CN109758398A - A kind of facial mask and preparation method thereof - Google Patents
A kind of facial mask and preparation method thereof Download PDFInfo
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- CN109758398A CN109758398A CN201910222392.9A CN201910222392A CN109758398A CN 109758398 A CN109758398 A CN 109758398A CN 201910222392 A CN201910222392 A CN 201910222392A CN 109758398 A CN109758398 A CN 109758398A
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Abstract
The invention discloses a kind of facial mask and preparation methods, belong to cosmetic field.Include: to pre-process water, moisturizer, film forming agent, thickener, emollient, dispersing agent, obtains basal liquid；Emulsion pot is added in the basal liquid, is stirred while adding, homogeneous, stirring and the processing that cools down then successively are carried out；When being cooled to the first preset temperature, vitamin E and deodorant tune is added, stirs evenly, and be cooled to the second preset temperature, forms facial mask.By facial mask prepared by the present invention is mild comfortably, fragrance harmony and natural, cost is relatively low.
Description
Technical field
The present invention relates to cosmetic field more particularly to a kind of facial masks.
Background technique
Fragrance in facial mask is mainly to pass through addition essence or essential oil obtains at present.The facial mask for wherein adding essence may
Allergic reaction or phototoxic injury can be generated due to essence and to skin, and the fragrance that essence generates is unnatural,
It is difficult to the approval by customer.The price of essential oil is prohibitively expensive, can obviously increase cost, does not have good economy.And
The fragrance of essential oil is excessively strong, and fragrance process is difficult to the harmony of fragrance.
Summary of the invention
The object of the invention is that overcome above-mentioned deficiency, a kind of facial mask and preparation method thereof is provided, by adding hydrosol, is avoided
Essence or essential oil are used in facial mask.Facial mask is more mild comfortable non-stimulated and can reduce the life that blending uses in facial mask
Produce cost.Using being used cooperatively for a variety of hydrosols, make the fragrance harmony and natural of facial mask.
To solve the above problems, one aspect of the present invention provides a kind of preparation method of facial mask, comprising:
S1: water, moisturizer, film forming agent, thickener, emollient, dispersing agent are pre-processed, basal liquid is obtained.
S2: being added emulsion pot for basal liquid, stir while adding, and then successively carries out homogeneous, stirring and the processing that cools down.
S3: when being cooled to the first preset temperature, vitamin E and deodorant tune is added, stirs evenly, and it is pre- to be cooled to second
If temperature, encapsulation forms facial mask.
Further, deodorant tune includes rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena
Hydrosol, flores aurantii hydrosol, in chamomile hydrosol, white pond lily hydrosol and/or lotus hydrosol.
It further include Rhododendron fastigiatum extracting solution in deodorant tune.
Further, the step S3 specifically includes following steps,
S31: when temperature is down to 45~55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot.
S32: taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pot, then taking parts by weight is 6~8
One of part rose, 2~5 parts of bodhi hydrosols, 5~13 parts of sweet osmanthus hydrosols and 5~10 parts of chamomile hydrosols are a variety of
Hydrosol is added in emulsion pot, then taking parts by weight is that emulsion pot is added in 2~6 parts of white pond lily hydrosols and/or 3~5 parts of lotus hydrosols
In.
S33: being cooled to 32~35 DEG C after mixing evenly, and encapsulation forms facial mask.
Further, in the step S1: the moisturizer includes propylene glycol and glycerol；The film forming agent includes card wave
Nurse, hydroxy-ethyl acrylate, sodium acryloyldimethyl taurate；The thickener includes xanthan gum or hydroxyethyl cellulose；It is described
Emollient includes three Miglyol 812s, dimethyl silicone polymer, cyclopolysiloxane, dimethiconol；Described point
Powder includes Tween-20 or Tween-80.
Further, the step S1 specifically includes the following steps:
S11: taking parts by weight respectively is 20~55 parts of water, 7~12 parts of moisturizer, 0.05~0.6 part of thickener
It is sequentially added in stirring container with 0.5~1.5 part of film forming agent.
S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, increase fluid temperature
To 80~85 DEG C.
S13: stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.
Further, the step S11 is specifically included:
S111: the water that parts by weight are 20~55 parts is taken to be added in stirring container.
S112: taking parts by weight is that 2~5 parts of glycerol and 5~7 parts of propylene glycol sequentially add in stirring container.
S113: parts by weight are taken to stir for 0.05~0.5 part of xanthan gum or the addition of 0.05~0.1 part of hydroxyethyl cellulose
It mixes in container.
S114: taking parts by weight is 0.3~1.0 part of carbomer, 0.2~0.5 part of hydroxy-ethyl acrylate, 0.2~0.5 part third
Alkene acyl dimethyltaurine sodium is added in stirring container.
Further, the step S1 is specifically further comprising the steps of:
S11 ': parts by weight are taken to sequentially add and stir for 4.4~10.4 parts of emollient, 0.2~0.6 part of dispersing agent respectively
It mixes in container.
S12 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, increase fluid temperature
To 75~80 DEG C.
S13 ': stopping heating being uniformly mixed up to emollient, obtains the second mixed liquor.
Further, the step S11 ' is specifically included:
S11 ' 1: taking parts by weight is 0.2~1.0 part of three Miglyol 812s, 2~5 parts of polydimethylsiloxanes
Alkane, 2~4 parts of cyclopolysiloxane, 0.2~0.4 part of dimethiconol are added in stirring container；
S11 ' 2: taking parts by weight is that 0.2~0.5 part of Tween-20 or 0.25~0.6 part of Tween-80 are sequentially added and stirred
It mixes in container.
Further, the step S1 is specifically further comprising the steps of:
First mixed liquor and second mixed liquor are mixed, basal liquid is obtained.The system of facial mask provided by the invention
Preparation Method, replacing the use of essence and essential oil that can not only reduce cost using the by-product hydrosol during extraction of essential oil can also make
Fragrance more harmony and natural.Facial mask does not stimulate mildly.And hydrosol is the essential oil aqueous solution of saturation, the function with a part of essential oil
The fragrance of effect, a variety of hydrosols made in facial mask is novel rich in level, smell, is liked by customer.
Specific embodiment
In order to make the objectives, technical solutions and advantages of the present invention clearer, With reference to embodiment, to this
Invention is further described.It should be understood that these descriptions are merely illustrative, and it is not intended to limit the scope of the invention.This
Outside, in the following description, descriptions of well-known structures and technologies are omitted, so as not to unnecessarily obscure the concept of the present invention.
According to the application embodiment, a kind of preparation method of facial mask, comprising the following steps:
S1: water, moisturizer, film forming agent, thickener, emollient, dispersing agent are pre-processed, basal liquid is obtained.Wherein,
Water can be pure water, deionized water or cosmetics dedicated water, but be not limited to it is above-mentioned enumerate, preferably deionized water.
S2: being added emulsion pot for basal liquid, stir while adding, and then successively carries out homogeneous, stirring and the processing that cools down.Its
Middle cool-down method can for cooling water cycle water is cold, fan for cooling and natural cooling, but be not limited to it is above-mentioned enumerate, preferably from
It is so cooling.
S3: when being cooled to the first preset temperature, vitamin E and deodorant tune is added, stirs evenly, and it is pre- to be cooled to second
If temperature, encapsulation forms facial mask.
In an alternative embodiment, deodorant tune includes rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon
Lemon Verbena officinalis hydrosol, flores aurantii hydrosol, in chamomile hydrosol, white pond lily hydrosol and/or lotus hydrosol.
It further include Rhododendron fastigiatum extracting solution in deodorant tune.
Hydrosol refers to essential oil during distillation extraction, the steaming that the one kind 100% separated when refining essential oil is saturated
Stoste is evaporated, is a kind of byproduct of essential oil, composition is naturally pure, and fragrance is light pleasant.Use hydrosol can be very as deodorant tune
Prevent the adverse reaction that allergy is generated because of addition essence well.Also there is no essential oil blending because essential oil fragrance is excessively strong
And it is discordant to lead to the problem of smell.Wherein, deodorant tune can also be other hydrosols for applying to cosmetic industry in the present invention；
Or the fragrance in plant is extracted using grease, such as use absolute oil.
Wherein, rose is that the way of distillation is refined, and just has slightly sour taste by high temperature and pressure, what essence blended out
Product does not have the taste of draft.Include inside rose is the volatile aromatic ingredient of a large amount of fresh rose flower, it is simultaneously
Fragrance ingredient containing macromolecular.Have the effects that keep the skin wet, moisturizing, quick anti-inflammatory, antiallergy, it is antipruritic, delay senescence.
Bodhi hydrosol has the fresh breath with a small gangs of wheat beer again of some fragrance of a flower.Releive with moisturizing, desalinate it is black
Spot, the effect repaired damage, resist aging, smoothing wrinkle, consolidation, anti-inflammatory.
Contain the substances such as sweet osmanthus alcohol, palmitinic acid, lauric acid, linalool and irisone in sweet osmanthus hydrosol.Content is high
Irisone, so the violet keynote as typical fruity can be drifted after dilution.With exclusion toxin, Whitening, spot, moisturizing
The effect of anti-ageing, consolidation skin.
Balm hydrosol smell is lighter, with bitter lemonene.Has effects that anti-oxidant and antiphlogistic.
The smell of lemon verbena hydrosol is simple and elegant, mixes the salubrious of green grass tender shoots with a lemonene, is very easy to allow
People receives.Have effects that restrain anti-inflammatory, disinfection and sterilization.
Flores aurantii hydrosol (flavouring agent, skin whitening, moisturizing ingredient) containing thatch alcohol, linalool, young tiger geraniol, nerol, stupid ethyl alcohol,
Geraniol, rose oxide, rosefuran, with Quercetin, flavonoids, tannin, vitamin B and vitamin E, beta carotene and
A variety of amino acid, several mineral materials.Smell has the lily flowery odour of a bitter taste, flavour of a drug.Have both the double action of whitening and moisturizing.
Chamomile hydrosol smell is strong, has the sense of moisturizing antiallergic, eliminates skin sensitivity, go black eye, restrains, anti-inflammatory, disappears
The effect of swollen analgesic, elimination red capillary, tightening pore, calm skin.
Deodorant tune be preferably rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol,
Two or more composition in flores aurantii hydrosol, chamomile hydrosol, the compound fragrance of a flower that a variety of hydrosols generate can more make us
Pleasure is further preferably rose, bodhi hydrosol, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, orange
The deodorant tune of flower hydrosol, four kinds of hydrosols composition in chamomile hydrosol, be further preferably rose, bodhi hydrosol,
Flores aurantii hydrosol, balm hydrosol, another is preferably that bodhi hydrosol, sweet osmanthus hydrosol, lemon verbena hydrosol, chamomile are pure
Dew.The smell of preferred hydrosol collocation is more coordinated, and mixed flavor can make one to feel comfortable.
In an alternative embodiment, step S3 specifically includes following steps,
S31: when temperature is down to 45~55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot.
S32: taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pot, then taking parts by weight is 6~8
One of part rose, 2~5 parts of bodhi hydrosols, 5~13 parts of sweet osmanthus hydrosols and 5~10 parts of chamomile hydrosols are a variety of
Hydrosol is added in emulsion pot, then taking parts by weight is that emulsion pot is added in 2~6 parts of white pond lily hydrosols and/or 3~5 parts of lotus hydrosols
In.Take parts by weight for 6~8 parts of roses, 2~5 parts of bodhi hydrosols, 5~13 parts of sweet osmanthus hydrosols and/or 5~10 parts again
One of chamomile hydrosol or a variety of hydrosols are added in emulsion pot.
S33: being cooled to 32~35 DEG C after mixing evenly, and encapsulation forms facial mask.
It should be noted that S31, S32, S33 are only the code name that step carries out, it is not offered as the successive suitable of step execution
Sequence also may be performed simultaneously for example, S31-S33 can be sequencing.
Being cooled to 45~55 DEG C can be 45 DEG C, 46 DEG C, 47 DEG C, 48 DEG C, 49 DEG C, 50 DEG C, 51 DEG C, 52 DEG C, 53 DEG C, 54
DEG C, 55 DEG C but be not limited to above-mentioned enumerate.For example, can be increased or decreased according to environmental condition is appropriate, for example, can for 35~
50 DEG C, or be 52~62 DEG C.
Being cooled to 32~35 DEG C can be 32 DEG C, 33 DEG C, 34 DEG C, 35 DEG C but be not limited to above-mentioned enumerate.For example, can basis
Environmental condition is appropriate to be increased or decreased, such as can be 20~32 DEG C, or be 33~40 DEG C.
The fragrance and effective component of hydrosol can not only be kept by adding plant hydrosol at 45~55 DEG C, moreover it is possible to mix facial mask
Uniformly, quality is more stable.
The fragrance for matching to obtain of deodorant tune according to the invention is more coordinated, not the fragrance in ratio range of the present invention
Harmony be deteriorated.
Wherein Rhododendron fastigiatum (scientific name: Rhododendron fastigiatum), evergreen shrubs, 0.8-1 meters high, branch is thick
It is close, often at cushion or prostrate.Sprout is short, band bronzing, by crineous scale.Leaf bud squama is caducous.Leaf collection is born in sprig top, leather
Matter, oblong, ellipse or it is oval above dirty-green, below celadon.Inflorescence basidixed, the total shape of umbrella shape, there is colored 3-5；Corolla
Wide funnel-form, 1-1.5 centimetres long, hyacinthine or fresh lilac red.Capsule oval.The month at florescence 5-6, the fruiting period 8-9 month.It is born in rock
Slope, cliff, high mountain gravel meadow, tor shrubbery, rose bay shrublet or occasionally under pine forest, produce Qinghai, Sichuan, Yunnan.It should
Species are because of flower beauty, bright-colored, artificial cultivation, horticultural importance with higher.
In the present embodiment, the parts by weight of Rhododendron fastigiatum extracting solution can for 10 parts, 11 parts, 12 parts, 13 parts, 14 parts,
15 parts it is equal but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 12~14 parts, 11
~13 parts, or be 11.5~14.5 parts.The pleasantly surprised discovery Rhododendron fastigiatum extracting solution of inventor can not only reconcile various hydrosols
Smell be allowed to more harmonious, there are also good bacteriostasis efficacy.When the parts by weight of addition are 10~15 parts, fungistatic effect reaches
To best, good fungistatic effect can not be played when the parts by weight of addition are less than 10 parts, when the parts by weight of addition are greater than
Fragrance can be made uncoordinated at 15 parts.
It is generally acknowledged that containing azalaic acid in azalea, also known as azelaic acid, azalaic acid have antibiotic property, and it is anti-to can be used as food
Rotten agent.Just there is apparent antibacterial effect when azalaic acid concentration reaches 20%.
The parts by weight of rose can for 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixed
The adjustment appropriate of the effect of conjunction, such as can be 5~10 parts, 8~15 parts, or be 3~20 parts.
The parts by weight of sweet osmanthus hydrosol can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts etc. but not
Be limited to it is above-mentioned enumerate, can according to the effect actually mixed adjustment appropriate, such as can be 5~15 parts, 15~20 parts, or
It is 16~25 parts.
The parts by weight of bodhi hydrosol can for 2 parts, 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can basis
The effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts, or be 6~15 parts.
The parts by weight of chamomile hydrosol can for 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to it is above-mentioned enumerate,
Can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts, or be 6~15 parts.May be used also
With include flores aurantii hydrosol parts by weight can for 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to it is above-mentioned enumerate, can be with
It according to the effect actually mixed adjustment appropriate, such as can be 2~8 parts, 6~12 parts, or be 3~15 parts.
The parts by weight of lemon verbena hydrosol can be 8 parts, 9 parts, 10 parts, 11 parts, 12 parts etc. but be not limited to above-mentioned column
It lifts, can be according to the effect actually mixed adjustment appropriate, such as can be 4~8 parts, 10~15 parts, or be 6~18 parts.
The parts by weight of balm hydrosol can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to
It is above-mentioned to enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~15 parts, or for 8~
20 parts.
In an alternative embodiment, can also include: before or after step S32 and in step S32
Taking parts by weight again is that 2~6 parts of white pond lily hydrosols and/or 3~5 parts of lotus hydrosols are added in emulsion pot.
The parts by weight of white pond lily hydrosol can for 2 parts, 3 parts, 4 parts, 5 parts, 6 parts etc. but be not limited to it is above-mentioned enumerate, can be with
It according to the effect actually mixed adjustment appropriate, such as can be 1~8 part, 5~10 parts, or be 6~15 parts.
The parts by weight of lotus hydrosol can for 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixed
The adjustment appropriate of the effect of conjunction, such as can be 1~6 part, 2~8 parts, or be 3~10 parts.
It is simple and elegant pure and fresh using white pond lily hydrosol and/or lotus hydrosol smell, the smell between a variety of hydrosols can be made more to assist
It adjusts, and increases the fragrance of white pond lily and/or lotus in smell, both smells are more rare in facial mask, make the perfume (or spice) of facial mask
Gas is more novel, has purification cuticula, prevents computer from radiating.
In an alternative embodiment, in step S1: moisturizer includes propylene glycol and glycerol；Film forming agent includes carbomer, third
Olefin(e) acid hydroxyl ethyl ester, sodium acryloyldimethyl taurate；Thickener includes xanthan gum or hydroxyethyl cellulose；Emollient includes three pungent
Sour glycerol decanoate, dimethyl silicone polymer, cyclopolysiloxane, dimethiconol；Dispersing agent includes Tween-20 or spits
Temperature -80.
In an alternative embodiment, step S1 specifically includes the following steps:
S11: taking parts by weight respectively is 20~55 parts of water, 7~12 parts of moisturizer, 0.05~0.6 part of thickener
It is sequentially added in stirring container with 0.5~1.5 part of film forming agent.In the present embodiment, the parts by weight of water can be 20 parts, 21
Part, 22 parts, 23 parts, 24 parts, 25 parts, 28 parts, 32 parts, 35 parts, 37 parts, 39 parts, 41 parts, 44 parts, 47 parts, 48 parts, 49 parts, 50
Part, 51 parts, 52 parts, 53 parts, 54 parts, 55 parts, etc. but be not limited to it is above-mentioned enumerate, can be according to the effect that actually mixes and other
The parts by weight of the content of substance adjustment water appropriate, it is further preferably 25~30 parts that preferably obtaining, which is 20~40 parts, such as
It can be 15~25 parts, 25~30 parts, 30~50 parts, or be 80~95 parts.
S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80
~85 DEG C.
S13: stopping heating being completely dissolved up to moisturizer, obtains the first mixed liquor.
In the present embodiment, heating can be 20 minutes, 21 minutes, 22 minutes, 23 minutes, 25 more than or equal to 20 minutes
Minute, 28 minutes, 32 minutes, 37 minutes, 44 minutes, 48 minutes, 50 minutes, 55 minutes, 60 minutes etc. but be not limited to above-mentioned column
It lifts, can be according to the duration of the degree adjustment heating appropriate of the effect and dissolution that actually mix, preferably obtaining is 20~60 points
Clock is further preferably 25~45 minutes.Temperature rise to 80~85 DEG C can for 80 DEG C, 81 DEG C, 82 DEG C, 83 DEG C, 84 DEG C,
85 DEG C but it is not limited to above-mentioned enumerate.For example, can be increased or decreased according to environmental condition is appropriate to the first preset temperature, such as
It can be 80~100 DEG C, or be 70~85 DEG C.
In an alternative embodiment, step S11 is specifically included:
S111: the water that parts by weight are 20~55 parts is taken to be added in stirring container.
S112: taking parts by weight is that 2~5 parts of glycerol and 5~7 parts of propylene glycol sequentially add in stirring container.Glycerol
Parts by weight can for 2 parts, 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be appropriate according to the effect actually mixed
Adjustment, such as can be 3~8 parts, 4~6 parts etc..The parts by weight of propylene glycol can be 5 parts, 6 parts, 7 parts etc. but be not limited to
It is above-mentioned to enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts etc..
S113: parts by weight are taken to stir for 0.05~0.5 part of xanthan gum or the addition of 0.05~0.1 part of hydroxyethyl cellulose
It mixes in container.The parts by weight of xanthan gum can for 0.05 part, 0.06 part, 0.07 part, 0.1 part, 0.2 part, 0.3 part, 0.4 part,
0.47 part, 0.48 part, 0.49 part, 0.5 part etc. but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed tune appropriate
It is whole, such as can be 0.02~0.6 part, 0.25~1.0 part etc..The parts by weight of hydroxyethyl cellulose can for 0.05 part,
It 0.06 part, 0.07 part, 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.47 part, 0.48 part, 0.49 part, 0.5 part etc. but is not limited to
It states and enumerates, can be according to the effect actually mixed adjustment appropriate, such as can be 0.02~0.6 part, 0.25~1.0 part etc..
S114: taking parts by weight is 0.3~1.0 part of carbomer, 0.2~0.5 part of hydroxy-ethyl acrylate, 0.2~0.5 part third
Alkene acyl dimethyltaurine sodium is added in stirring container.
The parts by weight of carbomer can be 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts
Deng but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 0.2~0.8 part, 0.4
~1.6 parts etc..
The parts by weight of hydroxy-ethyl acrylate can be 0.2 part, 0.3 part, 0.4 part, 0.5 part etc. but be not limited to above-mentioned column
It lifts, can be according to the effect actually mixed adjustment appropriate, such as can be 0.1~0.8 part, 0.4~1.5 part etc..
The parts by weight of sodium acryloyldimethyl taurate can be 0.2 part, 0.3 part, 0.4 part, 0.5 part etc. but be not limited to
It is above-mentioned to enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 0.1~0.8 part, 0.3~1.8 part etc..
It should be noted that S111, S112, S113, S114 are only the code name that step carries out, it is not offered as step execution
Sequencing also may be performed simultaneously for example, S111-S114 can be sequencing.
In an alternative embodiment, step S1 is specifically further comprising the steps of:
S11 ': parts by weight are taken to sequentially add and stir for 4.4~10.4 parts of emollient, 0.2~0.6 part of dispersing agent respectively
It mixes in container.
S12 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 75
~80 DEG C.Temperature, which rises to 75~80 DEG C, can be 75 DEG C, 76 DEG C, 77 DEG C, 78 DEG C, 79 DEG C, 80 DEG C but be not limited to above-mentioned enumerate.
It for example, can be increased or decreased according to environmental condition is appropriate to the first preset temperature, such as can be 60~100 DEG C, or
It is 70~85 DEG C.
S13 ': stop heating and be completely dissolved up to emollient is uniformly mixed, obtain the second mixed liquor.
In an alternative embodiment, step S11 is specifically included:
S11 ' 1: taking parts by weight is 0.2~1.0 part of three Miglyol 812s, 2~5 parts of polydimethylsiloxanes
Alkane, 2~4 parts of cyclopolysiloxane, 0.2~0.4 part of dimethiconol are added in stirring container.Three Caprylic Caprics
The parts by weight of ester can be 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts etc. but not
Be limited to it is above-mentioned enumerate, can according to the effect actually mixed adjustment appropriate, such as can be 0.3~0.8 part, 0.4~1.2 part
Deng.
The parts by weight of dimethyl silicone polymer can for 2 parts, 3 parts, 4 parts etc. but be not limited to it is above-mentioned enumerate, can basis
The effect actually mixed adjustment appropriate, such as can be 3~8 parts, 4~6 parts etc..
The parts by weight of cyclopolysiloxane can for 2 parts, 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can basis
The effect actually mixed adjustment appropriate, such as can be 3~8 parts, 4~6 parts etc..
The parts by weight of dimethiconol can for 0.2 part, 0.3 part, 0.4 part etc. but be not limited to it is above-mentioned enumerate,
Can be according to the effect actually mixed adjustment appropriate, such as can be 0.3~0.8 part, 0.4~0.6 part etc..
S11 ' 2: taking parts by weight is that 0.2~0.5 part of Tween-20 or 0.25~0.6 part of Tween-80 are sequentially added and stirred
It mixes in container.The parts by weight of Tween-20 can for 0.2 part, 0.3 part, 0.4 part, 0.5 part etc. but be not limited to it is above-mentioned enumerate, can
It with according to the effect actually mixed adjustment appropriate, such as can be 0.3~0.8 part, 0.4~0.6 part etc..The weight of Tween-80
Amount number can for 0.25 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixing
Effect adjustment appropriate, such as can be 0.3~0.8 part, 0.4~0.6 part etc..
In an alternative embodiment, step S1 is specifically further comprising the steps of:
First mixed liquor and the second mixed liquor are mixed, basal liquid is obtained.
Embodiment 1
The water that parts by weight are 55 parts is taken to be added in stirring container；Taking parts by weight is 2 parts of glycerol and 5 parts of propylene glycol
It sequentially adds in stirring container；The hydroxyethyl cellulose that parts by weight are 0.05 part is taken to be added in stirring container；Take parts by weight
It is added in stirring container for 0.3 part of carbomer, 0.2 part of hydroxy-ethyl acrylate, 0.2 part of sodium acryloyldimethyl taurate.To institute
It states stirring container to heat 20 minutes, and heats while stirring, fluid temperature is made to rise to 80 DEG C, stop heating until glycerol and third
Glycol is completely dissolved, and obtains the first mixed liquor.
Taking parts by weight is 0.2 part of three Miglyol 812s, 2 parts of dimethyl silicone polymer, the poly- silicon oxygen of 2 parts of ring
Alkane, 0.2 part of dimethiconol are added in stirring container；Take the Tween-20 that parts by weight are 0.2 part that stirring container is added
It is interior；Stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, so that fluid temperature is risen to 75 DEG C, stops
Only heating obtains the second mixed liquor up to being uniformly mixed.
First mixed liquor and second mixed liquor are mixed, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, homogeneous is then successively carried out 6 minutes, stirs and cool down
Processing；When temperature is down to 45 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot；Taking parts by weight is 10 parts
Emulsion pot is added in Rhododendron fastigiatum extracting solution, then taking parts by weight is 6 parts of roses, 3 parts of bodhi hydrosols, 5 parts of sweet osmanthus hydrosols
It is added in emulsion pot with 5 parts of chamomile hydrosols；Taking parts by weight again is that 2 parts of white pond lily hydrosols are added in emulsion pot.It stirs evenly
After be cooled to 32 DEG C, encapsulation forms facial mask.
Embodiment 2
The water that parts by weight are 35 parts is taken to be added in stirring container；Taking parts by weight is 3 parts of glycerol and 6 parts of propylene glycol
It sequentially adds in stirring container；The xanthan gum that parts by weight are 0.3 part is taken to be added in stirring container；Taking parts by weight is 0.4 part
Carbomer, 0.3 part of hydroxy-ethyl acrylate, 0.3 part of sodium acryloyldimethyl taurate are added in stirring container.The stirring is held
Device heats 25 minutes, and heats while stirring, and fluid temperature is made to rise to 83 DEG C, stops heating until glycerol and propylene glycol are complete
Dissolution, obtains the first mixed liquor.
Taking parts by weight is 0.5 part of three Miglyol 812s, 3 parts of dimethyl silicone polymer, the poly- silicon oxygen of 3 parts of ring
Alkane, 0.3 part of dimethiconol are added in stirring container；Take the Tween-20 that parts by weight are 0.3 part that stirring container is added
It is interior；The stirring container is heated 25 minutes, and is heated while stirring, fluid temperature is made to rise to 76 DEG C, stop heating until
It is uniformly mixed, obtains the second mixed liquor.
By first mixed liquor and second mixed liquor, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, homogeneous is then successively carried out 6 minutes, stirs and cool down
Processing；When temperature is down to 50 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot；Taking parts by weight is 13 parts
Emulsion pot is added in Rhododendron fastigiatum extracting solution, then taking parts by weight is 7 parts of roses, 4 parts of bodhi hydrosols, 10 parts of sweet osmanthus hydrosols
It is added in emulsion pot with 7 parts of chamomile hydrosols；Taking parts by weight again is that emulsification is added in 3 parts of white pond lily hydrosols and 4 parts of lotus hydrosols
In pot.It is cooled to 33 DEG C after mixing evenly, encapsulation forms facial mask.
Embodiment 3
The water that parts by weight are 20 parts is taken to be added in stirring container；Taking parts by weight is 5 parts of glycerol and 7 parts of propylene glycol
It sequentially adds in stirring container；The xanthan gum that parts by weight are 0.5 part is taken to be added in stirring container；Taking parts by weight is 1.0 parts
Carbomer, 0.5 part of hydroxy-ethyl acrylate, 0.5 part of sodium acryloyldimethyl taurate are added in stirring container.The stirring is held
Device heats 30 minutes, and heats while stirring, and fluid temperature is made to rise to 85 DEG C, stops heating until glycerol and propylene glycol are complete
Dissolution, obtains the first mixed liquor.
Taking parts by weight is 1.0 parts of three Miglyol 812s, 5 parts of dimethyl silicone polymer, the poly- silicon oxygen of 4 parts of ring
Alkane, 0.4 part of dimethiconol are added in stirring container；Take the Tween-80 that parts by weight are 0.6 part that stirring container is added
It is interior；The stirring container is heated 30 minutes, and is heated while stirring, fluid temperature is made to rise to 80 DEG C, stop heating until
It is uniformly mixed, obtains the second mixed liquor.
First mixed liquor and second mixed liquor are mixed, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, homogeneous is then successively carried out 6 minutes, stirs and cool down
Processing；When temperature is down to 55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot；Taking parts by weight is 15 parts
Emulsion pot is added in Rhododendron fastigiatum extracting solution, then taking parts by weight is 8 parts of roses, 5 parts of bodhi hydrosols, 13 parts of sweet osmanthus hydrosols
It is added in emulsion pot with 10 parts of chamomile hydrosols.It is cooled to 35 DEG C after mixing evenly, encapsulation forms facial mask.
Embodiment 4
The water that parts by weight are 40 parts is taken to be added in stirring container；Taking parts by weight is 4 parts of glycerol and 6 parts of propylene glycol
It sequentially adds in stirring container；The hydroxyethyl cellulose that parts by weight are 0.1 part is taken to be added in stirring container；The parts by weight are taken to be
0.8 part of carbomer, 0.4 part of hydroxy-ethyl acrylate, 0.4 part of sodium acryloyldimethyl taurate are added in stirring container.To described
Stirring container heats 28 minutes, and heats while stirring, and fluid temperature is made to rise to 82 DEG C, stops heating until glycerol and the third two
Alcohol is completely dissolved, and obtains the first mixed liquor.
Taking parts by weight is 0.7 part of three Miglyol 812s, 4 parts of dimethyl silicone polymer, the poly- silicon oxygen of 3 parts of ring
Alkane, 0.3 part of dimethiconol are added in stirring container；Take the Tween-20 that parts by weight are 0.5 part that stirring container is added
It is interior；The stirring container is heated 27 minutes, and is heated while stirring, fluid temperature is made to rise to 77 DEG C, stop heating until
It is uniformly mixed, obtains the second mixed liquor.
First mixed liquor and second mixed liquor are mixed, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, homogeneous is then successively carried out 6 minutes, stirs and cool down
Processing；When temperature is down to 52 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot；Taking parts by weight is 12 parts
Emulsion pot is added in Rhododendron fastigiatum extracting solution, then taking parts by weight is 8 parts of roses, 5 parts of bodhi hydrosols, 13 parts of sweet osmanthus hydrosols
It is added in emulsion pot with 5 parts of chamomile hydrosols；Taking parts by weight again is that emulsification is added in 6 parts of white pond lily hydrosols and 5 parts of lotus hydrosols
In pot.It is cooled to 33 DEG C after mixing evenly, encapsulation forms facial mask.
Essence, the facial mask of essential oil blending and facial mask of the present invention compare
(1) test specimen: facial mask prepared by the embodiment of the present invention 1~3；The facial mask of flavoring rose essence is added, additive amount is
0.15 part, do not add hydrosol；The facial mask of Rosa Damascana is added, additive amount is 0.15 part, does not add hydrosol；Only add a kind of hydrosol
Facial mask, add 8 parts of roses.
(2) subject: 60 healthy males and women (each 30), the age was at 20~40 years old.
(3) it application method: with after warm water face cleaning before sleeping at night, takes appropriate test specimen to be uniformly applied to face, makes test sample
Product stop 15 minutes in face, and to promote the absorption of test specimen effective component, every kind of sample is used continuously one week and then replaces
Test specimen.Subject does not use other cosmetics during the test.
(4) judgment criteria: technical staff provides cost required for every liter of facial mask by calculating facial mask cost.Test schedules to last
It 6 weeks, tests subject after expiring and the trial target that oneself is used is evaluated, be divided into fragrance and when use feeling is compared, each point
For three grades.
(5) test result is shown in Table 1
1 essence of table, the facial mask of essential oil blending and facial mask of the present invention compare
As seen from the above table, the facial mask cost for adding essential oil is higher compared with other facial masks, although adding the facial mask cost of essence just
Preferably but the comfort level of its fragrance and the use feeling of facial mask are all poor compared with other facial masks.Examples 1 to 3 is to add the facial mask of hydrosol, it
Be not much different in use feeling, but fragrance comparison on add the facial mask of a variety of hydrosols than only adding the facial mask of a kind of hydrosol more
Liked by subject, preferred embodiment 2 feels the comfortable people of fragrance up to 76.6%, it is believed that its fragrance is difficult to the people received
Number is also least.Embodiment 2 is added to lotus and white pond lily hydrosol, the evaluation of fragrance compared with facial mask prepared by embodiment 3 more
Also more preferable.
Facial mask antibacterial situation of the present invention
Test specimen is facial mask prepared by the embodiment of the present invention 1 and embodiment 3, and wherein Rhododendron fastigiatum extracting solution is scaled
Percentage concentration, the concentration of Rhododendron fastigiatum extracting solution is about 10% in embodiment 1, the concentration of Rhododendron fastigiatum extracting solution in embodiment 3
About 15%.Also it is prepared for the blank control group without Rhododendron fastigiatum extracting solution, and the face containing Rhododendron fastigiatum extracting solution 5%
Film is as control.Bacterium colony challenge experiment is carried out, the results are shown in Table 2.
2 facial mask antibacterial situation of table
Note: in one column of mushroom, " B " indicates mixed cell: Escherichia coli (ATCC11229), staphylococcus aureus
(ATCC6538), pseudomonas aeruginosa (ATCC15442)；" M " indicates mould: aspergillus niger (ATCC16404)；" Y " indicates white
Candida albicans (ATCC10231).Test temperature: bacterium is 32.5 ± 2.5 DEG C, and mould, saccharomycete are 28 ± 1 DEG C；28 days.
| Symbol | As a result | Micro organism quantity |
| - | Without growth | ﹤ 100 |
| ﹢ | A small amount of growth | About 102 |
| ﹢ ﹢ | Moderate growth | About 103 |
| ﹢+﹢ | Raised growth | About 104 |
| ﹢ ++ ﹢ | Severe growth | About 105 |
| C | Cover surface | ﹥ 106 |
The mask product of the Rhododendron fastigiatum extracting solution of description of test addition 10%~15% also has while providing fragrance
There is good bacteriostasis efficacy.
It should be understood that above-mentioned specific embodiment of the invention is used only for exemplary illustration or explains of the invention
Principle, but not to limit the present invention.Therefore, that is done without departing from the spirit and scope of the present invention is any
Modification, equivalent replacement, improvement etc. should all include within protection scope of the present invention.In addition, appended claims purport of the present invention
Covering the whole variations fallen into attached claim scope and boundary or this range and the equivalent form on boundary and is repairing
Change example.
In the description of the present invention, it should be noted that term " first ", " second ", " third " are used for description purposes only,
It is not understood to indicate or imply relative importance.
Claims (10)
1. a kind of preparation method of facial mask, which is characterized in that include the following steps,
S1: water, moisturizer, film forming agent, thickener, emollient, dispersing agent are pre-processed, basal liquid is obtained；
S2: emulsion pot is added in the basal liquid, is stirred while adding, homogeneous, stirring and the processing that cools down then successively are carried out；
S3: when being cooled to the first preset temperature, being added vitamin E and deodorant tune, stir evenly, and is cooled to the second default temperature
Degree, encapsulation form facial mask.
2. preparation method according to claim 1, which is characterized in that the deodorant tune includes that rose, bodhi are pure
Dew, sweet osmanthus hydrosol, balm hydrosol, lemon verbena hydrosol, flores aurantii hydrosol, chamomile hydrosol, white pond lily hydrosol, lotus hydrosol
One of or it is a variety of；
The deodorant tune further includes Rhododendron fastigiatum extracting solution.
3. preparation method according to claim 2, which is characterized in that the step S3 specifically includes following steps,
S31: when temperature is down to 45~55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot；
S32: taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pot, then taking parts by weight is 6~8 parts of roses
One of rare hydrosol, 2~5 parts of bodhi hydrosols, 5~13 parts of sweet osmanthus hydrosols and 5~10 parts of chamomile hydrosols or a variety of hydrosols
It is added in emulsion pot, then taking parts by weight is that 2~6 parts of white pond lily hydrosols and/or 3~5 parts of lotus hydrosols are added in emulsion pot.
S33: being cooled to 32~35 DEG C after mixing evenly, and encapsulation forms facial mask.
4. preparation method according to claim 1, which is characterized in that in the step S1:
The moisturizer includes propylene glycol and glycerol；
The film forming agent includes carbomer, hydroxy-ethyl acrylate, sodium acryloyldimethyl taurate；
The thickener includes xanthan gum or hydroxyethyl cellulose；
The emollient includes three Miglyol 812s, dimethyl silicone polymer, cyclopolysiloxane, dimethyl silicone polymer
Alcohol；
The dispersing agent includes Tween-20 or Tween-80.
5. the preparation method according to claim 4, which is characterized in that the step S1 specifically includes the following steps:
S11: taking parts by weight respectively is 20~55 parts of water, 7~12 parts of moisturizer, 0.05~0.6 part of thickener and 0.5
~1.5 parts of film forming agents sequentially add in stirring container；
S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80
~85 DEG C；
S13: stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.
6. preparation method according to claim 5, which is characterized in that the step S11 is specifically included:
S111: the water that parts by weight are 20~55 parts is taken to be added in stirring container；
S112: taking parts by weight is that 2~5 parts of glycerol and 5~7 parts of propylene glycol sequentially add in stirring container；
S113: the xanthan gum or 0.05~0.1 part of hydroxyethyl cellulose addition stirring appearance that parts by weight are 0.05~0.5 part are taken
In device；
S114: taking parts by weight is 0.3~1.0 part of carbomer, 0.2~0.5 part of hydroxy-ethyl acrylate, 0.2~0.5 part of acryloyl
Dimethyltaurine sodium is added in stirring container.
7. preparation method according to claim 5, which is characterized in that the step S1 is specifically further comprising the steps of:
S11 ': it takes parts by weight to sequentially add stirring for 4.4~10.4 parts of emollient, 0.2~0.6 part of dispersing agent respectively and holds
In device；
S12 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 75
~80 DEG C；
S13 ': stop heating up to being uniformly mixed, obtain the second mixed liquor.
8. preparation method according to claim 7, which is characterized in that the step S11 ' is specifically included:
S11 ' 1: take parts by weight be 0.2~1.0 part of three Miglyol 812s, 2~5 parts of dimethyl silicone polymer, 2~
4 parts of cyclopolysiloxane, 0.2~0.4 part of dimethiconol are added in stirring container；
S11 ' 2: taking parts by weight is that 0.2~0.5 part of Tween-20 or 0.25~0.6 part of Tween-80 sequentially add stirring and hold
In device.
9. preparation method according to claim 8, which is characterized in that the step S1 is specifically further comprising the steps of:
First mixed liquor and second mixed liquor are mixed, basal liquid is obtained.
10. a kind of facial mask, which is characterized in that be prepared using preparation method as claimed in claims 1-9.
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|---|---|---|---|
| CN201910222392.9A CN109758398A (en) | 2019-03-22 | 2019-03-22 | A kind of facial mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910222392.9A CN109758398A (en) | 2019-03-22 | 2019-03-22 | A kind of facial mask and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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ID=66459677
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
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| Country | Link |
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2019
- 2019-03-22 CN CN201910222392.9A patent/CN109758398A/en active Pending
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