CN109731696A - A kind of static flotation method suitable for coarse granule recycling - Google Patents

A kind of static flotation method suitable for coarse granule recycling Download PDF

Info

Publication number
CN109731696A
CN109731696A CN201910194532.6A CN201910194532A CN109731696A CN 109731696 A CN109731696 A CN 109731696A CN 201910194532 A CN201910194532 A CN 201910194532A CN 109731696 A CN109731696 A CN 109731696A
Authority
CN
China
Prior art keywords
cylinder
flotation
coarse granule
pipe
coal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201910194532.6A
Other languages
Chinese (zh)
Other versions
CN109731696B (en
Inventor
邢耀文
桂夏辉
丁世豪
徐梦迪
曹亦俊
张友飞
夏阳超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China University of Mining and Technology CUMT
Original Assignee
China University of Mining and Technology CUMT
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China University of Mining and Technology CUMT filed Critical China University of Mining and Technology CUMT
Priority to CN201910194532.6A priority Critical patent/CN109731696B/en
Publication of CN109731696A publication Critical patent/CN109731696A/en
Application granted granted Critical
Publication of CN109731696B publication Critical patent/CN109731696B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Separation Of Solids By Using Liquids Or Pneumatic Power (AREA)

Abstract

The present invention relates to a kind of static flotation methods suitable for coarse granule recycling, belong to mineral floating technical field, solve the problems, such as that existing method for floating processing capacity is small, separating effect is poor and be not able to satisfy coarse granule drying slime requirement.The static flotation method, includes the following steps: step 1: filling clear water into the second cylinder by water injection pipe, the clear water of 1/5~1/3 volume is injected into the first cylinder;Step 2: opening circulating pump and bubble generator, the intracorporal clear water of the second column are spilled over in the first cylinder, and microvesicle is generated in the second cylinder;Step 3: after the velocity-stabilization that the intracorporal clear water of the second column is overflowed into the first cylinder, the coal slime material of preparatory mineralising is fed into feed distributor, carries out flotation, wherein flotation concentrate is recycled by discharge nozzle, and tail coal is discharged through underflow pipe/outlet.Method for floating of the invention is easy to operate, good separation effect, can be widely applied for coarse granule drying slime.

Description

A kind of static flotation method suitable for coarse granule recycling
Technical field
The present invention relates to mineral floating technical field more particularly to a kind of static flotation methods suitable for coarse granule recycling.
Background technique
Coal is one of main energy pillar in China, and resourceful, reserves are big.Untreated coal storage and transportation, plus Work, the process utilized can bring pollution to environment, endanger human health.The continuous of National Sustainable Development Strategies is implemented, coal Clean utilization also become the focus that everybody constantly discusses warmly.In recent decades, it under the overall background with rapid changepl. never-ending changes and improvements of science and technology, mines Mechanization Level be continuously improved, dense-medium separation technology it is improved day by day, cause slime content during coal separation also sharply to increase, after giving Continuous coal slime processing links bring very big challenge.
At present coal preparation plant often with classifying cyclone to coal slime through row 0.25mm pre-classification ,+0.25mm coarse granule coal slime is used TBS interferes bed sorting, -0.25mm fine grained coal slime flotation device or flotation column recycling.But in the actual production process, on the one hand Classifying cyclone operational efficiency is difficult to ensure that another aspect TBS interference bed is also difficult to control coal grain separating effect near 1mm. Cause in practical floatation process, floatation feed particle size range is often between 0-1mm.And conventional flotation equipment to granularity model Enclose coal slime between 0.074-0.25mm can effectively stable recycling, for the coal slime between 0.25-1mm, mineral laden bubble is vulnerable to floating Ore pulp disturbing influence in optional equipment, the desorption phenomenon between coal grain and bubble is serious, and flotation effect is bad.
Conventional flotation column is compared with flotation device, though p- 0.074mm or less subparticle selection performance is controlled, flotation Ore pulp turbulivity in column can also decrease, but dynamic circulation of the ore pulp in flotation column, between bubble and coarse granule coal slime Stick there are still influence, be unfavorable for coarse granule recycling, leading to " running thick ", phenomenon takes place frequently, tail coal ash content is difficult to improve, calorific value occupies The problems such as height does not descend, entire flotation link morbid state operation.
Due to only one cylinder of traditional flotation column, the flotation section in cylinder middle and upper part completes froth flotation, the rotation of lower part It flows section and completes eddy flow centrifugal classification, the discharge of tailing is completed in bottom, and bottom separately sets interface and extracts ore pulp for recycling.Tradition is floating The purpose for selecting above-mentioned circulation in column is: coal (coal particle between cleaned coal and spoil) is occurred by circulating pump, microvesicle in The devices such as device feed flotation column lower part along cyclone pipe with certain pressure tangent line;The effect of circulation is: one side tangent line feeds to be formed Eddy flow completes eddy flow centrifugal classification and provides microvesicle on the other hand by releasing stress bubble for flotation section flotation.Therefore, Above-mentioned many processes in traditional flotation column occur in a flotation column, and especially extracting ore pulp from flotation column bottom, this is dynamic State process will certainly have an impact ore pulp fluid stability in flotation column, be unfavorable for sticking between bubble and ore particle.
Therefore, the characteristics of recycling, is difficult to coarse granule according to the increasing production status of slime content and conventional flotation column, Targetedly study, develop it is novel suitable for coarse granule recycling static flotation method it is significant, prospect is considerable.
Summary of the invention
In view of above-mentioned analysis, the present invention is intended to provide a kind of static flotation method suitable for coarse granule recycling, to solve The problem of certainly existing method for floating processing capacity is small, separating effect is poor and is not able to satisfy coarse granule drying slime requirement.
The purpose of the present invention is mainly achieved through the following technical solutions:
A kind of method for floating suitable for coarse granule recycling, includes the following steps:
Step 1: filling clear water into the second cylinder by water injection pipe, and 1/5~1/3 volume is injected into the first cylinder Clear water;
Step 2: opening circulating pump and bubble generator, the intracorporal clear water of the second column are spilled over in the first cylinder, the second column Microvesicle is generated in vivo;
Step 3: after the velocity-stabilization that the intracorporal clear water of the second column is overflowed into the first cylinder, by the coal of preparatory mineralising Mud material feeds feed distributor, carries out flotation, wherein flotation concentrate is recycled by discharge nozzle, and tail coal is arranged through underflow pipe/outlet Out.
Further, further includes:
Step 4: in floating-upward process, part cleaned coal particle enters in the first cylinder the cleaned coal particle in the second cylinder, the Ore pulp in one cylinder carries out external static circulation in fluid circulating line;
Step 5: the ore pulp in fluid circulating line tangentially feeds through the cyclone pipe of the second cylinder lower part with certain pressure The conical section of two cylinder lower parts;
Step 6: with the continuous progress of flotation, the bubble in the second cylinder carries cleaned coal particle and constantly floats and assemble Froth bed is formed, when foam layer height is more than the first cylinder upper surface, the flotation concentrate overflow in froth bed goes out the first cylinder, It is flowed out through overflow launder by discharge nozzle, the tail coal of the second cylinder bottom is discharged through underflow pipe/outlet, above-mentioned steps four to step 6 It circuits sequentially, until entire flotation terminates.
Further, it in step 3, specifically includes:
Process one: coal slime material is uniformly fallen into the second cylinder by self gravity, fills sieve plate and the second column by multilayer Ascending current forms adverse current in body, and the coal slime to cause to fall and break collides with ascending current, wherein the good cleaned coal of surface hydrophobic Grain sticks with bubble and is floated, and the spoil particle of surface hydrophobic difference does not stick with bubble and fallen;
Process two: the coal slime material of preparatory mineralising is fed in the froth bed of the first cylinder through being fed distributor, coal slime material First time sorting is carried out in froth zone;
Process three: it does not fall into the second cylinder, and is pressed from both sides in ascending current under the effect of gravity with the coal slime that foam floats Miscellaneous microvesicle collides contact, and second of flotation is carried out in the second cylinder.
Further, in process one, the adjusting intracorporal mineral syrup liquid of the first column is concordant with the second cylinder upper end, the second cylinder The middle bubble for carrying cleaned coal particle floating is assembled on mineral syrup liquid in the first cylinder, forms the froth bed of certain depth, and The height of froth bed is kept to maintain dynamic equilibrium during entire coal slime flotation.
Further, in step 5, the weight product in ore pulp containing spoil contains cleaned coal along the cone wall decline of the second cylinder eddy flow section It is gas-solid-liquid mixing liquid stream rise in the second cylinder.
Further, using the Static Flotation Column for being suitable for coarse granule recycling, Static Flotation Column includes the first cylinder and second Cylinder, the first cylinder and the second cylinder are barrel-like structure, and the second columnar part is nested in the first cylinder;Second cylinder top Feed distributor is equipped in opening to the space of the first cylinder top end opening, feed distributor is connect with feeding pipe;Feed distribution The top of device is equipped with water distributor;The top excircle of first cylinder is equipped with overflow launder;The bottom of first cylinder and the second cylinder Bottom connects to form fluid circulating line by diversion pipe.
Further, nested are as follows: the bottom plate of the first cylinder of top of the second cylinder is penetrated and sealed nested set on first In cylinder;Fluid flows to along fluid circulating line, and diversion pipe is successively arranged circulating pump, bubble generator and mineralising pipe.
Further, the bottom of the first cylinder is equipped with the first flow-guiding mouth, and the bottom of the second cylinder is equipped with the second flow-guiding mouth, leads The both ends of flow tube are connect with the first flow-guiding mouth, the second flow-guiding mouth respectively.
Further, cyclone pipe is equipped in the lower part of the second cylinder, cyclone pipe is connect with the second flow-guiding mouth;Second cylinder Lower sides are connected with water injection pipe;The bottom of second cylinder is pyramidal structure, and the bottom of the second cylinder is equipped with for bottom material to be discharged Underflow pipe/outlet.
Further, the second column body is equipped with multilayer and fills sieve plate.
Compared with prior art, the present invention one of at least has the advantages that:
A) method for floating provided by the invention suitable for coarse granule recycling, by inside and outside nested double-deck cylinder design, first Cylinder undertakes the effect of middling cycle, and compared to the second cylinder or common flotation column for carrying out flotation, floatation process realizes ore pulp External static circulation, reduces the disturbing influence to ore pulp in the second cylinder floatation process, realizes mild flotation environment, have Effect improves the collision sticking probability of particle and bubble, reduces coarse grained desorption, improves coarse grained recovering effect, can It is widely used in the coal slime flotation of coarse granule recycling.
B) method for floating provided by the invention suitable for coarse granule recycling, by setting and the feeding pipe of mineral syrup liquid, gives Expect distributor, the optimization of water distributor installation site, realization is fed in froth bed, and the collision for being conducive to cleaned coal particle and bubble is glutinous It is attached, cooperate the flushing water at top, coal slime is completed to sort in advance in froth bed, and the good cleaned coal particle of hydrophobicity easily sticks with bubble Bubble layer is rested on, the spoil particle of hydrophobicity difference, which is not easy to stick with bubble, falls into lower section the second cylinder of flotation column, cooperation first Water distributor in cylinder at the top of froth bed, flushing water go out the gangue particle being mingled between bubble, realize into float coal mud Primary effectively sorting, it is significant particularly with the recovering effect of coarse granule cleaned coal, reduce the hair of coarse granule and bubble desorption phenomenon It is raw, facilitate coarse grained recycling, promotes separating effect.
It in the present invention, can also be combined with each other between above-mentioned each technical solution, to realize more preferred assembled schemes.This Other feature and advantage of invention will illustrate in the following description, also, certain advantages can become from specification it is aobvious and It is clear to, or understand through the implementation of the invention.The objectives and other advantages of the invention can by specification, claims with And it is achieved and obtained in specifically noted content in attached drawing.
Detailed description of the invention
Attached drawing is only used for showing the purpose of specific embodiment, and is not to be construed as limiting the invention, in entire attached drawing In, identical reference symbol indicates identical component.
Fig. 1 is the schematic diagram of the section structure for being suitable for the Static Flotation Column of coarse granule recycling in embodiment.
Appended drawing reference:
1- feeding pipe;2- diversion pipe;The first cylinder of 3-;The second cylinder of 4-;5- cyclone pipe;6- circulating pump;7- overflow launder;8 Discharge nozzle;9- water distributor;10- is fed distributor;11- water injection pipe;12- bubble generator;13- fills sieve plate;14- mineralising pipe; 15- underflow pipe/outlet;16- water injection pipe;A, b, c, d, e- pulp flow direction.
Specific embodiment
Specifically describing the preferred embodiment of the present invention with reference to the accompanying drawing, wherein attached drawing constitutes the application a part, and Together with embodiments of the present invention for illustrating the principle of the present invention, it is not intended to limit the scope of the present invention.Phase in embodiment Close term and make following agreement: middle coal refers to that the coal particle between cleaned coal and spoil, chats refer to the ore pulp containing middle coal.Mine The direction of motion is starched, refers to ore pulp/clear water flowing direction in floatation process, a, b, c, d, e are Static Flotation Column section in Fig. 1 The signal direction of middle pulp flow.
Embodiment one
A specific embodiment of the invention discloses a kind of static flotation method suitable for coarse granule recycling, use Flotation rod structure is as shown in Figure 1, the static flotation method includes the following steps:
Step 1: it is filled the water into the first cylinder 3 and the second cylinder 4.Specifically, before starting coal slime flotation, the is closed One flow-guiding mouth and underflow pipe/outlet 15 are opened water injection pipe 11 and are switched, start water pump, fill clear water into the second cylinder 4, the After filling water in two cylinders 4, water, which overflows, to be flowed into the second cylinder 4, and the clear water of 1/5~1/3 volume is injected in the first cylinder 3, excellent It selects and injects 1/4 volume clear water into the first cylinder 3, water filling finishes, and closes water injection pipe 11.
Step 2: opening circulating pump 6 and bubble generator 12, and the clear water in the second cylinder 4 is spilled over in the first cylinder 3, In flotation column section as shown in Figure 1, the clear water in the second cylinder 4 is recycled according to direction of motion a, b;Adjust bubble Air door on device 12, making to generate in the second cylinder 4 is suitable for stable microvesicle (i.e. bubble).
Step 3: after the velocity-stabilization that the clear water in the second cylinder 4 is overflowed into the first cylinder 3, ore pulp is pre-processed The coal slime material of preparatory mineralising feeds the feed distributor 10 on 4 top of the second cylinder by feed pipe 1 in device, carries out flotation.Its In, step 3 specifically includes following three process:
Process one: initial procedure.Coal slime material is uniformly fallen into the second cylinder 4 by self gravity, is filled and is sieved by multilayer Ascending current forms adverse current in plate 13 and the second cylinder 4, and the coal slime to cause to fall and break collides with ascending current, wherein surface hydrophobicity The good cleaned coal particle of property sticks with bubble and is floated, and the spoil particle of surface hydrophobic difference does not stick with bubble and fallen.It adjusts Mineral syrup liquid in first cylinder 3 is concordant with 4 upper end of the second cylinder, and the bubble that cleaned coal particle floats is carried in the second cylinder 4 and is existed Assemble on mineral syrup liquid in first cylinder 3, forms the froth bed of certain depth, and pass through the air inlet of control bubble generator 12 Amount, the speed of the charging of feed pipe 1 and 15 discharge of underflow pipe/outlet and flow are to keep the height of froth bed floating in entire coal slime Dynamic equilibrium is maintained during choosing.
Process two: froth bed feed carries out first time sorting.The coal slime material of preparatory mineralising is distributed through feed pipe 1 by feed Device 10 is fed in the froth bed in the first cylinder 3 on mineral syrup liquid, and coal slime material is sorted in advance in froth zone.Wherein, The good cleaned coal particle of hydrophobicity and bubble, which collide to stick, to be rested in froth bed, the general cleaned coal of hydrophobicity and spoil particle And hydrophobicity it is good not with the cleaned coal particle of bubble floating under the effect of gravity, fall into the second cylinder 4 and then carry out second Sorting.In the process, the flushing water in water distributor 9 rinses the froth bed on 3 top of the first cylinder, flushing water hole between bubble The gangue particle being mingled with constantly is taken away to flowing down in road, due to flow fields environment mild in froth bed and a large amount of existing air waters circle Face improves the collision probability of cleaned coal particle and bubble, especially increases three-phase when coarse granule cleaned coal sticks with bubble and moistens Wetted perimeter edge lengths improve the sticking probability of coarse granule and bubble, reduce the desorption probability of coarse granule and bubble, realize to thick The first time selective recovery of particle and fine grained cleaned coal.
Second of flotation is carried out in three: the second cylinder 4 of process.It is not fallen under the effect of gravity with the coal slime that foam floats In second cylinder 4, collides and contact with the microvesicle being mingled in ascending current.Multilayer filling sieve plate 13 in second cylinder 4 is right Whereabouts coal slime plays buffer function, reduces because coal slime whereabouts effect of inertia leads to the disturbance to ore pulp, ensure that second The stabilization of ore pulp in cylinder 4, the good cleaned coal particle that is conducive to hydrophobicity is contacted with bubble hit to be sticked and floats, especially The desorption probability in coarse granule cleaned coal floatation process with bubble is reduced, coarse grained recycling is enhanced.
Step 4: chats external static circulation.(the movement in Fig. 1 in cleaned coal particle floating-upward process in second cylinder 4 Direction c), will receive ore pulp disturbing influence, and the general cleaned coal particle of partially hydrophobic enters the (fortune in Fig. 1 in the first cylinder 3 Dynamic direction a, b).Is mixed into during a small amount of coarse granule cleaned coal and spoil fall into the second cylinder 4 from froth bed in addition, also having In one cylinder 3.Ore pulp in first cylinder 3 carries out external static circulation in fluid circulating line, specifically, the first cylinder 3 In ore pulp through diversion pipe 2, pass sequentially through circulating pump 6, bubble generator 12, mineralising pipe 14 and realize external static circulation, improve Circulation reduces the turbulivity of ore pulp, improves cleaned coal particle and stick with bubble to the perturbation action of ore pulp in the second cylinder 4 Stability, be especially reduction of the desorption probability of coarse granule cleaned coal and bubble, enhance the flotation of coarse granule cleaned coal.Wherein, Ore pulp in first cylinder 3 refers to black water, the general cleaned coal particle of the hydrophobicity including falling into along direction of motion a, b and a small amount of The coarse granule cleaned coal and water fallen from froth bed.
Step 5: eddy flow section sorting.Ore pulp in fluid circulating line is (i.e. through diversion pipe 2, circulating pump in the first cylinder 3 6, bubble generator 12, mineralising pipe 14 recycle the ore pulp of mineralising) cyclone pipe 5 with certain pressure through 4 lower part of the second cylinder is tangential The conical section for feeding 4 lower part of the second cylinder is sorted in the second cylinder 4, and conical section is that the bottom of the second cylinder 4 is scanned Area.Wherein, the weight product in ore pulp containing spoil is along the cone wall decline of 4 eddy flow section of the second cylinder, gas-solid-liquid mixed liquor containing cleaned coal Stream rises in the second cylinder 4, is acted on, is improved to the selective recovery for entering float coal mud by the intensified sorting of centrifugal force field.
Step 6: discharging process.With the continuous progress of flotation, it is continuous that the bubble in the second cylinder 4 carries cleaned coal particle It floats, constantly aggregation forms froth bed on mineral syrup liquid in the first cylinder 3, when foam layer height is more than on the first cylinder 3 When end face, the flotation concentrate overflow in froth bed goes out the first cylinder 3 (direction of motion d, e in Fig. 1), through overflow launder 7 by going out Expects pipe 8 flows out, and the tail coal of 4 bottom of the second cylinder is discharged through underflow pipe/outlet 15, and above-mentioned steps four to step 6 are successively followed Ring, until entire flotation terminates.
Compared with prior art, the method for floating provided in this embodiment suitable for coarse granule recycling, by inside and outside nested double Layer cylinder design, floatation process realizes ore pulp external static circulation, can effectively improve the collision sticking probability of particle and bubble, dredges Aqueous good cleaned coal particle, which easily sticks with bubble, rests on bubble layer, and the spoil particle of hydrophobicity difference, which is not easy to stick with bubble, to be fallen into The second cylinder of lower section flotation column 4 cooperates the water distributor 9 in the first cylinder 3 at the top of froth bed, the arteries and veins that flushing water will be mingled between bubble Stone particle is gone out, and the first time realized into float coal mud effectively sorts, significant particularly with the recovering effect of coarse granule cleaned coal, is subtracted The generation for having lacked coarse granule and bubble desorption phenomenon, promotes separating effect.The coal slime of whereabouts is slowed down by filling sieve plate 13 And adverse current is formed with the ascending current in the second cylinder 4, it collides and sticks with the microvesicle being mingled in ascending current, hydrophobicity is good Cleaned coal particle be attached on bubble with bubble floating, the spoil particle of hydrophobicity difference does not adhere to bubble and is fallen, thus mentions The stability of separating effect is risen.Method for floating provided in this embodiment passes through the setting of mineral syrup liquid and feeding pipe 1, feed Foam feed is realized in the optimization of 10 installation site of distributor, and the collision for being conducive to cleaned coal particle and bubble is sticked, and promotes flotation effect Fruit;Ore pulp enters the second cylinder bottom through circulating pump 6, bubble generator 12,14 tangent line jet stream of mineralising pipe and scans in first cylinder 3 Area ensure that ore pulp is stable in the second cylinder 4 and move upwards, increase bubble buoyancy, and provide the eddy flow field of force and scan, Improve the rate of recovery.The feed distributor 10 being arranged on feeding pipe 1 is fed in froth bed, cooperates the flushing water at top, and coal slime exists Sorting in advance is completed in froth bed, facilitates coarse grained recycling.
Embodiment two
A specific embodiment of the invention discloses and is suitable in the static flotation method of coarse granule recycling in embodiment one What is used is suitable for the Static Flotation Column of coarse granule recycling, as shown in Figure 1, including the first cylinder 3 and the second cylinder 4, the first cylinder 3 It is barrel-like structure with the second cylinder 4,4 part of the second cylinder is nested in the first cylinder 3;Second cylinder, 4 top end opening is to Feed distributor 10 is equipped in the space of one cylinder, 3 top end opening, feed distributor 10 is connect with feeding pipe 1;It is fed distributor 10 top is equipped with the water distributor 9 connecting with flush water pump;The top excircle of first cylinder 3 is equipped with overflow launder 7;First cylinder 3 bottom connect to form fluid circulating line with the bottom of the second cylinder 4 by diversion pipe 2.
In the present embodiment, 4 part of the second cylinder is nested in the first cylinder 3, specific nested are as follows: the second cylinder 4 it is upper The bottom plate of the first cylinder of portion 3 is penetrated and is sealed nested set on the first cylinder 3.Fluid circulating line includes diversion pipe 2, along fluid Fluid flows in circulation line, and diversion pipe 2 is successively arranged circulating pump 6, bubble generator 12 and mineralising pipe 14;First cylinder 3 Bottom is equipped with the first flow-guiding mouth, and the bottom of the second cylinder 4 is equipped with the second flow-guiding mouth, the both ends of diversion pipe 2 respectively with the first water conservancy diversion Mouth, the connection of the second flow-guiding mouth.
In the present embodiment, cyclone pipe 5 is equipped in the lower part of the second cylinder 4, cyclone pipe 5 is connect with the second flow-guiding mouth;Second The lower sides of cylinder 4 are connected with water injection pipe 11;The bottom of second cylinder is pyramidal structure, and the bottom of the second cylinder, which is equipped with, to be used for Underflow pipe/outlet 15 of bottom material is discharged.Through diversion pipe 2, circulating pump 6, bubble generator 12, mineralising pipe 14 in first cylinder 3 Recycle the circular cone that cyclone pipe 5 of the ore pulp of mineralising with certain pressure through 4 lower part of the second cylinder tangentially feeds 4 lower part of the second cylinder Section, this section are that area is scanned in the bottom of the second cylinder 4.On the one hand it is inclined to provide rising for the second cylinder 4 for the flotation column of this structure Stream, effectively increases bubble buoyancy, on the other hand provides the eddy flow field of force and scan, and improves the rate of recovery.
For traditional flotation column in floatation process, coal particle whereabouts inertia is big, after coal particle is contacted with bubble hit, desorption Probability is very big, and flotation effect is poor.Thus, it is contemplated that trapping area's ore pulp turbulent velocity influences flotation effect, and the second column body is set There is multilayer to fill sieve plate 13, filling sieve plate 13 is set to 5 or more cyclone pipe, it is preferable that the quantity of filling sieve plate 13 is 3~6 layers, edge The spacing of the longitudinal centre line of second cylinder 4, adjacent two fillings sieve plate 13 is identical, alternatively, adjacent two fillings sieve plate from top to bottom 13 spacing is gradually reduced, the second cylinder 4 with multilayer filling sieve plate 13, can significantly reduce trapping area's ore pulp turbulent flow speed Degree increases buffer time, reduces the desorption of coarse granule coal, promotes the efficiency of separation.
In order to further decrease trapping area's ore pulp turbulent velocity, increase buffer time, filling sieve plate 13 is wavy shaped configuration, Sieve pore is set to the wave trough position of filling sieve plate 13, and the coal particle for falling in filling 13 crest location of sieve plate slides from crest location to wave Paddy position increases preparatory buffer stage on every layer of filling sieve plate 13, has compared with the filling sieve plate 13 of horizontal structure longer Buffer time, the efficiency of separation are more preferable.
In the present embodiment, the bottom plate of overflow launder 7 opens up discharge port 8, and the bottom plate of overflow launder 7 is lower than the top of the first cylinder 3 Opening;Preferably, the bottom plate of overflow launder 7 is obliquely installed, it is preferable that the angle of 3 longitudinal centre line of bottom plate and the first cylinder is 45 ° ~75 °, bottom plate has the overflow launder 7 of certain tilt angle, and flotation particle can quickly be discharged, avoid flotation in overflow launder 7 Grain accumulation causes to block, and ensure that the job stability of flotation column.The ore pulp to float in order to prevent overflows, and overflow launder 7 is equipped with lid Plate can prevent ore pulp/foam overflow, ensure that the stability of flotation column work.
In the present embodiment, water distributor 9 is 8 claw structure, and water distributor 9 is equipped with flow valve, and the water distributor 9 of this structure can It falls in water uniformly on the froth bed of 3 upper end of the first cylinder, avoids flotation dead angle area, and can be according to coal slurry flotation item Part setting and the amount of water sprayed and water-jet velocity for adjusting water distributor 9, coal slime are completed to sort in advance in froth bed, facilitate coarse granule Recycling, improve flotation effect, optimize flotation flowsheet.
Compared with prior art, the Static Flotation Column provided in this embodiment suitable for coarse granule recycling, passes through the first cylinder 3 With 4 nested designs of the second cylinder, structure is simple, stable, adaptable, processing capacity is strong, and the first cylinder 3 undertakes chats and follows The effect of ring, compared to carry out flotation the second cylinder 4 or common flotation column, ore pulp recycle the characteristics of be it is external, static, It is advantageously implemented ore pulp static external circulation, reduces the disturbing influence to ore pulp in the second cylinder floatation process, realizes temperature The flotation environment of sum, reduces coarse grained desorption, improves coarse grained recovering effect, can be widely applied for coarse granule and returns The coal slime flotation of receipts.In addition, the Static Flotation Column provided in this embodiment suitable for coarse granule recycling, is fed distributor 10 in foam Layer feed, the interior multilayer that is equipped with of the second cylinder 4 fill sieve plate 13, play buffer function to the coal slime particle to fall from froth bed, The disturbance to ore pulp is slowed down, mild flow fields environment is provided to the flotation of coal slime particle, is reduced to coarse granule cleaned coal Desorption.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, In the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of by anyone skilled in the art, It should be covered by the protection scope of the present invention.

Claims (10)

1. a kind of method for floating suitable for coarse granule recycling, which comprises the steps of:
Step 1: filling clear water in the second cylinder (4) by water injection pipe (11), to injection 1/5~1/3 in the first cylinder (3) The clear water of volume;
Step 2: opening circulating pump (6) and bubble generator (12), and the clear water in the second cylinder (4) is spilled over to the first cylinder (3) It is interior, microvesicle is generated in the second cylinder (4);
Step 3: after the velocity-stabilization that the clear water in the second cylinder (4) is overflowed into the first cylinder (3), by preparatory mineralising Coal slime material feeds feed distributor (10), carries out flotation, wherein flotation concentrate is recycled by discharge nozzle (8), and tail coal is through underflow Pipe/outlet (15) discharge.
2. the method for floating according to claim 1 suitable for coarse granule recycling, which is characterized in that further include:
Step 4: in floating-upward process, part cleaned coal particle enters in the first cylinder (3) the cleaned coal particle in the second cylinder (4), Ore pulp in first cylinder (3) carries out external static circulation in fluid circulating line;
Step 5: the ore pulp in fluid circulating line is tangentially fed with certain pressure through the cyclone pipe (5) of the second cylinder (4) lower part The conical section of the second cylinder (4) lower part;
Step 6: with the continuous progress of flotation, the bubble in the second cylinder (4) carries cleaned coal particle and constantly floats and assemble shape At froth bed, when foam layer height is more than the first cylinder (3) upper surface, the flotation concentrate overflow in froth bed goes out the first cylinder (3), it being flowed out through overflow launder (7) by discharge nozzle (8), the tail coal of the second cylinder (4) bottom is discharged through underflow pipe/outlet (15), Above-mentioned steps four to step 6 circuits sequentially, until entire flotation terminates.
3. the method for floating according to claim 1 or 2 suitable for coarse granule recycling, which is characterized in that in step 3, specifically Include:
Process one: coal slime material is uniformly fallen into the second cylinder (4) by self gravity, passes through multilayer filling sieve plate (13) and second Ascending current forms adverse current in cylinder (4), and the coal slime to cause to fall and break collides with ascending current, wherein the good essence of surface hydrophobic Coal particle sticks with bubble and is floated, and the spoil particle of surface hydrophobic difference does not stick with bubble and fallen;
Process two: the coal slime material of preparatory mineralising is fed in the froth bed of the first cylinder (3) through being fed distributor (10), coal slime object Material carries out first time sorting in froth zone;
Process three: it does not fall into the second cylinder (4), and is mingled in ascending current under the effect of gravity with the coal slime that foam floats Microvesicle collide contact, second of flotation is carried out in the second cylinder (4).
4. the method for floating according to claim 3 suitable for coarse granule recycling, which is characterized in that in process one, adjust the Mineral syrup liquid in one cylinder (3) is concordant with the second cylinder (4) upper end, and the gas that cleaned coal particle floats is carried in the second cylinder (4) Bubble is assembled on the first cylinder (3) interior mineral syrup liquid, forms the froth bed of certain depth, and keep the height of froth bed whole Dynamic equilibrium is maintained during a coal slime flotation.
5. the method for floating according to claim 2 suitable for coarse granule recycling, which is characterized in that in step 5, in ore pulp Weight product containing spoil is along the cone wall decline of the second cylinder (4) eddy flow section, and gas-solid-liquid mixing liquid stream containing cleaned coal is in the second cylinder (4) rise in.
6. the method for floating according to any one of claims 1 to 5 suitable for coarse granule recycling, which is characterized in that using suitable In coarse granule recycling Static Flotation Column, the Static Flotation Column include the first cylinder (3) and the second cylinder (4), described first Cylinder (3) and the second cylinder (4) are barrel-like structure, and second cylinder (4) is partially nested in the first cylinder (3);
Feed distributor is equipped in second cylinder (4) top end opening to the space of the first cylinder (3) top end opening (10), the feed distributor (10) connect with feeding pipe (1);
The top of feed distributor (10) is equipped with water distributor (9);
The top excircle of first cylinder (3) is equipped with overflow launder (7);
The bottom of first cylinder (3) connect to form fluid circulation with the bottom of second cylinder (4) by diversion pipe (2) Pipeline.
7. the method for floating according to claim 6 suitable for coarse granule recycling, which is characterized in that the nesting are as follows: described The bottom plate of the first cylinder of top (3) of second cylinder (4) penetrates and seals nested be set in first cylinder (3);
Fluid flows to along the fluid circulating line, and the diversion pipe (2) is successively arranged circulating pump (6), bubble generator (12) and mineralising pipe (14).
8. the method for floating according to claim 7 suitable for coarse granule recycling, which is characterized in that first cylinder (3) Bottom be equipped with the first flow-guiding mouth, the bottom of second cylinder (4) is equipped with the second flow-guiding mouth, the both ends of the diversion pipe (2) It is connect respectively with the first flow-guiding mouth, the second flow-guiding mouth.
9. the method for floating according to claim 7 or 8 suitable for coarse granule recycling, which is characterized in that second cylinder (4) cyclone pipe (5) are equipped in lower part, the cyclone pipe (5) connect with second flow-guiding mouth;
The lower sides of second cylinder (4) are connected with water injection pipe (11);
The bottom of second cylinder is pyramidal structure, and the bottom of second cylinder (4) is equipped with the underflow for bottom material to be discharged Pipe/outlet (15).
10. being suitable for the method for floating of coarse granule recycling described in -9 according to claim 1, which is characterized in that second cylinder Inside is equipped with multilayer filling sieve plate (13).
CN201910194532.6A 2019-03-14 2019-03-14 static flotation method suitable for coarse particle recovery Active CN109731696B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910194532.6A CN109731696B (en) 2019-03-14 2019-03-14 static flotation method suitable for coarse particle recovery

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910194532.6A CN109731696B (en) 2019-03-14 2019-03-14 static flotation method suitable for coarse particle recovery

Publications (2)

Publication Number Publication Date
CN109731696A true CN109731696A (en) 2019-05-10
CN109731696B CN109731696B (en) 2019-12-13

Family

ID=66370430

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910194532.6A Active CN109731696B (en) 2019-03-14 2019-03-14 static flotation method suitable for coarse particle recovery

Country Status (1)

Country Link
CN (1) CN109731696B (en)

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110773331A (en) * 2019-09-30 2020-02-11 河南大学 Enrichment device for separating micro-plastics in environmental soil and sediments
CN110882829A (en) * 2019-12-11 2020-03-17 郑州大学 Coarse particle tailing discarding sorting system based on hydraulic flotation technology
CN111389580A (en) * 2020-03-19 2020-07-10 中国矿业大学 Three-product hydraulic flotation machine for coarse particle recovery and separation method
CN112337655A (en) * 2020-09-27 2021-02-09 中国矿业大学 Three-product flotation column and method suitable for high-ash fine-fraction coal slime
CN112452552A (en) * 2020-10-30 2021-03-09 中国矿业大学 Coarse-grained mineral dissociation device and method integrating tailing discarding and dissociation
CN112691792A (en) * 2020-12-10 2021-04-23 中国矿业大学 Quality-improving dissociation device and method for coarse-grained minerals
CN112934457A (en) * 2021-02-02 2021-06-11 中国矿业大学 Gravity-flotation integrated coal slime separation equipment and method
CN113198619A (en) * 2021-05-18 2021-08-03 中南大学 Coarse particle flotation equipment and method adopting rotational flow and damping coupled fluidization
CN113457853A (en) * 2021-06-23 2021-10-01 湖南柿竹园有色金属有限责任公司 Unpowered gas stirring type flotation device and flotation method
CN113649163A (en) * 2021-07-15 2021-11-16 中煤科工集团唐山研究院有限公司 Pulse type continuous discharging device and method of interference bed separator
CN114700182A (en) * 2021-07-22 2022-07-05 中国矿业大学 Coarse particle fluidized flotation device and method for gradient air intake
CN114713380A (en) * 2021-10-19 2022-07-08 中国矿业大学 Coarse particle flotation device and method based on coupling of ultrasonic waves and mechanical damping blocks

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2431047Y (en) * 2000-07-07 2001-05-23 中国矿业大学(北京校区) Bidirectionally inflating jet flotation column
CN101653748A (en) * 2008-11-13 2010-02-24 湖南君毅科技发展有限公司 Cyclone-static microbubble floatation column
CN101773873A (en) * 2010-03-04 2010-07-14 中国矿业大学 Slime separation method and equipment
CN102327818A (en) * 2011-09-30 2012-01-25 湖南长高矿山机电设备有限公司 Floatation device
CA2837224A1 (en) * 2011-05-25 2013-05-23 Cidra Corporate Services Inc. Techniques for transporting synthetic beads or bubbles in a flotation cell or column
CN205095964U (en) * 2015-10-28 2016-03-23 中国矿业大学 Static microbubble flotation column of inflatable whirl
BR202015024339U2 (en) * 2015-09-22 2017-03-28 Pontual Consultoria Empresarial Pesquisa E Desenvolvimento Mineral Ltda Me double aeration flotation column

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2431047Y (en) * 2000-07-07 2001-05-23 中国矿业大学(北京校区) Bidirectionally inflating jet flotation column
CN101653748A (en) * 2008-11-13 2010-02-24 湖南君毅科技发展有限公司 Cyclone-static microbubble floatation column
CN101773873A (en) * 2010-03-04 2010-07-14 中国矿业大学 Slime separation method and equipment
CA2837224A1 (en) * 2011-05-25 2013-05-23 Cidra Corporate Services Inc. Techniques for transporting synthetic beads or bubbles in a flotation cell or column
CN102327818A (en) * 2011-09-30 2012-01-25 湖南长高矿山机电设备有限公司 Floatation device
BR202015024339U2 (en) * 2015-09-22 2017-03-28 Pontual Consultoria Empresarial Pesquisa E Desenvolvimento Mineral Ltda Me double aeration flotation column
CN205095964U (en) * 2015-10-28 2016-03-23 中国矿业大学 Static microbubble flotation column of inflatable whirl

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110773331A (en) * 2019-09-30 2020-02-11 河南大学 Enrichment device for separating micro-plastics in environmental soil and sediments
CN110882829A (en) * 2019-12-11 2020-03-17 郑州大学 Coarse particle tailing discarding sorting system based on hydraulic flotation technology
CN111389580A (en) * 2020-03-19 2020-07-10 中国矿业大学 Three-product hydraulic flotation machine for coarse particle recovery and separation method
CN111389580B (en) * 2020-03-19 2021-11-02 中国矿业大学 Three-product hydraulic flotation machine for coarse particle recovery and separation method
CN112337655B (en) * 2020-09-27 2021-09-10 中国矿业大学 Three-product flotation column and method suitable for high-ash fine-fraction coal slime
CN112337655A (en) * 2020-09-27 2021-02-09 中国矿业大学 Three-product flotation column and method suitable for high-ash fine-fraction coal slime
CN112452552A (en) * 2020-10-30 2021-03-09 中国矿业大学 Coarse-grained mineral dissociation device and method integrating tailing discarding and dissociation
CN112452552B (en) * 2020-10-30 2022-02-11 中国矿业大学 Coarse-grained mineral dissociation device and method integrating tailing discarding and dissociation
CN112691792A (en) * 2020-12-10 2021-04-23 中国矿业大学 Quality-improving dissociation device and method for coarse-grained minerals
CN112934457A (en) * 2021-02-02 2021-06-11 中国矿业大学 Gravity-flotation integrated coal slime separation equipment and method
CN113198619A (en) * 2021-05-18 2021-08-03 中南大学 Coarse particle flotation equipment and method adopting rotational flow and damping coupled fluidization
CN113198619B (en) * 2021-05-18 2022-02-11 中南大学 Coarse particle flotation equipment and method adopting rotational flow and damping coupled fluidization
CN113457853A (en) * 2021-06-23 2021-10-01 湖南柿竹园有色金属有限责任公司 Unpowered gas stirring type flotation device and flotation method
CN113649163A (en) * 2021-07-15 2021-11-16 中煤科工集团唐山研究院有限公司 Pulse type continuous discharging device and method of interference bed separator
CN114700182A (en) * 2021-07-22 2022-07-05 中国矿业大学 Coarse particle fluidized flotation device and method for gradient air intake
CN114713380A (en) * 2021-10-19 2022-07-08 中国矿业大学 Coarse particle flotation device and method based on coupling of ultrasonic waves and mechanical damping blocks
CN114713380B (en) * 2021-10-19 2022-12-27 中国矿业大学 Coarse particle flotation device and method based on coupling of ultrasonic waves and mechanical damping blocks

Also Published As

Publication number Publication date
CN109731696B (en) 2019-12-13

Similar Documents

Publication Publication Date Title
CN109731696A (en) A kind of static flotation method suitable for coarse granule recycling
CN109746124A (en) A kind of Static Flotation Column suitable for coarse granule recycling
CN102716814B (en) Novel flotation column serial connection test system for improving flotation granularity upper limit
CN103480502B (en) Three-product cyclone microbubble floatation column screening installation and method
CN109759241B (en) A kind of device and method of width particle size fraction coal slime flotation
CN102179314B (en) Sorting device and method for aerating cyclonic micro-bubble flotation column
CN103480503B (en) Settling cyclonic micro-bubble flotation column separation unit and method
CN106076658A (en) A kind of method for separating of difficult-to-float coal based on nano bubble
CN207521171U (en) Jet stream micro-bubble flotation machine
CN105127002A (en) Floating technology for effectively reducing pollution of high ash content slime in clean coal
CN105689155A (en) Multi-product flotation column separation equipment and method
CN203577994U (en) Magnetic flotation column
CN104069954B (en) A kind of Coal Flotation Column Process and method for sorting high-concentration ore slurry
CN109759242A (en) A kind of high ash fine slime screening installation and method
CN103447159B (en) Cyclone micro bubble floatation column separation equipment with built-in inclined plates, and method
CN104148164B (en) A kind of method utilizing carbon dioxide to carry out coal washing
CN111375483B (en) Separation system and separation process for coal slime recovery
CN102343309A (en) Machine-column combined three-section floating equipment
CN202270582U (en) Machine and post combined three-section floatation equipment
CN107537698B (en) Reinforced coarse slime flotation device
CN111389580B (en) Three-product hydraulic flotation machine for coarse particle recovery and separation method
CN202129149U (en) Inflated swirl microbubble floatation column sorting device
CN110280397A (en) A kind of floatation equipment and the floatation system comprising it
CN113578515B (en) Protective sorting equipment and method for large-scale graphite
CN105537007B (en) A kind of mineral floating system

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant