CN109736078A - A kind of postfinishing process of the nice and cool sportswear fabric of moisture absorption - Google Patents
A kind of postfinishing process of the nice and cool sportswear fabric of moisture absorption Download PDFInfo
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- CN109736078A CN109736078A CN201910049080.2A CN201910049080A CN109736078A CN 109736078 A CN109736078 A CN 109736078A CN 201910049080 A CN201910049080 A CN 201910049080A CN 109736078 A CN109736078 A CN 109736078A
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Abstract
The present invention relates to a kind of postfinishing process of the nice and cool sportswear fabric of moisture absorption, comprising: (1) prepares hydroxylating nanometer BN powder HO-BNNSs；(2) HO-BNNSs, hydrophilic finishing agent and titanate coupling agent are mixed, prepares dispersion finishing fluid；(3) polyester/polyurethane fabric is subjected to alkali modification processing；(4) alkali modification polyester/polyurethane fabric is padded in dispersion finishing fluid, second dipping and rolling, preliminary drying bakes, and obtains that moisture absorption is nice and cool to wash ammonia sportswear fabric.Arranging process of the invention is simple, and the fabric of arrangement has excellent moisture absorption and nice and cool performance.
Description
Technical field
The invention belongs to functional exercise fabric technical field, in particular to the final finishing of the nice and cool sportswear fabric of a kind of moisture absorption
Technique.
Background technique
Under the conditions of strenuous exercise, human body, which largely perspires, easily forms high temperature, high humidity climatic environment, especially in hot climate
Summer it is particularly evident, human skin surface's moist heat will have a direct impact on its wearing comfort at this time, gently can then generate and wear
Sense of discomfort, therefore people more favor moisture absorption in nice and cool, comfortable textile, to summer sports garment material, nice and cool performance
It also proposed requirements at the higher level, more focus on the functionality of clothes.Among current sportswear fabric, pure-cotton fabric hygroscopicity is strong, with skin
Contact is also easy to produce feeling of oppression and heat when its movement perspiration without any stimulation, is good for since sweat can not discharge in time to human body
Health can generate certain influence.For polyester/polyurethane fabric as the big main force's fabric of current sportswear fabric one, comprehensive advantage is stronger, has easy to wash
The advantages that quick-drying, elasticity is good, sun-proof, cheap more meets today's society people for the primary demand of sportswear fabric, but
There are a little shortcoming, such as hygroscopicity difference etc. to be still left to be desired.
In research before, some scholars carry out fabric by using graphene powder or peppermint oil microcapsule etc. cool
It is refreshing to arrange, assign its certain heating conduction, cooling effect reached with this, but graphite has a little disadvantage, such as to environment and
Human body can generate certain harm, will form graphite dust in air, and be easy to get pneumoconiosis after human body sucking, and it is strong to influence human body
Health and generation environment pollution problem；Graphite higher cost simultaneously, is not easy industrialized development；Its powder is in black, for fabric
Color can generate certain influence；And peppermint oil microcapsule cost of manufacture is high, production and processing also has certain requirement to equipment, no
Conducive to high-volume, industrialization production.
Chinese patent (201810078502.4) discloses a kind of difunctional knitting fabric of graphene, first respectively by graphite
Alkene and regenerated cellulose are modified processing, mix solution carry out melting later, obtain graphene viscose fiber；
Secondly, slices of caprone is mixed with modified graphene oxide, extruding pelletization, graphene-chinlon master batch, Zhi Houzai is made
It carries out melt-spinning technology and graphene-polyamide fibre composite fibre is made, functional fiber is finally subjected to different tissues structure again
Braiding, knits to obtain functional exercise fabric eventually.Including graphene composite fibre layer and ordinary fiber layer；The double function of its graphene developed
Fabric can be knitted and prepare graphene composite fibre layer by using the mixed yarn of graphene nylon fibre and graphene viscose rayon,
This functional knitted sportswear fabric utilizes the higher thermal conductivity of graphene polyamide fibre composite fibre and unique far infrared heating function
Can, keep sports fan's dress nice and cool, comfortable.Above by the modification of graphene, regenerated celulose fibre and nylon fibre,
The techniques such as melt spinning prepare functional fiber, then carry out the braiding of functional fabric, can assign fabric certain cooling effect, but
Its production and processing technology has biggish difficulty, and the high requirements on the equipment, process is relatively complicated, higher cost, is unfavorable for large quantities of
The production and processing of amount, industrialized development still have certain difficulty.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of postfinishing process of the nice and cool sportswear fabric of moisture absorption, overcome
Existing graphene powder or peppermint oil microcapsule etc. carry out the defect of nice and cool arrangement to fabric.
A kind of postfinishing process of the nice and cool sportswear fabric of moisture absorption of the invention, comprising:
(1) nanometer BN is aoxidized under hot steam, cooled and filtered washing is dry, obtains hydroxylating nanometer BN powder HO-
BNNSs；
(2) HO-BNNSs made from step (1) is dissolved in deionized water, magnetic agitation, while hydrophilic finishing agent is added
And titanate coupling agent, pH value 6.5~7.5 is stood and adjusts, ultrasonic disperse obtains dispersion finishing fluid；Wherein, HO-BNNSs,
The mass fraction of hydrophilic finishing agent and titanate coupling agent ratio is 2~6%:1~12%:1~6%；
(3) polyester/polyurethane fabric is placed in concussion in lye to handle, is washed after taking-up, dries, obtain alkali modification polyester/polyurethane fabric；
(4) alkali modification polyester/polyurethane fabric made from step (3) is padded in step (2) dispersion finishing fluid obtained, two leachings
Two roll, and preliminary drying bakes, and obtain that moisture absorption is nice and cool to wash ammonia sportswear fabric.
The process conditions aoxidized under hot steam in the step (1) are as follows: 850~1000 are raised the temperature in Muffle furnace
DEG C, keep the temperature 2~3h.
The process conditions of filtration washing in the step (1) are as follows: repeated filtration washing 3~5 times using deionized water.
Hydrophilic finishing agent in the step (2) is TF-620.
Titanate coupling agent in the step (2) is HY311W.
The time of magnetic agitation is 0.5~1h in the step (2).
The time of ultrasonic disperse is 1~2h in the step (2).
PH value is adjusted using ammonium hydroxide in the step (2).
Lye is the NaOH solution of 15~20g/L in the step (3).
The process conditions of concussion processing in the step (3) are as follows: be placed in oscillation treatment in 75~90 DEG C of shaking bath pot
20~40min.
The process conditions washed in the step (3) are as follows: washed repeatedly 3~5 times using deionized water.
The temperature dried in the step (3) is 100~110 DEG C.
The liquid carrying rate of second dipping and rolling is 90~110% in the step (4).
The technological parameter of preliminary drying in the step (4) are as follows: preliminary drying temperature is 100~110 DEG C, and preliminary drying time is 2~3min.
The technological parameter baked in the step (4) are as follows: stoving temperature is 150~170 DEG C, and baking the time is 1~2min.
Beneficial effect
(1) arranging process of the invention is simple, and the fabric of arrangement has excellent moisture absorption and nice and cool performance.
(2) present invention carries out nice and cool arrangement to polyester/polyurethane fabric by using nanometer BN powder.With existing nice and cool finishing technique
It is compared using graphene powder or peppermint oil microcapsule, the white powdery of nanometer BN is conducive to the commercialization of fabric.Its chemistry is steady
Qualitative higher, finish fabric has certain functions such as anti-oxidant, anticorrosive；It also has excellent heating conduction and graphite
Structure is similar, is layer structure, because it is white, person " white graphite ", while its production and processing cost are lower, are easy to produce
Industryization development, asepsis environment-protecting are widely used in women skin protection cosmetics, therefore can be safe to use among textile finishing.
(3) present invention chooses the hydrophilic agent of Polyester-polyether copolymer structure, carries out moisture absorption to fabric using padding method
Cooling function arranges, and fabric is first impregnated in 5-10min in dispersion finishing fluid, then makes it through roller on padding machine for finishing fluid
It squeezes to polyester/polyurethane fabric, later by preliminary drying, the process baked, promotes fabric segmented structure to stretch by high temperature, so that with
The part-structure of the similar hydrophilic finishing agent of fabric construction generates cocrystallization, and segment is shunk after cooling, by finishing agent hydrophobic portion
Separation structure is coated on fabric, and hydrophilic segment is exposed at surface, and the moisture absorption of strong, durable is reached with this.At the same time, it receives
Rice BN powder chemically reacts it with fabric by high-temperature process, firmly in conjunction with fabric under the action of coupling agent
Together, achieved the effect that with this nice and cool.And padding method process can be used for high-volume consecutive production, and it is high-efficient, it is at low cost,
It is easily controllable, be conducive to the industrialized development of such functional fabric.
Specific embodiment
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, those skilled in the art
Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Range.
The testing standard used in the embodiment of the present invention:
(1) hygroscopicity test: according to GB/T 21655.1-2008 " evaluation-part 1 of textile absorbing fast-drying:
Individual event composite test method " test of moisture absorbing and sweat releasing performance is carried out to fabric.
(2) property of feeling nice and cool test: according to GB/T 35263-2017 " detection and evaluation of textile Contact cool feeling performance "
Nice and cool performance test is carried out to fabric.
Polyester/polyurethane fabric (Quanzhou Lian Xingfa) door width that the present invention chooses is 165cm, grammes per square metre 260g/m2；(the Suzhou nanometer BN
Receive plain material) white powdery, granular size is 300~500nm；Hydrophilic finishing agent TF-620 (development of evil in febrile disease chemical industry)；Titanate esters
Coupling agent HY311W (and first chemical industry).
Embodiment 1
(1) nanometer BN is placed in temperature in Muffle furnace and is increased to 900 DEG C, 2.5h is kept the temperature, when through superheated steam high-temperature process
Aoxidize, then cool down, back edge exfoliating, by issuable in deionized water filtration washing high-temperature oxidation process
By-product, and repeat filtration washing 3 times, it finally dries, obtains hydroxylating nanometer BN powder HO-BNNSs.
(2) using deionized water as decentralized medium, the HO-BNNSs dispersion liquid that mass fraction is 3%, magnetic agitation are prepared
0.5h, stirring while 3% TF-620 hydrophilic finishing agent of addition and 1.5% HY311W stand observation and are simultaneously adjusted with ammonium hydroxide
The pH value of dispersion liquid is within the scope of 6.5-7.5, later ultrasonic disperse 1h, and it is whole to be finally configured to uniform and stable dispersion
Manage liquid.
(3) ammonia fabric will be washed to be put into the NaOH solution of 15g/L, is placed in 80 DEG C of shaking bath pot and carries out at oscillation
30min is managed, is then taken out, while being washed using deionized water, washing 3 times is repeated, is dried in 105 DEG C of baking ovens later,
It is final that alkali modification washs ammonia fabric.
(4) the alkali modification polyester/polyurethane fabric of step (3) is padded in the dispersion finishing fluid of step (2), second dipping and rolling (liquid carrying rate
90%), then preliminary drying (105 DEG C, 2min), bake (160 DEG C, 1min), obtain that moisture absorption is nice and cool to wash ammonia sportswear fabric.
Embodiment 2
(1) nanometer BN is placed in temperature in Muffle furnace and is increased to 900 DEG C, 2.5h is kept the temperature, when through superheated steam high-temperature process
Aoxidize, then cool down, back edge exfoliating, by issuable in deionized water filtration washing high-temperature oxidation process
By-product, and repeat filtration washing 3 times, it finally dries, obtains hydroxylating nanometer BN powder HO-BNNSs.
(2) using deionized water as decentralized medium, the HO-BNNSs dispersion liquid that mass fraction is 4%, magnetic agitation are prepared
0.5h stirs while being added 6% TF-620 hydrophilic finishing agent and 2% HY311W, stands observation and is adjusted with ammonium hydroxide and is divided
The pH value of dispersion liquid is within the scope of 6.5-7.5, later ultrasonic disperse 1h, is finally configured to uniform and stable dispersion and is arranged
Liquid.
(3) ammonia fabric will be washed to be put into the NaOH solution of 15g/L, is placed in 80 DEG C of shaking bath pot and carries out at oscillation
30min is managed, is then taken out, while being washed using deionized water, washing 3 times is repeated, is dried in 105 DEG C of baking ovens later,
It is final that alkali modification washs ammonia fabric.
(4) the alkali modification polyester/polyurethane fabric of step (3) is padded in the dispersion finishing fluid of step (2), second dipping and rolling (liquid carrying rate
90%), then preliminary drying (105 DEG C, 2min), bake (160 DEG C, 1min), obtain that moisture absorption is nice and cool to wash ammonia sportswear fabric.
Embodiment 3
(1) nanometer BN is placed in temperature in Muffle furnace and is increased to 900 DEG C, 2.5h is kept the temperature, when through superheated steam high-temperature process
Aoxidize, then cool down, back edge exfoliating, by issuable in deionized water filtration washing high-temperature oxidation process
By-product, and repeat filtration washing 3 times, it finally dries, obtains hydroxylating nanometer BN powder HO-BNNSs.
(2) using deionized water as decentralized medium, the HO-BNNSs dispersion liquid that mass fraction is 5%, magnetic agitation are prepared
0.5h, stirring while 7.5% TF-620 hydrophilic finishing agent of addition and 5% HY311W stand observation and are simultaneously adjusted with ammonium hydroxide
The pH value of dispersion liquid is within the scope of 6.5-7.5, later ultrasonic disperse 1h, and it is whole to be finally configured to uniform and stable dispersion
Manage liquid.
(3) ammonia fabric will be washed to be put into the NaOH solution of 15g/L, is placed in 80 DEG C of shaking bath pot and carries out at oscillation
30min is managed, is then taken out, while being washed using deionized water, washing 3 times is repeated, is dried in 105 DEG C of baking ovens later,
It is final that alkali modification washs ammonia fabric.
(4) the alkali modification polyester/polyurethane fabric of step (3) is padded in the dispersion finishing fluid of step (2), second dipping and rolling (liquid carrying rate
90%), then preliminary drying (105 DEG C, 2min), bake (160 DEG C, 1min), obtain that moisture absorption is nice and cool to wash ammonia sportswear fabric.
Embodiment 4
(1) nanometer BN is placed in temperature in Muffle furnace and is increased to 900 DEG C, 2.5h is kept the temperature, when through superheated steam high-temperature process
Aoxidize, then cool down, back edge exfoliating, by issuable in deionized water filtration washing high-temperature oxidation process
By-product, and repeat filtration washing 3 times, it finally dries, obtains hydroxylating nanometer BN powder HO-BNNSs.
(2) using deionized water as decentralized medium, the HO-BNNSs dispersion liquid that mass fraction is 6%, magnetic agitation are prepared
0.5h stirs while being added 12% TF-620 hydrophilic finishing agent and 6% HY311W, stands observation and is adjusted with ammonium hydroxide and is divided
The pH value of dispersion liquid is within the scope of 6.5-7.5, later ultrasonic disperse 1h, is finally configured to uniform and stable dispersion and is arranged
Liquid.
(3) ammonia fabric will be washed to be put into the NaOH solution of 15g/L, is placed in 80 DEG C of shaking bath pot and carries out at oscillation
30min is managed, is then taken out, while being washed using deionized water, washing 3 times is repeated, is dried in 105 DEG C of baking ovens later,
It is final that alkali modification washs ammonia fabric.
(4) the alkali modification polyester/polyurethane fabric of step (3) is padded in the dispersion finishing fluid of step (2), second dipping and rolling (liquid carrying rate
90%), then preliminary drying (105 DEG C, 2min), bake (160 DEG C, 1min), obtain that moisture absorption is nice and cool to wash ammonia sportswear fabric.
Embodiment 5
The performance survey washed ammonia sportswear fabric and carry out hygroscopicity and nice and cool property nice and cool to moisture absorption made from 1-4 of the embodiment of the present invention
Examination, the results are shown in Table 1, it is known that embodiment 1-4 obtain functional fabric, measure wicking height all>10cm, drip diffusion time all<
1s reaches moisture absorbing and sweat releasing textile standards (GB/T 21655.1)；Its maximum thermal transient flow Q simultaneouslymaxAll > 0.15J/
(cm2S), reach nice and cool property textile standards (GB/T 35263-2017).In conclusion textile fabric of the present invention have compared with
Moisture absorption well, nice and cool performance.
Fabric performance test result obtained by 1 embodiment 1-4 of table
Comparative example 1
This comparative example is selected from Chinese patent (201810078502.4), provides a kind of difunctional knitted side of graphene
Material, the invention firstly the need of different fibers are modified, the processing such as melt spinning, it is later that the setting of each fiber is different blended
Than spun yarn, then by changing institutional framework to be woven into different types of functional fabric, finally with test fabric heat
The mode of resistance characterizes its good heating conduction, does not measure the maximum transient heat flow magnitude of fabric, while the present invention directly so
It is compared with it, processing process is simple, and to the of less demanding of Dyeing & Finishing Equipment, processing cost is lower, more has
Conducive to the industrialized development of moisture cool fabric.
Comparative example 2
This comparative example is selected from document " multicomponent functional fibre blended wearing fabric research and product development ", provides
The several cool fabric as made of natural fiber and the braiding of jade modified fibre, and the blending ratio by changing different fibers is compiled
It is made into functional fabric, the maximum thermal transient flow Q that several fabrics of document braiding finally measuremaxAll < 0.156J/
(cm2S), while the present invention is compared with it, produce and process it is at low cost, it is also not special to braiding and dyeing process to want
It asks, manufacturing procedure is simple, is more advantageous to the industrialized development of moisture cool fabric.
Claims (10)
- The postfinishing process of sportswear fabric 1. a kind of moisture absorption is felt nice and cool, comprising:(1) nanometer BN is aoxidized under hot steam, cooled and filtered washing is dry, obtains hydroxylating nanometer BN powder HO- BNNSs；(2) HO-BNNSs made from step (1) is dissolved in deionized water, magnetic agitation, while hydrophilic finishing agent and titanium is added Acid esters coupling agent, stands and adjusts pH value 6.5~7.5, and ultrasonic disperse obtains dispersion finishing fluid；Wherein, HO-BNNSs, hydrophilic The mass fraction of finishing agent and titanate coupling agent ratio is 2~6%:1~12%:1~6%；(3) polyester/polyurethane fabric is placed in concussion in lye to handle, is washed after taking-up, dries, obtain alkali modification polyester/polyurethane fabric；(4) alkali modification polyester/polyurethane fabric made from step (3) is padded in step (2) dispersion finishing fluid obtained, second dipping and rolling, Preliminary drying bakes, and obtains that moisture absorption is nice and cool to wash ammonia sportswear fabric.
- 2. technique according to claim 1, it is characterised in that: the process conditions aoxidized under hot steam in the step (1) Are as follows: 850~1000 DEG C are raised the temperature in Muffle furnace, keep the temperature 2~3h；The process conditions of filtration washing are as follows: using go from Sub- water repeats filtration washing 3~5 times.
- 3. technique according to claim 1, it is characterised in that: the hydrophilic finishing agent in the step (2) is TF-620；Titanium Acid esters coupling agent is HY311W.
- 4. technique according to claim 1, it is characterised in that: in the step (2) time of magnetic agitation be 0.5~ 1h；The time of ultrasonic disperse is 1~2h.
- 5. technique according to claim 1, it is characterised in that: adjust pH value using ammonium hydroxide in the step (2).
- 6. technique according to claim 1, it is characterised in that: lye is that the NaOH of 15~20g/L is molten in the step (3) Liquid.
- 7. technique according to claim 1, it is characterised in that: the process conditions of concussion processing in the step (3) are as follows: set 20~40min of oscillation treatment in 75~90 DEG C of shaking bath pot.
- 8. technique according to claim 1, it is characterised in that: the process conditions washed in the step (3) are as follows: use and go Ionized water washes repeatedly 3~5 times；The temperature of drying is 100~110 DEG C.
- 9. technique according to claim 1, it is characterised in that: in the step (4) liquid carrying rate of second dipping and rolling be 90~ 110%.
- 10. technique according to claim 1, it is characterised in that: the technological parameter of preliminary drying in the step (4) are as follows: preliminary drying Temperature is 100~110 DEG C, and preliminary drying time is 2~3min；The technological parameter baked are as follows: stoving temperature is 150~170 DEG C, is baked Time is 1~2min.
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| CN114960193A (en) * | 2022-04-24 | 2022-08-30 | 雅戈尔服装制造有限公司 | Processing method of natural antibacterial hemp ultraviolet-proof cool fabric |
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