CN109793683A - A kind of lotion and preparation method thereof - Google Patents

A kind of lotion and preparation method thereof Download PDF

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Publication number
CN109793683A
CN109793683A CN201910221904.XA CN201910221904A CN109793683A CN 109793683 A CN109793683 A CN 109793683A CN 201910221904 A CN201910221904 A CN 201910221904A CN 109793683 A CN109793683 A CN 109793683A
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China
Prior art keywords
parts
weight
hydrosol
added
lotion
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CN201910221904.XA
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Chinese (zh)
Inventor
吴睿
赵春花
陈熙
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Jie Rofu (yunnan) Cosmetics Co Ltd
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Jie Rofu (yunnan) Cosmetics Co Ltd
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Priority to CN201910221904.XA priority Critical patent/CN109793683A/en
Publication of CN109793683A publication Critical patent/CN109793683A/en
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Abstract

The invention discloses a kind of lotion and preparation methods, belong to cosmetic field.It include: that water, moisturizer, thickener, emulsifier, emollient, assistant for emulsifying agent are prepared into basal liquid;Emulsion pot is added in the basal liquid, is stirred while adding, after carrying out homogeneous while agitating, continues to stir and carries out cooling processing;When being down to the first preset temperature to temperature, deodorant tune is added, stirs evenly, and be cooled to the second preset temperature, obtains lotion.By lotion prepared by the present invention is mild comfortably, fragrance harmony and natural, cost is relatively low.

Description

A kind of lotion and preparation method thereof
Technical field
The present invention relates to cosmetic field more particularly to a kind of lotions.
Background technique
Fragrance in type of latex type cosmetics is mainly to pass through addition essence or essential oil obtains at present.Wherein add essence Type of latex type cosmetics may generate allergic reaction or phototoxic injury due to essence and to skin, and essence produces Raw fragrance is unnatural, it is difficult to the approval by customer.And the price of essential oil is prohibitively expensive, obviously increase cost, does not have Standby good economy.Again since the fragrance of essential oil is excessively strong, fragrance process is difficult to the harmony of fragrance.
Summary of the invention
The object of the invention is that overcome above-mentioned deficiency, a kind of lotion and preparation method thereof is provided, by adding hydrosol, is avoided Essence or essential oil are used in lotion, and reaching keeps lotion more mild comfortable non-stimulated and can reduce blending in lotion The production cost used.Using being used cooperatively for a variety of hydrosols, make the fragrance harmony and natural of lotion.
To solve the above problems, the first aspect of the present invention provides a kind of preparation method of lotion, comprising:
S1: water, moisturizer, thickener, emulsifier, emollient, assistant for emulsifying agent are prepared into basal liquid;
S2: emulsion pot is added in the basal liquid, is stirred while adding, after carrying out homogeneous while agitating, continues to stir It mixes and carries out cooling processing;
S3: when being down to the first preset temperature to temperature, being added deodorant tune, stir evenly, and be cooled to the second preset temperature, Obtain lotion.
Further, the deodorant tune includes rose, peppermint hydrosol, lavender hydrosol, balm hydrosol, lemon horse Whip grass hydrosol, flores aurantii hydrosol, chamomile hydrosol, white pond lily hydrosol and/or lotus hydrosol.
The deodorant tune further includes Rhododendron fastigiatum extracting solution.
Further, the step S3 specifically includes the following steps:
S31: when temperature is down to 45~55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot;
S32: taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pot, then taking parts by weight is 6~9 One of part rose, 3~5 parts of peppermint hydrosols, 10~13 parts of lavender hydrosols, 4~8 parts of chamomile hydrosols are a variety of pure Dew is added in emulsion pot;
S33: being cooled to 32~35 DEG C after mixing evenly, and discharging, encapsulation obtain lotion.
Further, can also include: before or after step S32 and in step S32
Taking parts by weight again is that 3~5 parts of white pond lily hydrosols and/or 2~6 parts of lotus hydrosols are added in emulsion pot.
Further, in the step S1:
The moisturizer includes polyethylene glycol and glycerol;
The thickener includes xanthan gum or hydroxyethyl cellulose, preferably xanthan gum;
The emollient includes isobutyl palmitate, glyceryl monostearate, hexadecanol, stearic acid, lanolin;
The emulsifier includes hexadecanyl phosphate potassium;
The assistant for emulsifying agent includes monoglyceride or glyceryl monolaurate, is preferentially monoglyceride.
Further, the step S1 specifically includes the following steps:
S11: taking parts by weight respectively is 5~50 parts of water, 7~12 parts of moisturizer and 0.05~0.5 part of thickener It sequentially adds in stirring container;
S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, increase fluid temperature To 80~85 DEG C;
S13: stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.
Further, the step S11 is specifically included:
S111: the water that parts by weight are 5~50 parts is taken to be added in stirring container;
S112: taking parts by weight is that 2~5 parts of glycerol and 5~7 parts of polyethylene glycol sequentially add in stirring container;
S113: parts by weight are taken to stir for 0.05~0.5 part of xanthan gum or the addition of 0.1~0.4 part of hydroxyethyl cellulose It mixes in container.
Further, the step S1 is specifically further comprising the steps of:
S11 ': taking parts by weight respectively is 12.2~28 parts of emollient, 1~2 part of emulsifier, 2~5 parts of assistant for emulsifying agents It sequentially adds in stirring container;
S12 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, increase fluid temperature To 80~85 DEG C;
S13 ': stopping heating being uniformly mixed up to emollient, obtains the second mixed liquor.
Further, the step S11 ' is specifically included:
S11 ' 1: taking parts by weight is 3~8 parts of isobutyl palmitate, 5~10 parts of glyceryl monostearate, 1~3 part Hexadecanol, 3~5 parts of stearic acid, 0.2~2 part lanolin be added stirring container in;
S11 ' 2: the hexadecanyl phosphate potassium that parts by weight are 1~2 part is taken to be added in stirring container;
S11 ' 3: the monoglyceride or 2~5 parts of glyceryl monolaurate addition stirring container that parts by weight are 2~4 parts are taken It is interior.
Further, the step S1 is specifically further comprising the steps of:
By first mixed liquor and second mixed liquor, basal liquid is obtained.
Another aspect provides a kind of lotions, are prepared using preparation method as described above.
The preparation method of lotion provided by the invention replaces essence and essence using the by-product hydrosol during extraction of essential oil The use of oil, which can not only reduce cost, can also make fragrance more harmony and natural.Lotion does not stimulate mildly.And hydrosol is saturation Essential oil aqueous solution has the fragrance of the effect of a part of essential oil a variety of hydrosols made in lotion rich in level, smell Novelty is liked by customer.
Specific embodiment
In order to make the objectives, technical solutions and advantages of the present invention clearer, With reference to embodiment, to this Invention is further described.It should be understood that these descriptions are merely illustrative, and it is not intended to limit the scope of the invention.This Outside, in the following description, descriptions of well-known structures and technologies are omitted, so as not to unnecessarily obscure the concept of the present invention.
According to the application embodiment, a kind of preparation method of lotion, comprising the following steps:
S1: water, moisturizer, thickener, emulsifier, emollient, assistant for emulsifying agent are prepared into basal liquid.Wherein, water can be Pure water, deionized water or cosmetics dedicated water, but be not limited to it is above-mentioned enumerate, preferably deionized water.
S2: being added emulsion pot for basal liquid, stir while adding, and after carrying out homogeneous while agitating, continues stirring simultaneously Carry out cooling processing.Wherein cool-down method can be cold cooling water cycle water, fan for cooling and natural cooling, but be not limited to above-mentioned It enumerates, preferably natural cooling.
S3: when being down to the first preset temperature to temperature, being added deodorant tune, stir evenly, and be cooled to the second preset temperature, Obtain lotion.
In an alternative embodiment, deodorant tune includes rose, peppermint hydrosol, lavender hydrosol, balm hydrosol, lemon Lemon Verbena officinalis hydrosol, flores aurantii hydrosol, chamomile hydrosol, white pond lily hydrosol and/or lotus hydrosol.
The deodorant tune further includes Rhododendron fastigiatum extracting solution.
Hydrosol refers to essential oil during distillation extraction, the steaming that the one kind 100% separated when refining essential oil is saturated Stoste is evaporated, is a kind of byproduct of essential oil, composition is naturally pure, and fragrance is light pleasant.Deodorant tune can also be it in the present invention It applies to the hydrosol of cosmetic industry.
Wherein, rose is that the way of distillation is refined, and just has slightly sour taste by high temperature and pressure, what essence blended out Product does not have the taste of draft.Include inside rose is the volatile aromatic ingredient of a large amount of fresh rose flower, it is simultaneously Fragrance ingredient containing macromolecular.Have the effects that keep the skin wet, moisturizing, quick anti-inflammatory, antiallergy, it is antipruritic, delay senescence.
Peppermint hydrosol breath is pure and fresh.With being highly suitable for improving easy fecula thorn or the coarse skin of pore.To itching, Inflammation, the skin burnt have the effect of alleviation.
Lavender hydrosol has dense flowers and plants fragrant, it is easy to can recognize and draw, allow people to loosen completely and releive have excellent The effect of good anti-inflammation and sterilization and balanced adjustment skin fat secretion effect.
Balm hydrosol smell is lighter, with bitter lemonene.Has effects that anti-oxidant and anti-inflammatory.
The smell of lemon verbena hydrosol is simple and elegant, mixes the salubrious of green grass tender shoots with a lemonene, is very easy to allow People receives.Have effects that restrain anti-inflammatory, disinfection and sterilization.
Flores aurantii hydrosol (flavouring agent, skin whitening, moisturizing ingredient) containing thatch alcohol, linalool, young tiger geraniol, nerol, stupid ethyl alcohol, Geraniol, rose oxide, rosefuran, with Quercetin, flavonoids, tannin, vitamin B and vitamin E, beta carotene and more Kind amino acid, several mineral materials.Smell has the lily flowery odour of a bitter taste, flavour of a drug.Have both the double action of whitening and moisturizing.
Chamomile hydrosol smell is strong, has the sense of moisturizing antiallergic, eliminates skin sensitivity, go black eye, restrains, anti-inflammatory, disappears The effect of swollen analgesic, elimination red capillary, tightening pore, calm skin.
Deodorant tune be preferably rose, peppermint hydrosol, lavender hydrosol, balm hydrosol, lemon verbena hydrosol, Two or more composition in flores aurantii hydrosol, chamomile hydrosol, the compound fragrance of a flower that a variety of hydrosols generate can more make us Pleasure is further preferably rose, peppermint hydrosol, lavender hydrosol, balm hydrosol, lemon verbena hydrosol, orange The deodorant tune of four kinds of hydrosols composition in flower hydrosol, chamomile hydrosol, is further preferably rose, peppermint hydrosol, orange Flower hydrosol, balm hydrosol, another is preferably peppermint hydrosol, lavender hydrosol, lemon verbena hydrosol, chamomile hydrosol, Another is preferably peppermint hydrosol, lavender hydrosol, rose, chamomile hydrosol.The smell of preferred hydrosol collocation is more Coordinate, mixed flavor can make one to feel comfortable.
Wherein Rhododendron fastigiatum (scientific name: Rhododendron fastigiatum), evergreen shrubs, 0.8-1 meters high, branch is thick It is close, often at cushion or prostrate.Sprout is short, band bronzing, by crineous scale.Leaf bud squama is caducous.Leaf collection is born in sprig top, leather Matter, oblong, ellipse or it is oval above dirty-green, below celadon.Inflorescence basidixed, the total shape of umbrella shape, there is colored 3-5;Corolla Wide funnel-form, 1-1.5 centimetres long, hyacinthine or fresh lilac red.Capsule oval.The month at florescence 5-6, the fruiting period 8-9 month.It is born in rock Slope, cliff, high mountain gravel meadow, tor shrubbery, rose bay shrublet or occasionally under pine forest, produce Qinghai, Sichuan, Yunnan.It should Species are because of flower beauty, bright-colored, artificial cultivation, horticultural importance with higher.
It is generally acknowledged that containing azalaic acid in azalea, also known as azelaic acid, azalaic acid have antibiotic property, and it is anti-to can be used as food Rotten agent.Just there is apparent antibacterial effect when azalaic acid concentration reaches 20%.
In an alternative embodiment, step S3 specifically includes the following steps:
S31: when temperature is down to 45~55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot.
S32: taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pot, then taking parts by weight is 6~9 One of part rose, 3~5 parts of peppermint hydrosols, 10~13 parts of lavender hydrosols, 4~8 parts of chamomile hydrosols are a variety of pure Dew is added in emulsion pot.
S33: being cooled to 32~35 DEG C after mixing evenly, and discharging, encapsulation obtain lotion.
Being cooled to 45~55 DEG C can be 45 DEG C, 46 DEG C, 47 DEG C, 48 DEG C, 49 DEG C, 50 DEG C, 51 DEG C, 52 DEG C, 53 DEG C, 54 DEG C, 55 DEG C but be not limited to above-mentioned enumerate.For example, can be increased or decreased according to environmental condition is appropriate, for example, can for 35~ 50 DEG C, or be 52~62 DEG C.
Being cooled to 32~35 DEG C can be 32 DEG C, 33 DEG C, 34 DEG C, 35 DEG C but be not limited to above-mentioned enumerate.For example, can basis Environmental condition is appropriate to be increased or decreased, such as can be 20~32 DEG C, or be 33~40 DEG C.
The fragrance and effective component of hydrosol can not only be kept by adding plant hydrosol at 45~55 DEG C, moreover it is possible to mix lotion Uniformly, quality is more stable.
The fragrance for matching to obtain of deodorant tune according to the invention is more coordinated, not the fragrance in ratio range of the present invention Harmony be deteriorated.
In the present embodiment, the parts by weight of Rhododendron fastigiatum extracting solution can for 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts it is equal but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 12~14 parts, 11 ~13 parts, or be 11.5~14.5 parts.The pleasantly surprised discovery Rhododendron fastigiatum extracting solution of inventor can not only reconcile various hydrosols Smell be allowed to more harmonious, there are also good bacteriostasis efficacy.When the parts by weight of addition are 10~15 parts, fungistatic effect reaches To best, good fungistatic effect can not be played when the parts by weight of addition are less than 10 parts, when the parts by weight of addition are greater than Fragrance can be made uncoordinated at 15 parts.
The parts by weight of rose can for 6 parts, 7 parts, 8 parts, 9 parts etc. but be not limited to it is above-mentioned enumerate, can be according to reality The effect adjustment appropriate of border mixing, such as can be 10~15 parts, 8~20 parts, or be 5~12 parts.
The parts by weight of peppermint hydrosol can for 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixed The adjustment appropriate of the effect of conjunction, such as can be 2~6 parts, 5~10 parts, or be 2~15 parts.
The parts by weight of lavender hydrosol can for 10 parts, 11 parts, 12 parts, 13 parts etc. but be not limited to it is above-mentioned enumerate, can be with It according to the effect actually mixed adjustment appropriate, such as can be 5~15 parts, 2~16 parts, or be 9~18 parts.
The parts by weight of balm hydrosol can for 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, Can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~15 parts, or be 8~18 parts.
The parts by weight of lemon verbena hydrosol can for 1 part, 2 parts etc. but be not limited to it is above-mentioned enumerate, can be according to reality The adjustment appropriate of mixed effect, such as can be 2~6 parts, 3~10 parts, or be 2~15 parts.
The parts by weight of flores aurantii hydrosol can for 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, can be according to reality The effect adjustment appropriate of border mixing, such as can be 2~8 parts, 6~12 parts, or be 3~15 parts.
The parts by weight of chamomile hydrosol can for 4 parts, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to it is above-mentioned enumerate, can be with It according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts, or be 6~15 parts.
In an alternative embodiment, can also include: before or after step S32 and in step S32
Taking parts by weight again is that 3~5 parts of white pond lily hydrosols and/or 2~6 parts of lotus hydrosols are added in emulsion pot.
The parts by weight of white pond lily hydrosol can for 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be according to reality The adjustment appropriate of mixed effect, such as can be 2~6 parts, 5~10 parts, or be 6~15 parts.
The parts by weight of lotus hydrosol can for 2 parts, 3 parts, 4 parts, 5 parts, 6 parts etc. but be not limited to it is above-mentioned enumerate, Ke Yigen The factually effect adjustment appropriate of border mixing, such as can be 1~6 part, 2~8 parts, or be 3~10 parts.
The smell between a variety of hydrosols can be made more to coordinate using white pond lily hydrosol and/or lotus hydrosol, and in smell Increase the fragrance of white pond lily and/or lotus, both smells are more rare in lotion, keep the fragrance of lotion more novel.
In an alternative embodiment, which is characterized in that in step S1:
Moisturizer includes polyethylene glycol and glycerol;
Thickener includes xanthan gum or hydroxyethyl cellulose;
Emollient includes isobutyl palmitate, glyceryl monostearate, hexadecanol, stearic acid, lanolin;
Emulsifier includes hexadecanyl phosphate potassium;
Assistant for emulsifying agent includes monoglyceride or glyceryl monolaurate.
In an alternative embodiment, step S1 specifically includes the following steps:
S11: taking parts by weight respectively is 5~50 parts of water, 7~12 parts of moisturizer and 0.05~0.5 part of thickener It sequentially adds in stirring container.In the present embodiment, the parts by weight of water can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 Part, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 Part, 27 parts, 28 parts, 29 parts, 30 parts, 31 parts, 32 parts, 33 parts, 34 parts, 35 parts, 36 parts, 37 parts, 38 parts, 39 parts, 40 parts, 41 Part, 42 parts, 43 parts, 44 parts, 45 parts, 46 parts, 47 parts, 48 parts, 49 parts, 50 parts etc. but be not limited to it is above-mentioned enumerate, can be according to reality The parts by weight of the effect of border mixing and the content of other materials adjustment water appropriate, preferably 25~35 parts, such as can Think 45~55 parts, 65~70 parts, 30~60 parts, or is 35~65 parts.
S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C, heating time is preferably 20~60 minutes, is further preferably 25~45 minutes;In the present embodiment, it heats It can be 20 minutes, 21 minutes, 22 minutes, 23 minutes, 25 minutes, 28 minutes, 32 minutes, 37 points more than or equal to 20 minutes Clock, 44 minutes, 48 minutes, 50 minutes, 55 minutes, 60 minutes etc. but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed The duration of the degree of fruit and dissolution adjustment heating appropriate.Temperature rise to 80~85 DEG C can for 81 DEG C, 82 DEG C, 83 DEG C, 84 DEG C but it is not limited to above-mentioned enumerate.For example, can be increased or decreased according to environmental condition is appropriate to the first preset temperature, such as It can be 80~100 DEG C, or be 70~85 DEG C.
S13: stopping heating being completely dissolved up to moisturizer, obtains the first mixed liquor.
In an alternative embodiment, step S11 is specifically included:
S111: the water that parts by weight are 5~50 parts is taken to be added in stirring container;
S112: taking parts by weight is that 2~5 parts of glycerol and 5~7 parts of polyethylene glycol sequentially add in stirring container;It is sweet The parts by weight of oil can for 2 parts, 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be suitable according to the effect actually mixed When adjustment, such as can be 3~8 parts, 4~6 parts etc..The parts by weight of polyethylene glycol can be 5 parts, 6 parts, 7 parts etc. but not Be limited to it is above-mentioned enumerate, can according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts etc..
S113: parts by weight are taken to stir for 0.05~0.5 part of xanthan gum or the addition of 0.1~0.4 part of hydroxyethyl cellulose It mixes in container.The parts by weight of xanthan gum can for 0.05 part, 0.06 part, 0.07 part, 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.47 part, 0.48 part, 0.49 part, 0.5 part etc. but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed tune appropriate It is whole, such as can be 0.02~0.6 part, 0.25~1.0 part etc..The parts by weight of hydroxyethyl cellulose can be 0.1 part, 0.2 Part, 0.3 part, 0.4 part etc. but be not limited to it is above-mentioned enumerate, can be according to the effect actually mixed adjustment appropriate, such as can be 0.2~0.6 part, 0.5~1.0 part etc..
In an alternative embodiment, step S1 is specifically further comprising the steps of:
S11 ': taking parts by weight respectively is 12.2~28 parts of emollient, 1~2 part of emulsifier, 2~5 parts of assistant for emulsifying agents It sequentially adds in stirring container;
S12 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C.
S13 ': stopping heating being uniformly mixed up to emollient, obtains the second mixed liquor.
In an alternative embodiment, step S11 ' is specifically included:
S11 ' 1: taking parts by weight is 3~8 parts of isobutyl palmitate, 5~10 parts of glyceryl monostearate, 1~3 part Hexadecanol, 3~5 parts of stearic acid, 0.2~2 part lanolin be added stirring container in;
S11 ' 2: the hexadecanyl phosphate potassium that parts by weight are 1~2 part is taken to be added in stirring container;
S11 ' 3: the monoglyceride or 2~5 parts of glyceryl monolaurate addition stirring container that parts by weight are 2~4 parts are taken It is interior.
The parts by weight of isobutyl palmitate can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to above-mentioned column It lifts, can be according to the effect actually mixed adjustment appropriate, such as can be 2~9 parts, 5~15 parts etc..
The parts by weight of glyceryl monostearate can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to above-mentioned It enumerates, can be according to the effect actually mixed adjustment appropriate, such as can be 2~8 parts, 5~15 parts etc..
The parts by weight of hexadecanol can for 1 part, 2 parts, 3 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixing Effect adjustment appropriate, such as can be 3~8 parts, 4~6 parts etc..
Stearic parts by weight can for 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixing Effect adjustment appropriate, such as can be 2~6 parts, 5~15 parts etc..
The parts by weight of lanolin can be 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 Part, 1.0 parts, 1.1 parts, 1.2 parts, 1.3 parts, 1.4 parts, 1.5 parts, 1.6 parts, 1.7 parts, 1.8 parts, 1.9 parts, 2.0 parts etc. but unlimited It is enumerated in above-mentioned, can be according to the effect actually mixed adjustment appropriate, such as can be 0.1~0.8 part, 0.4~4.0 part Deng.
The parts by weight of hexadecanyl phosphate potassium can for 1 part, 2 parts etc. but be not limited to it is above-mentioned enumerate, can be according to reality The effect adjustment appropriate of border mixing, such as can be 3~5 parts, 4~8 parts etc..
The parts by weight of monoglyceride can for 2 parts, 3 parts, 4 parts etc. but be not limited to it is above-mentioned enumerate, can be according to practical mixing Effect adjustment appropriate, such as can be 1~5 part, 5~10 parts etc..
The parts by weight of glyceryl monolaurate can for 2 parts, 3 parts, 4 parts, 5 parts etc. but be not limited to it is above-mentioned enumerate, can be with It according to the effect actually mixed adjustment appropriate, such as can be 1~8 part, 5~10 parts etc..
In an alternative embodiment, step S1 is specifically further comprising the steps of:
By the first mixed liquor and the second mixed liquor, basal liquid is obtained.
Embodiment 1
Taking parts by weight is that 42 parts of water, 2 parts of glycerol and 5 parts of polyethylene glycol sequentially add in stirring container;It takes again The xanthan gum that parts by weight are 0.05 part is added in stirring container.The stirring container is heated 20 minutes, and is stirred in heating It mixes, fluid temperature is made to rise to 80 DEG C, stopping heating being completely dissolved up to glycerol and polyethylene glycol, obtains the first mixed liquor.
Taking parts by weight is 3 parts of isobutyl palmitate, 5 parts of glyceryl monostearate, 1 part of hexadecanol, 3 parts hard Resin acid, 0.2 part of lanolin, 1 part of hexadecanyl phosphate potassium, 2 parts of monoglyceride are added in another stirring container.To institute It states stirring container to heat 20 minutes, and heats while stirring, fluid temperature is made to rise to 80 DEG C, stop heating until mixing is equal It is even, obtain the second mixed liquor.
By first mixed liquor and second mixed liquor, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, carries out homogeneous after five minutes while agitating, is continued It stirs and carries out cooling processing;When temperature is down to 45 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot;Take weight Measure number and be that 10 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pots, then take parts by weight be 6 parts of roses, 3 parts of peppermint hydrosols, 10 parts of lavender hydrosols, 4 parts of chamomile hydrosols are added in emulsion pot;Taking parts by weight again is that emulsification is added in 2 parts of white pond lily hydrosols In pot.It is cooled to 32 DEG C after mixing evenly, discharging, encapsulation obtain lotion.
Embodiment 2
Taking parts by weight is that 20 parts of water, 2 parts of glycerol and 6 parts of polyethylene glycol sequentially add in stirring container;It takes again The xanthan gum that parts by weight are 0.3 part is added in stirring container.The stirring container is heated 25 minutes, and is stirred in heating It mixes, fluid temperature is made to rise to 83 DEG C, stopping heating being completely dissolved up to glycerol and polyethylene glycol, obtains the first mixed liquor.
Taking parts by weight is 6 parts of isobutyl palmitate, 8 parts of glyceryl monostearate, 2 parts of hexadecanol, 4 parts hard Another stirring container is added in resin acid, 1 part of lanolin, 1 part of hexadecanyl phosphate potassium, 3 parts of glyceryl monolaurate It is interior.The stirring container is heated 25 minutes, and is heated while stirring, fluid temperature is made to rise to 83 DEG C, stop heating until It is uniformly mixed, obtains the second mixed liquor.
By first mixed liquor and second mixed liquor, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, carries out homogeneous after five minutes while agitating, is continued It stirs and carries out cooling processing;When temperature is down to 50 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot;Take weight Measure number and be that 11 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pots, then take parts by weight be 7 parts of roses, 4 parts of peppermint hydrosols, 10 parts of lavender hydrosols, 6 parts of chamomile hydrosols are added in emulsion pot;Taking parts by weight again is 4 parts of white pond lily hydrosols and 4 parts of lotuses Hydrosol is added in emulsion pot.It is cooled to 33 DEG C after mixing evenly, discharging, encapsulation obtain lotion.
Embodiment 3
Taking parts by weight is that 5 parts of water, 5 parts of glycerol and 7 parts of polyethylene glycol sequentially add in stirring container;Weight is taken again Amount number is or 0.4 part of hydroxyethyl cellulose is added in stirring container.The stirring container is heated 30 minutes, and side is heated Side stirring makes fluid temperature rise to 85 DEG C, and stopping heating being completely dissolved up to glycerol and polyethylene glycol, obtains the first mixing Liquid.
Taking parts by weight is 8 parts of isobutyl palmitate, 10 parts of glyceryl monostearate, 3 parts of hexadecanol, 5 parts Stearic acid, 2 parts of lanolin, 2 parts of hexadecanyl phosphate potassium, 4 parts of monoglyceride are added in another stirring container.To institute It states stirring container to heat 30 minutes, and heats while stirring, fluid temperature is made to rise to 85 DEG C, stop heating until mixing is equal It is even, obtain the second mixed liquor.
By first mixed liquor and second mixed liquor, basal liquid is obtained.
Emulsion pot is added in the basal liquid, is stirred while adding, carries out homogeneous after five minutes while agitating, is continued It stirs and carries out cooling processing;When temperature is down to 55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot;Take weight Measure number and be that 15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pots, then take parts by weight be 9 parts of roses, 5 parts of peppermint hydrosols, 13 parts of lavender hydrosols, 8 parts of chamomile hydrosols are added in emulsion pot.It is cooled to 35 DEG C after mixing evenly, discharging, encapsulation obtain Lotion.
Essence, the lotion of essential oil blending and lotion of the present invention compare
(1) test specimen: the lotion of 1-3 of embodiment of the present invention preparation;Add the lotion of flavoring rose essence, additive amount 0.15 Part, do not add hydrosol;The lotion of Rosa Damascana is added, additive amount is 0.15 part, does not add hydrosol;Add a kind of cream of hydrosol Liquid adds 8 parts of roses.
(2) subject: 60 healthy males and women (each 30), the age was at 20~40 years old.
(3) it application method: before sleeping at night and after morning warm water face cleaning, takes appropriate test specimen to be applied to the centre of the palm, applies later The absorption pressed lightly in cheek to promote test specimen effective component is smeared, then replacement examination in one week is used continuously in every kind of sample Test sample.Subject does not use other cosmetics during the test.
(4) judgment criteria: Cost comparisons, technical staff by calculate lotion cost provide required for every liter of lotion at This.Test 6 weeks by a definite date, the test subject afterwards that expires evaluate the trial target that oneself is used, and are divided into fragrance to when using Sense comparison, is respectively divided into three grades.
(5) test result is shown in Table 1
1 essence of table, the lotion of essential oil blending and lotion of the present invention compare
As seen from the above table, the lotion cost for adding essential oil is higher compared with other lotions, although adding the lotion cost of essence just Preferably but the comfort level of its fragrance and the use feeling of lotion are all poor compared with other lotions.Embodiment 1-3 is the lotion for adding hydrosol, they Be not much different in use feeling, but add in fragrance comparison the lotions of a variety of hydrosols than only add the lotion of a kind of hydrosol more by To liking for subject, preferred embodiment 2 feels the comfortable people of fragrance up to 78%, it is believed that its fragrance is difficult to the number received It is least.The lotion that embodiment 2 is prepared compared with embodiment 3 is added to lotus and white pond lily hydrosol more, and the evaluation of fragrance is also more It is good.
Lotion antibacterial situation of the present invention
Test specimen is lotion prepared by the embodiment of the present invention 1 and embodiment 3, and wherein Rhododendron fastigiatum extracting solution is scaled Percentage concentration, the concentration of Rhododendron fastigiatum extracting solution is about 10% in embodiment 1, the concentration of Rhododendron fastigiatum extracting solution in embodiment 3 About 15%.Also it is prepared for the blank control group without Rhododendron fastigiatum extracting solution, and the cream containing Rhododendron fastigiatum extracting solution 5% Liquid is as control.Bacterium colony challenge experiment is carried out, the results are shown in Table 2.
2 lotion antibacterial situation of table
Note: in one column of mushroom, " B " indicates mixed cell: Escherichia coli (ATCC11229), staphylococcus aureus (ATCC6538), pseudomonas aeruginosa (ATCC15442);" M " indicates mould: aspergillus niger (ATCC16404);" Y " indicates white Candida albicans (ATCC10231).Test temperature: bacterium is 32.5 ± 2.5 DEG C, and mould, saccharomycete are 28 ± 1 DEG C;28 days.
Symbol As a result Micro organism quantity
- Without growth ﹤ 100
A small amount of growth About 102
﹢ ﹢ Moderate growth About 103
﹢+﹢ Raised growth About 104
﹢ ++ ﹢ Severe growth About 105
C Cover surface ﹥ 106
The product emulsion of the Rhododendron fastigiatum extracting solution of description of test addition 10%~15% also has while providing fragrance There is good bacteriostasis efficacy.
It should be understood that above-mentioned specific embodiment of the invention is used only for exemplary illustration or explains of the invention Principle, but not to limit the present invention.Therefore, that is done without departing from the spirit and scope of the present invention is any Modification, equivalent replacement, improvement etc. should all include within protection scope of the present invention.In addition, appended claims purport of the present invention Covering the whole variations fallen into attached claim scope and boundary or this range and the equivalent form on boundary and is repairing Change example.
In the description of the present invention, it should be noted that term " first ", " second ", " third " are used for description purposes only, It is not understood to indicate or imply relative importance.

Claims (10)

1. a kind of preparation method of lotion, which is characterized in that include the following steps,
S1: water, moisturizer, thickener, emulsifier, emollient, assistant for emulsifying agent are prepared into basal liquid;
S2: being added emulsion pot for the basal liquid, stir while adding, and after carrying out homogeneous while agitating, continues stirring simultaneously Carry out cooling processing;
S3: when being down to the first preset temperature to temperature, deodorant tune is added, stirs evenly, and be cooled to the second preset temperature, obtains Lotion.
2. changing the preparation method of lotion according to claim 1, which is characterized in that the deodorant tune includes rose, thin Lotus hydrosol, lavender hydrosol, balm hydrosol, lemon verbena hydrosol, flores aurantii hydrosol, chamomile hydrosol, white pond lily hydrosol and/ Or lotus hydrosol;
The deodorant tune further includes Rhododendron fastigiatum extracting solution.
3. preparation method according to claim 2, which is characterized in that the step S3 specifically includes the following steps:
S31: when temperature is down to 45~55 DEG C, taking parts by weight is that 0.3 part of vitamin E is added in emulsion pot;
S32: taking parts by weight is that 10~15 parts of Rhododendron fastigiatum extracting solutions are added in emulsion pot, then taking parts by weight is 6~9 parts of roses One of rare hydrosol, 3~5 parts of peppermint hydrosols, 10~13 parts of lavender hydrosols, 4~8 parts of chamomile hydrosols or a variety of hydrosols add Enter in emulsion pot, then taking parts by weight is that 2~6 parts of white pond lily hydrosols and/or 3~5 parts of lotus hydrosols are added in emulsion pot.
S33: being cooled to 32~35 DEG C after mixing evenly, and discharging, encapsulation obtain lotion.
4. the preparation method of lotion according to claim 1, which is characterized in that in the step S1:
The moisturizer includes polyethylene glycol and glycerol;
The thickener includes xanthan gum or hydroxyethyl cellulose;
The emollient includes isobutyl palmitate, glyceryl monostearate, hexadecanol, stearic acid, lanolin;
The emulsifier includes hexadecanyl phosphate potassium;
The assistant for emulsifying agent includes monoglyceride or glyceryl monolaurate.
5. the preparation method of lotion according to claim 4, which is characterized in that the step S1 specifically includes the following steps:
S11: take respectively parts by weight be 5~50 parts of water, 7~12 parts of moisturizer and 0.05~0.5 part of thickener successively It is added in stirring container;
S12: stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C;
S13: stopping heating being completely dissolved up to the moisturizer, obtains the first mixed liquor.
6. the preparation method of lotion according to claim 5, which is characterized in that the step S11 is specifically included:
S111: the water that parts by weight are 5~50 parts is taken to be added in stirring container;
S112: taking parts by weight is that 2~5 parts of glycerol and 5~7 parts of polyethylene glycol sequentially add in stirring container;
S113: the xanthan gum or 0.1~0.4 part of hydroxyethyl cellulose addition stirring appearance that parts by weight are 0.05~0.5 part are taken In device.
7. the preparation method of lotion according to claim 5, which is characterized in that the step S1 specifically further includes following step It is rapid:
S11 ': take respectively parts by weight be 12.2~28 parts of emollient, 1~2 part of emulsifier, 2~5 parts of assistant for emulsifying agents successively It is added in stirring container;
S12 ': stirring container heating is greater than or equal to 20 minutes, and is heated while stirring, fluid temperature is made to rise to 80 ~85 DEG C;
S13 ': stopping heating being uniformly mixed up to emollient, obtains the second mixed liquor.
8. the preparation method of lotion according to claim 7, which is characterized in that the step S11 ' is specifically included:
S11 ' 1: taking parts by weight is 3~8 parts of isobutyl palmitate, 5~10 parts of glyceryl monostearate, the ten of 1~3 part Six alcohol, 3~5 parts of stearic acid, 0.2~2 part of lanolin are added in stirring container;
S11 ' 2: the hexadecanyl phosphate potassium that parts by weight are 1~2 part is taken to be added in stirring container;
S11 ' 3: it takes in the monoglyceride or 2~5 parts of glyceryl monolaurate addition stirring container that parts by weight are 2~4 parts.
9. the preparation method of lotion according to claim 7, which is characterized in that the step S1 specifically further includes following step It is rapid:
First mixed liquor and second mixed liquor are mixed, basal liquid is obtained.
10. a kind of lotion, which is characterized in that be prepared using preparation method as claimed in claims 1-9.
CN201910221904.XA 2019-03-22 2019-03-22 A kind of lotion and preparation method thereof Pending CN109793683A (en)

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