CN109864340A - One kind is refreshed oneself the filter tip and preparation method thereof that hawks - Google Patents
One kind is refreshed oneself the filter tip and preparation method thereof that hawks Download PDFInfo
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- CN109864340A CN109864340A CN201910289947.1A CN201910289947A CN109864340A CN 109864340 A CN109864340 A CN 109864340A CN 201910289947 A CN201910289947 A CN 201910289947A CN 109864340 A CN109864340 A CN 109864340A
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Abstract
The present invention discloses one kind and refreshes oneself the filter tip that hawks, including the first filter fiber section, adsorption section, the second filter fiber section, tipping roll paper, quick-fried pearl, it is characterized in that, the first filter fiber section and the second filling-modified acetate fiber of filter fiber intersegmental part, adsorption section inside filling activation Mayan is blue；The invention also discloses a kind of preparation methods of filter tip of hawking of refreshing oneself, and include the following steps: the preparation of step S1, modified acetate fiber；Step S2, the preparation of Mayan indigo plant is activated；Step S3；Modified acetate fiber can enhance the filter effect to nicotine gas; also it can be improved the filter effect to harmful substances such as nicotines; Mayan indigo plant hole after activation is more small; specific surface area is bigger; the harmful substances such as adsorptive nicotine can further be gone; reduction is injured caused by smoker, and quick-fried pearl can reduce the mouthfeel of flue gas moderate stimulation and provide a kind of refrigerant sweet refreshing mouthfeel, while protect to the throat of smoker.
Description
Technical field
The present invention relates to a kind of cigarette filter, specially one kind is refreshed oneself the filter tip and preparation method thereof that hawks.
Background technique
Cigarette filter refers to the upper part of cigarette, for filtering out the tar in a part sucking flue gas, reduces smoker
Sense of discomfort after smoking.With the development of science and technology, the type of filter tip itself also has changed a lot.Currently, vinegar ester is fine
Filter tip made of tieing up is the one kind being widely used, and includes particle in cigarette smoke, normally referred to as tar.Contain in tar
There are a large amount of ingredients, is all tobacco imperfect combustion object.It also include other substances in cigarette smoke outside tar removing, such as " steam "
Or " gas " phase, it also include volatile result of combustion of tobacco substance, such as acetaldehyde and other low molecule weight items.In cigarette smoke
Other phases, such as " half volatile " phase be equal including many combustible substances with particle and steam phase.
But still there are many disadvantages for existing filter tip, the filter effect of acetate fiber is not ideal enough, still there is many nocuousness
Substance can enter human body, and the harmful substance in flue gas can cause to damage to the throat of smoker itself.
Summary of the invention
In order to overcome above-mentioned technical problem, the present invention provides one kind and refreshes oneself the filter tip and preparation method thereof that hawks.It is modified
Acetate fiber can enhance the filter effect to nicotine gas, also can be improved the filter effect to harmful substances such as nicotines, living
Mayan indigo plant hole after change is more small, and specific surface area is bigger, can further go the harmful substances such as adsorptive nicotine, reduction pair
It is injured caused by smoker, quick-fried pearl can reduce the mouthfeel of flue gas moderate stimulation and provide a kind of refrigerant sweet refreshing mouthfeel, simultaneously
The throat of smoker is protected.
The purpose of the present invention can be achieved through the following technical solutions:
One kind is refreshed oneself the filter tip that hawks, including the first filter fiber section, adsorption section, the second filter fiber section, tipping roll paper,
Quick-fried pearl, the first filter fiber section and the second filling-modified acetate fiber of filter fiber intersegmental part, adsorption section inside filling activation Ma
Refined indigo plant；
The hawk preparation method of filter tip of refreshing oneself includes the following steps:
Step S1, the preparation of modified acetate fiber:
(1) acetate fiber is put into the beaker equipped with dehydrated alcohol, places the beaker in 75 DEG C of water-bath, at the uniform velocity stirs
20min to be mixed, acetate fiber taking-up is placed in drying box dry 15min after stirring, control drying box temperature is 60 DEG C,
The weight ratio for controlling acetate fiber and dehydrated alcohol is 2: 7；
(2) oxalic acid is added in the beaker equipped with deionized water, beaker is carried out to be warming up to 60 DEG C, is at the uniform velocity stirred, to grass
After acid dissolution, the acetate fiber cleaned up is added, is taken out after reacting 2h, controls oxalic acid, deionized water, the weight of acetate fiber
Than being 1: 10: 3；
(3) vacuum dehydration after drying is added in the beaker equipped with dehydrated alcohol, and heating water bath reacts 30h, take to 80 DEG C
Out, being transferred to vacuum degree is -0.10MPa, and modified acetate fiber is made in dry 5h in the vacuum oven that temperature is 65 DEG C；
Step S2, it activates the preparation of Mayan indigo plant: (a) Mayan indigo plant being put into Muffle furnace after 350 DEG C of calcining 1h and is added
In 100mL10% sodium chloride solution, 70 DEG C of heating water bath 2h；(b) it is molten that 50mL20% sodium hydroxide is added into sodium chloride solution
Liquid, is warming up to 80 DEG C, and ultrasound stirs 20min；(c) it filters, the Mayan indigo plant after activation is placed in a beaker, is rushed with deionized water
It washes, until solution is in neutrality, filters again, after Mayan indigo plant is placed in 80 DEG C of drying boxes dry 2h, 50 meshes are crossed in grinding；
Step S3, modified acetate fiber sizing is regard as the first filter fiber section and the second filter fiber section, in the first mistake
It filters segment of fiber and quick-fried pearl is installed close to one end of pipe tobacco, the Mayan indigo plant after the installation activation of the first filter fiber section other end, which is used as, inhales
Attached section, the adsorption section other end connect the second filter fiber section, tipping roll paper by the first filter fiber section, the second filter fiber section,
Adsorption section coats to form filter tip.
Acetate fiber is widely used in preparing cigarette filter tip, but it is not good enough to nicotine gas filter effect, and can only
The quantity of the harmful substances such as less filtering nicotine, most of still by smoker, the present invention is by oxalic acid to acetate fiber
It is modified to carry out surface, oxalic acid molecule is grafted on acetate fiber molecule, still contains carboxyl in the oxalic acid molecule after grafting, so that
Modified acetate fiber polarity enhancing, can further enhance the filter effect to nicotine gas, can also enhance to nicotine
Etc. harmful substances filter effect.
Further, the quick-fried pearl is made of following raw material: 35-50 parts of Peppermint essential oils, 15-25 parts of Poria cocos essences
Oil, 20-30 parts of Radix Scrophulariae extracts, 10-15 parts of Fructus Monordicae extracts, 5-15 parts of tendril-leaved fritillary bulb extracts, 3-8 parts of Scaphium scaphigerum extracts.
Further, the quick-fried pearl is made by the following method:
(1) Peppermint essential oil, Poria cocos essential oil, Radix Scrophulariae extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, the sterculia seed are extracted
Object is uniformly mixed, and essence is made；
(2) olive oil is mixed with polyglyceryl fatty acid ester, sucrose fatty ester is added, 35 DEG C of heating water baths simultaneously stir
Essence obtained in step (1) is added in 30min, stirs 2h, and essential oil is made, and controls olive oil, polyglyceryl fatty acid ester, essence
Weight ratio be 5: 1: 3；
(3) essential oil is added in pill dripping machine hopper, dripping pill lapping is added in rubber cement tank, controlled at 65 DEG C,
Essential oil is wrapped in dripping pill lapping by pill dripping machine, quick-fried pearl is made in curing molding.
Further, dripping pill lapping is made by the following method in step (3): by sodium alginate and gelatin according to 6: 1
Ratio be placed in reaction kettle and mixed, deionized water is added, is warming up to 80 DEG C, stirring keeps the temperature 3h, wait steep at this temperature
Foam is filtered after floating, and dripping pill lapping is made.
A kind of preparation method of filter tip of hawking of refreshing oneself, includes the following steps:
Step S1, the preparation of modified acetate fiber:
(1) acetate fiber is put into the beaker equipped with dehydrated alcohol, places the beaker in 75 DEG C of water-bath, at the uniform velocity stirs
20min to be mixed, acetate fiber taking-up is placed in drying box dry 15min after stirring, control drying box temperature is 60 DEG C,
The weight ratio for controlling acetate fiber and dehydrated alcohol is 2: 7；
(2) oxalic acid is added in the beaker equipped with deionized water, beaker is carried out to be warming up to 60 DEG C, is at the uniform velocity stirred, to grass
After acid dissolution, the acetate fiber cleaned up is added, is taken out after reacting 2h, controls oxalic acid, deionized water, the weight of acetate fiber
Than being 1: 10: 3；
(3) vacuum dehydration after drying is added in the beaker equipped with dehydrated alcohol, and heating water bath reacts 30h, take to 80 DEG C
Out, being transferred to vacuum degree is -0.10MPa, and modified acetate fiber is made in dry 5h in the vacuum oven that temperature is 65 DEG C；
Step S2, it activates the preparation of Mayan indigo plant: (a) Mayan indigo plant being put into Muffle furnace after 350 DEG C of calcining 1h and is added
In 100mL10% sodium chloride solution, 70 DEG C of heating water bath 2h；(b) it is molten that 50mL20% sodium hydroxide is added into sodium chloride solution
Liquid, is warming up to 80 DEG C, and ultrasound stirs 20min；(c) it filters, the Mayan indigo plant after activation is placed in a beaker, is rushed with deionized water
It washes, until solution is in neutrality, filters again, after Mayan indigo plant is placed in 80 DEG C of drying boxes dry 2h, 50 meshes are crossed in grinding；
Step S3, modified acetate fiber sizing is regard as the first filter fiber section and the second filter fiber section, in the first mistake
It filters segment of fiber and quick-fried pearl is installed close to one end of pipe tobacco, the Mayan indigo plant after the installation activation of the first filter fiber section other end, which is used as, inhales
Attached section, the adsorption section other end connect the second filter fiber section, tipping roll paper by the first filter fiber section, the second filter fiber section,
Adsorption section coats to form filter tip.
Beneficial effects of the present invention:
(1) present invention will be by that will be modified acetate fiber as the first filter fiber section and the second filter fiber section, with activation
Mayan indigo plant installs quick-fried pearl as adsorption section, in the first filter fiber section, and modified acetate fiber can enhance the filtering to nicotine gas
Effect also can be improved the filter effect to harmful substances such as nicotines, and the Mayan indigo plant hole after activation is more small, specific surface area
It is bigger, can further go the harmful substances such as adsorptive nicotine, reduction is injured caused by smoker, by Peppermint essential oil,
The quick-fried pearl of the substances such as Poria cocos essential oil, Radix Scrophulariae extract preparation can reduce the mouthfeel of flue gas moderate stimulation and provide a kind of refrigerant
Sweet refreshing mouthfeel, while the throat of smoker is protected；
(2) it is prepared by the present invention refresh oneself hawk filter tip in use, pass through the first filter fiber section, second filtering
The synergistic effect of segment of fiber and adsorption section, not only absorbing particles phase product (tar, nicotine etc.) but also adsorption section can absorb
Vapor phase product (volatile result of combustion of tobacco substance), can effectively protect smoker.
Detailed description of the invention
In order to facilitate the understanding of those skilled in the art, the present invention will be further described below with reference to the drawings.
Fig. 1 is a kind of structural schematic diagram of filter tip of hawking of refreshing oneself of the present invention.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, all other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Referring to Fig. 1, being described in detail in conjunction with following examples:
Embodiment 1
One kind is refreshed oneself the filter tip that hawks, including the first filter fiber section 1, adsorption section 2, the second filter fiber section 3, tipping volume
Paper 4, quick-fried pearl 5, the first filter fiber section 1 and the inside of the second filter fiber section 3 filling-modified acetate fiber are filled out inside adsorption section 2
It is blue to fill activation Mayan；
The hawk preparation method of filter tip of refreshing oneself includes the following steps:
Step S1, the preparation of modified acetate fiber:
(1) acetate fiber is put into the beaker equipped with dehydrated alcohol, places the beaker in 75 DEG C of water-bath, at the uniform velocity stirs
20min to be mixed, acetate fiber taking-up is placed in drying box dry 15min after stirring, control drying box temperature is 60 DEG C,
The weight ratio for controlling acetate fiber and dehydrated alcohol is 2: 7；
(2) oxalic acid is added in the beaker equipped with deionized water, beaker is carried out to be warming up to 60 DEG C, is at the uniform velocity stirred, to grass
After acid dissolution, the acetate fiber cleaned up is added, is taken out after reacting 2h, controls oxalic acid, deionized water, the weight of acetate fiber
Than being 1: 10: 3；
(3) vacuum dehydration after drying is added in the beaker equipped with dehydrated alcohol, and heating water bath reacts 30h, take to 80 DEG C
Out, being transferred to vacuum degree is -0.10MPa, and modified acetate fiber is made in dry 5h in the vacuum oven that temperature is 65 DEG C；
Step S2, it activates the preparation of Mayan indigo plant: (a) Mayan indigo plant being put into Muffle furnace after 350 DEG C of calcining 1h and is added
In 100mL10% sodium chloride solution, 70 DEG C of heating water bath 2h；(b) it is molten that 50mL20% sodium hydroxide is added into sodium chloride solution
Liquid, is warming up to 80 DEG C, and ultrasound stirs 20min；(c) it filters, the Mayan indigo plant after activation is placed in a beaker, is rushed with deionized water
It washes, until solution is in neutrality, filters again, after Mayan indigo plant is placed in 80 DEG C of drying boxes dry 2h, 50 meshes are crossed in grinding；
Step S3, modified acetate fiber sizing is regard as the first filter fiber section 1 and the second filter fiber section 3, first
Filter fiber section 1 installs quick-fried pearl 5 close to one end of pipe tobacco, and the Mayan after the installation activation of 1 other end of the first filter fiber section is blue
As adsorption section 2,2 other end of adsorption section connects the second filter fiber section 3, is hinged with roll paper 4 for the first filter fiber section 1, second
Filter fiber section 3, the cladding of adsorption section 2 form filter tip；
The quick-fried pearl is made of following raw material: 35 parts of Peppermint essential oils, 15 parts of Poria cocos essential oils, and 20 portions of radix scrophulariaes extract
Object, 10 parts of Fructus Monordicae extracts, 5 parts of tendril-leaved fritillary bulb extracts, 3 parts of Scaphium scaphigerum extracts.
The quick-fried pearl is made by the following method:
(1) Peppermint essential oil, Poria cocos essential oil, Radix Scrophulariae extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, the sterculia seed are extracted
Object is uniformly mixed, and essence is made；
(2) olive oil is mixed with polyglyceryl fatty acid ester, sucrose fatty ester is added, 35 DEG C of heating water baths simultaneously stir
Essence obtained in step (1) is added in 30min, stirs 2h, and essential oil is made, and controls olive oil, polyglyceryl fatty acid ester, essence
Weight ratio be 5: 1: 3；
(3) essential oil is added in pill dripping machine hopper, dripping pill lapping is added in rubber cement tank, controlled at 65 DEG C,
Essential oil is wrapped in dripping pill lapping by pill dripping machine, quick-fried pearl is made in curing molding.
Embodiment 2
It is a kind of refresh oneself hawk filter tip preparation method it is as described in Example 1；
The quick-fried pearl is made of following raw material: 40 parts of Peppermint essential oils, 20 parts of Poria cocos essential oils, and 22 portions of radix scrophulariaes extract
Object, 12 parts of Fructus Monordicae extracts, 8 parts of tendril-leaved fritillary bulb extracts, 5 parts of Scaphium scaphigerum extracts.
The quick-fried pearl is made by the following method:
(1) Peppermint essential oil, Poria cocos essential oil, Radix Scrophulariae extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, the sterculia seed are extracted
Object is uniformly mixed, and essence is made；
(2) olive oil is mixed with polyglyceryl fatty acid ester, sucrose fatty ester is added, 35 DEG C of heating water baths simultaneously stir
Essence obtained in step (1) is added in 30min, stirs 2h, and essential oil is made, and controls olive oil, polyglyceryl fatty acid ester, essence
Weight ratio be 5: 1: 3；
(3) essential oil is added in pill dripping machine hopper, dripping pill lapping is added in rubber cement tank, controlled at 65 DEG C,
Essential oil is wrapped in dripping pill lapping by pill dripping machine, quick-fried pearl is made in curing molding.
Embodiment 3
It is a kind of refresh oneself hawk filter tip preparation method it is as described in Example 1；
The quick-fried pearl is made of following raw material: 45 parts of Peppermint essential oils, 22 parts of Poria cocos essential oils, and 28 portions of radix scrophulariaes extract
Object, 13 parts of Fructus Monordicae extracts, 12 parts of tendril-leaved fritillary bulb extracts, 6 parts of Scaphium scaphigerum extracts.
The quick-fried pearl is made by the following method:
(1) Peppermint essential oil, Poria cocos essential oil, Radix Scrophulariae extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, the sterculia seed are extracted
Object is uniformly mixed, and essence is made；
(2) olive oil is mixed with polyglyceryl fatty acid ester, sucrose fatty ester is added, 35 DEG C of heating water baths simultaneously stir
Essence obtained in step (1) is added in 30min, stirs 2h, and essential oil is made, and controls olive oil, polyglyceryl fatty acid ester, essence
Weight ratio be 5: 1: 3；
(3) essential oil is added in pill dripping machine hopper, dripping pill lapping is added in rubber cement tank, controlled at 65 DEG C,
Essential oil is wrapped in dripping pill lapping by pill dripping machine, quick-fried pearl is made in curing molding.
Embodiment 4
It is a kind of refresh oneself hawk filter tip preparation method it is as described in Example 1；
The quick-fried pearl is made of following raw material: 50 parts of Peppermint essential oils, 25 parts of Poria cocos essential oils, and 30 portions of radix scrophulariaes extract
Object, 15 parts of Fructus Monordicae extracts, 15 parts of tendril-leaved fritillary bulb extracts, 8 parts of Scaphium scaphigerum extracts.
The quick-fried pearl is made by the following method:
(1) Peppermint essential oil, Poria cocos essential oil, Radix Scrophulariae extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, the sterculia seed are extracted
Object is uniformly mixed, and essence is made；
(2) olive oil is mixed with polyglyceryl fatty acid ester, sucrose fatty ester is added, 35 DEG C of heating water baths simultaneously stir
Essence obtained in step (1) is added in 30min, stirs 2h, and essential oil is made, and controls olive oil, polyglyceryl fatty acid ester, essence
Weight ratio be 5: 1: 3；
(3) essential oil is added in pill dripping machine hopper, dripping pill lapping is added in rubber cement tank, controlled at 65 DEG C,
Essential oil is wrapped in dripping pill lapping by pill dripping machine, quick-fried pearl is made in curing molding.
Comparative example 1
This comparative example is not compared with Example 1 modified acetate fiber, and preparation method is as follows:
One kind is refreshed oneself the filter tip that hawks, including the first filter fiber section 1, adsorption section 2, the second filter fiber section 3, tipping volume
Acetate fiber is filled inside paper 4, quick-fried pearl 5, the first filter fiber section 1 and the second filter fiber section 3, is filled and is lived inside adsorption section 2
It is blue to change Mayan；
The hawk preparation method of filter tip of refreshing oneself includes the following steps:
Step S1, it activates the preparation of Mayan indigo plant: (a) Mayan indigo plant being put into Muffle furnace after 350 DEG C of calcining 1h and is added
In 100mL10% sodium chloride solution, 70 DEG C of heating water bath 2h；(b) it is molten that 50mL20% sodium hydroxide is added into sodium chloride solution
Liquid, is warming up to 80 DEG C, and ultrasound stirs 20min；(c) it filters, the Mayan indigo plant after activation is placed in a beaker, is rushed with deionized water
It washes, until solution is in neutrality, filters again, after Mayan indigo plant is placed in 80 DEG C of drying boxes dry 2h, 50 meshes are crossed in grinding；
Step S2, acetate fiber sizing is regard as the first filter fiber section 1 and the second filter fiber section 3, in the first filtering
Segment of fiber 1 installs quick-fried pearl 5 close to one end of pipe tobacco, the Mayan indigo plant conduct after the installation activation of 1 other end of the first filter fiber section
Adsorption section 2,2 other end of adsorption section connect the second filter fiber section 3, and tipping roll paper 4 filters the first filter fiber section 1, second
Segment of fiber 3, the cladding of adsorption section 2 form filter tip.
Comparative example 2
This comparative example compared with Example 1, does not activate Mayan indigo plant, preparation method is as follows:
One kind is refreshed oneself the filter tip that hawks, including the first filter fiber section 1, adsorption section 2, the second filter fiber section 3, tipping volume
Paper 4, quick-fried pearl 5, the first filter fiber section 1 and the inside of the second filter fiber section 3 filling-modified acetate fiber are filled out inside adsorption section 2
Fill Mayan indigo plant；
The hawk preparation method of filter tip of refreshing oneself includes the following steps:
Step S1, the preparation of modified acetate fiber:
(1) acetate fiber is put into the beaker equipped with dehydrated alcohol, places the beaker in 75 DEG C of water-bath, at the uniform velocity stirs
20min to be mixed, acetate fiber taking-up is placed in drying box dry 15min after stirring, control drying box temperature is 60 DEG C,
The weight ratio for controlling acetate fiber and dehydrated alcohol is 2: 7；
(2) oxalic acid is added in the beaker equipped with deionized water, beaker is carried out to be warming up to 60 DEG C, is at the uniform velocity stirred, to grass
After acid dissolution, the acetate fiber cleaned up is added, is taken out after reacting 2h, controls oxalic acid, deionized water, the weight of acetate fiber
Than being 1: 10: 3；
(3) vacuum dehydration after drying is added in the beaker equipped with dehydrated alcohol, and heating water bath reacts 30h, take to 80 DEG C
Out, being transferred to vacuum degree is -0.10MPa, and modified acetate fiber is made in dry 5h in the vacuum oven that temperature is 65 DEG C；
Step S2, modified acetate fiber sizing is regard as the first filter fiber section 1 and the second filter fiber section 3, first
Filter fiber section 1 installs quick-fried pearl 5 close to one end of pipe tobacco, in 1 other end of the first filter fiber section installation Mayan indigo plant as absorption
Section 2,2 other end of adsorption section connect the second filter fiber section 3, are hinged with roll paper 4 for the first filter fiber section 1, the second filter fiber
Section 3, the cladding of adsorption section 2 form filter tip.
Comparative example 3
This comparative example is a kind of quick-fried pearl filter tip in market.
The hawk mouthfeel of filter tip, tar reduced rate, resistance of refreshing oneself of preparing of embodiment 1-4 and comparative example 1-3 is increased
Amount carries out performance detection, as a result as shown in table 1 below；
Mouthfeel: selecting 50 professionals, the filter tip progress that hawks of refreshing oneself prepared to embodiment 1-4 and comparative example 1-3
Usage experience, including quick-fried pearl mouthfeel are experienced, and sensory evaluation is made, and are got score, 10 parts of full marks, are calculated the flat of evaluation score
Mean value.
Table 1
| Score | Tar reduced rate (%) | Resistance incrementss/Pa | |
| Embodiment 1 | 7.5 | 52 | 3.2 |
| Embodiment 2 | 8.2 | 53 | 3.3 |
| Embodiment 3 | 8.5 | 52 | 3.3 |
| Embodiment 4 | 9.1 | 54 | 3.2 |
| Comparative example 1 | 7.6 | 36 | 2.1 |
| Comparative example 2 | 7.8 | 28 | 1.9 |
| Comparative example 3 | 6.5 | 39 | 1.5 |
From upper table 1 it can be seen that embodiment 1-4 preparation refresh oneself hawk filter tip score between 7.5-9.1, it is right
The score of ratio 1-3 is between 6.5-7.8；Embodiment 1-4 preparation refresh oneself hawk filter tip to the reduced rate of tar in 52-
Between 54%, comparative example 1-3 tar reduced rate is within the scope of 28-39；The filter tip resistance increasing that hawks of refreshing oneself of embodiment 1-4 preparation
Dosage is between 3.2-3.3Pa range, and comparative example 1-3 resistance incrementss are within the scope of 1.5-2.1Pa；So prepared by the present invention
Refresh oneself and hawk filter tip not only by good filtering adsorption effect, can also enrich the mouthfeel of cigarette, preferably be experienced to smoker.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means
Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention
In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example.
Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close
Suitable mode combines.
Above content is only citing made for the present invention and explanation, affiliated those skilled in the art are to being retouched
The specific embodiment stated does various modifications or additions or is substituted in a similar manner, and without departing from invention or surpasses
More range defined in the claims, is within the scope of protection of the invention.
Claims (5)
- The filter tip that hawks 1. one kind is refreshed oneself, including the first filter fiber section (1), adsorption section (2), the second filter fiber section (3), connect Fill roll paper (4), quick-fried pearl (5), which is characterized in that the first filter fiber section (1) is internal filling-modified with the second filter fiber section (3) Acetate fiber, adsorption section (2) internal filling activation Mayan are blue；The hawk preparation method of filter tip of refreshing oneself includes the following steps:Step S1, the preparation of modified acetate fiber:(1) acetate fiber is put into the beaker equipped with dehydrated alcohol, places the beaker in 75 DEG C of water-bath, at the uniform velocity stirs Acetate fiber taking-up is placed in drying box dry 15mi n after stirring by 20min, and control drying box temperature is 60 DEG C, The weight ratio for controlling acetate fiber and dehydrated alcohol is 2: 7；(2) oxalic acid is added in the beaker equipped with deionized water, beaker is carried out to be warming up to 60 DEG C, is at the uniform velocity stirred, it is molten to oxalic acid The acetate fiber cleaned up is added in Xie Hou, takes out after reacting 2h, and control oxalic acid, deionized water, the weight ratio of acetate fiber are 1:10:3；(3) vacuum dehydration after drying is added in the beaker equipped with dehydrated alcohol, and heating water bath reacts 30h to 80 DEG C, takes out, turn Moving to vacuum degree is -0.10MPa, and modified acetate fiber is made in dry 5h in the vacuum oven that temperature is 65 DEG C；Step S2, it activates the preparation of Mayan indigo plant: (a) Mayan indigo plant being put into Muffle furnace after 350 DEG C of calcining 1h, 100mL10% is added In sodium chloride solution, 70 DEG C of heating water bath 2h；(b) 50mL20% sodium hydroxide solution is added into sodium chloride solution, is warming up to 80 DEG C, ultrasound stirs 20min；(c) it filters, the Mayan indigo plant after activation is placed in a beaker, is rinsed with deionized water, until molten Liquid is in neutrality, and is filtered again, and after Mayan indigo plant is placed in 80 DEG C of drying boxes dry 2h, 50 meshes are crossed in grinding；Step S3, modified acetate fiber sizing is regard as the first filter fiber section (1) and the second filter fiber section (3), first Filter fiber section (1) installs quick-fried pearl (5) close to one end of pipe tobacco, after the installation activation of first filter fiber section (1) other end Mayan indigo plant connects the second filter fiber section (3) as adsorption section (2), adsorption section (2) other end, is hinged with roll paper (4) for the first mistake Filter segment of fiber (1), the second filter fiber section (3), adsorption section (2) cladding form filter tip.
- The filter tip that hawks 2. one kind according to claim 1 is refreshed oneself, which is characterized in that the quick-fried pearl (5) is by following weight Part raw material is made: 35-50 parts of Peppermint essential oils, 15-25 parts of Poria cocos essential oils, 20-30 parts of Radix Scrophulariae extracts, 10-15 portions of Siraitia grosvenoriis mention Take object, 5-15 parts of tendril-leaved fritillary bulb extracts, 3-8 parts of Scaphium scaphigerum extracts.
- The filter tip that hawks 3. one kind according to claim 1 is refreshed oneself, which is characterized in that the quick-fried pearl (5) is by the following method It is made:(1) Peppermint essential oil, Poria cocos essential oil, Radix Scrophulariae extract, Fructus Monordicae extract, tendril-leaved fritillary bulb extract, Scaphium scaphigerum extract are mixed It closes uniformly, essence is made；(2) olive oil being mixed with polyglyceryl fatty acid ester, sucrose fatty ester is added, 35 DEG C of heating water baths simultaneously stir 30min, Essence obtained in step (1) is added, stirs 2h, essential oil, the weight of control olive oil, polyglyceryl fatty acid ester, essence is made Than being 5: 1: 3；(3) essential oil is added in pill dripping machine hopper, dripping pill lapping is added in rubber cement tank, controlled at 65 DEG C, is passed through Essential oil is wrapped in dripping pill lapping by pill dripping machine, curing molding, and quick-fried pearl (5) are made.
- The filter tip that hawks 4. one kind according to claim 3 is refreshed oneself, which is characterized in that dripping pill lapping in step (3) It is made by the following method: sodium alginate and gelatin being placed in reaction kettle according to 6: 1 ratio and mixed, deionization is added Water is warming up to 80 DEG C, and stirring keeps the temperature 3h at this temperature, is filtered after foam floating, dripping pill lapping is made.
- 5. a kind of preparation method of filter tip of hawking of refreshing oneself, which comprises the steps of:Step S1, the preparation of modified acetate fiber:(1) acetate fiber is put into the beaker equipped with dehydrated alcohol, places the beaker in 75 DEG C of water-bath, at the uniform velocity stirs Acetate fiber taking-up is placed in drying box dry 15mi n after stirring by 20min, and control drying box temperature is 60 DEG C, The weight ratio for controlling acetate fiber and dehydrated alcohol is 2: 7；(2) oxalic acid is added in the beaker equipped with deionized water, beaker is carried out to be warming up to 60 DEG C, is at the uniform velocity stirred, it is molten to oxalic acid The acetate fiber cleaned up is added in Xie Hou, takes out after reacting 2h, and control oxalic acid, deionized water, the weight ratio of acetate fiber are 1:10:3；(3) vacuum dehydration after drying is added in the beaker equipped with dehydrated alcohol, and heating water bath reacts 30h to 80 DEG C, takes out, turn Moving to vacuum degree is -0.10MPa, and modified acetate fiber is made in dry 5h in the vacuum oven that temperature is 65 DEG C；Step S2, it activates the preparation of Mayan indigo plant: (a) Mayan indigo plant being put into Muffle furnace after 350 DEG C of calcining 1h, 100mL10% is added In sodium chloride solution, 70 DEG C of heating water bath 2h；(b) 50mL20% sodium hydroxide solution is added into sodium chloride solution, is warming up to 80 DEG C, ultrasound stirs 20min；(c) it filters, the Mayan indigo plant after activation is placed in a beaker, is rinsed with deionized water, until molten Liquid is in neutrality, and is filtered again, and after Mayan indigo plant is placed in 80 DEG C of drying boxes dry 2h, 50 meshes are crossed in grinding；Step S3, modified acetate fiber sizing is regard as the first filter fiber section (1) and the second filter fiber section (3), first Filter fiber section (1) installs quick-fried pearl (5) close to one end of pipe tobacco, after the installation activation of first filter fiber section (1) other end Mayan indigo plant connects the second filter fiber section (3) as adsorption section (2), adsorption section (2) other end, is hinged with roll paper (4) for the first mistake Filter segment of fiber (1), the second filter fiber section (3), adsorption section (2) cladding form filter tip.
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Application publication date: 20190611 |