osmanthus hydrosol, 10 parts of lemon verbena hydrosol, 3 portions of bodhis Hydrosol, 6 parts of balm hydrosols, 3 parts of lotus hydrosols are added in the stirring container and stir evenly；Taking parts by weight is 1 part Safflower petal be added in the stirring container and stir evenly；Continue to be cooled to 35 DEG C, discharging encapsulation obtains toner.

Embodiment 5

The water that parts by weight are 50 parts is taken to be added in the stirring container；It is stirred described in the glycerol addition for taking 4 parts of parts by weight It mixes in container；6 parts of parts by weight of propylene glycol is taken to be added in the stirring container；The stirring container is heated 27 minutes, and It heats while stirring, fluid temperature is made to rise to 84 DEG C, stopping heating being completely dissolved up to glycerol and propylene glycol, and it is mixed to obtain first Close liquid.Cool down to the first mixed solution；When temperature is down to 47 DEG C, taking parts by weight is that 11 parts of Rhododendron fastigiatum extracting solution additions are stirred It mixes in container, takes parts by weight pure for 15 parts of rose, 9 parts of flores aurantii hydrosol, 7 portions of bodhi hydrosols, 8 portions of balms Dew, 5 parts of white pond lily hydrosols and 3 parts of lotus hydrosols are added in the stirring container and stir evenly；Continue to be cooled to 34 DEG C, out Material encapsulation, obtains toner.

The toner of essence, the toner of essential oil blending and preparation of the embodiment of the present invention compares

(1) test specimen: the toner of 1-3 of embodiment of the present invention preparation；The toner of flavoring rose essence is added, additive amount is 0.15 part, do not add hydrosol；The toner of Rosa Damascana is added, additive amount is 0.15 part, does not add hydrosol；It only adds a kind of pure The toner of dew adds 8 parts of roses.

(2) subject: 60 healthy males and women (each 30), the age was at 20~40 years old.

(3) application method: before sleeping at night and after morning warm water face cleaning, appropriate test specimen is taken to be applied to the centre of the palm, later gently It pats and beats cheek 1 minute, to promote the absorption of test specimen effective component, then replacement test in one week is used continuously in every kind of sample Sample.Subject does not use other cosmetics during the test.

(4) judgment criteria: Cost comparisons, technical staff are provided required for every liter of toner by calculating toner cost Cost.Test 6 weeks by a definite date evaluates the test specimen after a kind of test specimen of every use, is divided into fragrance to when using Sense comparison, is respectively divided into three grades.

(5) test result is shown in Table 1

1 essence of table, the toner of essential oil blending and toner of the present invention compare

As seen from the above table, the toner cost for adding essential oil is higher compared with other toners, adds the toner cost of essence Although cheap but the comfort level of its fragrance and the use feeling of toner are all poor compared with other toners.Embodiment 1-3 is addition hydrosol Toner, they are not much different in use feeling, but add the toners of a variety of hydrosols than only a kind of addition in fragrance comparison The toner of hydrosol is more liked that preferred embodiment 2 feels the comfortable people of fragrance up to 75%, it is believed that its fragrance by subject The number for being difficult to receive is also least.Embodiment 2 is added to lotus compared with toner prepared by embodiment 3 more and white pond lily is pure Dew, the evaluation of fragrance are also more preferable.

Toner antibacterial situation of the present invention

Test specimen is toner prepared by the embodiment of the present invention 1 and embodiment 3, the wherein conversion of Rhododendron fastigiatum extracting solution For percentage concentration, the concentration of Rhododendron fastigiatum extracting solution is about 10% in embodiment 1, and Rhododendron fastigiatum extracting solution is dense in embodiment 3 Degree about 15%.It is also prepared for the blank control group without Rhododendron fastigiatum extracting solution, and contains Rhododendron fastigiatum extracting solution 5% Toner is as control.Bacterium colony challenge experiment is carried out, the results are shown in Table 2.

2 toner antibacterial situation of table

Note: in one column of mushroom, " B " indicates mixed cell: Escherichia coli (ATCC11229), staphylococcus aureus (ATCC6538), pseudomonas aeruginosa (ATCC15442)；" M " indicates mould: aspergillus niger (ATCC16404)；" Y " indicates white Candida albicans (ATCC10231).Test temperature: bacterium is 32.5 ± 2.5 DEG C, and mould, saccharomycete are 28 ± 1 DEG C；28 days.

Symbol	As a result	Micro organism quantity
			-	Without growth	﹤ 100
﹢	A small amount of growth	About 102
			﹢ ﹢	Moderate growth	About 103
﹢+﹢	Raised growth	About 104
			﹢ ++ ﹢	Severe growth	About 105
C	Cover surface	﹥ 106

The makeup aquatic products of the Rhododendron fastigiatum extracting solution of description of test addition 10%~15% are gone back while providing fragrance With good bacteriostasis efficacy.

It should be understood that above-mentioned specific embodiment of the invention is used only for exemplary illustration or explains of the invention Principle, but not to limit the present invention.Therefore, that is done without departing from the spirit and scope of the present invention is any Modification, equivalent replacement, improvement etc. should all include within protection scope of the present invention.In addition, appended claims purport of the present invention Covering the whole variations fallen into attached claim scope and boundary or this range and the equivalent form on boundary and is repairing Change example.

In the description of the present invention, it should be noted that term " first ", " second ", " third " are used for description purposes only, It is not understood to indicate or imply relative importance.

Claims (10)

1. a kind of preparation method of toner, which comprises the following steps:

S1: water, moisturizer are sequentially added in stirring container, and heating the first scheduled duration makes temperature rise to the first default temperature Degree, and heat while stirring, stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor；

S2: being cooled to the second preset temperature to the first mixed liquor, while stirring after deodorant tune is added, and is cooled to the default temperature of third Degree, obtains toner.

2. the preparation method of toner according to claim 1, which is characterized in that the deodorant tune includes rose, Bodhisattva One of jacquard weave hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, flores aurantii hydrosol, chamomile hydrosol are more Kind.

3. the preparation method of toner according to claim 2, which is characterized in that

The moisturizer includes glycerol and/or propylene glycol；

First scheduled duration is greater than or equal to 20 minutes；

First preset temperature is 80~85 DEG C.

4. the preparation method of toner according to claim 3, which is characterized in that the step S1 specifically includes following step It is rapid:

S11: taking parts by weight is that 20~50 parts of the water and 7~13 parts of the moisturizer sequentially add the stirring container It is interior；

S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C；

S13: stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.

5. the preparation method of toner according to claim 3, which is characterized in that the step S1 specifically includes following step It is rapid:

S11 ': the water that parts by weight are 20~50 parts is taken to be added in the stirring container；

S12 ': 3~5 parts of parts by weight of the glycerol is taken to be added in the stirring container；

S13 ': 4~8 parts of parts by weight of the propylene glycol is taken to be added in the stirring container；

S14 ': 0.01~0.05 part of xanthan gum of parts by weight, 0.01~0.05 part of sodium alginate, 0.05~0.15 part are taken Gellan gum, 0.01~0.03 part of pectin are added in the stirring container；

S15 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C；

S16 ': stopping heating being completely dissolved up to the glycerol and the propylene glycol, obtains the first mixed liquor.

6. the preparation method of toner according to claim 3, which is characterized in that the step S2 the following steps are included:

S21: to the cooling of the first mixed solution and when temperature is down to 45~55 DEG C, the rose that parts by weight are 2~50 parts is added Hydrosol, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, flores aurantii hydrosol, one in chamomile hydrosol Kind or a variety of deodorant tunes, stir evenly；

S22: continue to be cooled to 32~35 DEG C, discharging encapsulation obtains the toner.

7. the preparation method of toner according to claim 6, which is characterized in that the deodorant tune further includes white pond lily hydrosol And/or lotus hydrosol；

Shown deodorant tune further includes Rhododendron fastigiatum extracting solution.

8. the preparation method of toner according to claim 7, which is characterized in that the step S2 the following steps are included:

S21 ': cool down to the first mixed solution；

S22 ': when temperature is down to 45~55 DEG C, taking parts by weight is that stirring container is added in 10~15 parts of Rhododendron fastigiatum extracting solutions Interior, taking parts by weight is 15~20 parts of rose, 5~10 parts of flores aurantii hydrosol, 3~8 parts of bodhi hydrosols, 3~10 parts Balm hydrosol, 3~8 parts of white pond lily hydrosols and/or 2~4 parts of lotus hydrosols are added in the stirring container and stir evenly；

S23 ': continue to be cooled to 32~35 DEG C, discharging encapsulation obtains the toner.

9. the preparation method of toner according to claim 7, which is characterized in that the step S2 the following steps are included:

S21 ": cool down to the first mixed solution；

S22 ": when temperature is down to 45~55 DEG C, taking parts by weight is 12~18 parts of sweet osmanthus hydrosol, 8~12 parts of lemon horse Whip grass hydrosol, 2~5 parts of bodhi hydrosols, 4.5~9 parts of balm hydrosols, 3~8 parts of white pond lily hydrosols and/or 2~4 parts of lotuses Hydrosol is added in the stirring container and stirs evenly；

S23 ": the safflower petal that parts by weight are 0.5~1.5 part is taken to be added in the stirring container and stir evenly；

S24 ": continue to be cooled to 32~35 DEG C, discharging encapsulation obtains the toner.

10. a kind of toner, which is characterized in that be prepared using any one of the claim 1-9 toner preparation method.