CN109738458A - A kind of crizzle detection method - Google Patents
A kind of crizzle detection method Download PDFInfo
- Publication number
- CN109738458A CN109738458A CN201910162017.XA CN201910162017A CN109738458A CN 109738458 A CN109738458 A CN 109738458A CN 201910162017 A CN201910162017 A CN 201910162017A CN 109738458 A CN109738458 A CN 109738458A
- Authority
- CN
- China
- Prior art keywords
- substrate
- crizzle
- detection method
- environmental protection
- protection type
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The present invention relates to a kind of crizzle detection methods, comprising the following steps: firstly, the foreign matter of substrate surface is processed and removed to substrate;Then, the substrate after processing is put into the solution containing environmental protection type dye and is dyed;Then, the environmental protection type dye solution wiping removal on rear substrate surface and drying will be dyed;Finally, it clean substrate will be surface-treated is placed under strong light and observe, the present invention carries out dyeing processing in substrate surface in advance by way of dyeing, make have apparent color difference between crackle and substrate, observation detection is carried out to substrate surface under strong light again, it detects more quick, accurately, revolutionize existing crack detecting method, and existing penetrating fluid and display liquid are substituted by using environmental protection type dye, it is more environment-friendly and safer, it is discharged in dyeing course without toxic gas, simultaneously, testing methods for tiny crack of the invention is easy to operate, without using complicated equipment and instrument, effectively reduce testing cost.
Description
Technical field
The present invention relates to surface detection technique fields, more particularly to a kind of crizzle detection method.
Background technique
Slag inclusion, micropore, crystal boundary and surface scratching of material internal etc. are likely to crack, these crackles be easy with
The increase of stress and gradually extend, and face crack can cause the performance of equipment, accessory, device sharply to decline, and endanger pole
Greatly, therefore, check that face crack has very important meaning in time.
Currently, osmosis is commonly used for a kind of method of crack nondestructive detection, osmosis is carried out using capillary phenomenon
Flaw detection.Firstly, by the very strong liquid applicator of permeability with fluorescence in substrate surface, because of its strong osmosis, fluorescent liquid
Body will penetrate into bottom along crackle, then wash away the penetrating fluid on surface, and coat display liquid, and since crackle is narrow, capillary is existing
As significant, the penetrating fluid that original penetrates into crackle rises and spreads, and lines is formed in substrate surface, to show the shape of crackle
Shape;This method is although easy to operate, detection sensitivity is high, is also convenient for observing, but detection speed is slower, moreover, because using
Detection agent be strong stimulation toxic chemical, have large effect to the health and environment of people.There is also have use in existing
What microscopy apparatus was detected, Chinese invention patent application specification CN108918549A discloses a kind of wiring board and its detection side
The crack detecting method of method, plated through-hole carries out aging process to board under test first, then, using metallography microscope spectroscopy
Whether the aging plate surface has crackle, using the micro- line in surface of the method detection sample to be tested, although easy to operate, using setting
It is standby few, but because without being handled by dyeing, crackle therein and substrate there is no apparent contrastive colours thus with the naked eye substantially without
Method distinguishes, is also easy to fail to judge, judge by accident even detecting crackle under metallographic microscope.
Summary of the invention
To solve the above problems, the present invention provides a kind of crizzle detection method, it is quick by staining method, quasi-
Substrate surface micro-crack really is detected, it is simple and convenient.
To solve above-mentioned purpose, the present invention adopts the following technical scheme.
A kind of crizzle detection method, comprising the following steps:
K1 is processed to substrate and is removed the foreign matter of substrate surface;
Substrate after processing is put into the solution containing environmental protection type dye and dyes by K2;
K3 will dye the environmental protection type dye solution wiping removal on rear substrate surface and drying;
K4 will be surface-treated clean substrate and be placed under strong light and observes.
Further, the main component proportion of the solution containing environmental protection type dye are as follows: emulsion stabilizer 1-2% eats dye
Expect 3-5%, environmentally friendly solvent 93-96%.
Further, the environmentally friendly solvent is mainly made of water and ethyl alcohol.
Further, food colour is mainly by eating red, edible yellow, edible orange, eating green and other color food colours
One or more of compositions.
Further, emulsion stabilizer mainly by one of gum arabic, animal glue and gelatin or several forms.
Further, in step K1, the procedure of processing to substrate includes but is not limited to laser index carving, chemical etching, machine
One of tool drilling, machine cuts and bending or several combinations.
It further, further include heating the solution step containing environmental protection type dye, heating temperature range exists in step K2
50 DEG C~95 DEG C.
Further, in step K4, it is using human eye or visual detection equipment to base that observation of steps are carried out under strong light
Material surface carries out observation detection.
Further, visual detection equipment includes but is not limited in metallographic microscope, electron microscope and image measurer
One or several kinds of combine.
Further, the substrate material is that the one or several kinds of of ceramics, metal, glass and composite material combine.
Beneficial effects of the present invention are as follows:
The present invention carries out dyeing processing in substrate surface in advance by way of dyeing, makes to have between crackle and substrate
Apparent color difference, then observation detection is carried out to substrate surface under strong light, detection is more quick, accurate, revolutionizes
Existing crack detecting method, and existing penetrating fluid and display liquid, more environmentally-friendly peace are substituted by using environmental protection type dye
Entirely, it is discharged in dyeing course without toxic gas, it is less to environment and body effect, meanwhile, testing methods for tiny crack of the invention
Equipment and instrument easy to operate, without using complexity, effectively reduce testing cost.
Detailed description of the invention
Fig. 1 is the method flow schematic diagram of one embodiment of the present of invention;
Fig. 2 is the substrate surface display schematic diagram of one embodiment of the present of invention.
Specific embodiment
The principles and features of the present invention are described below, and the given examples are served only to explain the present invention, is not intended to limit
Determine the scope of the present invention.
The present invention carries out dyeing processing in substrate surface in advance by way of dyeing, makes to have between crackle and substrate
Apparent color difference, then observation detection is carried out to substrate surface under strong light, detection is more quick, accurate, revolutionizes
Existing crack detecting method, and existing penetrating fluid and display liquid, more environmentally-friendly peace are substituted by using environmental protection type dye
Entirely, it is discharged in dyeing course without toxic gas, it is less to environment and body effect, meanwhile, testing methods for tiny crack of the invention
Equipment and instrument easy to operate, without using complexity, effectively reduce testing cost.
Embodiment one:
Referring to Fig.1 with 2, a kind of crizzle detection method, comprising the following steps:
K1 is processed to substrate and is removed the foreign matter of substrate surface, specifically, using laser index carving mode to aluminium nitride
Ceramic substrate 11 is processed, and obtains the pattern 12 that required processing is formed, and Fig. 2 a shows the base after working process
Material picture on surface 12 after working process, removes substrate surface foreign matter;
Substrate after processing is put into the solution containing environmental protection type dye and dyes by K2, specifically, will prepare in advance
The solution containing environmental protection type dye be heated to 90 DEG C, then the substrate after processing is put into solution and impregnates 10min;
K3 will dye the environmental protection type dye solution wiping removal on rear substrate surface and drying;Specifically, by substrate surface
After dye solution wipes completely, 20min is toasted in the environment of being placed in 90 DEG C, so that substrate surface is dry;
K4 will be surface-treated clean substrate and be placed under strong light and observe, specifically, substrate first can be placed on inspection
It looks into and crizzle 13 is with the naked eye observed and detected under platform, crizzle 13 is as shown in Figure 2 b, then again micro-
Detect that thinner crizzle 14, crizzle 14 are as shown in Figure 2 c under mirror.
Wherein, the main component proportion of the solution containing environmental protection type dye in above-mentioned detection method are as follows: emulsion stabilizer
1-2%, food colour 3-5%, environmentally friendly solvent 93-96%;Specifically, the environmentally friendly solvent is mainly made of water and ethyl alcohol, food
Red to eat with dyestuff, the ethyl alcohol in environmentally friendly solvent can enable food colour preferably soluble in water, and emulsion stabilizer is for I
Uncle's natural gum, gum arabic can make dye solution more stable, and gum arabic can also make dyestuff more after dye solution is dry
In the good crackle for remaining in substrate, use is more stable.
Embodiment two:
A kind of crizzle detection method, comprising the following steps:
K1 is processed to substrate and is removed the foreign matter of substrate surface, specifically, multiple to metal using chemical etching mode
It closes substrate to be processed, obtains the pattern that required processing is formed, after working process, remove substrate surface foreign matter;
Substrate after processing is put into the solution containing environmental protection type dye and dyes by K2, specifically, will prepare in advance
The solution containing environmental protection type dye be heated to 85 DEG C, then the substrate after processing is put into solution and impregnates 12min;
K3 will dye the environmental protection type dye solution wiping removal on rear substrate surface and drying;Specifically, by substrate surface
After dye solution wipes completely, using hot blast drying 18min, so that substrate surface is dry;
K4 will be surface-treated clean substrate and be placed under strong light and observe, specifically, can first be placed under inspection desk
It with the naked eye detects crizzle, comparison is then detected to thinner crizzle using image measurer automatically again.
Wherein, the main component proportion of the solution containing environmental protection type dye are as follows: emulsion stabilizer 1-2%, food colour 3-
5%, environmentally friendly solvent 93-96%;Specifically, the environmentally friendly solvent is mainly made of water and ethyl alcohol, and food colour is edible Huang, cream
Change stabilizer is gelatin, and gelatin can make dye solution more stable, and gelatin can also make dyestuff better after dye solution is dry
Remain in the crackle of substrate;Food colour also for edible orange or can eat green, play coloration, Environmental Safety, and emulsification is steady
Determining agent can also be animal glue, dye solution can be made more stable, the working process in step K1 can also be machine drilling, machinery
Cutting or mechanical bending, this is no longer going to repeat them.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
Limitations on the scope of the patent of the present invention therefore cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Protect range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of crizzle detection method, which comprises the following steps:
K1 is processed to substrate and is removed the foreign matter of substrate surface;
Substrate after processing is put into the solution containing environmental protection type dye and dyes by K2;
K3 will dye the environmental protection type dye solution wiping removal on rear substrate surface and drying;
K4 will be surface-treated clean substrate and be placed under strong light and observes.
2. a kind of crizzle detection method according to claim 1, which is characterized in that contain the molten of environmental protection type dye
The main component of liquid matches are as follows: emulsion stabilizer 1-2%, food colour 3-5%, environmentally friendly solvent 93-96%.
3. a kind of crizzle detection method according to claim 2, which is characterized in that the environmentally friendly solvent mainly by
Water and ethyl alcohol composition.
4. a kind of crizzle detection method according to claim 2, which is characterized in that food colour is mainly by eating
Red, edible yellow, edible orange eats green and other color food colours one or more of compositions.
5. a kind of crizzle detection method according to claim 2, which is characterized in that emulsion stabilizer mainly by Ah
Draw one of uncle's natural gum, animal glue and gelatin or several compositions.
6. a kind of crizzle detection method according to claim 1, which is characterized in that in step K1, to substrate
Procedure of processing include but is not limited to one of laser index carving, chemical etching, machine drilling, machine cuts and bending or several
Kind combines.
7. a kind of crizzle detection method according to claim 1, which is characterized in that in step K2, further include
The solution step containing environmental protection type dye is heated, heating temperature range is at 50 DEG C~95 DEG C.
8. a kind of crizzle detection method according to claim 1, which is characterized in that in step K4, in strong light
Lower progress observation of steps are to carry out observation detection to substrate surface using human eye or visual detection equipment.
9. a kind of crizzle detection method according to claim 8, which is characterized in that visual detection equipment include but
It is not limited to one of metallographic microscope, electron microscope and image measurer or several combinations.
10. a kind of crizzle detection method according to claim 1, which is characterized in that the substrate material is pottery
Porcelain, metal, glass and the one or several kinds of of composite material combine.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910162017.XA CN109738458A (en) | 2019-03-05 | 2019-03-05 | A kind of crizzle detection method |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910162017.XA CN109738458A (en) | 2019-03-05 | 2019-03-05 | A kind of crizzle detection method |
Publications (1)
Publication Number | Publication Date |
---|---|
CN109738458A true CN109738458A (en) | 2019-05-10 |
Family
ID=66369310
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910162017.XA Pending CN109738458A (en) | 2019-03-05 | 2019-03-05 | A kind of crizzle detection method |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN109738458A (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110132756A (en) * | 2019-06-04 | 2019-08-16 | Oppo广东移动通信有限公司 | The test method of shell |
CN110470674A (en) * | 2019-08-26 | 2019-11-19 | 哈尔滨工程大学 | A kind of visual analysis method for lubricating fluid injection porous surface damage |
CN111707566A (en) * | 2020-06-24 | 2020-09-25 | 太原理工大学 | Experimental system for researching dynamic response of structure under impact load and application method |
CN112378925A (en) * | 2020-09-24 | 2021-02-19 | 宁波市鄞州世纪耀达市政建设有限公司 | CCTV-based pipeline detection method |
CN113075237A (en) * | 2021-05-10 | 2021-07-06 | 佛山市东鹏陶瓷有限公司 | Method for detecting printing defects of ceramic tiles |
CN113155857A (en) * | 2021-05-13 | 2021-07-23 | 广东电网有限责任公司 | Cable breakage detection device |
CN116626058A (en) * | 2023-07-25 | 2023-08-22 | 天津正道机械制造有限公司 | Metal workpiece surface flatness detection device |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3931733A (en) * | 1974-12-16 | 1976-01-13 | Alburger James R | Method and means of accelerating removal of background entrapments in the inspection penetrant process |
JPH0266437A (en) * | 1988-09-01 | 1990-03-06 | Marktec Corp | Harmless liquid penetrant for dye penetrant testing |
CN102466644A (en) * | 2010-11-19 | 2012-05-23 | 江苏瑞特回转支承有限公司 | Penetrant testing method of opening defect on surface of workpiece |
CN102585761A (en) * | 2011-01-13 | 2012-07-18 | 归锦华 | Colorless transparent penetrating agent |
CN102721704A (en) * | 2012-06-26 | 2012-10-10 | 潮州三环(集团)股份有限公司 | Method and device for automatically detecting defects of electronic ceramic chips |
CN103409013A (en) * | 2013-06-21 | 2013-11-27 | 天长市润达金属防锈助剂有限公司 | Environment-friendly water-based crackle coating and preparation method thereof |
CN105738378A (en) * | 2016-02-23 | 2016-07-06 | 上海航天动力科技工程有限公司 | Multifunctional self-development dye penetrant and application thereof |
-
2019
- 2019-03-05 CN CN201910162017.XA patent/CN109738458A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3931733A (en) * | 1974-12-16 | 1976-01-13 | Alburger James R | Method and means of accelerating removal of background entrapments in the inspection penetrant process |
JPH0266437A (en) * | 1988-09-01 | 1990-03-06 | Marktec Corp | Harmless liquid penetrant for dye penetrant testing |
CN102466644A (en) * | 2010-11-19 | 2012-05-23 | 江苏瑞特回转支承有限公司 | Penetrant testing method of opening defect on surface of workpiece |
CN102585761A (en) * | 2011-01-13 | 2012-07-18 | 归锦华 | Colorless transparent penetrating agent |
CN102721704A (en) * | 2012-06-26 | 2012-10-10 | 潮州三环(集团)股份有限公司 | Method and device for automatically detecting defects of electronic ceramic chips |
CN103409013A (en) * | 2013-06-21 | 2013-11-27 | 天长市润达金属防锈助剂有限公司 | Environment-friendly water-based crackle coating and preparation method thereof |
CN105738378A (en) * | 2016-02-23 | 2016-07-06 | 上海航天动力科技工程有限公司 | Multifunctional self-development dye penetrant and application thereof |
Non-Patent Citations (1)
Title |
---|
杨红霞: "《饮料加工技术》", 28 February 2015, 重庆大学出版社 * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110132756A (en) * | 2019-06-04 | 2019-08-16 | Oppo广东移动通信有限公司 | The test method of shell |
CN110470674A (en) * | 2019-08-26 | 2019-11-19 | 哈尔滨工程大学 | A kind of visual analysis method for lubricating fluid injection porous surface damage |
CN110470674B (en) * | 2019-08-26 | 2021-10-19 | 哈尔滨工程大学 | Visual analysis method for damage of porous surface injected with lubricating liquid |
CN111707566A (en) * | 2020-06-24 | 2020-09-25 | 太原理工大学 | Experimental system for researching dynamic response of structure under impact load and application method |
CN112378925A (en) * | 2020-09-24 | 2021-02-19 | 宁波市鄞州世纪耀达市政建设有限公司 | CCTV-based pipeline detection method |
CN113075237A (en) * | 2021-05-10 | 2021-07-06 | 佛山市东鹏陶瓷有限公司 | Method for detecting printing defects of ceramic tiles |
CN113155857A (en) * | 2021-05-13 | 2021-07-23 | 广东电网有限责任公司 | Cable breakage detection device |
CN116626058A (en) * | 2023-07-25 | 2023-08-22 | 天津正道机械制造有限公司 | Metal workpiece surface flatness detection device |
CN116626058B (en) * | 2023-07-25 | 2023-10-13 | 天津正道机械制造有限公司 | Metal workpiece surface flatness detection device |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN109738458A (en) | A kind of crizzle detection method | |
CN105738378A (en) | Multifunctional self-development dye penetrant and application thereof | |
US8003009B2 (en) | Fluorescent and visible penetrant inspection | |
CN104389032B (en) | A kind of Degumming method being applicable to containing green fluorescent protein silk | |
CN104236980A (en) | Retained austenite contained dual phase steel color metallography coloring agent and coloring display method | |
CN103822922B (en) | The quick method for determining mortar/aggregate area fraction in concrete section | |
US2405078A (en) | Method and compositions for locating surface discontinuities | |
CN110320074A (en) | A kind of processing method after the metallographic specimen etch with crack defect | |
CN102539435A (en) | High-sensitivity coloring-fluorescence dual-purpose flaw detection permeation liquid | |
CN113218958B (en) | Water-washing type dye check penetrant using water as developer, and preparation method and use method thereof | |
CN104048933B (en) | In a kind of colorful cotton fibre, flavones content differentiates the method for natural color-cotton | |
CN105131647A (en) | Dye composition for biological HE dyeing and its application and use method | |
JP5093574B2 (en) | Penetration testing method | |
JP2551033B2 (en) | Crack detection agent | |
CN106932322A (en) | A kind of interior wall tests the method and apparatus of contaminated resistance | |
JP5720944B2 (en) | Penetration testing method using washable water based penetrant for penetration testing | |
CN208013093U (en) | Vaginal fluid visible component detection reagent external member | |
CN110579395A (en) | method for detecting color fastness to water rubbing of bamboo mat products | |
US4186304A (en) | Extender for dye penetrant composition | |
US3777157A (en) | Water washable dye penetrant composition and method of application | |
CN111595652B (en) | Coloring agent for identifying tissues in steel and method for identifying tissues in steel | |
US3929664A (en) | Water-washable inspection penetrant employing triglycerides and polyglycerides of fatty acids | |
CN106442275B (en) | A kind of method and kit of qualitative detection chyle | |
RU2593343C1 (en) | Method for staining the histological cuts in diagnosing trichinosis | |
CN105758807B (en) | A method of identifying waste lubricating oil |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190510 |