CN109745235A - A kind of toothpaste and application thereof based on labradorite - Google Patents
A kind of toothpaste and application thereof based on labradorite Download PDFInfo
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- CN109745235A CN109745235A CN201910214154.3A CN201910214154A CN109745235A CN 109745235 A CN109745235 A CN 109745235A CN 201910214154 A CN201910214154 A CN 201910214154A CN 109745235 A CN109745235 A CN 109745235A
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- labradorite
- toothpaste
- powder
- mixture
- extract powder
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- 239000011018 labradorite Substances 0.000 title claims abstract description 138
- 229910052659 labradorite Inorganic materials 0.000 title claims abstract description 138
- 239000000606 toothpaste Substances 0.000 title claims abstract description 124
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 124
- 239000000843 powder Substances 0.000 claims abstract description 98
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 49
- 239000011159 matrix material Substances 0.000 claims abstract description 32
- 239000004575 stone Substances 0.000 claims abstract description 17
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 87
- 239000000203 mixture Substances 0.000 claims description 85
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 66
- 239000000284 extract Substances 0.000 claims description 45
- 238000003756 stirring Methods 0.000 claims description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 37
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 36
- 235000013312 flour Nutrition 0.000 claims description 34
- 239000000377 silicon dioxide Substances 0.000 claims description 33
- 239000002562 thickening agent Substances 0.000 claims description 31
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 claims description 28
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 28
- 229940085605 saccharin sodium Drugs 0.000 claims description 28
- 229920000915 polyvinyl chloride Polymers 0.000 claims description 22
- 238000002360 preparation method Methods 0.000 claims description 20
- 239000008367 deionised water Substances 0.000 claims description 18
- 229910021641 deionized water Inorganic materials 0.000 claims description 18
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 18
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims description 18
- 229960002216 methylparaben Drugs 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 18
- 239000002245 particle Substances 0.000 claims description 16
- 239000000686 essence Substances 0.000 claims description 15
- 238000009835 boiling Methods 0.000 claims description 11
- 235000013339 cereals Nutrition 0.000 claims description 11
- 230000000694 effects Effects 0.000 claims description 6
- 208000006558 Dental Calculus Diseases 0.000 claims description 5
- 238000001125 extrusion Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 229960005150 glycerol Drugs 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 2
- 229920002554 vinyl polymer Polymers 0.000 claims description 2
- OALHHIHQOFIMEF-UHFFFAOYSA-N 3',6'-dihydroxy-2',4',5',7'-tetraiodo-3h-spiro[2-benzofuran-1,9'-xanthene]-3-one Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC(I)=C(O)C(I)=C1OC1=C(I)C(O)=C(I)C=C21 OALHHIHQOFIMEF-UHFFFAOYSA-N 0.000 claims 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims 1
- 239000004744 fabric Substances 0.000 claims 1
- 239000002304 perfume Substances 0.000 claims 1
- -1 sorbierite Chemical compound 0.000 claims 1
- 235000013599 spices Nutrition 0.000 claims 1
- 230000006378 damage Effects 0.000 abstract description 10
- 208000027418 Wounds and injury Diseases 0.000 abstract description 8
- 208000014674 injury Diseases 0.000 abstract description 8
- 210000000515 tooth Anatomy 0.000 description 37
- 238000012360 testing method Methods 0.000 description 11
- 150000002148 esters Chemical class 0.000 description 9
- 241000162403 Deloyala guttata Species 0.000 description 7
- 241001122767 Theaceae Species 0.000 description 7
- 235000019504 cigarettes Nutrition 0.000 description 6
- 210000003298 dental enamel Anatomy 0.000 description 6
- 210000002189 macula lutea Anatomy 0.000 description 6
- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- JUNWLZAGQLJVLR-UHFFFAOYSA-J calcium diphosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])(=O)OP([O-])([O-])=O JUNWLZAGQLJVLR-UHFFFAOYSA-J 0.000 description 4
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 description 4
- 229940043256 calcium pyrophosphate Drugs 0.000 description 4
- 235000019821 dicalcium diphosphate Nutrition 0.000 description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- FENRSEGZMITUEF-ATTCVCFYSA-E [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] FENRSEGZMITUEF-ATTCVCFYSA-E 0.000 description 3
- 230000001580 bacterial effect Effects 0.000 description 3
- 230000001680 brushing effect Effects 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- RBLGLDWTCZMLRW-UHFFFAOYSA-K dicalcium phosphate dihydrate Substances O.O.[Ca+2].[Ca+2].[O-]P([O-])([O-])=O RBLGLDWTCZMLRW-UHFFFAOYSA-K 0.000 description 3
- 239000010433 feldspar Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 229940083982 sodium phytate Drugs 0.000 description 3
- 241000259759 Cassida nobilis Species 0.000 description 2
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 2
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 2
- 239000012496 blank sample Substances 0.000 description 2
- 238000000338 in vitro Methods 0.000 description 2
- 150000004702 methyl esters Chemical class 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 210000003296 saliva Anatomy 0.000 description 2
- 230000002087 whitening effect Effects 0.000 description 2
- 229910021532 Calcite Inorganic materials 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- 235000005976 Citrus sinensis Nutrition 0.000 description 1
- 240000002319 Citrus sinensis Species 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- SHFGJEQAOUMGJM-UHFFFAOYSA-N dialuminum dipotassium disodium dioxosilane iron(3+) oxocalcium oxomagnesium oxygen(2-) Chemical compound [O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[Na+].[Na+].[Al+3].[Al+3].[K+].[K+].[Fe+3].[Fe+3].O=[Mg].O=[Ca].O=[Si]=O SHFGJEQAOUMGJM-UHFFFAOYSA-N 0.000 description 1
- 235000019700 dicalcium phosphate Nutrition 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 210000003128 head Anatomy 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000010451 perlite Substances 0.000 description 1
- 235000019362 perlite Nutrition 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 239000009306 yunnan baiyao Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The present invention provides a kind of toothpaste and application thereof based on labradorite.The toothpaste based on labradorite includes the toothpaste matrix and rubbing agent that mass ratio is 50-80:20-50, and rubbing agent includes at least the elongation stone powder that average grain diameter is no more than 10 μm, Mohs' hardness is 3.5-5, elongates stone powder and is prepared by labradorite；Toothpaste provided by the invention based on labradorite can effectively remove tooth stain and calculus dentalis, and can reduce to injury of teeth, and each age group crowd is suitble to be used for a long time.
Description
Technical field
The invention belongs to cosmetic field, in particular to a kind of toothpaste and application thereof based on labradorite.
Background technique
Toothpaste is common cleaning supplies in daily life, has the function of cleaning polishing facing, makes oral cavity refreshing, with
The quality and grade of the reach of science, toothpaste is also continuously improved, rubbing agent be in toothpaste can with toothbrush collective effect, for wiping
Dental surface tartar is removed, the solid material ingredient of the foreign substances such as calculus dentalis is mitigated, existing toothpaste has the disadvantages that 1. energy
Tooth stain and calculus dentalis are enough effectively removed, but larger to injury of teeth, 2. can reduce the degree of injury to enamel, but corresponding
Removal tooth stain and the effect of calculus dentalis be significantly reduced, therefore, tooth stain and tooth knot can be effectively removed by being badly in need of one kind now
Stone, and can reduce the toothpaste to injury of teeth.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of toothpaste and application thereof based on labradorite, this is based on
The toothpaste of labradorite can effectively remove tooth stain and calculus dentalis, and can reduce to injury of teeth.
Specific technical solution of the present invention is as follows:
The present invention provides a kind of toothpaste based on labradorite, which includes that mass ratio is 50-80:
The toothpaste matrix and rubbing agent of 20-50, rubbing agent include at least the drawing that average grain diameter is no more than 10 μm, Mohs' hardness is 3.5-5
Feldspar powder elongates stone powder and is prepared by labradorite.
Wherein, toothpaste matrix includes the auxiliary material for preparing toothpaste and/or the ingredient with whitening, permanent tooth and other effects, whitening at
Dividing includes but is not limited to perlite, calcium pyrophosphate and sodium phytate, and permanent tooth ingredient includes but is not limited to fluorine；It is provided by the invention to be based on
The toothpaste of labradorite can effectively remove tooth stain and calculus dentalis, and can reduce to injury of teeth, be suitble to each age group crowd
It is used for a long time.
Further, labradorite powder includes that raw mountain flour, labradorite extract powder and the labradorite of elongating includes one of powder
Or it is a variety of, the raw mountain flour that elongates is directly to grind labradorite to be made, and the raw average grain diameter for elongating mountain flour is no more than 4 μm, and Mohs is hard
Degree is 4-5, and labradorite extract powder is will to grind to be made after labradorite boiling, and the average grain diameter of labradorite extract powder is no more than 6 μm,
Mohs' hardness is 3.5-4, and labradorite inclusion powder is to be included labradorite extract powder with polyvinyl resin to be made, and labradorite includes powder
Average grain diameter be no more than 10 μm.
Further, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 5cm-10cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:3-1:4, and adjustment pressure is 150KPa-200KPa, primary every 5min-7min stirring, are stirred every time
10min-20min, mixing speed 600prm-800prm, boiling 8h-10h, measures primary extract every 50min-60min altogether
The pH value of liquid, and adjust pH value to neutrality, is down to room temperature, takes out labradorite pearl, be crushed to average grain diameter no more than 6 μm to get
Labradorite extract powder.
Further, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 220 DEG C -230 DEG C, keep the temperature 20-30min, melting is made
The polyvinyl resin of state；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:1-
1:2 stirs 30min-40min under conditions of temperature is 220 DEG C -230 DEG C, mixing speed is 250prm-300prm, is made poly-
Vinyl mixture；
C. the extrusion diameter of polyvinyl resin mixture made from step B is rodlike no more than 10 μm, it is cut after being water-cooled
It cuts to of length no more than 10 μm and includes powder to get labradorite.
Preferably, toothpaste matrix includes easin, sorbierite, deionized water, thickener, methylparaben, sugar
Smart sodium, glycerol, silica, essence and lauryl sodium sulfate, easin, sorbierite, deionized water, thickener,
Methylparaben, saccharin sodium, glycerol, silica, essence and lauryl sodium sulfate mass ratio be 1-2:33-51:4-8:
0.4-0.8:0.05-0.1:0.1-0.2:3.5-6:7-10:0.45-0.8:0.5-1.1。
Further, raw elongation stone powder, which is made a living, elongates mountain flour, and the raw partial size for elongating mountain flour is 5000 mesh.
Further, elongating stone powder is the raw elongation mountain flour and labradorite extract powder that mass ratio is 1:1, raw to elongate mountain flour
Partial size be 5000 mesh, the particle diameter distribution of labradorite extract powder are as follows: the mass fraction of the labradorite extract powder of r2≤1 μm be 0-
5%, the mass fraction of 3 μm of r2≤6 μm < is 95%-100%.
Wherein, when toothpaste made from the elongation stone powder using the above granularity, Brushing time should control 5min with
On, to reach better permanent tooth effect.
Further, elongating stone powder is the raw elongation mountain flour that partial size is r1, the raw particle diameter distribution for elongating mountain flour are as follows: r1≤
1 μm of the raw mass fraction for elongating mountain flour is 0-10%, and the mass fraction of 3 μm of r1≤4 μm < is 90%-100%, raw labradorite
The RDA < 240 of powder.
Further, labradorite powder include mass ratio be 1:2 partial size be r2 labradorite extract powder and partial size be r3
Labradorite include powder, the particle diameter distribution of labradorite extract powder are as follows: the mass fraction of the labradorite extract powder of r2≤1 μm be 0-
5%, the mass fractions of 3 μm of r2≤6 μm < is 95%-100%, the RDA < 240 of labradorite extract powder, and labradorite includes powder
Particle diameter distribution are as follows: the mass fraction of the labradorite inclusion powder of r3≤1 μm is 0-3%, and the mass fraction of 5 μm of r3≤10 μm < is
97%-100%.
Further, rubbing agent further includes conventional friction agent, and the mass ratio for elongating stone powder and conventional friction agent is 1:1,
Conventional friction agent includes dicalcium phosphate dihydrate, calcite in powder, precipitated silica, aluminium hydroxide, one in anhydrous calcium pyrophosphate
Kind is a variety of.
Further, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min-15min under conditions of 200prm-300prm, add sorbierite, raising is stirred
Speed is mixed to 400prm-450prm, 20min-30min is stirred, the first mixture is made；
S2: the thickener of definite quality ratio is added in glycerol, stirs 10min- under conditions of 100prm-200prm
The second mixture is made in 12min；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in 100prm-
20min-25min is stirred under conditions of 200prm, places 8h-10h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min-50min is stirred under conditions of 1000prm-1200prm to get toothpaste.
Based on the protective effect to gum, the partial size for elongating stone powder can be carried out as the case may be in actual use
Adjustment adjusts within design of the invention the simple of labradorite powder diameter with having the function that better permanent tooth.
Toothpaste provided by the invention based on labradorite can effectively remove tooth stain and calculus dentalis, and can reduce to tooth enamel
Matter damage.
Specific embodiment
Embodiment 1
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 50g toothpaste matrix
With 50g rubbing agent, rubbing agent, which is made a living, elongates mountain flour, the life elongate mountain flour be labradorite directly grind made from, the life elongation
The particle diameter distribution of mountain flour are as follows: the raw mass fraction for elongating mountain flour of r1≤1 μm is 10%, and the mass fraction of 3 μm of r1≤4 μm < is
90%, Mohs' hardness 4；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
G thickener in all embodiments of the invention is all made of xanthan gum, and g essence is all made of sweet orange g essence, above to be
A kind of performance of the invention can also use other kinds of g thickener and g essence, be not specifically limited herein.
Embodiment 2
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 80g toothpaste matrix
With 21g rubbing agent, the labradorite that rubbing agent includes the labradorite extract powder that 7g partial size is r2 and 14g partial size is r3 includes powder, draws
The particle diameter distribution of feldspar extract powder are as follows: the mass fraction of the labradorite extract powder of r2≤1 μm is 5%, the matter of 3 μm of r2≤6 μm <
Measuring score is 95%, and Mohs' hardness 3.5, labradorite includes the particle diameter distribution of powder are as follows: the matter of the labradorite inclusion powder of r3≤1 μm
Measuring score is 3%, and the mass fraction of 5 μm of r3≤10 μm < is 97%；
Toothpaste matrix includes 2g easin, 51g sorbierite, 8g deionized water, 0.8g thickener, 0.1g nipalgin
Methyl esters, 0.2g saccharin sodium, 6g glycerol, 10g silica, 0.8g essence and 1.1g lauryl sodium sulfate.
Embodiment 3
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 62g toothpaste matrix
With 40g rubbing agent, rubbing agent is that raw mountain flour and the 20g dicalcium phosphate dihydrate of elongating of 20g is made through physical mixed, which elongates mountain flour
Be labradorite is directly ground made from, which elongates the particle diameter distribution of mountain flour are as follows: the raw quality for elongating mountain flour point of r1≤1 μm
Number is 8%, and the mass fraction of 3 μm of r1≤4 μm < is 92%, Mohs' hardness 4.5；
Toothpaste matrix includes 1.5g easin, 39g sorbierite, 6g deionized water, 0.7g thickener, 0.15g Buddhist nun
Moor tortoise beetle ester, 0.15g saccharin sodium, 4.5g glycerol, 8.5g silica, 0.7g essence and 0.8g lauryl sodium sulfate.
Embodiment 4
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 50g toothpaste matrix
With 50g rubbing agent, rubbing agent, which is made a living, elongates mountain flour, the life elongate mountain flour be labradorite directly grind made from, the life elongation
The particle diameter distribution of mountain flour are as follows: the raw mass fraction for elongating mountain flour of r1≤1 μm is 10%, and the mass fraction of 3 μm of r1≤4 μm < is
90%, Mohs' hardness 4；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min under conditions of 200prm, add sorbierite, improve mixing speed extremely
400prm stirs 20min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 10min under conditions of 100prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 100prm
20min is stirred under part, places 8h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min is stirred under conditions of 1000prm to get toothpaste.
Embodiment 5
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 80g toothpaste matrix
With 21g rubbing agent, the labradorite that rubbing agent includes the labradorite extract powder that 7g partial size is r2 and 14g partial size is r3 includes powder, draws
The particle diameter distribution of feldspar extract powder are as follows: the mass fraction of the labradorite extract powder of r2≤1 μm is 5%, the matter of 3 μm of r2≤6 μm <
Measuring score is 95%, and Mohs' hardness 3.5, labradorite includes the particle diameter distribution of powder are as follows: the matter of the labradorite inclusion powder of r3≤1 μm
Measuring score is 3%, and the mass fraction of 5 μm of r3≤10 μm < is 97%；
Toothpaste matrix includes 2g easin, 51g sorbierite, 8g deionized water, 0.8g thickener, 0.1g nipalgin
Methyl esters, 0.2g saccharin sodium, 6g glycerol, 10g silica, 0.8g essence and 1.1g lauryl sodium sulfate；
Wherein, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 5cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:3.5, and adjustment pressure is 180KPa, primary every 6min stirring, stir 15min, mixing speed every time
For 700prm, boiling 9h, measures the pH value of an extracting solution every 55min, and adjust pH value to neutrality, is down to room temperature, takes altogether
Labradorite pearl out is crushed to average grain diameter no more than 6 μm to get labradorite extract powder；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 230 DEG C, keep the temperature 30min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:2,
40min is stirred under conditions of temperature is 230 DEG C, mixing speed is 300prm, polyvinyl resin mixture is made；
C. the extrusion diameter of polyvinyl resin mixture made from step B is rodlike no more than 10 μm, it is cut after being water-cooled
It cuts to of length no more than 10 μm and includes powder to get labradorite；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 15min under conditions of 300prm, add sorbierite, improve mixing speed extremely
450prm stirs 30min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 12min under conditions of 200prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 200prm
25min is stirred under part, places 10h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
50min is stirred under conditions of 1200prm to get toothpaste.
Embodiment 6
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 62g toothpaste matrix
With 40g rubbing agent, rubbing agent is that the raw elongation mountain flour of 20g and 20g precipitate g silica and be made through physical mixed, the life labradorite
Powder be labradorite is directly ground made from, which elongates the particle diameter distribution of mountain flour are as follows: the raw quality for elongating mountain flour of r1≤1 μm
Score is 8%, and the mass fraction of 3 μm of r1≤4 μm < is 92%, Mohs' hardness 4.5；
Toothpaste matrix includes 1.5g easin, 39g sorbierite, 6g deionized water, 0.7g thickener, 0.15g Buddhist nun
Moor tortoise beetle ester, 0.15g saccharin sodium, 4.5g glycerol, 8.5g silica, 0.7g essence and 0.8g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 13min under conditions of 250prm, add sorbierite, improve mixing speed extremely
420prm stirs 25min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 11min under conditions of 150prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 150prm
22min is stirred under part, places 9h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
45min is stirred under conditions of 1100prm to get toothpaste.
Embodiment 7
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 80g toothpaste matrix
With 21g rubbing agent, rubbing agent is the labradorite inclusion powder that partial size is r3, and labradorite includes the particle diameter distribution of powder are as follows: r3≤1 μm
The mass fraction that labradorite includes powder is 3%, and the mass fraction of 5 μm of r3≤10 μm < is 97%；
Toothpaste matrix include 2g easin, 50g sorbierite, 1 sodium phytate, 8g deionized water, 0.8g thickener,
0.1g methylparaben, 0.2g saccharin sodium, 6g glycerol, 10g silica, 0.8g essence and 1.1g lauryl sodium sulfate；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 225 DEG C, keep the temperature 25min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:
1.5,35min is stirred under conditions of temperature is 225 DEG C, mixing speed is 280prm, polyvinyl resin mixture is made；
C. the extrusion diameter of polyvinyl resin mixture made from step B is rodlike no more than 10 μm, it is cut after being water-cooled
It cuts to of length no more than 10 μm and includes powder to get labradorite；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 15min under conditions of 300prm, add sorbierite, improve mixing speed extremely
450prm stirs 30min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 12min under conditions of 200prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 200prm
25min is stirred under part, places 10h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
50min is stirred under conditions of 1200prm to get toothpaste.
Embodiment 8
A kind of toothpaste based on labradorite is present embodiments provided, being somebody's turn to do the toothpaste based on labradorite includes 80g toothpaste matrix
With 20g rubbing agent, rubbing agent, which is that 10g is raw, elongates mountain flour and 10g labradorite extract powder, and the raw partial size for elongating mountain flour is 5000 mesh,
The particle diameter distribution of labradorite extract powder are as follows: the mass fraction of the labradorite extract powder of r2≤1 μm is 1%, 3 μm of r2≤6 μm <
Mass fraction is 99%；
Toothpaste matrix include 2g easin, 50g sorbierite, 1 sodium phytate, 8g deionized water, 0.8g thickener,
0.1g methylparaben, 0.2g saccharin sodium, 6g glycerol, 10g silica, 0.8g essence and 1.1g lauryl sodium sulfate；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 225 DEG C, keep the temperature 25min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:
1.5,35min is stirred under conditions of temperature is 225 DEG C, mixing speed is 280prm, polyvinyl resin mixture is made；
C. the extrusion diameter of polyvinyl resin mixture made from step B is rodlike no more than 10 μm, it is cut after being water-cooled
It cuts to of length no more than 10 μm and includes powder to get labradorite；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 15min under conditions of 300prm, add sorbierite, improve mixing speed extremely
450prm stirs 30min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 12min under conditions of 200prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 200prm
25min is stirred under part, places 10h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
50min is stirred under conditions of 1200prm to get toothpaste.
Reference examples 1
A kind of toothpaste is present embodiments provided, which includes 50g toothpaste matrix and 50g rubbing agent, and rubbing agent is two water
Calcium monohydrogen phosphate；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min under conditions of 200prm, add sorbierite, improve mixing speed extremely
400prm stirs 20min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 10min under conditions of 100prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 100prm
20min is stirred under part, places 8h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min is stirred under conditions of 1000prm to get toothpaste.
Reference examples 2
A kind of toothpaste is present embodiments provided, which includes 50g toothpaste matrix and 50g rubbing agent, and rubbing agent is side's solution
Mountain flour；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min under conditions of 200prm, add sorbierite, improve mixing speed extremely
400prm stirs 20min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 10min under conditions of 100prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 100prm
20min is stirred under part, places 8h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min is stirred under conditions of 1000prm to get toothpaste.
Reference examples 3
A kind of toothpaste is present embodiments provided, which includes 50g toothpaste matrix and 50g rubbing agent, and rubbing agent is precipitating g
Silica；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min under conditions of 200prm, add sorbierite, improve mixing speed extremely
400prm stirs 20min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 10min under conditions of 100prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 100prm
20min is stirred under part, places 8h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min is stirred under conditions of 1000prm to get toothpaste.
Reference examples 4
A kind of toothpaste is present embodiments provided, which includes 50g toothpaste matrix and 50g rubbing agent, and rubbing agent is hydrogen-oxygen
Change aluminium；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min under conditions of 200prm, add sorbierite, improve mixing speed extremely
400prm stirs 20min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 10min under conditions of 100prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 100prm
20min is stirred under part, places 8h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min is stirred under conditions of 1000prm to get toothpaste.
Reference examples 5
A kind of toothpaste is present embodiments provided, which includes 50g toothpaste matrix and 50g rubbing agent, and rubbing agent is anhydrous
Calcium pyrophosphate；
Toothpaste matrix includes 1g easin, 33g sorbierite, 4g deionized water, 0.4g thickener, 0.05g Ni Bo
Tortoise beetle ester, 0.1g saccharin sodium, 3.5g glycerol, 7g silica, 0.45g essence and 0.5g lauryl sodium sulfate；
Wherein, toothpaste preparation method the following steps are included:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and go from
It is placed in container in sub- water, stirs 10min under conditions of 200prm, add sorbierite, improve mixing speed extremely
400prm stirs 20min, and the first mixture is made；
S2: the thickener of definite quality ratio being added in glycerol, stirs 10min under conditions of 100prm, is made the
Two mixtures；
S3: the second mixture made from step S2 is added in the first mixture made from step S1, in the item of 100prm
20min is stirred under part, places 8h under room temperature, and third mixture is made；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min is stirred under conditions of 1000prm to get toothpaste.
The effect test of the removal tartar of test example 1
It takes cigarette macula lutea, tea spot to adhere to serious 33 pieces of filemot Isolated Tooth and is divided into 11 groups in parallel at random, every group of 3 pieces of cigarette Huangs
Spot, tea spot attachment seriously refer to that the cigarette macula lutea of in vitro tooth surface and tea spot adhesive rate are higher than 50%, dip embodiment with toothbrush
The toothpaste 1.5g of 4-8, reference examples 1-5 and Yunnan Baiyao Lang Jian (removing smoke spots) scrub the surface of Isolated Tooth, and each Isolated Tooth is brushed
3min to be washed, rinses 5s every 0.5min clear water, every group of Isolated Tooth operates 30 days repeatedly in aforementioned manners, it operates daily twice,
The cigarette macula lutea of the in vitro tooth surface of each group and the adhesive rate of tea spot are observed after 30 days, and calculate calculus removal rate, calculus removal rate
(%)=(before brushing teeth cigarette macula lutea, tea spot adhesive rate-cigarette macula lutea, tea spot adhesive rate after brushing teeth)/brush teeth before cigarette macula lutea, tea spot attachment
Rate × 100%, each group of data are averaged, and the results are shown in Table 1.
The effect of 1. each group toothpaste of table removal tartar
As shown in Table 1, the embodiment of the present application 4-8 provide toothpaste calculus removal rate significantly be higher than reference examples 1-5 and
The toothpaste of Yunnan Baiyao Lang Jian, it was demonstrated that toothpaste provided by the present application can effectively remove tartar, when with dicalcium phosphate dihydrate, side
When solving the replacement elongation stone powders of the invention such as mountain flour, precipitating g silica, aluminium hydroxide, anhydrous calcium pyrophosphate, can it reduce
The calculus removal rate of toothpaste.
Test example 2 removes calculus dentalis test
Modeling: 36 pieces of Isolated Tooths being placed in people's saliva and cultivate plaque, then Isolated Tooth is placed in mineralized liquid makes
Its mineralising is divided into 12 groups, every group 3 pieces, uses the toothpaste of clear water, embodiment 4-8, reference examples 1-5 and Yunnan Baiyao Lang Jian respectively
Mineralising bacterial plaque on each group Isolated Tooth is handled, 2 times a day, scrubs 3min every time, rinses 5s every 0.5min clear water,
The dosage of each group toothpaste is 1.5g/ times, adheres to 30 days, is successively parsed bacterial plaque with sodium hydroxide and hydrogen chloride, analysis
Calcium ion content in mixed liquor calculates the calculus dentalis removal rate of each group toothpaste, calculus dentalis removal rate=(blank sample calcium content-
Test sample calcium content)/blank sample calcium content × 100%, the numerical value of each group result is averaged, and test result is shown in Table 2.
2. calculus dentalis removal rate measurement result of table
As shown in Table 2, the calculus dentalis removal rate for the toothpaste that 4-8 of the embodiment of the present invention is provided is higher than reference examples 1-5 significantly
With Yunnan Baiyao youth's toothpaste, it was demonstrated that toothpaste provided by the invention has good calculus dentalis cleaning capacity.
The test of 3 injury of teeth of test example
33 pieces of Isolated Tooths are placed in people's saliva and cultivate plaque, then Isolated Tooth is placed in mineralized liquid makes its mine
Change, is divided into 11 groups, every group 3 pieces, each group uses the toothpaste of embodiment 4-8, reference examples 1-5 and Yunnan Baiyao Lang Jian to mineralising respectively
Bacterial plaque is handled, and 2 times a day, scrubs 3min every time, rinses 5s every 0.5min clear water, and toothpaste dosage is 1.5g/ times,
After adhering to 30 days, 3500 μ N load are carried out to the enamel of each group Isolated Tooth and control nano-indenter test, are popped one's head in onesize
Power indentation, measure the mechanical property of the enamel of each group Isolated Tooth, mechanical property specifically includes elasticity modulus and hardness, tests
It the results are shown in Table 3.
Test result of the 3. each group toothpaste of table to injury of teeth
As shown in Table 3, after being brushed teeth 30 days using the toothpaste that the embodiment of the present application 4-8 is provided, the elasticity modulus of enamel and
Hardness is higher than the toothpaste and Yunnan Baiyao Lang Jian of reference examples 1-5 significantly, it was demonstrated that tooth enamel of the toothpaste provided by the invention to tooth
The damage very little of matter.
To sum up, only the preferred embodiments of the invention, is not limited the scope of protection of the present invention with this, all according to the invention patent
Equivalent changes and modifications made by range and description are all within the scope of the invention patent covers.
Claims (10)
1. a kind of toothpaste based on labradorite, which is characterized in that the toothpaste based on labradorite includes that mass ratio is 50-80:
The toothpaste matrix and rubbing agent of 20-50, the rubbing agent include at least average grain diameter and are no more than 10 μm, Mohs' hardness 3.5-5
Elongation stone powder, the elongation stone powder is prepared by labradorite.
2. as described in claim 1 based on the toothpaste of labradorite, which is characterized in that the labradorite powder includes raw labradorite
One of powder, labradorite extract powder and labradorite inclusion powder are a variety of, and the raw mountain flour that elongates is directly to grind labradorite
It is made, the raw average grain diameter for elongating mountain flour is no more than 4 μm, and Mohs' hardness 4-5, the labradorite extract powder is will to elongate
It grinds and is made after stone boiling, the average grain diameter of the labradorite extract powder is no more than 6 μm, Mohs' hardness 3.5-4, the elongation
Stone inclusion powder is to be included labradorite extract powder with polyvinyl resin to be made, and the average grain diameter of the labradorite inclusion powder is no more than
10μm。
3. as claimed in claim 2 based on the toothpaste of labradorite, which is characterized in that the preparation method of the labradorite extract powder
The following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 5cm-10cm, is cleaned；
(2) boiling: will be placed in reaction kettle and mix by pretreated labradorite pearl, boiling is added to boil, wherein labradorite pearl with
Water volume ratio is 1:3-1:4, and adjustment pressure is 150KPa-200KPa, primary every 5min-7min stirring, is stirred every time
10min-20min, mixing speed 600prm-800prm, boiling 8h-10h, measures primary extract every 50min-60min altogether
The pH value of liquid, and adjust pH value to neutrality, is down to room temperature, takes out labradorite pearl, be crushed to average grain diameter no more than 6 μm to get
Labradorite extract powder.
4. as claimed in claim 2 based on the toothpaste of labradorite, which is characterized in that the preparation method of the labradorite inclusion powder
The following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 220 DEG C -230 DEG C, keep the temperature 20min-30min, molten is made
The polyvinyl resin of state；
B. labradorite extract powder is added in extruder again, the mass ratio of the labradorite extract powder and polyvinyl resin is 1:1-
1:2 stirs 30min-40min under conditions of temperature is 220 DEG C -230 DEG C, mixing speed is 250prm-300prm, is made poly-
Vinyl mixture；
C. the extrusion diameter of polyvinyl resin mixture made from step B is rodlike no more than 10 μm, it is cut to after being water-cooled
Of length no more than 10 μm include powder to get labradorite.
5. as described in claim 1 based on the toothpaste of labradorite, which is characterized in that the toothpaste matrix includes tetraiodofluorescein
Sodium, sorbierite, deionized water, thickener, methylparaben, saccharin sodium, glycerol, silica, essence and dodecyl sulphate
Sodium, the easin, sorbierite, deionized water, thickener, methylparaben, saccharin sodium, glycerol, silica, perfume (or spice)
The mass ratio of essence and lauryl sodium sulfate is 1-2:33-51:4-8:0.4-0.8:0.05-0.1:0.1-0.2:3.5-6:7-
10:0.45-0.8:0.5-1.1。
6. as claimed in claim 2 based on the toothpaste of labradorite, which is characterized in that the raw partial size for elongating stone powder is
5000 mesh.
7. as claimed in claim 2 based on the toothpaste of labradorite, which is characterized in that it is r1's that the elongation stone powder, which is partial size,
It is raw to elongate mountain flour, the raw particle diameter distribution for elongating mountain flour are as follows: the raw mass fraction for elongating mountain flour of r1≤1 μm is 0-10%, 3
The mass fraction of μm r1≤4 μm < is 90%-100%.
8. as claimed in claim 2 based on the toothpaste of labradorite, which is characterized in that the labradorite powder includes that mass ratio is
The labradorite that the labradorite extract powder and partial size that the partial size of 1:2 is r2 are r3 includes powder, the partial size point of the labradorite extract powder
Cloth are as follows: the mass fraction of the labradorite extract powder of r2≤1 μm is 0-5%, and the mass fraction of 3 μm of r2≤6 μm < is 95%-
100%, the particle diameter distribution of labradorite inclusion powder are as follows: the raw mass fraction for elongating inclusion powder of r3≤1 μm is 0-3%, 5 μm
The mass fraction of r3≤10 μm < is 97%-100%.
9. as claimed in claim 5 based on the toothpaste of labradorite, which is characterized in that the preparation method of the toothpaste includes following
Step:
S1: by the easin of definite quality ratio, methylparaben, saccharin sodium, lauryl sodium sulfate and deionized water
In be placed in container, stir 10min-15min under conditions of 200prm-300prm, add sorbierite, improve stirring speed
Degree stirs 20min-30min, the first mixture is made to 400prm-450prm；
S2: the thickener of definite quality ratio is added in glycerol, stirs 10min- under conditions of 100prm-200prm
The second mixture is made in 12min；
S3: the second mixture made from step S2 is added in the first mixture made from step S1,100prm-200prm's
Under the conditions of stir 20min-25min, place 8h-10h under room temperature, be made third mixture；
S4: the rubbing agent, silica and essence of definite quality ratio are added in third mixture made from step S3,
40min-50min is stirred under conditions of 1000prm-1200prm to get toothpaste.
10. of any of claims 1 or 2 prepared with removal tartar based on the toothpaste of labradorite, mitigated calculus dentalis effect
Application in product.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116035925A (en) * | 2023-01-09 | 2023-05-02 | 四川大学 | Feldspar nano ceramic particle abrasive toothpaste containing simulated enamel mechanical properties |
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Application publication date: 20190514 |