CN109793882A - A kind of Chinese medicine composition and its preparation method and application containing ant - Google Patents
A kind of Chinese medicine composition and its preparation method and application containing ant Download PDFInfo
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Abstract
The invention discloses a kind of Chinese medicine composition and its preparation method and application containing ant, the composition are made of the component of following parts by weight: Polyhachis vicina Roger 20~30, Radix Notoginseng 12~18, safflower 6~10, Rhizoma Chuanxiong 10~15, cloves 5~8, peppermint oil 3~7, turpentine oil 8~12, rhizoma zingiberis 8~12.The traditional chinese medicine composition of the invention has anti-inflammatory and analgesic effect, cervical spondylosis, scapulohumeral periarthritis, lumbar vertebra disease, pain of the knee joint pain, rheumatoid arthritis is alleviated obviously, and the period is short, safely and effectively.
Description
Technical field
The invention belongs to technical field of traditional Chinese medicines, and in particular to a kind of Chinese medicine composition containing ant and preparation method thereof and answer
With.
Background technique
This noisy and society with fast rhythm at present, life and work is busy, and pressure is big, bends over one's desk working for a long time, using electricity
Brain, many people are negligent of the body to take care of number one, cause serious damage to body, lead to current cervical spondylosis, scapulohumeral periarthritis, lumbar vertebrae
The pain disease incidence of disease, the pain of the knee joint, rheumatoid arthritis etc. increases year by year.Also there is related lenitive externally applied drug at present
Object, but the period is long, curative effect is unobvious.
It would therefore be highly desirable to it is short to develop a kind of service life, eutherapeutic medicine for relieving pain composition.
Summary of the invention
The purpose of the present invention is overcoming above-mentioned shortcoming, providing one kind has anti-inflammatory and analgesic effect, for cervical spondylosis, shoulder
Zhou Yan, lumbar vertebra disease, arthralgia pain, rheumatoid arthritis are alleviated obviously, and service life is short, safely and effectively containing ant
Chinese medicine composition.
It is a further object of the present invention to provide the preparation methods of the Chinese medicine composition containing ant.
Further object of the present invention is to provide the Chinese medicine composition answering in the drug that preparation has anti-inflammatory and analgesic effect
With.
The purpose of the present invention is what is be accomplished by the following way:
A kind of Chinese medicine composition containing ant, the composition are made of the component of following parts by weight:
20~30 parts by weight of Polyhachis vicina Roger, 12~18 parts by weight of Radix Notoginseng, 6~10 parts by weight of safflower, 10~15 weight of Rhizoma Chuanxiong
Measure part, 5~8 parts by weight of cloves, 3~7 parts by weight of peppermint oil, 8~12 parts by weight of turpentine oil, 8~12 parts by weight of rhizoma zingiberis.
Above-mentioned composition is made of the component of following parts by weight:
25~30 parts by weight of Polyhachis vicina Roger, 12~15 parts by weight of Radix Notoginseng, 8~10 parts by weight of safflower, 12~15 weight of Rhizoma Chuanxiong
Measure part, 6~8 parts by weight of cloves, 4~6 parts by weight of peppermint oil, 8~10 parts by weight of turpentine oil, 8~10 parts by weight of rhizoma zingiberis.
Above-mentioned composition is most preferably made of the component of following parts by weight:
25 parts by weight of Polyhachis vicina Roger, 15 parts by weight of Radix Notoginseng, 10 parts by weight of safflower, 15 parts by weight of Rhizoma Chuanxiong, 8 weight of cloves
Part, 6 parts by weight of peppermint oil, 10 parts by weight of turpentine oil, 10 parts by weight of rhizoma zingiberis.
External preparation is made in above-mentioned composition and pharmaceutically acceptable auxiliary material, and preferably external preparation is patch.
The preparation method of the above-mentioned Chinese medicine composition containing ant, method includes the following steps:
Polyhachis vicina Roger, Radix Notoginseng, safflower, Rhizoma Chuanxiong, cloves, rhizoma zingiberis are uniformly mixed by formula rate, crushed, 60-80 is crossed
Mesh, in above-mentioned gross mass 1:6-8 ratio be added mass concentration 90%-95% ethanol percolation, collect filtrate, with peppermint oil,
Turpentine oil is prepared by formula rate.
It is preferred that mass concentration 90%-95% ethyl alcohol is added in the ratio of quality of medicinal material 1:7, diacolation speed is 3ml/min.
Above-mentioned Chinese medicine composition is in drug of the preparation with anti-inflammatory and analgesic effect using with significant effect.
It is preferred that the Chinese medicine composition is for treating cervical spondylosis, scapulohumeral periarthritis, lumbar vertebra disease, arthralgia, rheumatoid arthritis.
Fang Xie: Polyhachis vicina Roger taste is salty, sour, mild-natured, returns liver and kidney channel, can tonify the liver and kidney, bone is filled in strengthening the essence blood-nourishing, dissolving stasis is logical
Network is monarch drug in a prescription.Radix Notoginseng dissipating stasis and stanching bleeding, detumescence ding-tong；Rhizoma Chuanxiong acrid flavour, it is warm-natured, gas perfume (or spice) rise dissipate, can go it is scattered, go upward to mountain peak top, again
Blood system can be entered, come downwards to the sea of blood, extensively, wind-expelling pain-stopping effect is good for promoting blood circulation effect；Safflower promoting blood circulation, dredging channels, removing blood stasis and relieving pain, three
Seven, Rhizoma Chuanxiong, safflower are minister.The benefits of cloves acrid flavour, gas fragrance, pungent energy promoting qi circulation and relieving pain have middle benefit gas drop inverse, warming kidney and enhancing yang；Peppermint
Oily acrid flavour can dissipate, cool in nature and clear, with the edema that disappears, dissipate flesh heat, remove backache, draw medicine administered to bring out the cold and join the army and defend to dredge the stagnant gas of knot, moreover it is possible to accelerate
It absorbs, dissolution；Turpentine oil has disinfection analgesic activity and extremely strong to skin penetration power, and bitter is warm-natured, has and dispels pathogenic wind and remove dampness, and relaxes
The benefits of muscle dredging collateral, promoting blood circulation and stopping pain, cloves, peppermint oil, turpentine oil are assistant；Rhizoma zingiberis acrid flavour, it is warm-natured, have and accelerates human body new old generation
Thank, degrading the channel the effects of, to make.The present invention cooperates with a variety of medicinal material compatible uses, promoting blood circulation to remove blood stasis, dispelling cold and dehumidification, wind-expelling pain-stopping
It synergy and works rapid.
The present composition is using Polyhachis vicina Roger as primary raw material, in addition Rhizoma Chuanxiong, safflower, Radix Notoginseng, rhizoma zingiberis, cloves, peppermint
Oil, turpentine oil mix, and to massage as major way when use, can quickly be absorbed by human skin, and local blood is promoted to follow
Ring improves human body, alleviates muscular fatigue, aches, is obviously improved effect to arthralgia, and medicine stability is good.
Specific embodiment:
Below by way of specific embodiment, invention is further explained:
Embodiment 1
Weigh 250 grams of Polyhachis vicina Roger, 150 grams of Radix Notoginseng, 100 grams of safflower, 150 grams of Rhizoma Chuanxiong, 80 grams of cloves, 100 grams of rhizoma zingiberis,
Mixing crushes, and all crosses 60 meshes, and the medicinal second that mass concentration is 95% is added according to the ratio of Six-element medicinal material total quality 1:7
Alcohol, diacolation, diacolation speed are 3ml/min, after collect percolate, and 60 grams of peppermint oil, 100 grams of turpentine oil, mixing, i.e.,
?.At 40 DEG C ± 2 DEG C of temperature, 6 months are stood under conditions of humidity 75% ± 5%, is sampled respectively at 1,2,3,6 the end of month, still
Clear, no precipitating.
Embodiment 2
300 grams of Polyhachis vicina Roger are weighed, 120 grams of Radix Notoginseng, 80 grams of safflower, 120 grams of Rhizoma Chuanxiong, 60 grams of cloves, 80 grams of rhizoma zingiberis, is mixed
It closes, crushes, all cross 80 meshes, the medicinal alcohol that mass concentration is 95% is added according to the ratio of Six-element medicinal material total quality 1:7
Diacolation, diacolation speed are 3ml/min, collect percolate after diacolation, with Peppermint Oil 50 gram, 90 grams of turpentine oil, are mixed, i.e.,
?.At 40 DEG C ± 2 DEG C of temperature, 6 months are stood under conditions of humidity 75% ± 5%, is sampled respectively at 1,2,3,6 the end of month, still
Clear, no precipitating.
Embodiment 3
Weigh 230 grams of Polyhachis vicina Roger, 150 grams of Radix Notoginseng, 60 grams of safflower, 100 grams of Rhizoma Chuanxiong, 80 grams of cloves, 120 grams of rhizoma zingiberis,
Mixing crushes, and all crosses 80 meshes, and the medicinal second that mass concentration is 95% is added according to the ratio of Six-element medicinal material total quality 1:7
Alcohol percolation, diacolation speed are 3ml/min, collect percolate after diacolation, and 40 grams of peppermint oil, 80 grams of turpentine oil, mixing, i.e.,
?.At 40 DEG C ± 2 DEG C of temperature, 6 months are stood under conditions of humidity 75% ± 5%, is sampled respectively at 1,2,3,6 the end of month, still
Clear, no precipitating.
Comparative example 1 (no peppermint oil)
Weigh 250 grams of Polyhachis vicina Roger, 150 grams of Radix Notoginseng, 100 grams of safflower, 150 grams of Rhizoma Chuanxiong, 80 grams of cloves, 100 grams of rhizoma zingiberis,
Mixing crushes, and all crosses 60 meshes, and the medicinal second that mass concentration is 95% is added according to the ratio of Six-element medicinal material total quality 1:7
Alcohol, diacolation, diacolation speed are 3ml/min, after collect percolate, and 100 grams of turpentine oil, mixing to get.At 40 DEG C of temperature
± 2 DEG C, 6 months are stood under conditions of humidity 75% ± 5%, it is separately sampled at 1,2,3,6 the end of month respectively, start appearance in March
Containing trace suspension object, until 6 months gradually increase.
Explanation is further expalined to the present invention below by way of pharmacodynamic test example:
Test example 1
1. experimental material:
1 composition of 1.1 drugs and the reagent embodiment of the present invention (hereinafter referred to as ant polishes)；1% Vitalin Emulgel (Switzerland
Vapour Ba-Jia Ji company)；Carrageenan (Sigma company)；Polyrhachis alcoholic solution (is mentioned using only Polyhachis vicina Roger
It takes, extracting method is with embodiment 1)；Ant king is oily (Ruijin City Dongshan insect utilization research institute).
Polyrhachis alcoholic solution preparation method:
250 grams of Polyhachis vicina Roger are weighed, is crushed, 60 meshes are crossed, mass concentration, which is added, according to the ratio of quality of medicinal material 1:7 is
95% medicinal alcohol diacolation, diacolation speed are 3ml/min, collect percolate after diacolation.
1.2 animal SD rats, 180~250g of weight；Kunming mouse, 18~25g of weight are male mouse.
2 methods
2.1 anti-inflammatory experiments
2.1.1 rat paw edema experiment uses volumetric measurement method --- and capillary measurement by magnification vola pedis volumetric method evaluates medicine
The anti-inflammatory effect of object.Rat 50 are taken, 5 groups is randomly divided into, every group 10, makees a mark simultaneously in the left back ankle joint of every mouse
It injects 1% Irish moss 0.1ml and causes inflammation under vola pedis aponeurosis (aponeuroses), survey its sufficient pawl normal volume, applied respectively after 30min and put Voltarol latex on the skin
Agent 0.1g and physiological saline, polyrhachis alcoholic solution, ant king oil, each 0.5ml of ant polishes, respectively at cause it is scorching after 1,2,3,
4,5,6h surveys its volume, and swelling is calculated as follows.
Swelling (%)=(vola pedis volume before vola pedis volume-cause is scorching after cause is scorching)/causes vola pedis volume × 100% before inflammation
2.1.2 mouse auricular concha swelling experiment takes mouse 60, is randomly divided into 5 groups, every group 12.Under etherization, it uses
Two sides causes scorching, every mouse 0.02ml before and after dimethylbenzene is applied to the left ear of mouse, and 30min applies physiology salt at same position respectively after cause inflammation
It will be at mouse after water, polyrhachis alcoholic solution, ant king oil, each 0.5ml of ant polishes and Vitalin Emulgel 0.1g, 4h
Extremely, two ears are cut and lay round auricle with 9mm diameter punch, the swelling of each group mouse ear is calculated as follows in weighing scale to test twisting force weighing
Rate.
Swelling rate (%)=(Zuo Erchong-auris dextra weight)/auris dextra weight × 100%
2.2 analgesic experiment
2.2.1 40 mouse are randomly divided into 4 groups, i.e. saline control group, polyrhachis alcoholic solution by writhing method
Group, ant king's oil group, ant polishes group.Abdomen hair is shaved with shaver, negative control group is put on the skin with physiological saline and smears abdomen, other
3 groups --- polyrhachis alcoholic solution group, ant king's oil group, ant polishes group are put on the skin with corresponding medicine smear mouse web portion respectively.Outer wiping
Medicine is both needed under heat lamp continuous erasing mouse web portion 3min, and dosage is 1ml/.0.6% vinegar is injected intraperitoneally in each group after 30min
Sour (0.2ml/20g) observes writhing number of animals and writhing number in 30min.
2.2.2 male mice is placed in 10cm × 20cm × 15cm in (55.0 ± 0.5) DEG C constant water bath box by hot plate method
In iron sheet tube, uses stopwatch record mouse to put into hot plate to there is licking the time (s) of metapedes as the pain threshold of the mouse, screen the threshold of pain
It is worth mouse 50 in 5~30s, is randomly divided into 5 groups, after being smeared with drug respectively or impregnated mouse foot 5min, by mouse
Hot plate is put into, licking the time of metapedes occurs in record, respectively pain threshold before and after recording medicine.
3 experimental results
3.1 anti-inflammatory experimental rat pedal swelling experiments and mice auricle swelling experimental result are shown in Tables 1 and 2 respectively.
Influence of the 1 ant polishes of table to normal rat swelling degree of the paw%
Note: n=10
As shown in Table 1, compared with the control group, rat paw edema caused by ant polishes Carrageenan has significant suppression
Production is used；Compared with ant king's oil group, polyrhachis alcoholic solution group, ant polishes inhibiting effect is significant.
Influence of the 2 ant polishes of table to Mice Auricle inflammatory swelling%
Table 2 the result shows that, polyrhachis alcoholic solution, ant king oil, ant polishes can weaken small caused by dimethylbenzene
Mouse auricle inflammatory swelling；But ant polishes is significantly stronger than ant king oil and Polyhachis vicina Roger to the auricle inflammatory swelling inhibiting effect of mouse
Ant alcoholic solution.
3.2 analgesic experiment
3.2.1 mouse writhing method analgesic experiment the results are shown in Table 3.
The influence of 3 ant polishes Dichlorodiphenyl Acetate induced mice writhing response of table
As shown in Table 3, compared with the control group, the writhing response of ant polishes group mouse is relatively fewer, small caused by Dichlorodiphenyl Acetate
Mouse writhing assay has significant analgesic activity, and significant effect is better than polyrhachis alcoholic solution and ant king's oil, has significant
Sex differernce.
3.2.2 hot plate method in mice analgesic experiment the results are shown in Table 4
The influence that 4 ant polishes of table acts on hot plate method in mice induced pain
As shown in Table 4, ant polishes group can extend the time that mouse licks metapedes, can significantly improve the mouse threshold of pain, and with
Polyrhachis alcoholic solution and ant king's oil group compare, and ant polishes acts on hot plate method in mice induced pain significant in efficacy, have
Significant difference.
From above-mentioned experimental result, it can be seen that it is swollen that the present composition can significantly inhibit rat paw caused by carrageenan
Mice auricle swelling caused by swollen and dimethylbenzene reduces acetic acid induced mice writhing response frequency, significantly improves hot plate method
Mouse pain threshold, and this four indexs are significantly better than polyrhachis alcoholic solution and ant king's oil group, anti-inflammatory and analgesic effect is more
By force, curative effect is better.
Partial clinical test example:
Zhang's nineteen ninety is raw, and symptom: cervical spondylosis: neck acid is swollen, pain, can not FREE TORSION, rubbed in Dazhui acupoint position,
Twice daily, using the present composition one week, neck can be with FREE TORSION, and anacidity is swollen, feeling of pain, and has no adverse reaction.
Ma's nineteen sixty-eight is raw, symptom: arteriosclerosis and obstruction of lower limbs many years, rainy day humidity pain；It is rubbed in Zusanli position, twice daily,
Using the present composition one month, pain was significantly reduced.
Certain tall life in 1975, symptom: cervical spondylosis: neck ache；It is rubbed in Dazhui acupoint position, twice daily, uses this hair
Bright composition one week, neck ache is alleviated, and has no adverse reaction.
Chen's life in 1979, symptom: cervical vertebra pain and Low Back Pain；It sets and rubs in Dazhui acupoint and either side of the small of the back acupuncture point, twice daily, use
The present composition one month, cervical vertebra and flank pain sense obviously slowed down solution, and have no adverse reaction.
Sun's life in 1976, symptom: left shoulder scapulohumeral periarthritis；Jian Yu, which is set at acupuncture point, to be rubbed, and twice daily, is combined using the present invention
Object one month, feeling of pain obviously weakened, and stretching, extension is freely, it is no longer necessary to go acupuncture weekly, and have no adverse reaction.
Yuan's nineteen fifty-five is raw, symptom: prolapse of lumbar intervertebral disc, leg joint pain, respectively at Yaoyangkuan(Du 3), either side of the small of the back cave, Zusanli position
It sets and rubs, twice daily, using the present composition two months, stand, obvious light and handy on foot, waist and leg pain obviously delay
Solution, acid is swollen, and sense slows down.There is small erythema after using for the first time, self-healing after being discontinued 5 days, continuation dosage halves bad anti-using not occurring
It answers.
Yuan's life in 1976, symptom: Low Back Pain, respectively at Yaoyangkuan(Du 3), either side of the small of the back acupuncture point, which is set, to be rubbed, twice daily, after use
Feeling of pain weakens within two days, and using the present composition one month, pain disappeared, and has no adverse reaction.
Wei's nineteen sixty is raw, and symptom: prolapse of lumbar intervertebral disc, respectively at Yaoyangkuan(Du 3), either side of the small of the back cave, Zusanli position is rubbed, daily
Twice, using the present composition one month, waist acid is swollen and pain significantly reduces, and has no adverse reaction.
Mr. Luo nineteen thirty is raw, and symptom: shoulder is tight, and trick is ice-cold, flank pain；Respectively at Yaoyangkuan(Du 3), Dazhui acupoint position
It rubs, twice daily, using the present composition one month, shoulder muscle was not tight, and trick warm, flank pain alleviates and nothing
Adverse reaction.
Chen's life in 1973, symptom: cervical vertebra pain, respectively at Yaoyangkuan(Du 3), Dazhui acupoint position is rubbed, twice daily,
Using present composition two weeks, waist and cervical vertebra ache are alleviated and have no adverse reaction.
Ma's nineteen sixty-eight is raw, and rheumatoid arthritis, joint motion is obviously not flexible when especially get up in the morning, respectively at
Joint part, Dazhui acupoint position rub, and twice daily, using the present composition one month, morning stiffness was alleviated obvious.
Claims (10)
1. a kind of Chinese medicine composition containing ant, it is characterised in that the composition is made of the component of following parts by weight:
20~30 parts by weight of Polyhachis vicina Roger, 12~18 parts by weight of Radix Notoginseng, 6~10 parts by weight of safflower, 10~15 parts by weight of Rhizoma Chuanxiong,
5~8 parts by weight of cloves, 3~7 parts by weight of peppermint oil, 8~12 parts by weight of turpentine oil, 8~12 parts by weight of rhizoma zingiberis.
2. the Chinese medicine composition according to claim 1 containing ant, it is characterised in that the composition is by following parts by weight
Component is made:
25~30 parts by weight of Polyhachis vicina Roger, 12~15 parts by weight of Radix Notoginseng, 8~10 parts by weight of safflower, 12~15 parts by weight of Rhizoma Chuanxiong,
6~8 parts by weight of cloves, 4~6 parts by weight of peppermint oil, 8~10 parts by weight of turpentine oil, 8~10 parts by weight of rhizoma zingiberis.
3. the Chinese medicine composition according to claim 1 containing ant, it is characterised in that the composition is by following parts by weight
Component is made:
25 parts by weight of Polyhachis vicina Roger, 15 parts by weight of Radix Notoginseng, 10 parts by weight of safflower, 15 parts by weight of Rhizoma Chuanxiong, 8 parts by weight of cloves are thin
Lotus 6 parts by weight of oil, 10 parts by weight of turpentine oil, 10 parts by weight of rhizoma zingiberis.
4. Chinese medicine composition according to claim 1,2 or 3, it is characterised in that the composition and pharmaceutically acceptable auxiliary material
External preparation is made.
5. Chinese medicine composition according to claim 4, it is characterised in that the external preparation is patch.
6. a kind of preparation method of the Chinese medicine composition described in claim 1,2 or 3 containing ant, it is characterised in that this method packet
Include following steps:
Polyhachis vicina Roger, Radix Notoginseng, safflower, Rhizoma Chuanxiong, cloves, rhizoma zingiberis are uniformly mixed by formula rate, crushed, 60-80 mesh is crossed,
Mass concentration 90%-95% ethanol percolation is added in the ratio of above-mentioned Six-element quality of medicinal material 1:6-8, percolate is collected, with peppermint
Oil, turpentine oil are prepared by formula rate.
7. the preparation method of Chinese medicine composition according to claim 6, it is characterised in that add in the ratio of quality of medicinal material 1:7
Enter mass concentration 90%-95% ethyl alcohol.
8. the preparation method of Chinese medicine composition according to claim 6, it is characterised in that the diacolation speed is 3ml/
min。
9. the Chinese medicine composition described in claim 1,2 or 3 containing ant oil is in the drug that preparation has anti-inflammatory and analgesic effect
Application.
10. the Chinese medicine composition described in claim 1,2 or 3 containing ant oil treats cervical spondylosis, scapulohumeral periarthritis, lumbar vertebrae in preparation
Disease, arthralgia, rheumatoid arthritis drug in application.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112717098A (en) * | 2021-01-20 | 2021-04-30 | 谢存焱 | Ant oil liniment and preparation method thereof |
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Application publication date: 20190524 |