CN109797582A - Low bath raio soaping agent of a kind of low temperature and preparation method thereof - Google Patents
Low bath raio soaping agent of a kind of low temperature and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to technical field of textile printing, low bath raio soaping agent of especially a kind of low temperature and preparation method thereof, including 5-10 parts of silica, 20-30 parts of dehydrated alcohol, 5-7 parts of sodium carbonate, 3-5 parts of isomerous tridecanol polyoxyethylene ether, 3-5 parts of ammonium persulfate, adjacent 3-5 parts of the sodium of ethylenediamine two, silicone oil 1-3 parts, 20-30 parts of deionized water of washing, 5-8 parts of ethanedioic acid di-ammonium salts, 3-7 parts of silicate, 4-7 parts of fatty acid ester, 3-8 parts of aromatic alcohol, 5-8 parts of desizing enzyme, 6-10 parts of cellulase, 8-13 parts of 1,2-diaminocyclohexane tetraacetic acid, 11-15 parts of sodium trifluoroacetate；It by heating, stirs, dispersion, low temperature stirring is cooling, finished product not only saves electricity consumption in design application, while also saving time, artificial, reduces the dosage of water, for incorporated business, the energy and cost is greatly saved, and do not destroy pigment composition, dyeing quality is effectively ensured.
Description
Technical field
The present invention relates to technical field of textile printing, low bath raio soaping agent of especially a kind of low temperature and preparation method thereof.
Background technique
The soaping agent that textile uses after dyeing or stamp, uses soap earliest, soaps and also just gains the name therefrom,
Because soap is easy to produce staining problem intolerant to hard water, so gradually by detergent or others surface-active through screening
The compound of agent it is replaced it, these detergents being made of surfactant, washing effect has in textile and dyeing industry
Bigger raising, but it is to anti-pickup effect still undesirable, especially when soaping to fabric, Yi Fasheng white background or light color
Partial staining problem influences product quality, therefore there have been more professional soaping agents.Soaping agent must be in height at present
Warm Shi Jinhang not only wastes electric energy, increases working time and cost of labor, and waste water resource.
In textile printing and dyeing industry, bath raio refers to the weight ratio during dyeing process between textile material and dye liquor, leads to
Often bath raio in 1:10 referred to as short liquor ratio below, 1:7 is below to be known as low bath raio, and 1:3 .5 is below to be known as ultra-low bath ratio.
The height of bath raio directly affects the product quality of dyeing and printing process, after also determining the water consumption and process in process
Wastewater discharge, therefore, the development of low bath ratio dyeing technology lower consumption for textile enterprise's control of product quality, energy-saving and emission-reduction, are clear
Clean production is of great significance.In the prior art, using high temperature and pressure pot type jet dyeing machine can by bath raio control 1:5-7 it
Between, high temperature and high pressure environment can seriously destroy pigment composition, and when being dyed in particular by natural pigment, pigment is destroyed more
Be it is serious, cause dyeing effect poor.
Summary of the invention
In view of the above shortcomings of the prior art, low bath raio soaping agent of a kind of low temperature and preparation method thereof is provided, not only
Save electricity consumption, while also saving time, artificial, reduce the dosage of water, for incorporated business, be greatly saved the energy and at
This, and pigment composition is not destroyed, dyeing quality is effectively ensured.
In order to solve the above technical problems, the technical solution adopted by the present invention is that, a kind of low bath raio soaping agent of low temperature and its
Preparation method, including 5-10 parts of silica, 20-30 parts of dehydrated alcohol, 5-7 parts of sodium carbonate, isomerous tridecanol polyoxyethylene ether
3-5 parts, 3-5 parts of ammonium persulfate, adjacent 3-5 parts of the sodium of ethylenediamine two, washing silicone oil 1-3 parts, 20-30 parts of deionized water,
5-8 parts of ethanedioic acid di-ammonium salts, 3-7 parts of silicate, 4-7 parts of fatty acid ester, 3-8 parts of aromatic alcohol, 5-8 parts of desizing enzyme, cellulase
6-10 parts, 8-13 parts of 1,2-diaminocyclohexane tetraacetic acid, 11-15 parts of sodium trifluoroacetate；Preparation method is, step 1, in a kettle
It is added deionized water 20-30 parts, oil bath heating is condensed back, and increases temperature to 80-100 DEG C；Step 2, isomery 13 is added
Adjacent 3-5 parts of the sodium of 3-5 parts of alcohol polyoxyethylene ether, 3-5 parts of ammonium persulfate, ethylenediamine two, is stirred by 500-1000 revs/min
It mixes 10-20 minutes；Step 3, first it is by 5-10 parts of silica, 20-30 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power
500-1000W, jitter time are 20-30 minutes；Step 4,30-40 DEG C of temperature is reduced, the solution of step 3 is poured into step 2
In solution, 500-1000 revs/min, stir 20-30 minutes；Step 5, sodium carbonate 5-7 parts of addition, 500-1000 revs/min,
Stirring 10-20 minutes；Step 6,5-8 parts of ethanedioic acid di-ammonium salts of addition, 3-7 parts of silicate, 4-7 parts of fatty acid ester, aromatic alcohol 3-
8 parts, 5-8 parts of desizing enzyme, 6-10 parts of cellulase, 8-13 parts of 1,2-diaminocyclohexane tetraacetic acid, 11-15 parts of sodium trifluoroacetate, washing silicon
It is 1-3 parts oily, it 500-1000 revs/min, stirs 10-20 minutes；Step 7, stirring is shut down, prepared liquid dyeing auxiliaries is obtained；
Step 8, it stands and is cooled in reaction kettle liquid dyeing auxiliaries and is lower than 20 DEG C, blowing encapsulation, finished product.
Low bath raio soaping agent of above-mentioned low temperature and preparation method thereof, including 8 parts of silica, 25 parts of dehydrated alcohol, carbonic acid
Adjacent 4 parts of the sodium of 6 parts of sodium, 4 parts of isomerous tridecanol polyoxyethylene ether, 4 parts of ammonium persulfate, ethylenediamine two, washing silicone oil 2
Part, 25 parts of deionized water are 7 parts of ethanedioic acid di-ammonium salts, 4 parts of silicate, 5 parts of fatty acid ester, 6 parts of aromatic alcohol, 6 parts of desizing enzyme, fine
Plain 8 parts of the enzyme of dimension, 10 parts of 1,2-diaminocyclohexane tetraacetic acid, 13 parts of sodium trifluoroacetate；Preparation method is, step 1, in a kettle plus
Enter 25 parts of deionized water, oil bath heating is condensed back, and increases temperature to 90 DEG C；Step 2, isomerous tridecanol polyoxyethylene is added
Adjacent 4 parts of the sodium of 4 parts of ether, 4 parts of ammonium persulfate, ethylenediamine two, is stirred 15 minutes by 700 revs/min；Step 3, first will
8 parts of silica, 25 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power are 700W, and jitter time is 25 minutes；Step 4,
35 DEG C of temperature are reduced, the solution of step 3 is poured into the solution of step 2,600 revs/min, is stirred 25 minutes；Step 5, add
Enter 6 parts of sodium carbonate, 500-1000 revs/min, stirs 15 minutes；Step 6,7 parts of ethanedioic acid di-ammonium salts of addition, 4 parts of silicate,
5 parts of fatty acid ester, 6 parts of aromatic alcohol, 6 parts of desizing enzyme, 8 parts of cellulase, 10 parts of 1,2-diaminocyclohexane tetraacetic acid, sodium trifluoroacetate 13
Part, 2 parts of silicone oil of washing, are stirred 15 minutes by 700 revs/min；Step 7, stirring is shut down, prepared liquid dyeing auxiliaries is obtained；
Step 8, it stands and is cooled in reaction kettle liquid dyeing auxiliaries and is lower than 20 DEG C, blowing encapsulation, finished product.
A kind of beneficial effect of the low bath raio soaping agent of low temperature of the present invention and preparation method thereof is not only to save electricity consumption,
Time, artificial is also saved simultaneously, is reduced the dosage of water, for incorporated business, the energy and cost is greatly saved, and do not destroy
Dyeing quality is effectively ensured in pigment composition.
Specific embodiment
It elaborates combined with specific embodiments below to the present invention.
Embodiment 1, low bath raio soaping agent of a kind of low temperature and preparation method thereof, including 5 parts of silica, dehydrated alcohol 20
Part, 5 parts of sodium carbonate, 3 parts of isomerous tridecanol polyoxyethylene ether, 3 parts of ammonium persulfate, adjacent 3 parts of the sodium of ethylenediamine two, washing
1 part of silicone oil, 20 parts of deionized water, 5 parts of ethanedioic acid di-ammonium salts, 3 parts of silicate, 4 parts of fatty acid ester, 3 parts of aromatic alcohol, desizing enzyme 5
Part, 6 parts of cellulase, 8 parts of 1,2-diaminocyclohexane tetraacetic acid, 11 parts of sodium trifluoroacetate；Preparation method is, step 1, in reaction kettle
Middle 20 parts of addition deionized water, oil bath heating is condensed back, and increases temperature to 80 DEG C；Step 2, isomerous tridecanol polyoxy is added
Adjacent 3 parts of the sodium of 3 parts of vinethene, 3 parts of ammonium persulfate, ethylenediamine two, is stirred 10 minutes by 500 revs/min；Step 3,
It is first 500W by 5 parts of silica, 20 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power, jitter time is 20 minutes；Step
Rapid 4,30 DEG C of temperature are reduced, the solution of step 3 is poured into the solution of step 2,500 revs/min, is stirred 20 minutes；Step
5,5 parts of sodium carbonate are added, 500 revs/min, is stirred 10 minutes；Step 6,5 parts of ethanedioic acid di-ammonium salts of addition, 3 parts of silicate, rouge
4 parts of fat acid rouge, 3 parts of aromatic alcohol, 5 parts of desizing enzyme, 6 parts of cellulase, 8 parts of 1,2-diaminocyclohexane tetraacetic acid, 11 parts of sodium trifluoroacetate, water
1 part of silicone oil is washed, 500 revs/min, is stirred 10 minutes；Step 7, stirring is shut down, prepared liquid dyeing auxiliaries is obtained；Step
8, standing is cooled to liquid dyeing auxiliaries in reaction kettle and is lower than 20 DEG C, and blowing encapsulates, finished product.
Embodiment 2, low bath raio soaping agent of low temperature and preparation method thereof, including 8 parts of silica, 25 parts of dehydrated alcohol, carbon
Adjacent 4 parts of the sodium of 6 parts of sour sodium, 4 parts of isomerous tridecanol polyoxyethylene ether, 4 parts of ammonium persulfate, ethylenediamine two, washing silicone oil 2
Part, 25 parts of deionized water are 7 parts of ethanedioic acid di-ammonium salts, 4 parts of silicate, 5 parts of fatty acid ester, 6 parts of aromatic alcohol, 6 parts of desizing enzyme, fine
Plain 8 parts of the enzyme of dimension, 10 parts of 1,2-diaminocyclohexane tetraacetic acid, 13 parts of sodium trifluoroacetate；Preparation method is, step 1, in a kettle plus
Enter 25 parts of deionized water, oil bath heating is condensed back, and increases temperature to 90 DEG C；Step 2, isomerous tridecanol polyoxyethylene is added
Adjacent 4 parts of the sodium of 4 parts of ether, 4 parts of ammonium persulfate, ethylenediamine two, is stirred 15 minutes by 700 revs/min；Step 3, first will
8 parts of silica, 25 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power are 700W, and jitter time is 25 minutes；Step 4,
35 DEG C of temperature are reduced, the solution of step 3 is poured into the solution of step 2,600 revs/min, is stirred 25 minutes；Step 5, add
Enter 6 parts of sodium carbonate, 500-1000 revs/min, stirs 15 minutes；Step 6,7 parts of ethanedioic acid di-ammonium salts of addition, 4 parts of silicate,
5 parts of fatty acid ester, 6 parts of aromatic alcohol, 6 parts of desizing enzyme, 8 parts of cellulase, 10 parts of 1,2-diaminocyclohexane tetraacetic acid, sodium trifluoroacetate 13
Part, 2 parts of silicone oil of washing, are stirred 15 minutes by 700 revs/min；Step 7, stirring is shut down, prepared liquid dyeing auxiliaries is obtained；
Step 8, it stands and is cooled in reaction kettle liquid dyeing auxiliaries and is lower than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3, embodiment 1, low bath raio soaping agent of a kind of low temperature and preparation method thereof, including 0 part of silica 1, nothing
The adjacent sodium of 30 parts of water-ethanol, 7 parts of sodium carbonate, 5 parts of isomerous tridecanol polyoxyethylene ether, 5 parts of ammonium persulfate, ethylenediamine two
5 parts, washing 3 parts of silicone oil, 30 parts of deionized water, 8 parts of ethanedioic acid di-ammonium salts, 7 parts of silicate, 7 parts of fatty acid ester, 8 parts of aromatic alcohol,
8 parts of desizing enzyme, 10 parts of cellulase, 13 parts of 1,2-diaminocyclohexane tetraacetic acid, 15 parts of sodium trifluoroacetate；Preparation method is, step 1,
30 parts of deionized water are added in a kettle, oil bath heating is condensed back, and increases temperature to 100 DEG C；Step 2, isomery is added
Adjacent 5 parts of the sodium of 5 parts of tridecanol polyoxyethylene ether, 5 parts of ammonium persulfate, ethylenediamine two, 1000 revs/min, stirring 20
Minute；It step 3, by 0 part of silica 1,30 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power is first 1000W, when dispersion
Between be 30 minutes；Step 4,40 DEG C of temperature are reduced, the solution of step 3 is poured into the solution of step 2,1000 revs/min, is stirred
It mixes 30 minutes；Step 5,7 parts of sodium carbonate are added, 1000 revs/min, is stirred 20 minutes；Step 6, ethanedioic acid di-ammonium salts are added
8 parts, 7 parts of silicate, 7 parts of fatty acid ester, 8 parts of aromatic alcohol, 8 parts of desizing enzyme, 10 parts of cellulase, 1,2-diaminocyclohexane tetraacetic acid 13
Part, 15 parts of sodium trifluoroacetate, 3 parts of silicone oil of washing, stir 20 minutes by 1000 revs/min；Step 7, stirring is shut down, is prepared
Good liquid dyeing auxiliaries；Step 8, it stands and is cooled in reaction kettle liquid dyeing auxiliaries and is lower than 20 DEG C, blowing encapsulation, finished product.
The embodiment of the above is only the preferred embodiments of the invention, and but not intended to limit the scope of the present invention,
Therefore change made by all principles according to the present invention, it should all be included within the scope of protection of the present invention.
Claims (2)
1. low bath raio soaping agent of a kind of low temperature and preparation method thereof, which is characterized in that including 5-10 parts of silica, dehydrated alcohol
20-30 parts, 5-7 parts of sodium carbonate, 3-5 parts of isomerous tridecanol polyoxyethylene ether, 3-5 parts of ammonium persulfate, the adjacent phenyl second of ethylenediamine two
Sour sodium 3-5 parts, washing silicone oil 1-3 parts, 20-30 parts of deionized water, 5-8 parts of ethanedioic acid di-ammonium salts, 3-7 parts of silicate, fatty acid
4-7 parts of rouge, 3-8 parts of aromatic alcohol, 5-8 parts of desizing enzyme, 6-10 parts of cellulase, 8-13 parts of 1,2-diaminocyclohexane tetraacetic acid, trifluoroacetic acid
11-15 parts of sodium；Preparation method is step 1, deionized water 20-30 parts to be added in a kettle, oil bath heating is condensed back to
Stream increases temperature to 80-100 DEG C；Step 2, isomerous tridecanol polyoxyethylene ether 3-5 parts, 3-5 parts of ammonium persulfate, second two is added
Adjacent 3-5 parts of the sodium of amine two, is stirred 10-20 minutes by 500-1000 revs/min；Step 3, first by silica 5-10
Part, 20-30 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power are 500-1000W, and jitter time is 20-30 minutes；Step
4,30-40 DEG C of temperature is reduced, the solution of step 3 is poured into the solution of step 2,500-1000 revs/min, 20-30 points of stirring
Clock；Step 5, it is added sodium carbonate 5-7 parts, 500-1000 revs/min, is stirred 10-20 minutes；Step 6, ethanedioic acid diammonium is added
5-8 parts of salt, 3-7 parts of silicate, 4-7 parts of fatty acid ester, 3-8 parts of aromatic alcohol, 5-8 parts of desizing enzyme, 6-10 parts of cellulase, hexamethylene
8-13 parts of ethylenediamine tetraacetic acid (EDTA), 11-15 parts of sodium trifluoroacetate, silicone oil 1-3 parts of washing, 500-1000 revs/min, 10-20 points of stirring
Clock；Step 7, stirring is shut down, prepared liquid dyeing auxiliaries is obtained；Step 8, it stands and is cooled to liquid dyeing auxiliaries in reaction kettle
Lower than 20 DEG C, blowing encapsulation, finished product.
2. low bath raio soaping agent of low temperature according to claim 1 and preparation method thereof, characterized in that including silica 8
Part, 25 parts of dehydrated alcohol, 6 parts of sodium carbonate, 4 parts of isomerous tridecanol polyoxyethylene ether, 4 parts of ammonium persulfate, the adjacent phenyl of ethylenediamine two
4 parts of sodium acetate, washing 2 parts of silicone oil, 25 parts of deionized water, 7 parts of ethanedioic acid di-ammonium salts, 4 parts of silicate, 5 parts of fatty acid ester, fragrance
6 parts of alcohol, 6 parts of desizing enzyme, 8 parts of cellulase, 10 parts of 1,2-diaminocyclohexane tetraacetic acid, 13 parts of sodium trifluoroacetate；Preparation method is,
Step 1,25 parts of deionized water are added in a kettle, oil bath heating is condensed back, and increases temperature to 90 DEG C；Step 2, it is added
Adjacent 4 parts of the sodium of 4 parts of isomerous tridecanol polyoxyethylene ether, 4 parts of ammonium persulfate, ethylenediamine two, 700 revs/min, stirring
15 minutes；It step 3, by 8 parts of silica, 25 parts of progress ultrasonic disperses of dehydrated alcohol, dispersion power is first 700W, when dispersion
Between be 25 minutes；Step 4,35 DEG C of temperature are reduced, the solution of step 3 is poured into the solution of step 2,600 revs/min, is stirred
25 minutes；Step 5,6 parts of sodium carbonate are added, 500-1000 revs/min, is stirred 15 minutes；Step 6, ethanedioic acid diammonium is added
7 parts of salt, 4 parts of silicate, 5 parts of fatty acid ester, 6 parts of aromatic alcohol, 6 parts of desizing enzyme, 8 parts of cellulase, 1,2-diaminocyclohexane tetraacetic acid 10
Part, 13 parts of sodium trifluoroacetate, 2 parts of silicone oil of washing, stir 15 minutes by 700 revs/min；Step 7, stirring is shut down, is prepared
Good liquid dyeing auxiliaries；Step 8, it stands and is cooled in reaction kettle liquid dyeing auxiliaries and is lower than 20 DEG C, blowing encapsulation, finished product.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102619113A (en) * | 2012-04-01 | 2012-08-01 | 祝洪哲 | Short-process low temperature soaping additive and preparation method thereof |
| CN102660404A (en) * | 2012-05-04 | 2012-09-12 | 冠宏股份有限公司 | Low-temperature soaping agent as well as preparation method and application thereof |
| CN106637987A (en) * | 2016-12-16 | 2017-05-10 | 吴江市北厍盛源纺织品助剂厂 | Low-temperature alkali-resistant fabric refining agent and production method thereof |
| CN108130764A (en) * | 2017-12-13 | 2018-06-08 | 江苏新瑞贝科技股份有限公司 | A kind of low temperature soaping agent and preparation method thereof |
-
2018
- 2018-12-25 CN CN201811586025.9A patent/CN109797582A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102619113A (en) * | 2012-04-01 | 2012-08-01 | 祝洪哲 | Short-process low temperature soaping additive and preparation method thereof |
| CN102660404A (en) * | 2012-05-04 | 2012-09-12 | 冠宏股份有限公司 | Low-temperature soaping agent as well as preparation method and application thereof |
| CN106637987A (en) * | 2016-12-16 | 2017-05-10 | 吴江市北厍盛源纺织品助剂厂 | Low-temperature alkali-resistant fabric refining agent and production method thereof |
| CN108130764A (en) * | 2017-12-13 | 2018-06-08 | 江苏新瑞贝科技股份有限公司 | A kind of low temperature soaping agent and preparation method thereof |
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Application publication date: 20190524 |