CN109699672A - A kind of environment-friendly pesticide - Google Patents
A kind of environment-friendly pesticide Download PDFInfo
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- CN109699672A CN109699672A CN201811593420.XA CN201811593420A CN109699672A CN 109699672 A CN109699672 A CN 109699672A CN 201811593420 A CN201811593420 A CN 201811593420A CN 109699672 A CN109699672 A CN 109699672A
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Abstract
The present invention relates to technical field of insecticide to provide a kind of environment-friendly pesticide aiming at the problem that insecticide be easy to cause environmental pollution as solvent using kerosene, the component including following mass fraction: 0.15-0.2 parts of etrafluorine ethofenprox；0.45-0.6 parts of Permethrin；15-20 parts of ethyl alcohol；Resin 1.5-2 parts of absorption；75-100 parts of deionized water；6.75-9 parts of allicin；4.5-6 parts of capsaicine；The mass ratio of etrafluorine ethofenprox and Permethrin is 1:3.Etrafluorine ethofenprox and Permethrin are dissolved using ethyl alcohol and deionized water as solvent, ethyl alcohol hypotoxicity, and high volatility, to be conducive to enhance the environmental-protecting performance of insecticide, so that advantageously reducing the harm that insecticide generates human health while insecticide is not easy to pollute the environment.
Description
Technical field
The present invention relates to technical field of insecticide, more specifically, it relates to a kind of environment-friendly pesticide.
Background technique
Insecticide refers to a kind of medicament to kill off the insect pests.
The main component that insecticidal action is played in insecticide is the pyrethroids raw medicine such as tetramethrin, due to pyrethroid
The solubility of class raw medicine in water is smaller, thus it is usually necessary to use kerosene as solvent in insecticide.But kerosene have compared with
Big peculiar smell is also easy to pollute the environment, and is easy to affect human health, and therefore, still there is improved space.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of environment-friendly pesticide, there is less toxic ring
The advantages of guarantor.
To achieve the above object, the present invention provides the following technical scheme that
A kind of environment-friendly pesticide, the component including following mass fraction:
0.15-0.2 parts of etrafluorine ethofenprox；
0.45-0.6 parts of Permethrin；
15-20 parts of ethyl alcohol；
Resin 1.5-2 parts of absorption；
75-100 parts of deionized water；
6.75-9 parts of allicin；
4.5-6 parts of capsaicine；
The mass ratio of the etrafluorine ethofenprox and Permethrin is 1:3.
By adopting the above technical scheme, etrafluorine ethofenprox and chlorine chrysanthemum are dissolved using ethyl alcohol and deionized water as solvent
Ester, ethyl alcohol hypotoxicity, and high volatility, to be conducive to enhance the environmental-protecting performance of insecticide, so that insecticide is not easy to ring
The harm that insecticide generates human health is advantageously reduced while border pollutes；By the way that etrafluorine ethofenprox, desinsection is added
The content of etrafluorine ethofenprox, which need to only reach 0.06%, in agent can play good insecticidal effect, and other with disinsection efficiency at
Point generally require reach 0.3% it is even more could play insecticidal effect, because the dosage that etrafluorine ethofenprox needs are added is few, be conducive to
The harm to human body is reduced, so that the environmental-protecting performance of insecticide improves, meanwhile, also help the pollution reduced to environment；Pass through
Absorption resin is added, so that the peculiar smell that the Permethrin in insecticide with penetrating odor gives out is easy to be adsorbed resin suction
It is attached, it is sucked and affected human health by human body to advantageously reduce peculiar smell, so that the environmental-protecting performance of insecticide improves；
By the way that allicin and capsaicine is added, be conducive to the irritation for improving insecticide, so that the disinsection efficiency of insecticide enhances, together
When, garlic and capsicum also have effects that sterilizing, are conducive to the growth for inhibiting various moulds, bacterium, have good
Anti-mold effect；Ingredient used in insecticide is harmless components, it is not easy to affect human health, be conducive to improve
The environmental-protecting performance of insecticide；By the mass ratio of etrafluorine ethofenprox and Permethrin be 1:3, be conducive to improve etrafluorine ethofenprox with
Cooperation effect of Permethrin, so that the insecticidal effect after etrafluorine ethofenprox cooperates with Permethrin is more preferable.
The present invention is further arranged to: the absorption resin is polyacrylate resin.
By adopting the above technical scheme, resin is adsorbed for semi-polarity due to polyacrylate resin, both adsorbable polar gas,
Adsorbable non-polar gas again is conducive to absorption resin and as much as possible adsorbs the peculiar smell in insecticide completely, so that desinsection
Agent is not easy to distribute the gas of irritant smell, so that insecticide is not easy to affect human health.
The present invention is further arranged to: further include the component of following mass fraction:
0.15-0.2 parts of sodium benzoate.
By adopting the above technical scheme, by the way that sodium benzoate is added, be conducive to the antiseptic property for enhancing insecticide, so that desinsection
Agent is not allowed perishable, is conducive to insecticide and keeps good insecticidal effect, so that the pot-life of insecticide extends；Meanwhile benzene
Sodium formate also helps the sterilization of enhancing insecticide, bacteria resistance function.
The present invention is further arranged to: further include the component of following mass fraction:
0.15-0.2 parts of antioxidant.
By adopting the above technical scheme, by addition antioxidant, be conducive to the oxidation for delaying insecticide, so that insecticide
Antiseptic property improves, so that desinsection is not allowed perishable, is conducive to extend the pot-life of insecticide, is conducive to insecticide guarantor
Hold good insecticidal effect.
The present invention is further arranged to: further include the component of following mass fraction:
1.05-1.4 parts of antifreeze.
By adopting the above technical scheme, by the way that antifreeze is added, be conducive to the freezing tolerance for improving insecticide, so that killing
The resistance to low temperature of worm agent improves, so that insecticide is not allowed perishable under cryogenic, is conducive to insecticide and keeps good
Insecticidal effect.
The present invention is further arranged to: further include the component of following mass fraction:
0.3-0.4 parts of emulsifier.
By adopting the above technical scheme, by the way that emulsifier is added, the surface energy of insecticide solution is advantageously reduced, so that milkiness
The droplet surface of liquid forms layer protecting film, enhances insecticide in the wetting on pest surface, spread and adhesive ability, thus
Be conducive to improve the insecticidal effect of insecticide.
The present invention is further arranged to: further include the component of following mass fraction:
45-60 parts of propellant.
By adopting the above technical scheme, by the way that propellant is added, be conducive to provide pressure for insecticide so that desinsection dosage form
At aerosol to spray medicinal cupping, is conducive to insecticide and is formed by spraying.
The present invention is further arranged to: the propellant is the third butane.
It by adopting the above technical scheme, is the third butane by propellant, the third butane is from Oilfield Natural Gas Plant condensate or straight run
Separation and purification obtains in gasoline, not olefin-containing, and sulfur content is extremely low, advantageously reduces the pollution to environment, can be used as aerosol and pushes away
It is uniform convenient for the sprinkling of insecticide into agent.
In conclusion the invention has the following advantages:
1. etrafluorine ethofenprox and Permethrin are dissolved using ethyl alcohol and deionized water as solvent, ethyl alcohol hypotoxicity, and
High volatility, to be conducive to enhance the environmental-protecting performance of insecticide, while so that insecticide is not easy to pollute the environment
Advantageously reduce the harm that insecticide generates human health；
2. by the way that absorption resin is added, so that the peculiar smell that the Permethrin in insecticide with penetrating odor gives out is easy
It is adsorbed resin adsorption, is sucked to advantageously reduce peculiar smell and human body is impacted by human body, so that the environmental protection of insecticide
Performance improves；
3. being conducive to the irritation for improving insecticide, so that the desinsection of insecticide by the way that allicin and capsaicine is added
Effect enhancing, meanwhile, garlic and capsicum also have effects that sterilizing, be conducive to the growth for inhibiting various moulds, bacterium,
With good anti-mold effect；
4. ingredient used in insecticide is harmless components, it is not easy to affect human health, be conducive to mention
The environmental-protecting performance of high insecticide；
5. the mass ratio for passing through etrafluorine ethofenprox and Permethrin is 1:3, be conducive to improve etrafluorine ethofenprox and Permethrin
Cooperate effect, so that the insecticidal effect after etrafluorine ethofenprox cooperates with Permethrin is more preferable.
Specific embodiment
With reference to embodiments, invention is further described in detail.
In following embodiment, etrafluorine ethofenprox uses the article No. of Guangdong Weng Jiang chemical reagent Co., Ltd for PB08245 tetra-
Fluorine ethofenprox.
In following embodiment, Permethrin uses the article No. of Guangdong Weng Jiang chemical reagent Co., Ltd for the chlorine chrysanthemum of PC04280
Ester.
In following embodiment, polyacrylate resin uses the trade mark of Guangzhou Bo Feng Chemical Industry Science Co., Ltd for 934
Polyacrylate resin.
In following embodiment, allicin uses the article No. of Baoji Run Dekang Biotechnology Co., Ltd for the garlic of rdk633
Element.
In following embodiment, capsaicine use the article No. of south jiangxi natural perfume material oil Co., Ltd, Jiangxi Province for 569 capsicum
Alkali.
In following embodiment, sodium benzoate uses the article No. of Jinan Heng Teng Chemical Co., Ltd. for 0531 sodium benzoate.
In following embodiment, antioxidant use the article No. of Dongguan City Kang Jin new material Science and Technology Ltd. for 1076 it is anti-
Oxidant.
In following embodiment, emulsifier uses the emulsifier of the model 400MO of Jiangsu Mao Heng Chemical Co., Ltd..
Embodiment 1
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.15kg, Permethrin 0.45kg, ethyl alcohol is added
15kg, acrylate 1.5kg, deionized water 75kg, allicin 6.75kg, capsaicine 4.5kg, with the revolving speed of 80r/min
It is stirred, stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 140g is filled in iron flask to get environment-friendly pesticide.
Embodiment 2
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.17kg, Permethrin 0.52kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, with the revolving speed of 80r/min
It is stirred, stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 142g is filled in iron flask to get environment-friendly pesticide.
Embodiment 3
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.2kg, Permethrin 0.6kg, ethyl alcohol is added
20kg, acrylate 2kg, deionized water 100kg, allicin 9kg, capsaicine 6kg, are stirred with the revolving speed of 80r/min
It mixes, stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 145g is filled in iron flask to get environment-friendly pesticide.
Embodiment 4
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.17kg, Permethrin 0.52kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, sodium benzoate 0.15kg,
Antioxidant 0.15kg, antifreeze 1.05kg, emulsifier 0.3kg, are stirred with the revolving speed of 80r/min, stir evenly to kill
Worm liquid；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 138g is filled in iron flask to get environment-friendly pesticide.
Embodiment 5
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.17kg, Permethrin 0.52kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, sodium benzoate 0.17kg,
Antioxidant 0.17kg, antifreeze 1.2kg, emulsifier 0.35kg, are stirred with the revolving speed of 80r/min, stir evenly to kill
Worm liquid；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution liquid feeding of each aerosol container
Amount is 260g, and the valve of aerosol container and aerosol container are then packaged into an entirety, finally filled in each aerosol container
Enter the third butane of 136g to get environment-friendly pesticide.
Embodiment 6
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.17kg, Permethrin 0.52kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, sodium benzoate 0.2kg,
Antioxidant 0.2kg, antifreeze 1.4kg, emulsifier 0.4kg, are stirred with the revolving speed of 80r/min, stir evenly to obtain desinsection
Liquid；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 139g is filled in iron flask to get environment-friendly pesticide.
Embodiment 7
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.17kg, Permethrin 0.52kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, sodium benzoate 0.19kg,
Antioxidant 0.18kg, antifreeze 1.1kg, emulsifier 0.33kg, are stirred with the revolving speed of 80r/min, stir evenly to kill
Worm liquid；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 140g is filled in iron flask to get environment-friendly pesticide.
Comparative example 1
In the present embodiment, essence uses the article No. of Jiangmen city Xin Yi fragrance Co., Ltd for the fruit essence of JR4085.
Method for producing insecticide is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, tetramethrin 0.6kg, Permethrin 0.5kg, efficient chlorine cyanogen chrysanthemum is added
Ester 0.06kg, emulsifier 0.09kg, kerosene 64kg, essence 0.5kg, are stirred with the revolving speed of 80r/min, stir evenly to kill
Worm liquid；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 142g is filled in iron flask to get insecticide.
Comparative example 2
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.17kg, Permethrin 0.52kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, are stirred with the revolving speed of 80r/min, stir evenly to obtain desinsection
Liquid；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 145g is filled in iron flask to get environment-friendly pesticide.
Comparative example 3
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.23kg, Permethrin 0.46kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, with the revolving speed of 80r/min
It is stirred, stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 143g is filled in iron flask to get environment-friendly pesticide.
Comparative example 4
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.2kg, Permethrin 0.5kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, with the revolving speed of 80r/min
It is stirred, stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 142g is filled in iron flask to get environment-friendly pesticide.
Comparative example 5
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.15kg, Permethrin 0.525kg, second is added
Alcohol 17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, with turning for 80r/min
Speed is stirred, and stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 144g is filled in iron flask to get environment-friendly pesticide.
Comparative example 6
Environment-friendly pesticide the preparation method is as follows:
(1) in the stirred tank of 200L, under normal temperature condition, etrafluorine ethofenprox 0.14kg, Permethrin 0.56kg, ethyl alcohol is added
17.5kg, acrylate 1.7kg, deionized water 87kg, allicin 7.8kg, capsaicine 5.2kg, with the revolving speed of 80r/min
It is stirred, stirs evenly to obtain insecticidal solution；
(2) insecticidal solution obtained in step (1) is filled in aerosol iron flask, the insecticidal solution of each aerosol iron flask adds
Liquid measure is 260g, the valve of aerosol iron flask and aerosol iron flask is then packaged into an entirety, finally in each aerosol
The third butane of 138g is filled in iron flask to get environment-friendly pesticide.
Each embodiment and the detection data of comparative example are shown in Table 1-2.
Experiment 1
The ejection rate (g/s) and spray of insecticide are detected according to GB/T14449-2008 " aerosol products test method "
Extracting rate (%).
Experiment 2
It is used after insecticide according to GB/T27784-2011 " measurement of hygienic insecticide field efficacy and evaluation general provisions " detection
Mosquito Relative density decline rate (%).
Table 1
Table 2
Can be obtained according to embodiment 1-3 in table 1 and table 2 and the data comparison of comparative example 1, by using etrafluorine ethofenprox with
Permethrin cooperation desinsection is conducive to enhance the insecticidal effect of insecticide, so that using under the mosquito relative density after environment-friendly pesticide
Drop rate is bigger than the mosquito Relative density decline rate after using conventional pesticides, so that the insecticidal effect of insecticide enhances.
It can be obtained according to embodiment 1-3 in table 1 and table 2 and the data comparison of comparative example 2, by the way that allicin and peppery is added
Green pepper alkali can enhance the insecticidal effect of insecticide to a certain extent, so that using the mosquito Relative density decline rate after insecticide
Increase；Meanwhile allicin and capsaicine are food extracts, are conducive to the environmental-protecting performance for enhancing insecticide, so that insecticide
It is not easy to have an impact human health.
It can be obtained according to the data comparison of embodiment 1-3 and comparative example 3-6 in table 1 and table 2, when etrafluorine ethofenprox and chlorine chrysanthemum
The ratio of ester is gradually increased using the mosquito Relative density decline rate after insecticide with the increase of ratio in the range of 1:2-3
Greatly, when range when the ratio of etrafluorine ethofenprox and Permethrin in 1:3-4, the mosquito Relative density decline rate after insecticide is used
It is gradually reduced with the increase of ratio, therefore, when the ratio of etrafluorine ethofenprox and Permethrin is 1:3, the desinsection effect of insecticide
Fruit is best.
It can be obtained according to the data comparison of embodiment 1-3 in table 2 and embodiment 4-7, by the way that emulsifier is added, be advantageously reduced
The surface energy of insecticide solution enhances insecticide on pest surface so that the droplet surface of emulsion forms layer protecting film
Wetting, spread and adhesive ability, the insecticidal effect of insecticide can be enhanced to a certain extent, so that after using insecticide
Mosquito Relative density decline rate increases.
The embodiment of present embodiment is presently preferred embodiments of the present invention, not limits protection of the invention according to this
Range, therefore: the equivalence changes that all structures under this invention, shape, principle are done, should all be covered by protection scope of the present invention it
It is interior.
Claims (8)
1. a kind of environment-friendly pesticide, it is characterized in that: including the component of following mass fraction:
0.15-0.2 parts of etrafluorine ethofenprox；
0.45-0.6 parts of Permethrin；
15-20 parts of ethyl alcohol；
Resin 1.5-2 parts of absorption；
75-100 parts of deionized water；
6.75-9 parts of allicin；
4.5-6 parts of capsaicine；
The mass ratio of the etrafluorine ethofenprox and Permethrin is 1:3.
2. a kind of environment-friendly pesticide according to claim 1, it is characterized in that: the absorption resin is polyacrylate tree
Rouge.
3. a kind of environment-friendly pesticide according to claim 1 to 2, it is characterized in that: further including the group of following mass fraction
Point:
0.15-0.2 parts of sodium benzoate.
4. a kind of environment-friendly pesticide according to claim 1 to 2, it is characterized in that: further including the group of following mass fraction
Point:
0.15-0.2 parts of antioxidant.
5. a kind of environment-friendly pesticide according to claim 1 to 2, it is characterized in that: further including the group of following mass fraction
Point:
1.05-1.4 parts of antifreeze.
6. a kind of environment-friendly pesticide according to claim 1 to 2, it is characterized in that: further including the group of following mass fraction
Point:
0.3-0.4 parts of emulsifier.
7. a kind of environment-friendly pesticide according to claim 1 to 2, it is characterized in that: further including the group of following mass fraction
Point:
45-60 parts of propellant.
8. a kind of environment-friendly pesticide according to claim 7, it is characterized in that: the propellant is the third butane.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115553289A (en) * | 2022-11-04 | 2023-01-03 | 佛山市南海奥帝精细化工有限公司 | Insecticidal aerosol and preparation method thereof |
| CN115584169A (en) * | 2022-09-27 | 2023-01-10 | 英德市东顺精细化工实业有限公司 | Rat repelling foam for preventing rat bite |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115584169A (en) * | 2022-09-27 | 2023-01-10 | 英德市东顺精细化工实业有限公司 | Rat repelling foam for preventing rat bite |
| CN115553289A (en) * | 2022-11-04 | 2023-01-03 | 佛山市南海奥帝精细化工有限公司 | Insecticidal aerosol and preparation method thereof |
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Application publication date: 20190503 |